Reference Manual Refractometer Excellence

R4/R5
Table of Contents

1 Introduction 5

2 Safety information 6
2.1 Definitions of signal words and warning symbols ................................................................. 6
2.2 Product specific safety notes .............................................................................................. 6

3 Design and function 8

3.1 Overview refractometer ...................................................................................................... 8
3.2 Rear panel ....................................................................................................................... 9
3.3 Terminal .......................................................................................................................... 10
3.4 The principle of measuring the refractive index ..................................................................... 10
3.5 Design of measuring cell ................................................................................................... 11

4 Installation and commissioning 12

4.1 Scope of delivery .............................................................................................................. 12
4.2 Download the Reference Manual......................................................................................... 12
4.3 Unpack the refractometer ................................................................................................... 13
4.4 Position the refractometer................................................................................................... 13
4.5 Connect the refractometer to the power supply...................................................................... 13
4.6 Disconnect the refractometer from the power supply.............................................................. 14
4.7 Connect, adjust and disconnect the terminal ........................................................................ 14
4.7.1 Connect the terminal........................................................................................... 14
4.7.2 Adjust the angle of the terminal............................................................................ 15
4.7.3 Disconnect the terminal ...................................................................................... 15
4.8 Setup .............................................................................................................................. 15
4.8.1 Adjustments & Tests ........................................................................................... 16
4.8.1.1 Adjustment Sets ............................................................................................ 16
4.8.1.2 Test Sets ...................................................................................................... 17
4.8.2 Hardware .......................................................................................................... 17
4.8.2.1 Cell ............................................................................................................. 17
4.8.2.2 Automation................................................................................................... 18
4.8.2.3 External Instruments ...................................................................................... 20
4.8.2.4 Peripherals ................................................................................................... 21
4.8.2.5 Sensors ....................................................................................................... 25
4.8.2.6 Auxiliary instruments ..................................................................................... 25
4.8.3 Language.......................................................................................................... 26
4.8.4 Screen .............................................................................................................. 27
4.8.5 Beep................................................................................................................. 27
4.8.6 Shortcuts........................................................................................................... 27
4.8.7 Keyboards......................................................................................................... 27
4.8.8 Global Settings .................................................................................................. 28
4.8.8.1 System ........................................................................................................ 28
4.8.8.2 User Management ......................................................................................... 28
4.8.8.3 Analysis and Resources Behavior.................................................................... 30
4.8.8.4 Physical Properties........................................................................................ 31
4.8.9 Tables & Values................................................................................................. 31
4.8.9.1 Tables ......................................................................................................... 32
4.8.9.2 Auxiliary Values ............................................................................................ 33
4.8.10 Maintenance & Service ....................................................................................... 33
4.8.10.1 MT Service ................................................................................................... 34
4.8.10.2 Import / Export .............................................................................................. 34
4.8.10.3 Add External Cell ........................................................................................... 35
4.8.10.4 Reset to Factory Settings ................................................................................ 35
4.8.10.5 Firmware...................................................................................................... 35
4.8.10.6 Update ......................................................................................................... 35

Refractometer Excellence Table of Contents 1

 4.8.10.7 Hardware / Firmware summary....................................................................... 36
4.8.10.8 Board Tests .................................................................................................. 36
4.8.10.9 Cell ............................................................................................................. 37
4.8.10.10 Export Adjustments / Tests / Measurements ...................................................... 37

5 Configuration of measurement methods 38

5.1 Establishing Methods ........................................................................................................ 38
5.2 Creating a Method Copy .................................................................................................... 40
5.3 Modifying or Deleting Methods ........................................................................................... 40
5.4 Method Syntax.................................................................................................................. 40
5.5 Standard Data .................................................................................................................. 43
5.6 Condition ......................................................................................................................... 43
5.7 Method functions .............................................................................................................. 44
5.7.1 Title .................................................................................................................. 44
5.7.2 Configuration..................................................................................................... 45
5.7.3 Sample ............................................................................................................. 45
5.7.4 Fill.................................................................................................................... 47
5.7.5 Measure............................................................................................................ 48
5.7.6 Calculation........................................................................................................ 51
5.7.7 Clean................................................................................................................ 51
5.7.8 Online Display ................................................................................................... 53
5.7.9 Report............................................................................................................... 53
5.7.10 Cell Test............................................................................................................ 54
5.7.11 Temperature Compensation................................................................................. 54
5.7.12 Adjustment ........................................................................................................ 55
5.7.13 Test .................................................................................................................. 55
5.7.14 Instruction ......................................................................................................... 56
5.7.15 Auxiliary Value................................................................................................... 56
5.7.16 Wait ................................................................................................................. 56
5.7.17 Auxiliary instrument............................................................................................ 56
5.7.18 PowerShower .................................................................................................... 58
5.7.19 Stir ................................................................................................................... 59
5.7.20 Line rinse .......................................................................................................... 59
5.7.21 Park ................................................................................................................. 59

6 Configuration of products 61
6.1 Create Products ................................................................................................................ 61
6.2 Linking Methods with Products ........................................................................................... 61
6.3 Parameters for Products .................................................................................................... 61
6.4 Calculations in Products .................................................................................................... 63

7 Series 64
7.1 Delete Series .................................................................................................................... 65
7.2 Creating a series copy ....................................................................................................... 65

8 Operation 66
8.1 Start up the refractometer ................................................................................................... 66
8.2 Shut down the refractometer ............................................................................................... 66
8.3 Typical phases of refractive-index determinations ................................................................. 67
8.3.1 Fill the measuring cell......................................................................................... 67
8.3.2 Rinse the measuring cell..................................................................................... 67
8.3.3 Dry the measuring cell........................................................................................ 68
8.4 Example: refractive-index determination without automation .................................................. 68
8.4.1 Create the measurement method.......................................................................... 68
8.4.2 Configure the measurement method ..................................................................... 69
8.4.3 Create a shortcut on the home screen................................................................... 70
8.4.4 Determine the refractive index .............................................................................. 70
8.5 Viewing the results ............................................................................................................ 73

2 Table of Contents Refractometer Excellence

 8.6 Automation ...................................................................................................................... 73
8.6.1 Action: Dry ........................................................................................................ 74
8.6.2 Action: Rinse ..................................................................................................... 74
8.6.3 Action: Drain ..................................................................................................... 74
8.6.4 Action: Pump sample ......................................................................................... 74
8.6.5 Action: PowerShower.......................................................................................... 75
8.6.6 Action: Stir......................................................................................................... 75
8.6.7 Action: Move to position...................................................................................... 75
8.6.8 Action: Move lift ................................................................................................. 75

9 Maintenance 76
9.1 Maintenance schedule....................................................................................................... 76
9.2 Clean the refractometer ...................................................................................................... 76
9.2.1 Clean the housing and the lid .............................................................................. 76
9.3 Clean the measuring cell ................................................................................................... 77
9.3.1 Typical phases of cleaning the measuring cell....................................................... 77
9.3.2 Example: clean with deionized water.................................................................... 77
9.3.2.1 Create the cleaning method ............................................................................ 77
9.3.2.2 Configure the cleaning method........................................................................ 78
9.3.2.3 Clean using deionized water........................................................................... 79
9.4 Check the measurement accuracy....................................................................................... 80
9.4.1 Typical phases of checking the measurement accuracy .......................................... 80
9.4.2 Example: test with a water standard ..................................................................... 81
9.4.2.1 Create the test method ................................................................................... 81
9.4.2.2 Configure the test method............................................................................... 82
9.4.2.3 Perform the test............................................................................................. 83
9.5 Replace the protection plate ............................................................................................... 85
9.5.1 Remove the protection plate ................................................................................ 85
9.5.2 Install the protection plate ................................................................................... 86
9.6 Replace the lid.................................................................................................................. 86
9.6.1 Remove the lid................................................................................................... 86
9.6.2 Install the lid...................................................................................................... 87
9.7 Replace the measuring-cell cover ....................................................................................... 87
9.7.1 Remove the measuring-cell cover ........................................................................ 87
9.7.2 Install the measuring-cell cover ........................................................................... 88
9.8 Replace the measuring-cell O-ring ...................................................................................... 88
9.8.1 Remove the measuring-cell O-ring ....................................................................... 88
9.8.2 Install the measuring-cell O-ring .......................................................................... 89
9.9 Replace the O-ring of the measuring-cell cover..................................................................... 89
9.9.1 Remove the O-ring of the measuring-cell cover...................................................... 89
9.9.2 Install the O-ring of the measuring-cell cover......................................................... 90
9.10 View the firmware version .................................................................................................. 90
9.11 Update the firmware .......................................................................................................... 90
9.12 Prepare the refractometer for storage ................................................................................... 91
9.13 Transport the refractometer................................................................................................. 91
9.14 Dispose of the refractometer ............................................................................................... 91

10 Troubleshooting 92
10.1 View and export system information.................................................................................... 92
10.1.1 View system information of the refractometer ......................................................... 92
10.1.2 View system information of connected accessories ................................................ 92

11 Technical data 93
11.1 Refractometer ................................................................................................................... 93
11.2 Terminal .......................................................................................................................... 94
11.3 Measurement ................................................................................................................... 95

Refractometer Excellence Table of Contents 3

 12 Accessories 96
12.1 Standards ........................................................................................................................ 96
12.2 Sensors ........................................................................................................................... 96
12.3 Sample changers and pumps............................................................................................. 96
12.4 External measuring cells.................................................................................................... 100
12.5 External instruments.......................................................................................................... 100
12.6 Peripheral instruments....................................................................................................... 102
12.7 Software .......................................................................................................................... 103
12.8 Miscellaneous accessories................................................................................................. 103

Index 105

4 Table of Contents Refractometer Excellence

 1 Introduction
Thank you for choosing a METTLER TOLEDO refractometer. The refractometers R4 and R5 are easy-to-operate,
high-performance instruments for measuring the refractive index of liquid samples.
About this document
The instructions in this document refer to refractometers R4 and R5 running firmware version 1.0 or higher.
The firmware license is subject to the End User License Agreement EULA version 3.0. See the following link for
the license text:
u www.mt.com/legal

For third party licenses and open source attribution files, see the following link:
u www.mt.com/licenses

If you have any additional questions, contact your authorized METTLER TOLEDO service representative or
dealer.
u www.mt.com/contact

Conventions and symbols

Note For useful information about the product.

Refers to an external document.

Elements of instructions
§ Prerequisites
1 Steps
2 Steps
ð Intermediate results
3 Steps
ð Results

Refractometer Excellence Introduction​​ 5

 2 Safety information
Two documents named "User Manual" and "Reference Manual" are available for this instrument.
• The User Manual is printed and delivered with the instrument.
• The electronic Reference Manual contains a full description of the instrument and its use.
• Keep both documents for future reference.
• Include both documents if you transfer the instrument to other parties.
Only use the instrument according to the User Manual and the Reference Manual. If you do not use the
instrument according to these documents or if the instrument is modified, the safety of the instrument may be
impaired and Mettler-Toledo GmbH assumes no liability.
User Manual and Reference Manual are available online.

u www.mt.com/library

2.1 Definitions of signal words and warning symbols

Safety notes contain important information on safety issues. Ignoring the safety notes may lead to personal
injury, damage to the instrument, malfunctions and false results. Safety notes are marked with the following
signal words and warning symbols:
Signal words
WARNING A hazardous situation with medium risk, possibly resulting in death or severe injury if
not avoided.

CAUTION A hazardous situation with low risk, resulting in minor or moderate injury if not avoided.

NOTICE A hazardous situation with low risk, resulting in damage to the instrument, other
material damage, malfunctions and erroneous results, or loss of data.

Warning symbols
Electrical shock

Hot surface

2.2 Product specific safety notes

Intended use
The refractometers R4 and R5 are designed to be used by trained staff. The refractometers are intended for
measuring the refractive index of liquid samples that are compatible with the materials with which they come
into contact.
Any other type of use and operation beyond the limits of use stated by Mettler-Toledo GmbH without consent
from Mettler-Toledo GmbH is considered as not intended.
Responsibilities of the instrument owner
The instrument owner is the person holding the legal title to the instrument and who uses the instrument or
authorizes any person to use it, or the person who is deemed by law to be the operator of the instrument. The
instrument owner is responsible for the safety of all users of the instrument and third parties.
METTLER TOLEDO assumes that the instrument owner trains users to safely use the instrument in their
workplace and deal with potential hazards. METTLER TOLEDO assumes that the instrument owner provides the
necessary protective gear.

6 Safety information​​ Refractometer Excellence

 Protective clothing
Gloves that protect your hands from contact with hot or cold surfaces.

Safety notes

WARNING
Danger of death or serious injury due to electric shock!
Contact with parts that carry a live current can lead to death or injury.
1 Only use the METTLER TOLEDO power supply cable and AC adapter designed for your
instrument.
2 Connect the power cable to a grounded power outlet.
3 Keep all electrical cables and connections away from liquids and moisture.
4 Check the cables and the power plug for damage and replace damaged cables and
power plugs.

CAUTION
Slight burns due to hot surface
The measuring cell can become hot enough to cause slight burns.
1 Do not touch the measuring cell without gloves before the measuring cell has cooled
down.
2 Wear gloves that protect from contact heat if you need to touch the hot measuring cell.

NOTICE
Risk of damage to the instrument due to the use of unsuitable parts!
Using unsuitable parts with the instrument can damage the instrument or cause it to
malfunction.
− Only use parts from METTLER TOLEDO that are intended to be used with your instrument.

FCC Rules
This equipment has been tested and found to comply with the limits for a Class A digital device, pursuant to
Part 15 of the FCC rules. These limits are designed to provide reasonable protection against harmful inter-
ference when the equipment is operated in a commercial environment. This equipment generates, uses, and
can radiate radio frequency energy and, if not installed and used in accordance with the instruction manual,
may cause harmful interference to radio communications. Operation of this equipment in a residential area is
likely to cause harmful interference in which case the user will be required to correct the interference at his own
expense.

Refractometer Excellence Safety information​​ 7

 3 Design and function
3.1 Overview refractometer

9
3
8
7 4

No. Name Function

1 Lid Protects the measuring cell
2 Measuring-cell cover Closes off the measuring cell and permits the formation of a stable vapour-
liquid equilibrium
3 Measuring cell Holds the sample
4 Prism Refracts the light at its surface
5 Safety label Warns that the measuring cell can be hot and cause slight burns if you touch
it without protective gloves
6 Terminal Displays information and is used to enter information
7 Power button Starts up and shuts down the refractometer
8 Instrument status light Provides information about the status of the refractometer.
(StatusLight™)
9 Protection plate Collects spilled sample or cleaning solution

Status light
StatusLight Refractometer status
Steady, green light The refractometer is ready for operation.
Blinking, green light The refractometer is performing a task.
Steady, orange light The refractometer waits for the user to perform an action.
Blinking, orange light The task has been interrupted, for example because a value lies outside of its
limits.
Steady,red light An error has occurred during task execution.

8 Design and function​​ Refractometer Excellence

 3.2 Rear panel

13 12 11 10 9 8 7 6 5 4 3 2

No. Name Function

1 Fan and ventilation Move air over the heat sink of the Peltier element
openings
2 CAN out RJ12 socket to connect a LevelSens box
3 Power Supply DC Socket to connect the AC adapter
4 USB 1 / USB 2 USB-A socket to connect USB devices, for example printers, barcode readers
or an InMotion™ Autosampler
5 PC USB-B socket to connect a computer
6 SPR200 6-pin Mini-DIN socket to connect the filling pump SPR200
7 Terminal 19-pin Mettler-HDMI socket with non-standard pin assignment, reserved to
connect the terminal and no other display device
8 DryPro 5-pin Mini-DIN socket to connect the drying pump DryPro
9 Ethernet RJ45 socket to connect a network
10 Aux 5-pin Mini-DIN socket to connect an auxiliary instrument
11 Automation 9-pin male D-sub socket to connect a sample delivery and cleaning unit
12 LevelSens 5-pin Mini-DIN socket to connect the fluid-level sensor LevelSens
13 ErgoSens 3.5 mm jack socket to connect the infrared motion-sensor ErgoSens

See also
2 Accessories } Page 96

Refractometer Excellence Design and function​​ 9

 3.3 Terminal

6 5 4

No. Name Function

1 Touch screen Displays information and can be used to enter information
2 USB-A socket Is used to transfer data to and from a USB flash drive
3 Terminal status light Provides information about the status of the refractometer
(StatusLight™)
4 Opens a window with general information about the refractometer

5 Opens the home screen

6 Ends all running tasks

3.4 The principle of measuring the refractive index

Definition of the refractive index
The refractive index of a substance is the ratio of the speed of a light beam in a vacuum to its speed in the
substance (dimensionless).
n1 If a light beam crosses at a certain angle from an optically less
dense to an optically denser medium (e.g. from air to water), it
is deflected; when the beam crosses from one medium to
another perpendicularly no directional change takes place.
According to Snell's law, the ratio of the refractive index of the
two media is proportional to the ratio of the incident and
refractive angle of the light beam:
n1 β
= sin
n2 sin α

n2

If a light beam passes from an optically denser to a less dense

medium, it is also deflected. If the angle of incidence α is
increased, then it reaches a critical value, at which the light
beam no longer enters the less dense medium (refractive angle
β = 90°). When this "critical angle" is exceeded, total internal
reflection occurs. The refractive index is calculated from this
critical angle α :
β = 90o —> sin β = 1
1 2 1: Critical angle
2: Total internal reflection

10 Design and function​​ Refractometer Excellence

 As refraction depends on the wavelength of the incident light, the refractive index n is measured as standard
with the D line of sodium (wavelength 589.3 nm) and designated nD.
The refractive index not only depends on the wavelength of the light but also on the temperature of the
measured sample. For this reason the temperature must always be stated along with the result, e.g. nD25.
The standard temperature is 20 °C.
Measuring the refractive index
3 The light emitted from the light source passes through the
prism and hits the sample. In the process it is partly refracted
(angle of incidence < critical angle) and partly reflected (angle
2 of incidence > critical angle).
The reflected light is measured by means of an optical sensor
(CCD). The boundary between the dark and light area corre-
sponds to the critical angle required for calculation of the
refractive index.
1
1: Light source
4
2: Prism
3: Sample
4: Optical sensor (CCD)

3.5 Design of measuring cell

The light source is a light-emitting diode (LED), whose beam passes through a polarization filter, an inter-
ference filter (589.3 nm) and various lenses before it reaches the sample via the sapphire prism. The reflected
light (angle of incidence > critical angle) is deflected via a lens to the optical sensor that determines the critical
angle. The temperature in the prism/sample boundary is measured with a built-in sensor.

