INSTRUMENT CONTROL PARAMETERS:
Instr
ument #1
---------------------------------------------C:\MSDCHEM\1\METHODS\UNDERGRADYEASTPROJECT\SPME_and_StaticHeadspace.M
Control Information
------- ----------Sample Inlet
:
Injection Source :
Injection Location:
Mass Spectrometer :
GC
Manual
Rear
Enabled
=============================================================================
6890 GC METHOD
=============================================================================
OVEN
Initial temp: 35 'C (On)
Initial time: 2.00 min
Ramps:
# Rate Final temp Final time
1 10.00
250
0.00
2 0.0(Off)
Post temp: 50 'C
Post time: 0.00 min
Run time: 23.50 min
CRYO (N2)
Cryo: Off
Cryo fault: Off
Cryo timeout: 120.00 min (Off)
Quick cryo cool: Off
Ambient temp: 30 'C
FRONT INLET (SPLIT/SPLITLESS)
Mode: Split
Initial temp: 230 'C (On)
Pressure: 8.06 psi (On)
Split ratio: 50:1
Split flow: 71.6 mL/min
Total flow: 81.6 mL/min
Gas saver: On
Saver flow: 20.0 mL/min
Saver time: 2.00 min
Gas type: Hydrogen
BACK INLET (SPLIT/SPLITLESS)
Mode: Splitless
Initial temp: 250 'C (On)
Pressure: 17.53 psi (On)
Purge flow: 6.5 mL/min
Purge time: 1.00 min
Total flow: 14.5 mL/min
Gas saver: On
Saver flow: 15.0 mL/min
Saver time: 1.00 min
Gas type: Hydrogen
COLUMN 1
Capillary Column
Model Number: Restek Rtx-5
COLUMN 2
Capillary Column
Nominal length: 30.0 m
Nominal diameter: 250.00 um
Nominal film thickness: 0.50 um
Mode: constant pressure
Pressure: 8.06 psi
Nominal initial flow: 1.4 mL/min
Average velocity: 39 cm/sec
Inlet: Front Inlet
Outlet: Front Detector
Outlet pressure: ambient
Max temperature: 330 'C
Nominal length: 40.0 m
Nominal diameter: 180.00 um
Nominal film thickness: 0.40 um
Mode: constant flow
Initial flow: 1.0 mL/min
Nominal init pressure: 17.55 psi
Average velocity: 46 cm/sec
Inlet: Back Inlet
Maximum temp: 330 'C
Equilibration time: 0.50 min
Outlet: MSD
Outlet pressure: vacuum
FRONT DETECTOR (FID)
Temperature: 250 'C (Off)
Hydrogen flow: 40.0 mL/min (Off)
Air flow: 450.0 mL/min (Off)
Mode: Constant makeup flow
Makeup flow: 45.0 mL/min (Off)
Makeup Gas Type: Nitrogen
Flame: Off
Electrometer: Off
Lit offset: 2.0
BACK DETECTOR (TCD)
Temperature: 250 'C (Off)
Reference flow: 20.0 mL/min (Off)
Mode: Constant makeup flow
Makeup flow: 7.0 mL/min (Off)
Makeup Gas Type: Nitrogen
Filament: Off
Negative polarity: Off
SIGNAL 1
Data rate: 50 Hz
Type: test plot
Save Data: On
Zero: 0.0 (Off)
Range: 0
Fast Peaks: Off
Attenuation: 0
SIGNAL 2
Data rate: 20 Hz
Type: back detector
Save Data: Off
Zero: 0.0 (Off)
Range: 0
Fast Peaks: Off
Attenuation: 0
COLUMN COMP 1
Derive from front detector
COLUMN COMP 2
Derive from back detector
THERMAL AUX 1
Use: MSD Transfer Line Heater
Description:
Initial temp: 270 'C (On)
Initial time: 0.00 min
# Rate Final temp Final time
1 0.0(Off)
VALVES
Valve 7 Remote Start
TIME TABLE
Time
POST RUN
Post Time: 0.00 min
Specifier
Parameter & Setpoint
GC Injector
Front Injector:
No parameters specified
Back Injector:
Injector not configured, use these parameters if it becomes configured
Sample Washes
0
Sample Pumps
5
Injection Volume
0.50 microliters
Syringe Size
PostInj Solvent A Washes
PostInj Solvent B Washes
Viscosity Delay
Plunger Speed
5.0 microliters
3
0
1 seconds
Fast
Column 1 Inventory Number : AB008
Column 2 Inventory Number : AB001
MS ACQUISITION PARAMETERS
General Information
------- ----------Tune File
Acquistion Mode
: atune.u
: Scan
MS Information
-- ----------Solvent Delay
: 0.00 min
EM Absolute
Resulting EM Voltage
: True
: 1952.9
[Scan Parameters]
Low Mass
High Mass
Threshold
Sample #
:
:
:
:
40.0
200.0
0
1
A/D Samples
[MSZones]
MS Quad
MS Source
Timed Events
----- ------
: 150 C
: 230 C
maximum 200 C
maximum 250 C
[Timed MS Detector Entries]
Time (min)
0.01
State (MS on/off)
On
END OF MS ACQUISITION PARAMETERS
TUNE PARAMETERS for SN: US91922553
-----------------------------
EMISSION
ENERGY
REPELLER
IONFOCUS
ENTRANCE_LE
EMVOLTS
AMUGAIN
:
:
:
:
:
:
:
34.610
69.922
29.955
90.157
0.000
2941.176
2483.000
AMUOFFSET
FILAMENT
DCPOLARITY
ENTLENSOFFS
MASSGAIN
MASSOFFSET
:
:
:
:
:
:
120.000
2.000
1.000
25.098
273.000
-10.000
END OF TUNE PARAMETERS
------------------------------------
END OF INSTRUMENT CONTROL PARAMET
ERS
-----------------------------------
