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Solvent Pairs for Benzoic Acid Recrystallization

This document contains a laboratory experiment on recrystallization and melting point determination of benzoic acid. It includes 6 questions about recrystallization techniques and solvent selection. Specifically, it asks about how fluted filter paper hastens filtration, techniques to prevent premature crystallization, choosing a solvent based on solubility data, determining purity after one recrystallization, identifying which solvent pairs can be used for mixed solvent recrystallization, and comparing advantages and disadvantages of mixed versus single solvent recrystallization.

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Joone Xyron Creencia
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172 views2 pages

Solvent Pairs for Benzoic Acid Recrystallization

This document contains a laboratory experiment on recrystallization and melting point determination of benzoic acid. It includes 6 questions about recrystallization techniques and solvent selection. Specifically, it asks about how fluted filter paper hastens filtration, techniques to prevent premature crystallization, choosing a solvent based on solubility data, determining purity after one recrystallization, identifying which solvent pairs can be used for mixed solvent recrystallization, and comparing advantages and disadvantages of mixed versus single solvent recrystallization.

Uploaded by

Joone Xyron Creencia
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd

J. E. Birdwell / Chemistry 31.

1 (2019) P a g e |1

RECRYSTALLIZATION AND MELTING POINT DETERMINATION OF


BENZOIC ACID
Joone Xyron V. Creenciaa,*
aCollege
of Arts and Letters, University of the Philippines, Diliman, Quezon City
Performed 11 January 2019; Submitted 18 January 2019

ANSWERS TO QUESTIONS

1. How does the fluted filter paper hasten filtration?


 Answer 1

2. Explain two techniques that can help prevent premature crystallization. What could be the consequences of
premature recrystallization?
 Answer 2

3. A mixture containing 2.0 g of A and 8.0 g of B is to be separated by recrystallization. The components were
purified by single crystallization using 100mL of solvent. Their solubilities are given in the table below:
A B
Solvent
Hot Cold Hot Cold
Ethanol 0.5 10.0 5.0 20.0
Acetone 5.0 20.0 0.1 8.0
Water 0.6 15.0 0.5 10.0
a. Which solvent would you choose? Explain your choice by means of a schematic diagram.
b. Theoretically, what is the purity of A and B after one recrystallization?

 Answer 3

4. A mixture of three compounds. A, B, and C is purified using recrystallization method.


Their solubilities in g/100mL ethanol are given below:
Solvent A B C
Cold 1.05 5.6 4.2
Hot 20.5 2.3 3.5

a. If a mixture containing 4.0 g each of A, B, and C is recrystallized from 100mL ethanol, which compound
can be obtained pure?
b. If the filtrate from (a) is evaporated to 50mL, which of the compound(s) will separate upon cooling?
What is its purity?

 Answer 4

5. You were asked to perform recrystallization using a mixed-solvent system. Which of the following solvents
cannot be used as solvent pairs for the experiment? Explain your answer.
a. Hexane and water
b. Chloroform and diethyl ether
c. Acetone and methanol

 Answer 5

*Corresponding author. Mobile: 09051434752


E-mail address: [Link]@[Link]
J. E. Birdwell / Chemistry 31.1 (2019) P a g e |2

6. What are the advantages/disadvantages of mixed solvent recrystallization over single solvent
recrystallization?

 Answer 6

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