1: Light source
2: Polarization filter
3: Interference filter
4: Lens
5: Lens
6: Prism
7: Lens
8: Measuring cell
9: Optical sensor (CCD)

Refractometer Excellence Design and function​​ 11

 4 Installation and commissioning
4.1 Scope of delivery
Part Order number R4 R5
Refractometer – • •

Extern. Power Supply 120W 30298362 • •

Power cable (country-specific) – • •

Terminal WVGA 7 inch AnaChem – • •

• Terminal
• HDMI cable

Combined water standard 51338010 • •

9 mL, density/refractive index

Plastic pipettes (3 pcs) – • •

PP (polypropene)

User Manual – • •

Declaration of conformity – • •

Test report – • •

4.2 Download the Reference Manual

1 Go to the website www.mt.com/library.
2 Select the Technical Documentation tab.
3 Enter the product type in the search field and start the search.
4 Select the Reference Manual from the result list.
5 Select the link.
ð The Reference Manual is either opened or downloaded depending on the browser settings.
6 Check which firmware version is installed on your refractometer.

12 Installation and commissioning​​ Refractometer Excellence

 7 If the Reference Manual is not written for the installed firmware version, contact your authorized METTLER
TOLEDO service representative or dealer.
u www.mt.com/contact

See also
2 Introduction } Page 5
2 View the firmware version } Page 90

4.3 Unpack the refractometer

1 Remove the refractometer from the protective packaging.
2 Store the packing material for later transport over long distances.
3 Check if you received all parts listed in the scope of delivery.
4 Inspect the parts visually for flaws or damage.
5 If parts are missing or damaged, report it to your authorized METTLER TOLEDO service representative or
dealer.
u www.mt.com/contact

See also
2 Scope of delivery } Page 12

4.4 Position the refractometer

The refractometer has been developed for indoor operation in a room with stable temperature and ventilation as
needed by the chemicals that are used.
The following site requirements apply:
• Dew point below the measurement temperature
• Ambient conditions within the limits specified in the technical data
• No powerful vibrations
• No direct sunlight
• No corrosive gas atmosphere
• No explosive atmosphere
• No powerful electric or magnetic fields

Procedure
1 Place the refractometer on a level surface.
2 Make sure that there are at least 15 cm clearance behind the refractometer.
3 Make sure that nothing blocks the ventilation openings at back of the refractometer.

See also
2 Technical data } Page 93

4.5 Connect the refractometer to the power supply

The AC adapter is suitable for all supply line voltages ranging from 100...240 V AC and 50/60 Hz.

Refractometer Excellence Installation and commissioning​​ 13

 WARNING
Danger of death or serious injury due to electric shock!
Contact with parts that carry a live current can lead to death or injury.
1 Only use the METTLER TOLEDO power supply cable and AC adapter designed for your
instrument.
2 Connect the power cable to a grounded power outlet.
3 Keep all electrical cables and connections away from liquids and moisture.
4 Check the cables and the power plug for damage and replace damaged cables and
power plugs.

NOTICE
Danger of damage to the AC adapter due to overheating!
If the AC adapter is covered or in a container, it is not sufficiently cooled and overheats.
1 Do not cover the AC adapter.
2 Do not put the AC adapter in a container.

1 Install the cables in such a way that they cannot be damaged or interfere with operation.
2 Insert the plug of the power cable in the socket of the AC adapter.
3 Insert the plug of the AC adapter in the Power
Supply (1) socket on the rear panel.
4 Insert the plug of the power cable into a grounded
power outlet that is easily accessible.

4.6 Disconnect the refractometer from the power supply

§ The refractometer is shut down.
1 Pull the plug of the power cable out of the power outlet.
2 Pull the plug of the AC adapter out of the Power Supply socket on the rear panel.

4.7 Connect, adjust and disconnect the terminal

4.7.1 Connect the terminal

§ The refractometer is shut down.

1 2

1 Insert one of the plugs of the supplied terminal cable in the socket (1) on the back of the terminal.
2 Insert the other plug of the terminal cable into the Terminal socket (2) on the rear panel.
3 Start up the refractometer.
ð The refractometer automatically detects the terminal and activates it.

14 Installation and commissioning​​ Refractometer Excellence

 See also
2 Start up the refractometer } Page 66

4.7.2 Adjust the angle of the terminal

The angle of the terminal has two positions.
Procedure
§ No task is running.
− To increase the angle of the terminal, fold out the two
feet (1) at the underside of the terminal.

4.7.3 Disconnect the terminal

§ The refractometer is shut down.
1 Pull the plug of the terminal cable out of the socket on the back of the terminal.
2 Pull the plug of the terminal cable out of the Terminal socket on the rear panel.

See also
2 Shut down the refractometer } Page 66

4.8 Setup
This section tells you how to set up the refractometer acccordance with your requirements so that you can carry
out the measurements.
The following summary shows the buttons available in Setup for the various setting options:
Adjustments & Tests Adjustment sets
Test sets

Hardware Cell
Automation
External instruments
Peripherals
Sensors
Auxiliary instruments

User settings Language

Screen
Beep
Shortcuts
Keyboards

Refractometer Excellence Installation and commissioning​​ 15

 Global settings System
User management
Analysis and resources behavior
Physical Properties

Tables & Values Tables

Auxiliary values

Maintenance & Service MT service

Import / Export
Add external cell
Reset to factory settings
Firmware
Update
Hardware / Firmware summary
Cell
Touch screen adjustment
Export of adjustments / Tests / Measurements
The "Expired Resources" button
The Expired Resources button is located on the setup overview screen. It provides you with a summary of all
expired resources, stating the: type, name and expiration date of the respective resource.
Expired resources are entered if the setting "Monitoring adjustment set/test set/auxiliary value" is activated
during setup.
Below you will find a detailed description of the setting options available in setup:

4.8.1 Adjustments & Tests

Navigation: Home > Setup > Adjustments & Tests
Adjustment and test sets can be administered as described below. You can create new sets and delete existing
ones (when deleting you receive a prompt with the option to cancel). Before an adjustment or test can be
performed, an adjustment or test set must be defined.
A maximum of six different adjustment sets or test sets respectively can be entered in the set list.
Before an adjustment or test can be performed, an adjustment or test set must be defined.

4.8.1.1 Adjustment Sets

Via the button Adjustment sets you will obtain a list of the defined sets. The default set "Air&Water20.00C" is
always available and cannot be deleted. When you click the sets, you obtain more detailed information about
the individual sets. The parameters "Adjustment mode", "Temperature" and "Set name" are displayed.
Creating adjustment sets
You can create your own adjustment sets via the button New. The Adjustment set parameters dialog opens.
Parameter Description Values
Adjustment mode Defines the standard that is used for the adjustment procedure. Air&Water |
Standards requires a valid adjustment with Air&Water at this Air&Standard |
temperature. (Air&Standard and Water&Standard are not Water&Standard |
available for refractometers). Standards
Temperature Defines the temperature at which the procedure is performed. 0.00…100.00 °C |
32.00…212.00 °F
Set name Specify a descriptive name of your choice. 1…30 characters

16 Installation and commissioning​​ Refractometer Excellence

 Delete adjustment sets
1 To delete a created set, click the desired entry in the Adjustment sets dialog.
2 In the Adjustment set parameters dialog, click the button Delete.
ð When a set is deleted, the set history will also be deleted. Methods that refer to the deleted set are no
longer executable.

4.8.1.2 Test Sets

Via the button Test sets you receive a list of the defined sets. The default set "Water20.00C" is always available
and cannot be deleted. When you click the test sets, you obtain more detailed information about the individual
sets. The parameters "Test mode", "Temperature", "Set name" and depending on the mode "Standard name" are
displayed.
Creating test sets
You can create your own test sets via the button New. The Test set parameters dialog is opened.
Parameter Description Values
Test mode Defines the standard that is used for the test procedure. Air | Standard | Brix
standard
Temperature Defines at which temperature the test will be performed. -
Standard name Specify a descriptive name of your choice. 1…30 characters
Set name Specify a descriptive name of your choice. 1…30 characters
Delete test sets
1 To delete a created set, click the desired entry in the Test sets dialog.
2 In the Test set parameters dialog click the button Delete.
ð When a set is deleted, the set history will also be deleted. Methods that relate to the deleted set are no
longer executable.

4.8.2 Hardware
Navigation: Setup>Hardware
In this dialog window you can configure all the hardware components connected to the meter. These include:
• Cell
• Automation
• External instruments
• Peripherals
• Sensors
• Auxiliary instruments

4.8.2.1 Cell
Navigation: Home > Setup > Hardware > Cell
The measuring cell is connected via an internal interface in the compact device. The instrument can be
extended to create a 2–cell instrument (see also "Setup: Maintenance & Service > [Add external
cell } Page 35]").
− Touch the button Cell in the Hardware dialog.
ð With single cell instruments you go directly to the list with the cell parameters
ð In the case of two cell instruments the connected cells are listed. You have to touch one of the displayed
cells so that the Cell parameters dialog opens.
ð The Cell parameters dialog is opened.

Refractometer Excellence Installation and commissioning​​ 17

 Parameter Description Values
Cell Name of the measuring cell -
Type Measuring cell type -
Status Shows whether the cell is connected. -
Serial number Serial number of the cell -
If an adjustment has been performed, an entry in the adjustment set appears in the setup of the corresponding
cell. If you touch the entry, the data of the most recent adjustment that was executed with the set will be
displayed.
Parameter Description Values
Adjustment set By touching the set entry, you obtain the values for the most -
recent adjustment of this set.
Monitoring Monitoring of the service life of the adjustment can be activated. -
adjustment set The process, if the service life of a set has expired, is defined in
the method function "Measure".
Adjustment Validity of adjustment "Monitoring adjustment
interval set" activated
Reminder Before the set expires, a message appears indicating that the "Monitoring adjustment
adjustment or test has expired. set / test set" activated
Days before Specifies the number of days after which a warning is triggered. "Reminder" activated
expiration
If a test has been performed, an entry in the test set appears in the setup of the corresponding cell. If you touch
the entry, the data of the most recent adjustment that were executed with the set will be displayed.
Parameter Description Values
Test set By touching the set you go to the values for the most recent test -
for this set.
Monitoring test Monitoring of the service life of the test can be activated. The -
set process, if the service life of a set has expired, is defined in the
method function "Measure".
Test interval Service life of test "Monitoring test set"
activated

Parameter Description Values

Reminder Before the set expires, a message appears indicating that the "Monitoring adjustment
adjustment or test has expired. set / test set" activated
Days before Specifies the number of days after which a warning is triggered. "Reminder" activated
expiration
Via the button History you go to a list that contains a maximum of ten adjustment or test entries for the selected
set. In the process the measured refractive index values are displayed (in the adjustment mode air and water
only the value for water). The history can be displayed in graphic form via the button Graph. You can view the
history data by touching an entry.

4.8.2.2 Automation
Navigation: Home > Setup > Hardware > Automation
The automation units that can be installed are listed below:
• DryPro (drying pump)
• SPR200 (sample pump)
• SC1 (automation unit for a sample)
• SC30 (automation unit for 30 samples)

18 Installation and commissioning​​ Refractometer Excellence

 • InMotion (automation unit for up to 303 samples)
The peripheral devices have an automatic PnP (Plug and Play) – identification. They can also be manually
created in the setup.
Via the button Automation in the Hardware dialog, you access a list with defined automation units. By
touching a list entry, you obtain more detailed information about the corresponding automation unit.
Parameter Description Values
Type Instrument Type -
Power purge unit The external diaphragm (Optional) has a much higher output "Type" = "SC1" / "SC30"
than the diaphragm pump integrated in the SC1/SC30. The pump
is actually adjusted at the SC1/SC30.
Heating option This is where the heating option is activated. The temperature is "Type" = "SC1" / "SC30"
directly set on the heating unit.
Limit sensor Optical sensor that detects the sample and prevents it leaving the "Type" = "SC1" / "SC30"
heated area of the heating option (info field).
External drain Located in the heating unit. Prevents the samples flowing back "Type" = "SC1"/"SC30"
valve after filling process (info field).
Solvent 1 Specifies the solvent at the connection Rinse 1 "Type" = "SC1" / "SC30"
Solvent 2 Specifies the solvent at the connection Rinse 2 "Type" = "SC1" / "SC30"
Speed "Low" Value for speed level "Low" of the SPR200 or InMotion "Type" = "SPR200" /
autosampler (in % of the maximum speed). "InMotion"
Speed "Medium" Value for speed level "Medium" of the SPR200 or InMotion "Type" = "SPR200" /
autosampler (in % of the maximum speed). "InMotion"
Speed "High" Value for speed level "High" of the SPR200 or InMotion "Type" = "SPR200" /
autosampler (in % of the maximum speed). "InMotion"
Rate at 100% Value for max. possible pump output (depending on the installed "Type" = "InMotion"
pump which is defined as sampling pump).

Stirrer output Specifies the pump/stirrer port on the InMotion where your stirrer "Type" = "InMotion"
is connected.

Sampling pump Specifies the pump/stirrer port on the InMotion where your "Type" = "InMotion"
output sampling pump is connected.

PowerShower Specifies the pump/stirrer port on the InMotion where your pump "Type" = "InMotion"
output for PowerShower is connected.

Rate Value for required pump output for PowerShower. "Type" = "InMotion"

Beaker height Specifies the height of the used beakers. "Type" = "InMotion"
A distinction should be made between the following two cases in the installation of instruments:
1. There is still no setup entry available in the unit (delivery state).
A new entry has been generated and the parameters automatically generated.
2. A setup entry was previously manually created in the instrument:
The PnP parameters are automatically entered, the remaining parameters, previously edited by the user,
remain unchanged.
When a PnP instrument is unplugged, the status changes to "not installed".
Below is described how you can administer the various devices in setup. This includes the creation of devices
or changing the parameters in the setup.
Create automation units
So that methods for the application of automation units can be created and configured without the automation
unit being connected, these units must be created in the setup via the button New.

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 Delete automation unit
It is not possible to delete the entry of a connected device.
Note
If you want to delete an entry for a unit that is not connected from the list, a message with the termination
option appears indicating that after deletion the methods that use the external instruments will no longer be
executable.

4.8.2.3 External Instruments

Navigation: Home > Setup > Hardware > External instruments
The external instruments that can be installed are listed below. They all have automatic PnP – identification:
• METTLER TOLEDO S20 – SevenEasy™ pH
• METTLER TOLEDO S30 – SevenEasy™ Conductivity
• METTLER TOLEDO S220 - SevenCompact™ pH/Ion
• METTLER TOLEDO S220 - SevenCompact™ Conductivity
• Lovibond colorimeters PFX880 / PFXi880, PFX950 / PFXi950 and PFX995 / PFXi995 series, Tintometer
• Minolta colorimeters CM-5 / CR-5

Note
• The Lovibond colorimeters can be connected to the USB interfaces. For this purpose the USB – RS232
adapter is required (contained in the connection kit).
• For each device type only one entry is possible.

Install devices
A distinction should be made between the following two cases in the installation of instruments:
1. There is still no setup entry available in the unit (delivery state).
A new entry has been generated and the parameters automatically generated.
2. A setup entry was previously manually created in the instrument:
The PnP parameters are automatically entered, the remaining parameters, previously edited by the user,
remain unchanged.
When a PnP instrument is unplugged, the status changes to "not installed".
• Via the button External instruments in the Hardware dialog, you can obtain the list of instruments. By
touching a list entry, you obtain more detailed information about the corresponding instrument.
Create device
So that methods can be created and configured with external instruments, without having to connect the
instrument, the setup entries of the external instruments can be manually created via the button New.
Note
• The pH and conductivity meters can be assigned names individually using the "Instrument" parameter.

Delete devices
It is not possible to delete the entry of a connected device.
Note
If you want to delete an entry for a unit that is not connected from the list, a message with the termination
option appears indicating that after deletion the methods that use the external instruments will no longer be
executable.
SevenEasy™ / SevenCompact™ pH/ion and conductivity meters
1 Select the following for the SevenEasy™ and SevenCompact™ measuring instruments (also refer to the
operating instructions for the measuring instrument concerned):
Manual end point measured value acquisition,
set the unit [pH]" ([mV] not supported).

20 Installation and commissioning​​ Refractometer Excellence

 2 For the SevenCompact pH and conductivity meters, the following must also be selected (also refer to the
relevant operating instructions):
an interval time of 1 s (in menu>Interval measurements),
interface=printer (in menu>Data transmission),
"Send data to interface" (in "Type of data transmission").
3 For temperature compensation, set the unit [°C] at the measuring instruments. Two types of temperature
compensation exist:
- ATC (automatic temperature compensation) with a temperature sensor connected.
- MTC (manual temperature compensation) with no temperature sensor connected.
Note:
The pH or conductivity meters switch automatically, depending on the arrangement.
If the temperature unit at the pH meter or conductivity meter is set to [°C], the results "TpH" and "TCond" will
be converted to the temperature unit set in the instrument, i.e. either [°C] or [°F] . By contrast, if [°F] is set
at the pH or conductivity meter, no result will be calculated. "--" will be output in the results field.
Note
The conductivity units are [mS/cm] / [μS/cm] (depending on the range) or [mS/m] [μS/m] (depending on the
range). However, the results are expressed in [μS/cm]. If you wish to have the result displayed in [mS/cm] or
[mS/m] [μS/m], it will be necessary to recalculate the result using the "Calculation" method function.
Colorimeter
- Lovibond
The Lovibond colorimeter can be used for extinction or transmission measurements. The wavelengths are
output in 5 nm (in the range 420 – 710 nm).
Note
A color measurement may take longer than 25 s.
- Minolta colorimeters CM-5 / CR-5
The Minolta colorimeters can be used for transmission measurements (liquids).
Transmission data are supplied in 10 nm increments within the spectral range 360 – 740 nm.
A color measurement takes approximately 1 s.
The measurements involve high-energy light flashes. For this reason, color scales are not offered for reflection
measurements in the crude oil industry.

Note
• The CR-5 colorimeter does not supply any spectral data.
• Calibration is possible directly at the colorimeter only. The USB link must be disconnected.
• "Illuminant" and "Observer" can be set in the "Configuration" method function. For more information, see
"[Methods and products: Method functions > Configuration } Page 45]".
- Color scales
Navigation: Home > Setup > Hardware > External instruments > Parameters
− Click on "Colorimeter".
ð The "External instrument parameters" dialog appears.
If a device has been connected, a list of color scales is displayed via the Color scales button, that were
available in the most recently connected device. If the device has been manually configured and no device has
yet been connected, then the list is empty.

4.8.2.4 Peripherals
Navigation: Home > Setup > Hardware > Peripherals
In the dialog Peripherals, the following devices and settings can be configured:
• Barcode reader
• USB stick

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 • Fingerprint reader
• Printer
• Personal Computer (PC) – settings
• Network settings
• Network storage
Below is described how you can administer the various devices in setup. This includes the creation of devices
or changing the parameters in the setup.
Barcode reader
Barcode readers have Plug&Play (PnP) recognition and can be installed via the USB interface.
The following barcode readers can be installed:
• Handheld readers
• Built-in readers
You can create the barcode readers via New. A maximum of one entry can be created for both types.
Parameter Description Values
Type Instrument Type -
Serial number Serial number of the corresponding device -
Barcode Infor- Sample ID: on the barcode there is only the sample ID. -
mation Method ID: on the barcode there is the method ID (with this a
saved method can be selected during scanning).
Product ID: on the barcode there is the product ID (with this a
saved product can be selected during scanning).
Sample ID/Method ID: on the barcode there are the sample ID and
method ID (with this a saved method can be selected during
scanning).
Sample ID/Product ID: on the barcode there are the sample ID
and product ID (with this a saved product can be selected during
scanning).
Start pos. sample Start position of the sample ID on the barcode "Barcode information"
ID with sample ID
Number of Length of the sample ID on the barcode "Barcode information"
characters with sample ID
Start pos. method Start position of the method ID on the barcode "Barcode information"
ID with method ID
Number of Length of the method ID on the barcode "Barcode information"
characters with method ID
Start pos. product Start position of the product ID on the barcode "Barcode information"
ID with product ID
Number of Length of the product ID on the barcode "Barcode information"
characters with product ID
Immediate start If this parameter has been activated, when a task is started with "Type" = "Handheld
the barcode reader, the Start analysis dialog is skipped and the reader",
task is started immediately. "Barcode information"
with method ID, product
ID or sample ID
Example of barcode with sample ID and method ID (161218522). (Sample ID=1612 and method ID 18522).
• Start pos. sample ID 1
• Number of characters 4
• Start pos. method ID 5
• Number of characters 5

22 Installation and commissioning​​ Refractometer Excellence

 USB stick
Commercially available USB sticks from USB Version 1.1 are supported.
Fingerprint reader
You can use a fingerprint reader to authenticate users on the titrator. In order to do this, the fingerprint reader
must be activated on the titrator. The following parameters are available for this:
Parameter Description Values
Activate Activates the connected fingerprint reader. -
fingerprint reader
Printer (and USB-RS232 data export)
• Date can be printed with the USB-P25 (strip printer) or with a network printer.
• Data can be exported using the USB data export box. The data are exported in the XML (UTF-8) formats.

Note
• For data export to an RS interface, you need the USB RS232 adapter (USB data export box).
• As desired, data can be printed either as a summary or in a user defined format (via "Print Mode" parameter
"Report" method function; also see "Methods and products: Methods > Method functions > Report")
Note
For printing/USB data export, the following should be taken into consideration:
• In the "Report" method function, the "Print / USB-RS232 data export" parameter must be selected.
You can define the following parameters via the Printer button (Home > Setup > Hardware > Peripherals):
Parameter Description Values
Printer type USB compact printer -
The USB compact printer does not support all languages. This
printer can only print out a limited quantity of analysis data and
results.
USB-RS232 data export
For the RS-232 data export, the data is transmitted regardless of
the selected language. Only a limited quantity of data and results
can be exported.
Network printer
Every connected printer in your local network that supports HP
PLC 3 or Epson ESC/P 2 can be used.
Status Indicates whether the selected printer type is installed (info field). Only for printer type
"USB compact printer"
and "USB-RS232 data
export"
Baud rate The baud rate for data transmission via the USB-RS232 interface. "Printer type" = "USB-
RS232 data export"
Data bit The number of data bits is displayed (info field). "Printer type" = "USB-
RS232 data export"
Stop bit The number of stop bits is displayed (info field). "Printer type" = "USB-
RS232 data export"
Parity Defines the parity protocol. ("Even", "Odd", "None") . "Printer type" = "USB-
RS232 data export"
Handshake Data transmission via the RS-232 interface ("Xon-Xoff", "None"). "Printer type" = "USB-
RS232 data export"
Type Choose the printer protocol. "Printer type" = "Network
printer"

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 Network name Define your local network name here. "Printer type" = "Network
printer"

Port number Define your local port number here. "Printer type" = "Network
printer"

Paper size Choose the print-format of the report (A4 / Letter). "Printer type" = "Network
printer"
PC settings
Only one PC connected per measuring instrument can be present at one time. You can select if you wish to set
up a connection to the laboratory program "LabX".
Parameter Description Values
Set up connection If this parameter is activated, a connection to LabX will be estab- -
to LabX at start lished on startup.
up
Note
Changes to the PC settings are not implemented until after the measuring instrument is rebooted.
Network settings
You can define the following parameters for the network – settings:
Parameter Description Values
Type Type of network connection -
Obtain IP address If this device has been activated, the device automatically obtains "Type" = "Ethernet"
automatically an IP address.
IP Address IP address of the instrument -
Subnet mask Subnet mask of the device -
Standard gateway Standard gateway of the device "Type" = "Ethernet"
Note
The device automatically reboots after any change to the network settings.
Network storage
You can define the following parameters for a network – storage:
Parameter Description Values
Transfer via Method for transferring data (only Network share). -
Server PC or server name. Users should have read-write access. -
Maximum 60 alphanumeric characters.
Share name Name of the share which is defined for the shared folder. -
User name Type in the user name for accessing the shared folder. The user -
name must be defined in the setup for the shared folder.
Domain Domain name of the server where the shared folder is located. -
Password Password for the network share. -
Target folder Defines the name of the Target folder where the data is saved. -
The Target folder is a subfolder in the shared folder.
First folder level If specified, the First folder level is a sub-folder in the Target -
folder. This folder can optionally be used to sort data. (None |
User name | Titrator ID | Date | Method ID)
Default: None

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 Second folder If specified, the Second folder level is a second sub-folder in the -
level Target folder. This folder can optionally be used to sort data.
(None | User name | Titrator ID | Date | Method ID)
Default: None
Only if First folder level = activated

4.8.2.5 Sensors
Navigation: Home > Setup > Hardware > Sensors
Sensors can be activated in the setup. The following sensors can be connected:
ErgoSens: Infrared sensor for contactless start of measurement (see "Analysis sequence: Start of analyses").
Before you can use ErgoSens, it has to be activated:
Parameter Description Values
Activate ErgoSens Activates the ErgoSens -
WasteSens or LevelSens: Level sensors for waste bottle.
It is determined whether the maximum filling level of the waste bottle is reached. If the maximum filling level
has been reached, a message appears prompting the operator to empty the waste bottle. The task is then inter-
rupted.
Before you can use WasteSens or LevelSens, it has to be activated:
Parameter Description Values
Activate activates the WasteSens or LevelSens -
WasteSens/
LevelSens
If you connect the density - module, you can use an air pressure sensor:
AtmoSens: Atmospheric pressure sensor for measuring the absolute air pressure.
If an AtmoSens is connected, the atmospheric pressure (if required) is measured with the AtmoSens. If no
AtmoSens is connected, the air pressure is read out from the current value from Home > Setup > Global
settings> Physical properties.

Parameter Description Values

Verify AtmoSens If this parameter is activated, the use of the AtmoSens is enforced -
availability for tasks which require the pressure.

4.8.2.6 Auxiliary instruments

Navigation: Setup>Hardware>Auxiliary Instruments
Auxiliary instruments can be any instruments that access the 24V output or USB-RS232 adapter of the
measuring instrument and that are to be used in a method.
An auxiliary instrument that accesses the 24 V output is switched on for a predefined period and then switched
off again via the corresponding command. The instruments are controlled via the "Auxiliary instrument" method
function.
Auxiliary instruments form part of a method, while peripheral devices are classified as input/output devices
(printers, barcode readers etc.), which do not have direct access to methods.
Starting from the auxiliary instrument list, you can add new auxiliary instruments or select existing ones or
modify their parameters. In addition, the selected auxiliary instruments can be deleted.
Note
A maximum of 30 auxiliary instruments can be entered.

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 § Choose the New button in the Auxiliary Instruments dialog window to open the Auxiliary Instrument
Parameters dialog.
1 Before a new auxiliary instrument can be added, you must first use the "Control type" parameter to select
the manner in which the auxiliary instrument is to be controlled:. The following values are available for
"Control type":
ð 24V output
ð USB-RS-232
2 You can assign a name of your choice to the auxiliary instrument.
The parameters for the control types are listed below:
24V output
Parameter Description Values
Control type The control type of the auxiliary instrument. USB-RS232 | Output
24 V
Name Defines the name of the auxiliary instrument. -
USB-RS-232 interface
Parameter Description Values
Control type The control type of the auxiliary instrument. USB-RS232 | Output
24 V
Name Defines the name of the auxiliary instrument. -
Adapter Defines which adapter is used. Maximum 2 auxiliary instruments "Control type" = "USB-
of type USB-RS-232 can be used in the same method (by using RS232"
adapter 1 and 2)

Parameter Description Values

Baud rate The baud rate for data transmission via the RS-232 interface of "Control type" = "USB-
the adapter. RS232"
Data bit Defines the number of data bits. "Control type" = "USB-
RS232"
Stop bit Defines the number of stop bits. (2 stop bits can only be selected "Control type" = "USB-
if 7 data bits are also selected at the same time.) RS232"
Parity Defines the parity protocol. "Control type" = "USB-
RS232"
Handshake Data transmission via the RS-232 interface of the adapter. "Control type" = "USB-
RS232"
Note
A suitable adapter (USB data export box) is required for the USB-RS-232 connection.

4.8.3 Language
Navigation: Home > Setup > User settings > Language
The following languages are available:
• German
• English
• French
• Italian
• Polish
• Portuguese
• Spanish

26 Installation and commissioning​​ Refractometer Excellence

 • Chinese
• Russian
The language can be defined both for the operation of the terminal as well as for the protocols that are to be
printed out from a printer.
Parameter Description Values
Touchscreen Language of the user interface -
Report Language of the printout* -

Note
*
Chinese can not be selected as language for reports

4.8.4 Screen
Navigation: Home > Setup > User – settings > Screen

The following parameters can be set in the screen settings:

Parameter Description Values
Primary color Color of the user interface -
Brightness Brightness of the display -
Button shape Shape of buttons on the touchscreen -
Screen saver Activates screen saver -
Wait time Time for the display of the screen saver Activates screen saver

4.8.5 Beep
Navigation: Home > Setup > User settings> Beep
The audio signal is set specifically for each user. You can activate the audio signal in the Audio-Signal
settings dialog.

4.8.6 Shortcuts
Navigation: Home > Setup > User – settings > Shortcuts
In this dialog, every user has the opportunity to administer his or her own selected shortcuts.
The list of all shortcuts for the logged in user can be viewed. Individual shortcuts can be selected and deleted.
You can determine the following parameters:
Parameter Description Values
Description This text is the name of the shortcut that is displayed in the -
Homescreen.
Immediate start When the shortcut is pressed, the display switches directly over to -
the online screen without opening the Start analysis dialog.
Homescreen Selection of the position on the Homescreen -
Position

4.8.7 Keyboards
Navigation: Home > Setup > User – settings > Keyboards
In the Keyboard settings dialog, you can define the layout for the alphanumeric and the numeric input fields.
The following settings are available:
Parameter Description Values
ABC keyboard Defines the layout of the alphanumeric input field. -

Refractometer Excellence Installation and commissioning​​ 27

 123 keyboard Defines the arrangement of the keys for the numeric input field. -

4.8.8 Global Settings

Navigation: Home > Setup > Global setting
In the Global Settings, you can make general settings to the measuring instrument that apply to all users of the
instrument. The settings in this dialog can only be changed by users with the appropriate authorizations.
Global settings include:
• The system settings
• User management for creating user accounts and assigning rights.
• The settings for Analysis and resources behavior.
• Physical properties for defining the "Temperature unit" and the air pressure.

4.8.8.1 System
Navigation: Home > Setup > Global settings > System
In the System settings dialog the following buttons are available:
• Identification:In this menu you can give the measuring instrument a freely definable ID consisting of at
least four characters.
In addition the following information is displayed: Device, serial number and firmware version.
• Date / time:You can define the format used to display the date and time and set the device date and time.
• Data storage: If this parameter is activated, all results that are saved under Home > Results are deleted
(only when device is shut down).

4.8.8.2 User Management

Navigation: Home > Setup > Global settings > User management
By means of the User management dialog you can administer users and account policies for the instrument.
A maximum of 30 different users can be defined, from which only maximum one may be logged in with the
instrument (1 user operation).
User accounts can be deleted and edited.
There is a default user with the user name "Administrator" (user group: Administrators). This cannot be deleted.

4.8.8.2.1 Users
Navigation: Home > Setup > Global settings > User management > User
Via the button New in the User dialog you can open the User parameters of the dialog. It is possible to define
new users here.
Note
"User management" is the only area in which users with administrator rights are able to edit settings and,
therefore, create or make changes to users.
Create a new user in the User parameters dialog as follows:
1 Define a user name.
2 Assign the user to a group. The following user groups are available:
Administrator
Expert
Technician
Operator
Note
For information on the rights of these user groups, see "[Setup (Setup: Global settings > User management >
User groups } Page 29]".
The following parameters are available in the User parameters dialog:

28 Installation and commissioning​​ Refractometer Excellence

 Parameter Description Values
User name The user is uniquely identified in the system via the name. -
Full Name Complete name of the user. -
User Group Selection of the user group for the user. Depending on the user -
group the user has various rights.
Reset password Resets the password for the user to "123456". Activates "Enforce
password/fingerprint"
Lock user Locks the user. Activates "Enforce
password/fingerprint"
Enforce password With the next login the entry of a new password will be enforced. Activates "Enforce
change password/fingerprint"
Created by The administrator logged in at time of creation -
Created on Date of creation and time (info field) -
Modified by The administrator logged in at time of creation -
Modified at Change date and time (info field) -

4.8.8.2.2 Account Policy

Navigation: Home > Setup > Global setting > User management > Account policies
The following parameters can be edited in the dialog:
Parameter Description Values
Enforce If this parameter has been activated, you can only log in by -
password / finger entering the password (or via the fingerprint reader, if the
print parameter "Activate fingerprint reader" is activated, in Home >
Setup > Hardware > Peripherals > Fingerprint
reader).
Min. password The minimum length of the user passwords Activates "Enforce
length password/fingerprint"
If the parameter "Enforce password" is deactivated, then the instrument starts directly, i.e. not via the login
screen (only if one user is defined – corresponds to the factory settings). If several users are defined, the user
name can be selected in the login screen from a list.

4.8.8.2.3 User Groups

Each user is assigned to a user group. The following four user groups (with decreasing rights going
downward) should be distinguished:
• Administrator
• Expert
• Technician
• Operator
The following table presents the user rights that are assigned to the corresponding user group:
List of user rights
Right Minimum required user group
Start analysis via Shortcuts. Operator
Start analysis via Start button in the Homescreen Operator
Start analysis with ErgoSens Operator
Start analysis from method editor (for method type: Technician
measurement, cleaning and test), product and series
editor (for method type: measurement, cleaning, test
and adjustment)

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 Right Minimum required user group
Adding/deleting items for series in the Start analysis Technician
dialog (does not apply for adjustment-type methods)
Executing manual operations Technician
Editing shortcuts Technician
(Setup>User settings)
Including and excluding results Technician
Deleting results Expert
Adding/deleting items for series in the Start analysis Expert
dialog (also applies for adjustment-type methods)
Setting the language for touchscreen and reports Expert
Start analysis from method editor (for method type: Expert
measurement, cleaning, test and adjustment)
Editing methods, products, series Expert
Editing "Adjustments & Tests" Expert
(Home > Setup )
Editing "Hardware" Expert
(Home > Setup)
Editing "Analysis and resources behavior" Expert
(Home > Setup > Global setting)
Editing "Tables & Values" Expert
(Home > Setup)
Setting the language for reports Expert
Editing "Physical properties" Expert
(Home > Setup > Global setting)
Running "Maintenance & Service" in Home > Setup, Expert
except:
• Importing/exporting user management and
memory copy
Running "Maintenance & Service" Administrator
(Home > Setup),
including:
• Importing/exporting user management and
memory copy
Editing "User management" Administrator
(Home > Setup > Global setting)

4.8.8.3 Analysis and Resources Behavior

Navigation: Home > Setup > Global settings > Analysis and resources behavior.
The following settings can be defined:
Parameter Description Values
Show required If this parameter is activated, all resources are shown during -
resources at start startup that are required for performance of the analysis.
Note: If a required resource is not available, the "Needed
resources" dialog is also shown without this parameter having
being activated.

30 Installation and commissioning​​ Refractometer Excellence

 Confirm end of If this parameter is activated, the OK button is shown at the end of -
the analysis the task. The task is not ended until you confirm with OK. This
parameter is especially used if the result should remain on the
online screen at the end of the measurement so that, for example,
it can be copied.
Reset statistics if If this parameter is activated, the rolling statistics will be inter- -
sample ID rupted, if the sample ID differs from the previous analysis. If it is
changes not activated, the rolling statistics will only be interrupted if the
method ID (or product ID) differs from the previous analysis.
Verify USB stick If this parameter is activated and a USB stick is used in the -
availability method, the task will be checked when the start is started to see if
the USB stick is available. If none is available the task cannot be
started.

Parameter Description Values

Verify printer If this parameter is activated and a printer is used in the method, -
availability the task will be checked when the task is started to see if the
printer is available. If the printer is not available the task cannot
be started (does not work for network printers).
Information on If this parameter is activated, a message is shown when a PnP -
identification of resource is detected.
PnP resources
Verify network If this parameter is activated and network storage is used in the -
storage avail- method, the task will be checked when the task is started to see if
ability a network storage is available. If no network storage is available,
the task cannot be started.

4.8.8.4 Physical Properties

Navigation: Home > Setup > Global setting > Physical properties
In the Physical properties dialog you can defined the parameters "Temperature unit" [oC] or [oF] and
"Atmospheric pressure" in [hPa].
Parameter Description Values
Temperature unit Temperature unit applicable for all ranges of the instrument -
(global setting). Either Celsius or Fahrenheit can be selected. All
inputs or outputs are in the temperature unit selected here. The
setting is saved after a restart.
Atmospheric Input of atmospheric pressure that is used for calculating the -
pressure nominal value of the air density. The atmospheric pressure is
required for an adjustment or a test with air or a cell test. If the
AtmoSens is connected, the reading will be displayed here.
Note
The atmospheric pressure is only required when using the density - module.

4.8.9 Tables & Values

Navigation: Home > Setup > Tables & values
The instrument has tables and auxiliary values that can be used for the calculation of results (see also
"Results").
With measurements the raw data (e.g. temperature value and refractive index) are delivered. These results are
fed into the relevant tables so that corresponding results can be displayed in the respective units.
Tables are always assigned to an application. The list can be sorted according to application.

Refractometer Excellence Installation and commissioning​​ 31

 There are two types of tables:
• METTLER TOLEDO tables:
These tables are included in the factory settings, they are only listed and can be neither edited, viewed nor
deleted.
• User-defined tables:
Tables are laid out in the form of a value table (X-Y). They can be created, edited and deleted.
Below is a description of how to create your own tables.
In addition to the tables, you can also administer the auxiliary values in setup. The auxiliary values can thereby
be used in formulas. By means of the method function "Auxiliary value", an auxiliary value from any desired
formula can be assigned raw data or calculated results.

4.8.9.1 Tables
Navigation: Home > Setup > Tables & values > Tables
By opening the Tables dialog you can see a list of available tables (METTLER TOLEDO and user-defined).
How to create tables in the setup is described below.
You can create a table with the New button.
Parameter Description Values
Name Table name: The name uniquely identifies the table in the system. -
The name is entered into the formula in the method function
"Calculation".
Application Application area of table. Facilitates the sorting of the table list. -
Input value Table heading for the input value. -
Output value Table heading for the output value. -
Fit type Definition of the curve type for the calculation. -
• Linear interpolation: Corresponds to a segmented curve.
• Lagrange interpolation: Lagrange fit via four points
• 1 order polynom
• 2 order polynom
• 3 order polynom
1 Save the new table.
ð A dialog opens with the name of the new table.
2 Enter value pairs via New.
Parameter Description Values
"Input value" Input value of the value pair (corresponding to the measuring cell -
used, e.g. density or refractive index)
"Output value" Output value of the value pair (e.g. Brix) -
At least four value pairs must be entered and then saved via the Save button.
− Touch the button Graph. The fit function is graphically presented (the button Graph is only displayed if the
table has been saved).
Note: The axis labeling corresponds to the specified "Input" – (x-axis) and "Output" parameters (y-axis).
ð The table has been successfully entered. The coefficients are calculated according to the selected function.
There is a "delta" column that shows the deviation from the calculated value at the effective table point (only
for the "Fit type" = "Polynomial"). This column is not shown when the table is being edited.
Note
• In the Table – parameters dialog, you can again remove the table via the Delete button.
• A table must contain at least 4 and contain a maximum of 200 value pairs.
• A maximum of 30 user-defined tables may be defined.
• Tables cannot be deleted or modified when they are currently in use.

32 Installation and commissioning​​ Refractometer Excellence

 • The table name must be unique.

4.8.9.2 Auxiliary Values

Navigation: Home > Setup > Tables & Values> Auxiliary values
Via the New button, you open the Auxiliary values parameters dialog. In it you can use the following
parameters to define the auxiliary value:

Parameter Description Values

Name Unique designation of the auxiliary value: The name is entered -
into the formula in the method function "Calculation".
Comment Short comment on the auxiliary value (e.g. about the unit) -
Value Numerical value -
Determination Type of determination method (info field) -
method
Determination Date on which determination was performed (info field) -
date
Performed by Person who performed determination -
Monitoring Specifies whether the auxiliary value is to be monitored. -
auxiliary value
Interval Specifies the time period for monitoring of the auxiliary value. "Monitoring auxiliary
value" activated
Expiry date Expiry date of auxiliary value (info field) "Monitoring auxiliary
value" activated
Reminder Defines whether a reminder should be issued before expiry of the "Monitoring auxiliary
auxiliary value. value" activated
Days before Specifies the number of days after which a warning is triggered. "Reminder" activated
expiration
Note
• A maximum of 100 auxiliary values can be saved in the instrument.
• Auxiliary values cannot be deleted or modified when they are currently in use.
• When an auxiliary value is assigned with the "Auxiliary value" method function, this is updated in the setup
immediately after completion of the method function.

4.8.10 Maintenance & Service

Navigation: Home > Setup > Maintenance & Service
The following functions are available to you:
• MT service
• Import / Export
• Add external cell
• Reset to factory settings
• Firmware
• Update
• Hardware / Firmware summary
• Cell
– One-point temperature alignment (only for density - module)
– Whole-range temperature alignment
– Fan check

Refractometer Excellence Installation and commissioning​​ 33

 – Add manual adjustment
• Export of adjustments / tests / measurements

4.8.10.1 MT Service
Navigation: Home > Setup > Maintenance & Service> MT Service
Via the button MT Service you can open the Last MT services dialog window.
In this dialog, you can view and print out a list of the most recent (max. 10) METTLER TOLEDO services. Under
each date, the user name of the METTLER TOLEDO service technicians and the date and time of the service
appointment are displayed. The most recently performed service always appears at the top of the list.
Via the Settings button in the Last MT services dialog window you can open the Service data dialog window,
via which you can edit the service life of the last service due date. You can define whether a warning should be
issued before the service life expires (requires administrator rights). You can define the following parameters:
• "Service life" (in days) of the most recently performed service.
• "Reminder": Defines whether a reminder should be issued before expiry of the service life of the service.
• "Days before expiration" Number of days before expiration of the service life on which the instrument should
issue a warning.
The entered value must be smaller than the value for the service life (only appears if "Reminder" has been
activated).

4.8.10.2 Import / Export

Navigation: Home > Setup > Maintenance & Service> Import / Export
With the aid of this feature you can save the data on a UBS stick (export) or import data from a stick.
The following can be imported or exported:
• Single method
• All methods
• Single product
• All products
• Single series
• All series
• Single table (only affects user-specific tables)
• All tables (only affects user-specific tables)
• User management
• Memory copy
The following rules apply for Import / Export:
1. Import/Export is only possible when a USB stick is connected.
2. Import/Export is only possible when no task is running.
3. Products can only be imported if referenced methods are already available on the device required for the
import.
4. Series can only be imported if referenced methods or products of the series are already available on the
device required for the import.
− In the Maintenance & Service dialog, open the Import / Export dialog window. In this dialog, you can
define the following parameters:
ð "Action": Data can be exported to a USB stick or imported back from a USB stick.
ð "Data": Data that is to be exported or imported can be selected.

34 Installation and commissioning​​ Refractometer Excellence

 Memory copy
You can create a memory copy from your data. This includes adjustment and test data, auxiliary values,
shortcuts and fingerprints, data relating to automation, peripherals and external instruments. When a firmware
upgrade of the instrument has to be done, the instrument can be restored from the memory copy. The memory
copy can also be imported to another instrument. In this case, the Test and Adjustment history are not imported
and an adjustment of the instrument is required.
Uploading data from a backup copy results in the existing data being overwritten by the data in the memory
copy. In this way you can restore the initial status.
Note
• Not contained in a memory copy are
any saved results, default parameters for manual operations, internal tables, hardware for cell creation or
parameters for added external cells.
• When you import / export user management settings the entire user management settings with all users and
their properties are exported or imported.
• If the import is canceled, all previously imported users are deleted and only a default user (administrator) is
created.
• You must have administrator rights before you can create and reimport a backup copy.

4.8.10.3 Add External Cell

Navigation: Home > Setup > Mainten. & Service > Add external cell
Perform the action "Add external cell". In the Cell dialog box, the cell type must be selected (Home > Setup
> Hardware > Cell).
When you connect the external cell (module), the status changes to "installed" and the effective serial number
is entered.
If the external cell is removed, the entry in the cell list is retained. The status changes to "not installed". The
serial number and the cell type however continue to be displayed.

4.8.10.4 Reset to Factory Settings

Navigation: Home > Setup > Maintenance & Service > Reset to factory settings
With the button Reset to factory settings you can reset your settings.
If you do this all created data, amendments, settings, setup entries or results are lost.
Before you activate "Reset to factory settings" you should create a memory copy.

4.8.10.5 Firmware
Navigation: Home > Setup > Maintenance & Service > Firmware
With the aid of this feature you can display a list showing the most recent firmware updates. The first entry in
the list corresponds to initial operation.
All list entries are saved with a date and FW version.

4.8.10.6 Update
Navigation: Home > Setup > Maintenance & Service > Update
With the aid of this feature a firmware update of the instrument, device board and cells can be performed via a
USB stick. After the button update is touched, all available and associated components that contain firmware
are presented in a list (Instrument FW, cell FW, Device Board FW).

Refractometer Excellence Installation and commissioning​​ 35

 § You must have administrator access rights.
- The instrument is in idle mode (no task is active).
- To update a cell, the cell must be connected. In the process each update must be performed separately for
each connected cell that is to be updated.
1 Via the button update you can open the Firmware – List dialog. Select the relevant components from this
list.
2 Plug in the USB stick with the firmware update files into the instrument.
ð The instrument recognizes the USB stick and enables the update.
3 Start the update.
ð The instrument reboots and starts the update program via the USB stick. The update can be performed in
the update program.
4 When the update program is terminated, the instrument reboots with the normal application.
Instrument update:
All results, settings, setup entries, methods, products and individual modifications are lost during the instrument
firmware update. On the other hand, the service history, the instrument firmware history and serial number are
all retained.
Cell update:
• Only updates from connected and recognized cells are offered, whose update file is on the USB stick.
• With the cell update, no changes are made to the application program and to the individual settings and
methods.
Device board update:
With the device board update, no changes are made to the application program and to the individual settings
and methods.

4.8.10.7 Hardware / Firmware summary

Navigation: Home > Setup > Maintenance & Service > Hardware / Firmware summary
You can view a list with all connected components along with the corresponding information on hardware or
firmware. The list can be saved as a file on a USB stick. The file name contains the serial number of the device
and the current date and time. Example:
HW_SW_Info_5124560983_23_03_2010_08_23.cvs

4.8.10.8 Board Tests

Navigation: Home > Setup > Maintenance & Service > Board tests
With this function, the interfaces of various boards can be tested:
• Main board
• Device board
• External cell board, if an external cell is connected
The sequence for testing the boards is described below:
1 Via the button Board tests you can open the Boards dialog. In this dialog, buttons are provided, which
guide you to the corresponding board information for the connections.
2 Touch the button for the desired board and you will receive an information list with the connections on the
board and the required resources that must be plugged into the corresponding connection.
3 Touch the Start button, to go to the list of test functions.
- By touching a test, you change over to the corresponding test and this can then be started. Pop-ups guide
you through the test process and show you any errors identified.
- The test result is also displayed in the interface list.
4 You can select another interface and proceed as described above or you can cancel the test with the Stop
button.
ð When all interfaces for the selected board have been tested and all have the status "successfully
passed", the results can be written onto the USB stick.

36 Installation and commissioning​​ Refractometer Excellence

 4.8.10.9 Cell
Navigation: Home > Setup > Maintenance & Service > Cell
Via the Cell you get to the service function of the cells.
This dialog window contains the following buttons:
Button Parameters
One-point temperature alignment Adjustment of the cell temperature to the set temperature. The
block thermistor is adjusted to the certified cell thermistor at the
current set temperature.
The One-point temperature alignment dialog shows the selected
cell, the set (Tset), the cell (Tcell) and the cell block temperature
(Tblock).
Whole-range temperature alignment Adjustment of the cell temperature to the set temperature across
the entire temperature range.
Note: The alignment takes about two hours.

The Whole range temperature alignment dialog shows the selected cell, the current values of the set (Tset),
cell (Tcell), cell block- (Tblock) and the ambient temperature (Tambient).
The alignment can be started when the temperature in the cell is stable and the cell is dry and clean.
Note:
• If there is an error message, the current values are saved on the display so that it can be seen at which
temperature the error occurred.
• With Stop the alignment can be interrupted at any time.
• During alignment, the temperature per interval is saved in a file. This file can be saved on the USB stick.
Fan check The functional efficiency of the fans is tested.
The display is periodically updated.
Note: The instrument is not switched off when there is an error
display.
Add manual adjustment This function simulates an adjustment. It is used in order to
perform a measurement without previously adjusting the
instrument.
Note: Only use for demonstration or method development
processes!

4.8.10.10 Export Adjustments / Tests / Measurements

Navigation: Home > Setup > Maintenance & Service > Export of adjustments / Tests /
Measurements
With the aid of this function, the adjustment, test and measurement history can be saved on the USB stick so
that it can then be imported into an EXCEL file.
• The histories can be viewed and exported.
• The measurement history is only exported if the measured data agree with the current cell configuration (if
the external cell type is changed, the measured data cannot be exported from the previous cell).

Refractometer Excellence Installation and commissioning​​ 37

 5 Configuration of measurement methods
A method basically consists of the configuration, sample feed, the actual measurement, cleaning, result calcu-
lation and the creation of a report. These steps are defined as functions. The individual functions in turn consist
of parameters, whose values or names can be changed.
Method types
The instrument distinguishes between the following method types with different objectives:
• MS (Measurement), for the performance of a measurement
• ADJ (Adjustment), for an adjustment of the measuring cell(s)
• TE (Test), for testing the measuring cell(s)
• CL (Cleaning), for cleaning the measuring cell(s)

5.1 Establishing Methods

When creating methods (max. number of methods: 30) you can make use of method templates with
predefined method types and hence structures. The corresponding parameters thereby contain suitable default
values.
Select: Home > Methods / Products > Methods
1 Choose New to create a new method on the basis of a template.
2 Select the desired method type from the available templates. Now you can adjust this method to your own
specifications by adding or deleting method functions, or by adjusting the settings.
ð After a template has been chosen, the Configuration dialog opens. Here, according to the defined setup,
you can select the cell mode, the cell, automation unit and the external devices (pH, conductivity and
colorimeter) with which you wish to carry out the method.

Parameter Description Values

Cell mode Defines the type of cells (Density/Refractometry). D | R | D+R | D+D | R+R
Automation Defines the automation unit used by the method. The choice -
available depends on the automation units defined in Home >
Setup > Hardware > Automation.
Note
• If the filling and rinsing is performed with "SPR200" and
drying with "DryPro", then "SPR200+DryPro" must be
selected.
• If the InMotion autosampler is used together with a DryPro in
method type "Clean", both (InMotion and DryPro) must be
selected.
Lid handling Defines whether CoverUp (optional lid handling system on Automation unit" =
InMotion) is used in the method. "InMotion"

Parameter Description Values

pH Defines whether the pH meter is used in the method. "Method type" =
"Measurement"
pH meter is defined in
"Home > Setup >
Hardware >
External
instruments".

38 Configuration of measurement methods​​ Refractometer Excellence

 Conductivity Defines whether the conductivity meter is used in the method. "Method type" =
"Measurement"
Conductivity meter is
defined in "Home >
Setup > Hardware >
External
instruments"
Color Defines whether the colorimeter is used in the method. "Method type" =
"Measurement"
Colorimeter is defined in
"Home > Setup >
Hardware >
External
instruments".

Note
Up to the automation unit, these settings cannot be retrospectively modified.
Parameter Description Values
Color settings Activates "Illuminant" so that the illuminant type can be defined Active | Inactive
(Minolta only) and "Observer" so that the angle can be entered.
Illuminant Defines the illuminant to be used. A | C | 65 | D50 | ID65 |
ID50 | F2 | F12
Observer Defines the viewing angle. Default 2°. 2° | 10°
Note
The parameters "Color settings" (Minolta only), "Illuminant" and "Observer" are used only with Minolta
colorimeters.
1 Confirm with OK.
2 In the "Title" method function, enter a new method ID. Afterwards, the new method will be stored under this
method ID.
3 Save the method.
ð You have now created a new method with its own ID. This method already has predefined method
functions. To change the method functions proceed as follows:
4 Select available method functions to modify their parameters in line with your requirements.
5 Choose Insert to add additional method functions to the method.
6 Now use the arrow-shaped "Insert" button to select the required position for the new method function in the
method. (You will only be able to insert the method functions that are allowed in the corresponding location
based on the method syntax.)
Note: It is a good idea to save at regular intervals.
7 From the list, select the method function that you want to insert.
8 Modify the individual parameters of the method function.
ð The new method function will be displayed in the method.
9 To delete a method function, select the function in question and then choose Delete.
ð The method function will disappear from the method.
Note: Some essential method functions cannot be deleted.
(The "Delete" button is not available in these cases.)
10 After inserting all desired method functions, you can store the new method in the device by choosing Save.
Note
When creating a new method, follow the rules specified by the device. These are described in Chapter "Method
Syntax – Rules for Establishing methods".

Refractometer Excellence Configuration of measurement methods​​ 39

 5.2 Creating a Method Copy
You can copy an existing method by changing the ID of the method in the method function "Title". When the
method is saved a new method is created.

5.3 Modifying or Deleting Methods

Modifying a method
To modify a method, select: Home > Methods / Products > Methods
1 From the displayed list of methods, select the method that you want to modify.
2 As soon as the methods functions of the selected method appear on the screen, you can edit and save the
method.
Delete Method
It is simple to delete newly created methods. Select: Home > Methods.
1 Select the method that you want to delete.
2 Choose Delete method to delete the method from the memory.
Note
Shortcuts, products and series that refer to the method will also be deleted.

5.4 Method Syntax

The following rules describe in which point method functions can be inserted or deleted. Only the available
method functions are displayed for insertion.
Rules for method type "Measurement" (MS)
• The following method functions cannot be deleted: Title, configuration, sample, filling, measure and online
display.
• The method functions "Calculation" (R1, R2,….Rx) and "Temperature compensation" (TC1, TC2,…TCx) are
indexed.
• A maximum of 20 method functions "Calculation" can be inserted.
The method function "Temperature compensation" can be inserted a maximum of five times, in each case
immediately after the method function "Measure".
Insertion of the "Report" method function is limited for the following method types:
- twice for "Measurement" and "Test"
- once for "Adjustment" and
- "Report" cannot be inserted for "Cleaning".
Method functions can be inserted in the method as follows:
Template Method function
Title
Instruction, Auxiliary
instrument
Configuration
Instruction, Auxiliary
instrument
Sample
Calculation, Clean,
Instruction, Auxiliary
value, Wait, Auxiliary
instrument, Stir, Line
rinse
Fill

40 Configuration of measurement methods​​ Refractometer Excellence

 Calculation,
Instruction, Auxiliary
value, Wait, Auxiliary
instrument, Stir
Measure
Calculation, Report,
Clean, Instruction,
Auxiliary value,
Temperature compen-
sation, Wait, Auxiliary
instrument
PowerShower, Line
rinse
Calculation R1
Calculation, Report,
Clean, Instruction,
Auxiliary value,
Temperature compen-
sation, Wait, Auxiliary
instrument,
PowerShower, Line
rinse
Clean
Calculation, Report,
Clean, Instruction,
Auxiliary value,
Temperature compen-
sation, Wait, Auxiliary
instrument,
PowerShower, Line
rinse
Online Display
Report
Report

Rules for method type "Adjustment" (ADJ)

• The following method functions cannot be deleted: Title, Configuration, sample, Filling, Measuring and
adjustment.
• The method functions are executed twice between "Sample" and "Adjustment".
The following method functions can be inserted in the method template:
Template Method function
Title
Instruction, Auxiliary instrument
Configuration
Instruction, Auxiliary instrument
Sample
Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument, Line
rinse
Fill
Instruction, Auxiliary value, Instruction, Wait, Auxiliary instrument
Measure

Refractometer Excellence Configuration of measurement methods​​ 41

 Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument, Line
rinse
Clean
Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument, Line
rinse
Adjustment
Instruction, Auxiliary instrument
Report

Rules for method type "Test" (TE)

The following method functions cannot be deleted: Title, Configuration, Sample, Filling, Measure and Test.
The following method functions can be inserted in the method template:
Template Method function
Title
Instruction, Auxiliary instrument
Configuration
Instruction, Auxiliary instrument
Sample
Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument, Line
rinse
Fill
Instruction, Auxiliary value, Wait, Auxiliary instrument
Measure
Report, Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument,
PowerShower, Line rinse
Clean
Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument
Test
Report, Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument,
PowerShower, Line rinse
Clean
Report, Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument,
PowerShower, Line rinse
Report
Report, Clean, Instruction, Auxiliary value, Wait, Auxiliary instrument,
PowerShower, Line rinse

Note
The "Report" method function can be inserted a maximum of two times. There is no limit on the other method
functions.
Rules for method type "Clean" (CL)
The following method functions cannot be deleted: Title and Configuration.
For the method type "Clean" at least a method function "Clean" or "Cell test" must be available.
The following method functions can be inserted in the method template:
Template Method function
Title

42 Configuration of measurement methods​​ Refractometer Excellence

 Instruction, Auxiliary instrument
Configuration
Clean, Instruction, Wait, Auxiliary instrument, Stir, Park, PowerShower,
Line rinse
Clean
Clean, Instruction, Wait, Auxiliary instrument, Stir, Park, PowerShower,
Line rinse

5.5 Standard Data

The standard data are editable according to mode and standard.
Parameter Description Values
Standard name Specify a descriptive name of your choice. 0…30 characters
Lot number The lot or batch number of the standard. 0…30 characters
Date of certifi- The certification date of the standard. Date
cation
Expiry date Std The expiry date of the standard. Date
nD nominal Defines the nominal refractive index value of the standard. 1.32…1.7
d nominal Defines the nominal density value of the standard. 0.00000…3.00000
Uncertainty d [g/ Limits of error of the standard (with reference to the nominal 0…0.001
cm3] value).

5.6 Condition
A logical condition can be defined to determine whether a particular method function should be executed based
on a result (true or false). The condition is in the format of a formula. An empty condition is interpreted as true.
Formulas can be used in various method functions. In formulas you can enter the calculated results Rx,
temperature-compensated values (TCx), tables, auxiliary values and raw data.
Formula Editor
Navigation: Home > Methods / Products > Methods > Method > Calculation
With the formula editor both numerical values and symbols can be entered. The symbols H, T and C are made
available when you select the 1 button in the formula editor.
If you touch H, the list of auxiliary values opens; T opens the table list; C opens the list of color scales for the
colorimeters. For colorimeters, it is possible to define whether measurements should be carried out in extinction
or transmission mode.
You can enter raw data manually or via insert via the button "Proposal". You will find the raw data in the
"Annex: Raw data".
Mathematical Functions and Operators
The following mathematical functions and operators can be used in formulas:
Functions Comparison operators
Logarithm to the base 10 lg(x) equal to =
Logarithm to the base e ln(x) larger than >
Exponential to base 10 pw(x) or larger than or equal to >=
scientific notation
Exponential to base e ex(x) smaller than <
Square sq(x) smaller than or equal to <=
Square root sr(x) x in the range of ... < x < ...
not equal to <>
approximately ~

Refractometer Excellence Configuration of measurement methods​​ 43

 Mathematical operators Logical operators
Addition + and AND
Subtraction - or OR
Multiplication *
Division /
Note
• Logical operators are only permitted within formulas of the subfunction "Condition".
• The use of mathematical operators (+, -, * and /) within a parenthetical expression is not possible.

Formula Syntax
- Brackets
There are three types of brackets that can be used in formulas:
• Round brackets "( )":
e.g. T[Table_name(d)] and mathematical operators ln(d)
• Square brackets "[ ]"
- Table name T[Table_name()] , e.g. T[Brix_d_NBS(d)];
- Auxiliary value H[Auxiliary_value], e.g. H[Auxiliary_Value_1]
• Curly brackets "{ }": Relation to the cell, e.g. d{DX}. if the cell is not specified, then the internal cell is used
as default.
- Fixed abbreviations
The following abbreviations are defined:
R Internal refractive index cell

RX Refractive index module

R1 ... Rx Results from the method function "Calculation"
TC1 … TCx Results from the method function "temperature compensation"
A, B, C, D, x, y Coefficients (A-D) and variables (x,y) can be used in formulas, e.g. Ax + B.

- Syntax examples
• Simple raw result: R1 = nD
• Temperature compensation: R1 = TC1
• Tables: R1 = T[Brix_nD_20C (nD)]
The following values can be entered for tables:
- Internal tables: d, dRaw, TC
- User-defined tables: All generated analysis data
- Density modules: d, dRaw, TC
- Internal refractive index cell: nD, TC

5.7 Method functions

5.7.1 Title
The method function "Title" contains general method data.
Parameter Description Values
Type Method type (measurement, adjustment, test, cleaning): Defined -
by the selection of the method template during creation of the
method (info field).
Method ID The method is uniquely identified in the system via the method ID. -
Once the method has been saved, the method ID can no longer
be changed. A change of the method ID results in the creation of
a copy of the method.

44 Configuration of measurement methods​​ Refractometer Excellence

 Title Title of the method. -
Author Name of creator (info field) -
Created on Date of creation and time (info field) -
Modified at Change date and time (info field) -
Modified by User who made change (info field) -
Protect When this is activated, only the author or an administrator can -
edit or delete the method.
SOP On activation a text is displayed before the start. -
SOP-Text Displayed SOP text "SOP" activated

5.7.2 Configuration
Used for making settings for cells, automation and external instruments.
The settings in the method function "Configuration" affect the parameters of the following method functions.
Parameter Description Values
Cell mode Display of cells to be used in the method (info field) -
Automation Defines the automation unit used by the method. The choice -
available depends on the automation units defined in Home >
Setup > Hardware > Automation.
Note
• If the filling and rinsing is performed with "SPR200" and
drying with "DryPro", then "SPR200+DryPro" must be
selected.
• If the InMotion autosampler is used together with a DryPro in
method type "Clean", both (InMotion and DryPro) must be
selected.
Lid handling Defines whether CoverUp (optional lid handling system on Active | Inactive
InMotion) is used in the method.
External Display of external instruments (pH, conductivity, color) to be -
instruments used in the method is to be measured (info field)
Color settings Activates "Illuminant" so that the illuminant type can be defined Active | Inactive
(Minolta only) and "Observer" so that the angle can be entered.
Illuminant Defines the illuminant to be used. A | C | 65 | D50 | ID65 |
ID50 | F2 | F12
Observer Defines the viewing angle. Default 2°. 2° | 10°
Note
The parameters "Color settings" (Minolta only), "Illuminant" and "Observer" are used only with Minolta
colorimeters.

5.7.3 Sample
By means of the method function "Sample", sample data for the following method types are defined:
Method type: Measurement
Parameter Description Values
Viscosity Activation of the viscosity correction Density - Module
correction defined

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 Viscosity ≤2000: Density - Module
For samples with viscosity less than 2000 mPa*s connected
>2000: Viscosity correction
For samples with viscosity greater than 2000 mPa*s activated
- Set value:
With this selection, a known viscosity can be entered
Viscosity value Defines the viscosity value of the sample. 1…99999
[mPa*s]
Sample ID Sample ID can be entered; you can still change this ID at the "Method type" =
analysis start. "Measurement"
Correction factor This factor (f) can be included in the calculations. It can be -
changed before performance of the analysis in the Start analysis
dialog.
Comment A comment was entered before performance of the analysis in the -
Start analysis dialog.
Method type "Adjustment" / "Test" = The standards will be shown
additionally.
Method type: Adjustment
Parameter Description Values
Viscosity Activation of the viscosity correction Density - Module
correction defined
Viscosity ≤2000 (info field) Density - Module
defined
Viscosity correction
activated
Adjustment mode Controls the selection of the adjustment sets and the standard -
specific data. The selection is filtered according to the modes of
the available sets in the Method > Setup > Adjustment
sets. The following adjustment modes are available:
- Air&Water (recommend settings)
- Air&Standard (only for density - module)
- Water&Standard (only for density - module)
- Standards
Adjustment set The adjustment set defines the standards and the temperature at Air&Water |
which the adjustment is performed. The selection of sets is filtered Air&Standard |
according to the selection in Cell mode. Water&Standard |
Air&Water: The instrument accesses its internally saved nominal Standards
value tables.
Standards: The nominal value must be entered.
Adj. temperature The adjustment temperature is displayed (info field). 15 °C | 20 °C | 25 °C
Standard 1 ... 2 Shows the parameters of the standard -
Comment A comment was entered before performance of the analysis in the -
Start analysis dialog.
Method type "Adjustment" / "Test" = The standards will be shown
additionally.
Note
Please note: For using an adjustment set "Standards" in an R/RX, a valid adjustment based on Air&Water
must be stored in the instrument for the same temperature.

46 Configuration of measurement methods​​ Refractometer Excellence

 Method type: Test
Parameter Description Values
Viscosity Activation of the viscosity correction Density - Module
correction defined
Viscosity ≤2000: Density module
For samples with viscosity less than 2000 mPa*s specified and
>2000: viscosity correction
For samples with viscosity higher than 2000 mPa*s. activated
Test mode Controls the selection of the test sets and the standard specific -
data. The selection is filtered according to the modes of the
available sets in the Home > Setup > Test sets. The
following test modes are available:
- Air (Internal standard value table) (only for density - module)
- Water (internal standard value table)
- Default
- Brix standard
Test set The test set defines the standards and the temperature at which Air&Water |
the test is performed. The selection of sets is filtered according to Air&Standard |
the selection in Cell mode. Water&Standard |
Air&Water: The instrument accesses its internally saved nominal Standards
value tables.
Standards: The nominal value must be entered.
Test temperature The test temperature is displayed (info field). 15 °C | 20 °C | 5 °C
Standard Shows the parameters of the standard -
Comment A comment was entered before performance of the analysis in the -
Start analysis dialog.
Method type "Adjustment" / "Test" = The standards will be shown
additionally.
You can find detailed information on the standards in "[Methods and products: Methods > Standard
data } Page 43]".

5.7.4 Fill
Sample feed via the automation unit specified in the method function "Configuration".
Parameter Description Values
Prompt for When activated, a confirmation appears on completion of the Active | Inactive
sample method function Fill, stating that the task is paused until
confirmed.
Speed Pump speed "Automation" =
"SC1" / "SC30": "SPR200" / "SC1" /
• "Maximum": Sample feed with maximum pump speed "SC30" / "InMotion"
• "Reduced": Sample feed with speed set at the automation unit
• "Automatic": The pump speed changes according to the defined
time period from "Reduced" to "Maximum".
"SPR200" / "InMotion":
• "High"
• "Medium"
• "Low"
The corresponding pump speed can be set under Home >
Setup > Hardware > Automation .
Max. filling speed Defines the period of time [s] after which the pump speed 1…10000
after changes to maximum speed.

Refractometer Excellence Configuration of measurement methods​​ 47

 Filling mode Defines the way in which the sample feed is to be stopped. Fixed duration |
Fixed duration: The sample feed is stopped after a certain time. Automatic
Automatic: The measuring signal is used to detect when the
sample has reached the measuring cell. (Not possible with
InMotion sample changer).
Filling duration Defines the fixed duration [s] for the filling. 0…10000
Fill ratio Defines the percentage by which the cell is "overfilled" for 100…1000
automatic filling. For example: After 10 s pumping, the sample is
recognized in the cell, the fill ratio is 150%, i.e. the pump
switches off after 15 s.
(Filling duration + Filling duration x (Fill ratio -100) / 100).
Sample detection Selection of the cell in which the sample detection is carried out. D|R
at
Max. fill duration After this time at the latest, the sample feed for automatic filling is 1…10000
stopped if no new sample is detected in the cell.
Pressure release Determines whether the pressure should be released after filling Active | Inactive
the cells for SC1 and SC30 sample changer.

5.7.5 Measure
Via the method function "Measure", the measurement, data capture and error detection can be configured. It
contains the following subfunctions that are described below:
"Cell"
"Measured value acquisition"
"Error detection"
Subfunction Cell – method type: Measurement
Parameter Description Values
Meas. Defines the measuring temperature. 0.00…91.00 | 0.00…
temperature 95.00
Adjustment set Defines the adjustment set applicable for the measurement. List of available
adjustment sets
Action when This parameter defines the behavior if an adjustment set expired. -
expired In Home > Setup > Cell the monitoring of the adjustment set
can be set.
Action:
• "Block": The method is no longer executable.
• "Warn: A message is shown at the method start. In spite of this,
the method is performed. The analysis is labeled with the status
"OK*".
• "None": No action
Adj. temperature The adjustment temperature is displayed (info field). 15 °C | 20 °C | 25 °C
Verify test set Defines that a method can be executed for the valid test set (the -
last test was passed with the corresponding test set).
Test set Selection of test set to be verified "Verify test set" activated
Action This parameter defines the behavior with an expired test set and "Verify test set" is
whether the last test was valid or not. enabled
(in Home > Setup > Cell it is possible to configure
monitoring of the test set):
• "Block": The method can no longer be run.
• "Warn": A notification is displayed when the method is started.
The method is still executed despite this notification. The analysis
is tagged with the status "OK*".

48 Configuration of measurement methods​​ Refractometer Excellence

 Subfunction cell – method type: Adjustment
Parameter Description Values
Adj. temperature The adjustment temperature is displayed (info field). 15 °C | 20 °C | 25 °C
Subfunction cell – method type: Test
Parameter Description Values
Test temperature The test temperature is displayed (info field). 15 °C | 20 °C | 5 °C
Adjustment set Defines the adjustment set applicable for the measurement. List of available
adjustment sets
Action when This parameter defines the behavior if an adjustment set expired. -
expired In Home > Setup > Cell the monitoring of the adjustment set
can be set.
Action:
• "Block": The method is no longer executable.
• "Warn: A message is shown at the method start. In spite of this,
the method is performed. The analysis is labeled with the status
"OK*".
• "None": No action
Adj. temperature The adjustment temperature is displayed (info field). 15 °C | 20 °C | 25 °C
Subfunction measurement acquisition – method types: Measurement, adjustment and test
Parameter Description Values
Wait time R The refraction index measurement begins after this time has 0…9999
elapsed. This wait time ensures that the prism is completely
wetted with liquid. In the case of multiple measurements, each
measurement is started after this wait time has elapsed.
Wait time Col The colorimetric measurement begins after this time has elapsed. 0…9999
In the case of multiple measurements, only the first measurement
is started after this wait time has elapsed. All other measurements
begin with no wait time.
Endpoint Automatic: The measurement is ended if the defined stability Automatic | Fixed
criteria have been achieved. This is fixed for the method types duration
Adjustment and Test.
Fixed duration: The measurement is stopped after a certain time.
This function is used to shorten the measurement time if high
precision is not required. The measurement is stopped on
achievement of the maximum measurement reliability at the
latest.
Meas. duration Defines the duration of measurement in [s]. 1…9999
Meas. reliability Setting of stability criteria for measurement value acquisition. Medium | High |
Maximum
Max. meas. Maximum duration of measurement. If the measured value has 1…9999
duration not stabilized by this time, the measurement will be canceled with
the status Error. This depends on the stability criteria of the
parameter Meas. reliability.
You record the following measuring errors with the bubble check or a multiple measurement:
• air bubbles in the measuring cell (Bubble Check)
• Solvent residues in the measuring cell
• Solid particles in the sample
With the Bubble Check variations in the measuring signal are analyzed.

Refractometer Excellence Configuration of measurement methods​​ 49

 With Multiple measurement, n measurements are performed. Between measurements, the sample is subject
to continual movement. The standard deviation of the n measurements is added, and checked to see whether it
is smaller than the maximum standard deviation (Max. SD) defined in the method.
Parameter Description Values
Bubble check If activated, the system verifies whether bubbles are present in the Active | Inactive
density cell.
Multiple If activated, several measurements are performed with the same Active | Inactive
measurement sample.
No. of Defines the number of measurements. 2…10
measurements
Refill ratio Used for the calculation of the further movement of the sample 10…100
between two measurements. The refill rate [%] is calculated over
the duration of the sample addition.
Example: The fill duration is 10 s and the refill ratio 50%, i.e.
pumping is activated for 5 seconds.
Max. SD Maximum permitted absolute standard deviation of the 4 | 5 | 6 decimal places
measurements for density, refractive index or color. When the
deviation is exceeded the measurement is interrupted with the
status Error.
The maximum standard deviation must be entered in the function
of the measuring cell type.
Note
For the calculation of the standard deviation SD of the color results, the first color result in the formula of the
"Calculation" method function with the smallest Rx index is used.
If no color result is included in the calculation, "–" will be displayed for the standard deviation, i.e. SD is within
Max. SD.
Single values (d1 to d10) are available as raw results and can be used in a calculation (i.e. for a 3-fold
measurement all 3 single values can be reported).
Parameter Description Values
Repeat if failed If activated, the measurement is repeated if bubble check has Active | Inactive
failed or if Max. SD or Max. deviation are exceeded.
Note: If Multiple measurement is activated, all measurements
are repeated.
Note
For "Repeat if failed", no wait time is included.
Parameter Description Values
No. of meas. Defines the number of measured points used for determining the 1…10
points mean value. Preferably use a high number of 10 measuring
points.
Note: If multiple measurement is activated, only the measured
values from the last measurement repetition are used.
Max. deviation The maximum permissible absolute deviation [pH] of the 0.01…7.00
measured values for pH or conductivity meters. If this is
exceeded, the results are marked accordingly.
Subfunction Error detection – method type: Adjustment / Test
If you are using a density - module, the following additional functions are available:
Parameter Description Values
Bubble check If activated, the system verifies whether bubbles are present in the Active | Inactive
density cell.

50 Configuration of measurement methods​​ Refractometer Excellence

 5.7.6 Calculation
A result can be defined by means of the method function "Calculation". For this purpose any desired formula
with raw data, tables or other calculated results can be entered (see also "Formula syntax and tables" and
"Results"). Results are displayed on the online screen. They are saved after the final "Calculation" method
function has completed.
Results receive an index Rx, by which they can be referenced in formulas of other method functions. The calcu-
lation number (Rx) is increased (from R1 to R20) when the "Calculation" method function is inserted, indepen-
dently of the sequence of the method functions. By means of the button "Results proposals" you can select the
predefined results with unit, coefficients and formulas. You will find the list of predefined results in the Annex.
Parameter Description Values
Name Defines the name of the result generated in the calculation. 1…30 characters
Unit Specifies the unit used for the result. 0…18 characters
Formula Specifies the formula for calculating the result. Mathematical calcu-
lation
Coefficients Activates the coefficients that can be used in the formula. Active | Inactive
For powers to the base 10 the "e"-convention may be used (e.g.
1.2e-4 --> 0.00012).
Variable x / Defines the variables that can be used in the formula. -
Variable y
A/B/C/D Defines the coefficients that can be used in the formula. -
Decimal places Defines the number of decimal places in the calculated result. 0…6
Result limits Limit values for going above and below a result -
Lower limit Lower limit of the result "Result limits" activated
Upper limit Upper limit of the result "Result limits" activated
Interrupt if limits Defines that the measurement will be interrupted if the result is "Result limits" activated
exceeded outside the limits. It then receives the status "Error".
If this parameter is not activated, the measurement continues
even if the limit value is exceeded.
The analysis then receives the status "Limit exceeded"
Statistics For the calculation, rolling statistics are activated. -
Print statistics Defines whether the statistics should be printed out for each "Statistics" activated
sample.
Formula Define a specific condition for calculation. "Condition" activated
(Condition)

See also
2 Calculations in Products } Page 63

5.7.7 Clean
Cleaning the measuring cell by means of the automation unit specified in the method function "Configuration".
Parameter Description Values
Drain Defines whether the contents of the measuring cell should be Active | Inactive
drained.
Drain direction Defines the pumping direction. Waste | Vial | Beaker
Waste: The liquid is pumped through the cell and into the waste
container.
Vial: The liquid is pumped back into the sample vial (SC1/SC30).
Beaker: The liquid is pumped back into the sample beaker
(InMotion).

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 Drain mode Fixed duration: Draining is stopped after a defined time. Fixed duration |
Automatic: The drain duration depends on the sample feed (total Automatic
duration equals the time for which the pump was in operation
during filling).
Drain duration Defines the fixed pumping time [s] for draining. 1…1000
Drain ratio Duration of draining in percentage of filling duration. 10…1000
Rinse cycle 1 Activates a first rinse cycle. Active | Inactive
Solvent Automation unit SC1 / SC30: Selecting the solvent. The selection "Rinse cycle" activated
depends on the solvents entered in Home > Setup >
Hardware > Automation
The solvents are listed in the list field along with the connection.
The name of the solvent is displayed during method execution in
the notification that prompts the rinse process.
Rinse mode 1 Fixed duration: Rinsing is stopped after a defined time. Fixed duration |
Automatic: The rinse duration depends on the sample feed (total Automatic
duration equals the time for which the pump was in operation
during filling).
Rinse duration 1 Defines the fixed rinse time in [s]. 1…1000
Rinse ratio 1 Duration of rinsing as percentage of filling duration. 10…1000
Air addition To increase the efficiency of rinsing, air is mixed with the solvent. Normal | Low | Very low
A higher air ratio causes a more turbulent flow, meaning more
intensive cleaning and lower consumption of fluid.
Rinse cycle 2 Activates a second rinse cycle. Active | Inactive
Dry Activates drying the cell. Active | Inactive
Dry mode Fixed duration: Drying activated
Drying is stopped after a defined time
For the density - the "dry mode" can also be set to "Automatic":
Automatic:
Drying is interrupted, when the oscillation value becomes stable.
Dry duration Defines the fixed drying time in [s]. 1…1000
Max. dry duration Maximum drying time: Density - Module
If the oscillation value has not stabilized by the end of this period, defined
drying is terminated. Dry mode = Automatic
Interrupt if failed If this parameter is activated, the measurement is given the status "Dry mode" =
"Error", if with dry mode "automatic" the oscillation value has not "Automatic"
stabilized within the defined "Max. dry duration". The task list is
then interrupted. If the parameter has not been activated, the
measurement proceeds as normal, even if drying failed.
This parameter is necessary, for example, for when execution of
the "Drying" method function is associated with a condition.
Prompt for DryPro Select if you want a prompt on the homescreen for connecting the "Automation" =
DryPro to the aspiration tube for drying. "InMotion"
"Dry" activated

Suppress prompts Choose if you want to suppress prompts on the homescreen for "Automation" =
the cleaning process. "SPR200" /
"SPR200&DryPro"

Formula Define a specific condition for cleaning. "Automation" =

(Condition) "InMotion"
Only if "Condition"
activated

52 Configuration of measurement methods​​ Refractometer Excellence

 5.7.8 Online Display
You can define the number of displayed results for the online screen (two or four). You can also specify where
the results should be placed.
Parameter Description Values
Displayed results The number of results on the online screen can be selected. -
Top / bottom Place at which the calculated results can be displayed on the "Displayed results" = "2"
screen.
Top left / Top Place at which the calculated results can be displayed on the "Displayed results" = "4"
right / Bottom screen.
left / Bottom right

5.7.9 Report
This method function defines the type and scope of the data to be output for a report sent to network, a USB
stick, printer (stripe printer or network printer) or via a USB-RS232 interface. The "Report" method function
refers to all previous method functions. "Report" contains the following parameters:
Parameter Description Values
Export to USB Analysis data can be exported to a USB stick in a CSV or/and PDF -
stick format. Multiple measurements are arranged in succession in the
same file.
Data export to the USB stick is only possible when the USB stick
is available. This can be checked using the option "Verify USB
stick availability" (Home>Setup>Global settings>Analysis and
resources behavior).
Export to network Analysis data can be exported to a network folder in a XML, CSV -
or/and PDF format. Multiple measurements are arranged in
succession in the same file.
Data export to the network is only possible when the network
connectivity is available. This can be checked using the option
"Verify network storage availability" (Home>Setup>Global
settings>Analysis and resources behavior).

Parameter Description Values

Print / USB- Data are either sent to a USB compact printer, to a network printer -
RS232 data or exported via the USB-RS232 interface. You can define the type
export of data transfer using the "Printer type" parameter in the Setup
menu (Home>Setup>Hardware>Peripherals>Printer).
Print Mode The following values are available: "Summary" or "User defined". -
If "Summary" has been selected, a brief summary of the most
important data is printed.
If "User defined" has been selected, you are presented with
additional parameters enabling you to define which data should
be printed.
Note
"Print Mode" applies only to printing on the printer. For USB-RS232 data export, a fixed data record is exported.
For information on the scope and syntax of the data export, see "RS232 Interface Description"
The following parameters are displayed for "Print Mode"="User defined":
Parameter Description Values
Method/Product Method information is printed or exported, e.g. method ID or "Print Mode" = "User
information product ID, method type. A complete method is not printed. defined"

Refractometer Excellence Configuration of measurement methods​​ 53

 Calculated results The results from the "Calculation" method functions can be printed "Print Mode" = "User
or exported. defined"
Data The raw results produced during the determination and used in "Print Mode" = "User
the calculations are printed or exported. defined"
Sample infor- Information on the sample (e.g. sample ID, viscosity, standard "Print Mode" = "User
mation name) can be printed or exported. defined"
Resource infor- Information on the resource used (e.g. auxiliary value, adjustment "Print Mode" = "User
mation set, cell type) can be printed or exported. defined"
The "Condition" and "Formula" parameters can be found in "Methods and products: Methods: Conditions and
formulas".
The "Report" method function can be inserted a maximum of two times per method for the method types
"Measurement" and "Test" and only once for "Adjustment". See also the flow chart in "Methods and products:
Methods: Method Syntax".

5.7.10 Cell Test

The cell test can only be performed for the density - module.
Use this method function to verify the cleanliness and dryness of a cell, either before or after performing a
measurement, test, or adjustment.
A measurement of the empty (clean and dry) cell is performed, and compares the measured density to the
nominal air density under the current pressure conditions. A warning is shown if the difference exceeds the
defined tolerance.
Parameter Description Values
Tolerance Maximum permissible deviation of the measured air density from 0.0001…0.001
the theoretical value [g/cm3].
Max. test duration Defines the maximum duration of the cell test in [s]. If the 1…9999
measured value has not stabilized by this time, the cell test is
interrupted and is treated as failed.
Interrupt if failed Active: the measurement receives the status Error if the cell test Active | Inactive
fails. The task list is interrupted.
Inactive: the measurement proceeds, even if the cell test has
failed.

5.7.11 Temperature Compensation

Temperature compensation allows you to measure a sample at a temperature and then to output the measured
value at another temperature. This temperature compensation is used in the following cases:
• The measured value must for example be stated at 15 °C, however the sample is too viscous at this
temperature. Therefore these samples must be measured at correspondingly higher temperatures so that
they can be pumped to the measuring cell and remain fluid there.
• For accelerated measurements. If the sample is delivered at 35 °C for example and the measured value is
required at 15 °C, the sample can be measured at 35 °C and the measured value can be compensated to
15 °C.
• If the required reference temperature is outside the range of the measuring instrument (e.g. 120 °C), the
sample can be measured at 75 °C and the result compensated to 120 °C.
To use the temperature compensation, the temperature dependence of the sample must be known.
If you have connected a density - module, you can also use the API table (ASTM-D 1250). The following tables
are used (for crude oils, refined products, lubricants):
• 53A, 53B and 53D for 15 °C
• 5A, 5B and 5D for 60 °F
• 59A, 59B and 59D, for 20 °C

54 Configuration of measurement methods​​ Refractometer Excellence

 The aforementioned ASTM or API tables take as input values the readings taken from a hydrometer, which do
not however make allowance for the coefficient of expansion of the glass hydrometer. Therefore the measured
density cannot be directly used as the input value for these tables.
The measured values are converted to the desired temperature. The output value (TC) of this method function
can be used in the method function "Calculation".
Parameter Description Values
Compensation API (only for external density measuring cell): -
type Temperature compensation with API tables
Formula:
Temperature compensation by entering any desired formula
API table Selection of the relevant API table: Crude oil, refined products, Density - Module
lubricants defined
Compensation type =
API
Compensation - Compensation type = API (only for density - module) -
temp. You can choose from among three reference temperatures (15 °C,
60 °F, 20 °C). The temperature is entered as the input value in
the algorithm for calculating the API compensation.
Compensation type = Formula
The defined value is for information purposes only and is not
included in the calculation.
Output Defines the unit in which the temperature compensated value is to °API | d | SG4 | SG
be expressed.
Formula Specifies the formula for the temperature compensation. Mathematical calcu-
lation
Coefficients Activates the coefficients that can be used in the formula. Active | Inactive
For powers to the base 10 the "e"-convention may be used (e.g.
1.2e-4 --> 0.00012).
A/B/C/D Defines the coefficients that can be used in the formula. -

5.7.12 Adjustment
You can use the "Adjustment" method function to store the adjustment data in the setup for the corresponding
cell(s). Here you can also perform an adjustment analysis that should be used to verify the accuracy of the
determined adjustment data. In this process, the system checks the deviation from the last adjustment. If the
maximum deviation is exceeded, you can decide at the end of the adjustment whether the data is transferred.
Parameter Description Values
Adjustment Defines whether the adjustment should be used to verify the Active | Inactive
analysis accuracy of the determined adjustment data. The system checks
the deviation from the last adjustment. If the maximum deviation
is exceeded, you can decide at the end of the adjustment whether
the data is transferred.
Standard 1 Information of the used standard. -
Max. deviation Input of the maximum permissible deviation. "Adjustment analysis"
activated

5.7.13 Test
This method compares the measured with the theoretical test value. The data from the test is saved in the setup
of the corresponding cell(s).
Parameter Description Values
Tolerance d/nD Allowed tolerance for the test -

Refractometer Excellence Configuration of measurement methods​​ 55

 5.7.14 Instruction
You can determine the output of a message to be displayed during the analysis process. The analysis is inter-
rupted while the message is displayed.
Parameter Description Values
Instruction Freely definable text. Via the input %x% reference can be made to -
results or raw data, e.g. %R1%.
Continue after Confirmation: The analysis will continue as soon as the user Confirmation | Time
confirms the instructions. interval
Time interval: The analysis is continued after the defined time
period has elapsed.
Time interval The time period, in [sec], during which the analysis is paused 0…106
and the instructions are displayed on the screen.
Print The specified text is printed out from the printer. -

5.7.15 Auxiliary Value

By means of the method function "Auxiliary value" a result can be assigned an auxiliary value. These auxiliary
values can be accessed in a formula (also in other methods).
Parameter Description Values
Name Selection of auxiliary value The selection relations to the list in the -
setup (Home > Setup > Tables & Values > Auxiliary
values)
Formula H= Formula for the calculation of the auxiliary value. -
Limits By means of limits, the checking of the calculated value can be -
defined. If the value is outside the limits, it will not be saved as an
auxiliary value.
Lower limit Lower limit for the calculated value. "Limits" activated
Upper limit Upper limit for the calculated values "Limits" activated

5.7.16 Wait
By means of the method function "Wait" a method can be interrupted.
Parameter Description Values
Wait time Defines a waiting time, in [sec]. 1…3600

5.7.17 Auxiliary instrument

This method function activates auxiliary instruments and enables the instrument to communicate with these
auxiliary instruments. Auxiliary instruments can be connected either to the "Aux" (24 Volt) socket on the
instrument board or to a USB interface, using a USB-RS232 adapter. The parameters described in the following
apply to all control types.
These are followed by parameters that can be defined explicitly for the relevant control type:
Parameter Description Values
Control type The control type of the auxiliary instrument. USB-RS232 | Output
24 V
Name Defines the name of the auxiliary instrument. -
Condition Logical condition that determines whether or not a method Active | Inactive
function is executed based on a result (true or false).
A method function can be executed using a specified calculation
formula (see the parameter Formula).

56 Configuration of measurement methods​​ Refractometer Excellence

 Formula Specifies the formula for calculating the result. Mathematical calcu-
lation
Note
A method function can be executed using a specified calculation formula (see also "Methods and products:
Methods > Calculations and formulas").
Control type: 24V output

Parameter Description Values

Mode Defines the mode for controlling the control output. On | Off | Fixed duration
Fixed duration: The control output is switched on for the defined
time interval.
On | Off: The control outlet is switched on or off. After a sample
series the control outlet is automatically switched off.
Duration A time span in [sec] can be defined here for which the control 0…106
outlet should be switched on.
Control type: USB-RS232

Parameter Description Values

Send output Defines whether the instrument sends an output sequence to the Active | Inactive
sequence auxiliary instrument.
Output sequence Defines the output sequence the instrument sends to the auxiliary 1…120 characters
instrument.
The control sequence for the signal receiver - can also contain a
formula or result enclosed in characters % or control characters
in format \xxx where xxx is the decimal number of the ASCII
control character.
\013 for Carriage Return
\010 for line feed.
Wait for input Defines whether the instrument waits for a defined input sequence Active | Inactive
sequence before continuing the method.
Maximum time Defines the maximum time the method function waits for the input 0…1000000 s | ∞ s
sequence. When the maximum time has passed, the method
continues even if no input sequence was detected.
Input sequence Defines the input sequence the spectrophotometer expects from 1…20 characters
the auxiliary instrument.
Input sequence Defines whether the input sequence contains data that is used in Active | Inactive
with results calculations.
Inactive: The instrument waits for the input sequence defined in
Input sequence.
Active: The instrument waits for the input sequence with results
as defined by the various parameters.
Start sequence, Total length, Number of results, Start position
1…Start position 10, Max. length 1…Max. length 10
Start sequence Defines the start sequence that the instrument expects from the 0…20 characters
auxiliary instrument.
The start sequence can contain ASCII control characters in the
format \xxx. Here, xxx is the decimal code of the control
character.
Total length Defines the total length of the input sequence. 1…1000 characters

Refractometer Excellence Configuration of measurement methods​​ 57

 Number of results Defines the number of relevant values that are included in the 1…10
input sequence.
Start position 1… Defines the absolute position of first character of the relevant 1…1000
Start position 10 value. Leading space characters before the result will be ignored.
Max. length Defines the maximum length of the relevant value. 1...1000 characters
1Max. length
10…
Note
• The ASCII control characters can be found at: http://www.asciitable.com/
• Results are stored under the variables "AuxInst x[y]" (x: result number; y: number of the "Auxiliary
instrument" method function). For example: AuxInst 3[2]; where "3" represents the third result in the input
sequence, which was received in the second auxiliary instrument method function in the method.

5.7.18 PowerShower
The PowerShower rinsing offers an automated and effective cleaning mechanism, eliminating carryover thanks
to strong solvent stream that cleans the tubes from top to bottom with the defined number of rinse cycles.
Parameter Description Values
Beaker position Define the position of the rinse beaker. "Automation" =
Current position: "InMotion"
Rinsing is performed in the same beaker.
Next beaker:
Rinsing is performed in the beaker next to the tower (current
position + 1).
Absolute position:
Rinsing is performed in a fix defined beaker on the sample rack.
Position Define the position of your rinse beaker on the sample rack. "Automation" =
"InMotion"
Only if "Absolute
position" is selected
Drain beaker Drains the beaker before rinsing with the complete beaker volume. Active | Inactive
The maximum pumping speed is used for draining.
PowerShower Rinse using the PowerShower pump. During rinsing, the sampling Active | Inactive
rinse pump is always active with maximum speed to prevent overfilling
of the beaker.
Rinse cycles Defines the number of rinse cycles that are performed. 1…100
Volume per cycle Defines the volume of rinsing liquid that the PowerShower pump 0…1000 mL
moves to the sample vessel during each cycle.
Fill beaker Defines whether the PowerShower pump moves the volume Active | Inactive
defined in Volume to the sample vessel.
Volume Defines the volume of rinse liquid, pumped into the beaker, per 0…1000 mL
cycle. The lift will go to position Sample for that.
Fill cell and tubes Fills the cell and tubes with the defined volume using the Active | Inactive
sampling pump.
Volume Defines the volume of rinse liquid, pumped towards the cell. The 0…1000 mL
lift will go to position Sample for that.
Fill beaker Defines whether the PowerShower pump moves the volume Active | Inactive
defined in Volume to the sample vessel.
Volume Defines the volume of rinse liquid, pumped into the beaker, per 0…1000 mL
cycle. The lift will go to position Sample for that.

58 Configuration of measurement methods​​ Refractometer Excellence

 Formula Define a specific condition for rinsing with PowerShower. "Automation" =
(Condition) "InMotion"
Only if "Condition" is
activated

5.7.19 Stir
With this method function you can define a fixed pre-stirring duration and also, if the stirrer shall be activated
after the defined pre-stirring duration.
Parameter Description Values
Speed 1 Define the stirrer speed in percent depending on the maximum 1…100
speed of the stirrer (pre-stirring).
Stir duration Define the stirring time [s] for the pre-stirring. You can define two 0…10000
stirring sections (e.g. 10 s higher speeded for pre-stirring
followed lower speeded until the end of measurement).
Continue stirring Continued stirring after the defined stirring time in Stir duration. Active | Inactive
Speed 2 Define the stirrer speed after pre-stirring in percent depending on 1…100
the maximum speed of the stirrer.
Formula Define a specific condition for stirring. "Automation" =
(Condition) "InMotion"
Only if "Condition" is
activated

5.7.20 Line rinse

This function for InMotion sample changer, starts at Position Rinse (or when using higher beakers at a higher
position) and moves down at a variable speed (Descent rate). Air bubbles are introduced with the rinsing
liquid in the beaker for mechanical cleaning of the system.
Parameter Description Values
Beaker position Absolute position: Defines the absolute position that is Absolute position |
approached by the sample changer. Current position | Next
Current position: The beaker at the current position is used. beaker
Next beaker: The sample changer will move to the beaker which
is next to the tower (home position + 1). If no beaker can be
detected, the sample changer moves to the next position (home
position + 2) and repeats until a beaker is detected.
Duration Defines the cleaning time, which depends on the installed tubes Short | Medium | Long
and the desired degree of cleanliness.
Descent rate Defines the speed at which the lift of the autosampler is lowered. Very low | Low | Medium
This parameter affects the ratio of intake air and liquid. The | High | Very high
suction of air improves the cleaning effect.
Formula Define a specific condition for line rinse. "Automation" =
(Condition) "InMotion"
"Condition" is activated

5.7.21 Park
With this method function you can park the InMotion head in a beaker, e.g. parking the pH electrode in a
beaker with buffer.

Refractometer Excellence Configuration of measurement methods​​ 59

 Parameter Description Values
Park position Absolute position: Defines the absolute position that is Absolute position |
approached by the sample changer. Current position | Next
Current position: The beaker at the current position is used. beaker
Next beaker: The sample changer will move to the beaker which
is next to the tower (home position + 1). If no beaker can be
detected, the sample changer moves to the next position (home
position + 2) and repeats until a beaker is detected.
Position Define the position of the park beaker on the sample rack. "Automation" =
"InMotion"
"Park position" =
"Absolute position"
Formula Define a specific condition for method function "park". "Automation" =
(Condition) "InMotion"
"Condition" is activated

60 Configuration of measurement methods​​ Refractometer Excellence

 6 Configuration of products
By means of products, product-specific adjustments to methods can be made. Each product is respectively
associated with one method. and several products can be association with the same method. The product
parameters are a subset of the method parameters. Products are created and managed in the product editor.
When a method is saved, the products that access this method are updated.

6.1 Create Products

Select: Home > Methods / products > Products
You create a new product if you either select and configure defined products from the list and save them under
a new ID or generate a completely new product. The following description shows how you can generate a new
product:
§ Open the method selection window via the button New in the Products dialog. Here all the methods of the
type Measurement are listed that can be assigned to a product.
1 Touch the corresponding method in the list that should be assigned to the product.
ð The Product dialog is opened. The parameter "Linked method" shows the ID of the selected methods.
Note: You can retrospectively assign another method to the product (same configuration).
2 You can edit and configure product parameters, assign the product an ID and a title.
You can start the product immediately or return to the product editor.

6.2 Linking Methods with Products

A distinction is made between two cases:
1. A product is created and linked with a method.
On linking of a product to a method (before saving the first time) the values are taken over from the linked
method.
2. A product has been previously created, the linked method is changed (relinking).
In this case only the methods for the relinking are suggested that agree with the currently linked method in
the configuration. After initial saving, the product parameters are not overwritten by the parameters of the
method.
For the measurement the product parameters are: such as e.g. Multiple measurements, Calculations
(Coefficients and result limits) are used and not the parameters of the corresponding method. The entries in
the method however remain unchanged.
Note
• When you start a product measurement, the parameters defined in the method are "overwritten" by the
product parameters.
• A maximum of 100 products can be defined.
• If no measurement methods have been defined on the device, no product can be created.
• Product ID’s can be used for barcode recognition.
• Several products can be linked to the same method.
• A product is always assigned to exactly one method.
• When a method is deleted, all linked products are also deleted.
• If a product is saved under a new ID, the values are retained in the product and are not overwritten by
standard values from the method.

6.3 Parameters for Products

The following parameters can be defined:
Parameter Description Values
Product ID The product is uniquely identified in the system via the product ID. -
Product title Name of the product -

Refractometer Excellence Configuration of products​​ 61

 Linked method Selection of methods used in the product. With a new link, only -
methods with the same configuration (cell mode and external
instruments) are shown.
Cell mode Display of cells to be used in the method (info field) -
External Display of external instruments (pH, conductivity, color) to be -
instruments used in the method is to be measured (info field)
Color settings Activates "Illuminant" so that the illuminant type can be defined Active | Inactive
(Minolta only) and "Observer" so that the angle can be entered.
Illuminant Defines the illuminant to be used. A | C | 65 | D50 | ID65 |
ID50 | F2 | F12
Observer Defines the viewing angle. Default 2°. 2° | 10°
Speed Pump speed "Automation" =
"SC1" / "SC30": "SPR200" / "SC1" /
• "Maximum": Sample feed with maximum pump speed "SC30" / "InMotion"
• "Reduced": Sample feed with speed set at the automation unit
• "Automatic": The pump speed changes according to the defined
time period from "Reduced" to "Maximum".
"SPR200" / "InMotion":
• "High"
• "Medium"
• "Low"
The corresponding pump speed can be set under Home >
Setup > Hardware > Automation .
Max. filling speed Defines the period of time [s] after which the pump speed 1…10000
after changes to maximum speed.
Multiple If activated, several measurements are performed with the same Active | Inactive
measurement sample.
No. of Defines the number of measurements. 2…10
measurements
Refill ratio Used for the calculation of the further movement of the sample 10…100
between two measurements. The refill rate [%] is calculated over
the duration of the sample addition.
Example: The fill duration is 10 s and the refill ratio 50%, i.e.
pumping is activated for 5 seconds.
Max. SD Maximum permitted absolute standard deviation of the 4 | 5 | 6 decimal places
measurements for density, refractive index or color. When the
deviation is exceeded the measurement is interrupted with the
status Error.
The maximum standard deviation must be entered in the function
of the measuring cell type.
No. of meas. Defines the number of measured points used for determining the 1…10
points mean value. Preferably use a high number of 10 measuring
points.
Note: If multiple measurement is activated, only the measured
values from the last measurement repetition are used.
Max. deviation The maximum permissible absolute deviation [pH] of the 0.01…7.00
measured values for pH or conductivity meters. If this is
exceeded, the results are marked accordingly.

62 Configuration of products​​ Refractometer Excellence

 Repeat if failed If this is activated, the measurement is repeated if "Max. SD" or "Multiple measurement"
"Max. Deviation" are exceeded. activated, or
Note: If "Multiple measurement" is activated, all measurements External instrument
are repeated. defined (pH meter,
conductivity meter,
colorimeter)
Author Name of creator (info field) -
Created on Date of creation and time (info field) -
Modified at Change date and time (info field) -
Modified by User who made change (info field) -
Protect When this is activated, only the author or an administrator can -
edit or delete the method.
For the density module the following parameters are available:
Parameter Description Values
Bubble check If activated, the system verifies whether bubbles are present in the Active | Inactive
density cell.
Viscosity Activation of the viscosity correction Density - Module
correction defined
Viscosity ≤2000: Density - Module
For samples with viscosity less than 2000 mPa*s connected
>2000: Viscosity correction
For samples with viscosity greater than 2000 mPa*s activated
- Set value:
With this selection, a known viscosity can be entered
Viscosity value Defines the viscosity value of the sample. 1…99999
[mPa*s]

6.4 Calculations in Products

The calculations defined in the method (Rx) are listed in the product. Press the button Calculations in the
product dialog (Navigation: Home > Methods / products > Products). For a description of the
parameters also see "[Methods and products: Methods > Method functions > Calculation } Page 51]".
The following rules apply for calculations in products:
1. When the methods are saved calculations in methods and products are compared on the basis of calcu-
lation indexes (R1 – R1, R2 – R2 etc.). If these indices from product and linked method do not coincide,
they will be automatically aligned, i.e. product calculations that do not occur in the method will be
automatically deleted and method calculations that do not occur in the product will be automatically
inserted.
2. If a parameter is changed in the method function "Calculation" that is only visible in the product (non-
editable, e.g. formula), then the entire product calculation will be overwritten in the associated product.

Refractometer Excellence Configuration of products​​ 63

 7 Series
Series act as a starting aid for several tasks. The tasks are individually lined up in the task list after the series
start.
Series can be created, edited saved and deleted.
• You can create shortcuts for series.
• A maximum of 5 series can be saved.
• The maximum number of series entries is 60.
• Series can consist of products and / or methods.
• Series can consist of the same or different entries (i.e. several entries (from the type method or product).
All entries can be deleted.
• Series can also be saved without entries.
• If you are in the Start analysis dialog of the series, series entries can be deleted, inserted or selected.
Via the Insert button, you open the Series item dialog to define parameters; see also "Create series".
If a change of series is made in the Start analysis dialog and a shortcut is created, this shortcut does not
point to the changed series but to the series created in the series editor.
• If no methods are defined in the instrument, no new series can be created.

Create series
Navigation: Home > Series
§ Via the button Series in the Homescreen you open the Series list dialog.
The available series are displayed.
1 Touch the button New.
ð A new series is generated. You can enter a series ID or use the default ID.
2 Save the series.
ð A dialog with the title of the newly created series opens. You can add new entries or edit existing ones.
To edit an existing entry, touch the relevant entry.
The Series item dialog opens.
3 For a new series entry, press the button Insert in the dialog of the selected series.
ð The Series item dialog is opened.
4 Enter the parameters and confirm with OK.
ð In the case of multiple entries, "Insert" markers appear behind the series entries.
5 Press the Insert marking area at the desired point.
ð The Series item dialog is opened.
6 Enter the parameters and confirm with OK.
7 Save the series.
The parameters for the Series item dialog are listed below:
Parameter Description Values
Item type The series item can either be a product or a method (only if at -
least one product is defined in the system).
Product ID Selection of product "Item type" = "Product"
Method ID For "Item type"="Method", it is possible to select the relevant -
method here.
For "Item type"="Product", the associated method is displayed
here (Info Field).
Method type Displays the type of method, e.g. measurement -
Sample ID Input of the sample ID "Method type" =
"Measurement"
Number of entries To define the quantity of series entries. -

64 Series​​ Refractometer Excellence

 For the entry type "Method" of the type "Adjustment" and "Test", you can change the associated standard data
using the parameter "Standard". For this, see also "[Methods and products: Methods > Standard
data } Page 43]".
Parameter Description Values
Standard For "Method type"="Adjustment", it is possible to modify the "Method type" =
standard data. "Adjustment"
For "Method type"="Test", the standard used is displayed (Info "Method type" = "Test"
Field).
A series can also be saved without entries.
All entries can be deleted.
In the dialog of the corresponding series the Start button is found with which you can open the Start analysis
dialog. In this you have the option to change your items again before the actual analysis start. To do this press
the button Items.
In addition to the parameters described above, the following parameters are displayed:
Parameter Description Values
Correction factor Defines a correction factor that can be used in calculations. 0.000001…1000000
For more information on the parameters in the Start analysis dialog, see also "Analysis sequence: Starting an
analysis".

7.1 Delete Series

1 Touch the series to be deleted in the Series list dialog.
ð A list with the corresponding items for the series appears.
2 In the dialog press the Parameters button.
ð In the dialog there is a Delete button with which you can delete the series.
Note
A prompt with the interruption criterion appears before you finally delete the series.

7.2 Creating a series copy

Using the Parameters button, you can then copy an existing series by changing the "Series ID". When the
series is saved a new series is created.

Refractometer Excellence Series​​ 65

 8 Operation
8.1 Start up the refractometer
− Press the power button (2).
ð The StatusLight (1) turns green.
ð The refractometer starts up and detects connected 1
devices.
ð The welcome screen on the terminal opens. 2
ð The refractometer is ready for use when the
StatusLight of the terminal turns green.

8.2 Shut down the refractometer

Shut down the refractometer using the touch screen
§ No task is running.
§ The measuring cell is clean and dry.
§ The home screen is open.
1 Tap Log out.
ð The Login window opens.
2 Tap Shut down.
ð METTLER TOLEDO is displayed and the StatusLight (1) starts blinking.
ð When the StatusLight and the screen are dark, the refractometer is shutdown.
ð The control circuit for the power button is energized. The rest of the refractometer is no longer energized.
Shut down the refractometer using the power button
§ No task is running.
§ The measuring cell is clean and dry.
− Press the power button (2).
ð METTLER TOLEDO is displayed and the
StatusLight (1) starts blinking.
1
ð When the StatusLight and the screen are dark, the
refractometer is shutdown. 2
ð The control circuit for the power button is energized.
The rest of the refractometer is no longer energized.

Forced shutdown
The refractometer should only be shut down in this way if it is absolutely necessary.
− Press and hold the power button (2) for more
than 10 s.
ð If an analysis is running, it is terminated prema-
1
turely and any data produced during this time is
lost.
2
ð The StatusLight (1) turns red.
ð When the StatusLight and the screen are dark, the
refractometer is shutdown.
ð The control circuit for the power button is energized.
The rest of the refractometer is no longer energized.

66 Operation​​ Refractometer Excellence

 Shut down the refractometer in emergency situations
− Pull the plug of the power cable out of the power outlet.

8.3 Typical phases of refractive-index determinations

Refractive-index determinations usually include three phases.
• Fill the measuring cell and measure the refractive index.
• Rinse the measuring cell to remove residue of the sample.
• Dry the measuring cell.

8.3.1 Fill the measuring cell

This chapter describes how to fill the measuring cell using a plastic pipette. How to work with
automation is described in the Reference Manual.

u www.mt.com/library

If you work without automation, METTLER TOLEDO recommends to use small sample volumes. For small
volumes, the temperatures of the sample and the measuring cell equalize faster and the analysis therefore takes
less time.
• Samples with high surface tension: 0.5 mL
• Samples with low surface tension: 1 mL
If you have samples that contain particles, it is important, that you always use the same sample volume.

8.3.2 Rinse the measuring cell

At the end of this phase, the residue in the measuring cell must have the following properties.
• Evaporate without leaving incrustations.
• Evaporate easily.
To clean the measuring cell, it has to be rinsed with one or two different cleaning solutions.
• Purpose of the cleaning solution 1: Dissolve and remove the sample, so that the residue in the measuring
cell is pure cleaning solution 1. If the cleaning solution 1 does not easily evaporate, a second cleaning
solution must be used.
• Purpose of the cleaning solution 2: Dissolves the cleaning solution 1 and evaporates easily without leaving
any residue.
METTLER TOLEDO recommends the following cleaning solutions if you work without a flow cell.
Sample Cleaning solution 1 Cleaning solution 2
Water, water based Deionized water Measuring temperature <20 °C:
acetone, ethanol (100%)
Measuring temperature >20 °C:
none
Acids (concentrated) Water (flush the measuring cell with Measuring temperature <20 °C:
plenty of water to remove the heat acetone, ethanol (100%)
from the reaction of water and acid) Measuring temperature >20 °C:
none
Alkaline solutions (concentrated) 0.3…0.5 % deconex solution Measuring temperature <20 °C:
acetone, ethanol (100%)
Measuring temperature >20 °C:
water

Refractometer Excellence Operation​​ 67

 Sample Cleaning solution 1 Cleaning solution 2
Samples with fats or oily 0.3…0.5 % deconex solution Measuring temperature <20 °C:
components acetone, ethanol (100%)
Measuring temperature >20 °C:
water
Petrochemical samples, edible oils Toluene, xylene or petrol ether Room temperature: low-boiling
and fats mixtures petrol ether mixture or acetone
Temperature > 30 °C: hexane or
similar organic solvents

8.3.3 Dry the measuring cell

At the end of this phase, the measuring cell contains no residue and is ready for a new analysis or storage.

8.4 Example: refractive-index determination without automation

The following chapters show you how to configure a measurement method and determine the refractive index of
tap water at 20 °C.
You can find more information about the configuration of methods in the chapter .

8.4.1 Create the measurement method

§ The home screen is open. Home Administrator 08/15/2018 Tasks

R5
1 Go to Methods / Products (1) > Methods. 1 Methods /
Products 20.00

ð The Methods window opens. Series

Results

Setup

Manual

Log out User data Barcode start Start

2 Select the method M8501 nD manual (1). Methods Tasks

Type ID Title °C

MS M8501 nD manual 20.00

1
MS M8502 Brix manual 20.00

MS M8503 Brix w. SPR200 20.00

MS M8504 Brix & pH (S220) w. InMotion 20.00

MS M8505 Clean&Park electrode InMotion 20.00

Back New

ð The method window with the list of the method M8101: nD manual Tasks

functions opens.
Line Method function

Title

Configuration

Sample

Fill

Measure

Cancel Print Insert Save

68 Operation​​ Refractometer Excellence

 8.4.2 Configure the measurement method
1 Select the Title (1) method function. M8101: nD manual Tasks

Line Method function

Title
1
Configuration

Sample

Fill

Measure

Cancel Print Insert Save

2 Change Method ID (1) as needed. The following Title Tasks

format is reserved for METTLER TOLEDO predefined

Method type Measurement
methods: "M" followed by a number.
Method ID A0001 1
3 Change Title (2) as needed and tap OK (3). Title Water 20°C 2
ð The method window with the list of the method Author Administrator

functions opens. Created on 08/15/2018

Modified on 08/15/2018

Cancel OK 3

4 Select the Sample method function. Sample Tasks

5 Enter for Sample ID (1) the default value for the Sample ID Sample
sample identification and tap OK (2). Correction factor 1
ð The default value is used in the Start analysis Comment

window.
ð The method window with the list of the method
functions opens.
6 Move your finger upward on the touch screen to scroll
Cancel OK
2
down.
7 Select the Report method function. Report Tasks

8 Deactivate Print / USB-RS232 data export (1) and tap Export to USB stick None

OK (2). Export to network None

Print / USB-RS232 data export 1

Condition

Cancel Delete OK 2

9 Tap Save (1). M8101: nD manual Tasks

ð The method is listed with Method ID and Title in the Line Method function
Methods window. Measure

Calculation

Clean

Online display

Report

Cancel Print Insert Save

1

Refractometer Excellence Operation​​ 69

 8.4.3 Create a shortcut on the home screen
1 Tap Start (1). A0001: Water20°C Tasks

Line Method function

Measure

Calculation

Clean

Online display

Report

Back Print Delete method Insert Start

1

2 Tap AddToHome (1). Start analysis Tasks

Type Method

Method ID A0001

Method type Measurement

Number of samples

Sample ID Sample

Continuous run

1 AddToHome Start

3 For Description (1), enter a name to identify the Shortcut parameters Tasks

shortcut on the home screen and tap Save (2).

Type Method

Description Water20°C 1
Method ID A0001

Immediate start

Homescreen position

Created by Administrator

Cancel Delete Save 2

ð The home screen with the shortcut (1) opens. Home Administrator 08/15/2018 Tasks

Methods / R5
Products 20.00

Series

Results
1
Setup

Manual

Log out User data Barcode start Start

8.4.4 Determine the refractive index

Material
• Tap water
• Deionized water
• Plastic pipettes
• Waste container
• Lint free tissues

70 Operation​​ Refractometer Excellence

 Start the method
§ The lid is closed.
1 Tap the shortcut (1) of the method you configured. Home Administrator 08/15/2018 Tasks

Methods / R5
Products 20.00

Series

Results
1
Setup

Manual

Log out User data Barcode start Start

2 If needed, change the entry in Sample ID (1). Start analysis Tasks

3 Tap Start (2). Type Method

ð The temperature of the measuring cell is brought to Method ID A0001

the temperature defined in the method. Method type Measurement

ð A message prompts you to add the sample. Number of samples

Sample ID Sample 1
Continuous run

AddToHome Start 2

Fill the measuring cell

1 Fill a clean plastic pipette with 0.5 mL of tap water.
2 Open the lid.
3 Place the pipette tip on the prism (1) and move it in
circles over the prism while you empty it into the
measuring cell.
4 Close the lid.

5 Tap OK (1). A0001: Water 20°C

Info

Add sample.

OK
1

ð The temperature of the measuring cell (2) is A0001: Water 20°C Tasks

brought to the temperature defined in the

Measuring
method (1).
10 s
ð The currently measured value is displayed (3). 1.33299
1
ð The measured value is saved as result when the
criteria for measurement reliability are met.
3 1.33299 20.00
2
ð A message prompts you to drain the measuring cell.
Calculated results Stop

Refractometer Excellence Operation​​ 71

 Drain the measuring cell
1 Open the lid.
2 Place the pipette tip on the prism (1) and aspirate the
content of the measuring cell.
3 Empty the pipette into a suitable waste container.
4 Tap OK.
ð A message prompts you to rinse the measuring cell
with deionized water.

Rinse the measuring cell with deionized water

1 Fill a clean plastic pipette with deionized water.
2 Place the pipette tip on the prism (1) and move it in
circles over the prism while you empty it into the
measuring cell.

3 Place the pipette tip on the prism (1) and aspirate the
content of the measuring cell.
4 Empty the pipette into a suitable waste container.
5 Repeat the steps above two or three times.
6 Tap OK.
ð A message prompts you to dry the measuring cell.

Dry the measuring cell

1 Wipe the measuring cell with a dry, clean and lint-free tissue.
2 Tap OK.
ð The home screen opens.
3 Wait a few seconds until any remaining residue of the deionized water has evaporated.
4 Close the lid.
ð The measuring cell is clean and dry.

72 Operation​​ Refractometer Excellence

 8.5 Viewing the results
− Tap Home > Results.
ð The Analysis list dialog screen appears.
1 Select a measurement from the Analysis list.
ð The MS dialog screen appears.
2 Tap the Calculated results button.
ð The Calculated results dialog screen with the
desired result appears.

− Tap on a desired Value.

ð A dialog screen with detailed information to the result is
shown.

8.6 Automation
Navigation: Home > Manual operations > Automation
You can perform the following manual operations with the automation units:
Action DryPro SPR200 SC1 SC30 InMotion
Dry X X X
Rinse X X X X
Drain X
Pump sample X X X X
PowerShower X
Stir X
Move to position X X
Move lift X
If no automation is defined in the setup, the manual operation "Automation" does not appear.
− Open the Automation dialog window via the button Automation in Manual operations.
In it you can define the following parameters to perform a manual operation with an automation unit:
Parameter Description Values
Cell mode Defines the type of cells (Density/Refractometry). D | R | D+R | D+D | R+R
Automation Defines the automation unit for manual operation. List of available
automation units
Action Defines the action to be executed on the automation unit. List of actions
Below the parameters are listed that are to be entered for the selected action:

Refractometer Excellence Operation​​ 73

 8.6.1 Action: Dry

Parameter Description Values

Dry mode Fixed duration: Drying is stopped after a defined time. Fixed duration |
Automatic: The oscillation is measured. Drying is stopped, when Automatic
the oscillation value becomes stable.
Dry duration Defines the fixed drying time in [s]. 1…1000
Max. dry duration If the oscillation value has not stabilized by the end of this period 1…10000
[s], drying is stopped.

8.6.2 Action: Rinse

Parameter Description Values

Solvent Definition of the solvent at the connections Rinse 1 and Rinse 2. List of solvents
Rinse duration Defines the fixed rinse time in [s]. 1…10000 | ∞
Rinse position Absolute position: Defines the absolute position that is Absolute position |
approached by the sample changer. Current position | Next
Current position: The beaker at the current position is used. beaker
Next beaker: The sample changer will move to the beaker which
is next to the tower (home position + 1). If no beaker can be
detected, the sample changer moves to the next position (home
position + 2) and repeats until a beaker is detected.

8.6.3 Action: Drain

Drain
Parameter Description Values
Drain duration Defines the fixed drain duration in [s]. 1…10000 | ∞

8.6.4 Action: Pump sample

Parameter Description Values
Direction Defines the pumping direction. Waste | Vial | Beaker
Waste: The liquid is pumped through the cell and into the waste
container.
Vial: The liquid is pumped back into the sample vial.
Beaker: The liquid is pumped back into the sample beaker.
Speed Pump speed Automation =
"SC1" / "SC30": "SPR200" / "SC1" /
• "Maximum": Filling with maximum pump speed "SC30" / "InMotion"
• "Reduced": Filling with speed set at the automation unit
"SPR200" / "InMotion":
• "High"
• "Medium"
• "Low"
The appropriate pump speed can be set in Home > Setup >
Hardware > Automation.
Duration Defines the fixed pumping duration in [s]. 1…10000 | ∞

74 Operation​​ Refractometer Excellence

 8.6.5 Action: PowerShower
Parameter Description Values
Rinse cycles Number of rinse cycles that should be performed. 1…100
Volume per cycle Defines the rinse volume in [mL] per cycle. 10…1000

8.6.6 Action: Stir

Parameter Description Values
Speed Defines the speed of the stirrer in percent of the maximum speed. 0…100 %
0 %: The stirrer is off.
100 %: The stirrer moves at maximum speed.
Stir duration Defines the fixed stir time in [s]. 1…10000 | ∞

8.6.7 Action: Move to position

Parameter Description Values

Go to Home: To move the sample rack to the home position. Home | Relative position
Relative position: To move the sample rack a definable number | Absolute position | Next
of steps. vial | Next beaker
Absolute position: To move the sample rack to a defined
position.
Next vial / Next beaker: To move the sample rack to the next vial
or beaker.
Position Defines the absolute position on the sample rack. 1…303 | 1…30
Direction Defines the moving direction of the sample rack. Forward | Backward
Lift position Defines the position of the lift to approach. Sample | Rinse | Rotate

8.6.8 Action: Move lift

Parameter Description Values
Lift position Defines the position of the lift to approach. Sample | Rinse | Rotate

Refractometer Excellence Operation​​ 75

 9 Maintenance
In this chapter you find descriptions of the maintenance tasks you should perform on your refractometer. Any
other maintenance tasks need to be performed by a service technician that has been qualified by METTLER
TOLEDO.
If you experience problems with your refractometer, contact your authorized METTLER TOLEDO dealer or service
representative.
METTLER TOLEDO recommends that a preventive maintenance and calibration certification is done at least once
a year through your authorized METTLER TOLEDO dealer or service representative.
u www.mt.com/contact

9.1 Maintenance schedule

If the standard operating procedures of your company require other maintenance intervals, use the intervals
listed in the standard operating procedures.
Frequency Task Link
Daily Clean the measuring cell at the end of the work [Clean the measuring
day. cell } Page 77]
Perform a test with deionized water. [Check the measurement
accuracy } Page 80]

9.2 Clean the refractometer

NOTICE
Danger of damage to the refractometer due to inappropriate cleaning methods!
Inappropriate cleaning agents can damage the housing or other parts of the refractometer. If
liquids enter the housing they can damage the refractometer.
1 Make sure the cleaning agent is compatible with the material of the part you want to
clean.
2 Make sure that no liquid enters the interior of the refractometer.

If you have questions about the compatibility of cleaning agents, contact your authorized METTLER TOLEDO
dealer or service representative.
u www.mt.com/contact

See also
2 Technical data } Page 93

9.2.1 Clean the housing and the lid

METTLER TOLEDO recommends the following cleaning agents:
• Water
• Water with a mild detergent

Procedure
§ The refractometer is shut down.
§ The measuring cell has cooled down to room temperature.
1 Wipe the housing with a cloth moistened with the cleaning agent.
2 Wipe the inside and the outside of the lid with a cloth moistened with the cleaning agent.
3 Wait until the lid and the space between the lid and the measuring-cell cover are dry.
4 Close the lid.

76 Maintenance​​ Refractometer Excellence

 9.3 Clean the measuring cell

9.3.1 Typical phases of cleaning the measuring cell

Cleaning the measuring cell usually includes two phases:
• Rinse the measuring cell to remove residue of the sample.
• Dry the measuring cell.

See also
2 Rinse the measuring cell } Page 67
2 Dry the measuring cell } Page 68

9.3.2 Example: clean with deionized water

The following chapters show you how to configure a cleaning method and clean the measuring cell with
deionized water.
You can find more information about the configuration of methods in the chapter .

9.3.2.1 Create the cleaning method

§ The home screen is open. Home Administrator 08/15/2018 Tasks

R5
1 Go to Methods / Products (1) > Methods. 1 Methods /
Products 20.00

ð The Methods window opens. Series

Results

Setup

Manual

Log out User data Barcode start Start

2 Tap New (1). Methods Tasks

Type ID Title °C

MS M8501 nD manual 20.00

MS M8502 Brix manual 20.00

MS M8503 Brix w. SPR200 20.00

MS M8504 Brix & pH (S220) w. InMotion 20.00

MS M8505 Clean&Park electrode InMotion 20.00

Back New
1

3 Select the template CLEAN (1). Method templates Tasks

Type ID Title

MS T001 MEASURE

ADJ T002 ADJUSTMENT

TE T003 TEST

CL T004 CLEAN
1

Cancel

Refractometer Excellence Maintenance​​ 77

 4 For Automation select None (1) and tap OK (2). Configuration Tasks

Cell mode R

Automation None
1

Cancel OK
2

ð The method window with the list of the method U8001: CLEAN Tasks

functions opens.
Line Method function

Title

Configuration

Clean

Cancel Print Insert Save

9.3.2.2 Configure the cleaning method

1 Select the Title (1) method function. U8001: CLEAN Tasks

Line Method function

Title
1
Configuration

Clean

Cancel Print Insert Save

2 Change Method ID (1) as needed. The following Title Tasks

format is reserved for METTLER TOLEDO predefined

Method type Clean
methods: "M" followed by a number.
Method ID A0002 1
3 Change Title (2) as needed and tap OK (3). Title Clean water based 2
ð The method window with the list of the method Author Administrator

functions opens. Created on 08/15/2018

Modified on 08/15/2018

Cancel OK 3

4 Select the Clean method function. Clean Tasks

5 Deactivate Drain (1). Automation None

6 Enter for Solvent 1 (2) "Deionized water". Drain 1

7 Deactivate Rinse cycle 2 (3) and tap OK (4) Rinse cycle 1

Solvent 1 Deionized water 2

Rinse cycle 2 3
Dry

Cancel OK
4

78 Maintenance​​ Refractometer Excellence

 8 Tap Save (1). U8001: CLEAN Tasks

ð The method is listed with Method ID and Title in the Line Method function
Methods window. Title

Configuration

Clean

Cancel Print Insert Save

1

9.3.2.3 Clean using deionized water

Material
• Deionized water
• Plastic pipettes
• Waste container
• Lint-free tissues

Start the method

§ The home screen is open. Home Administrator 08/15/2018 Tasks

§ The measuring cell is drained. 1 Methods /

Products
R5
20.00

1 Go to Methods / Products (1) > Methods. Series

ð The Methods window opens. Results

Setup

Manual

Log out User data Barcode start Start

2 Select the cleaning method that you configured (1). Methods Tasks

Type ID Title °C

MS A0001 Water 20°C 20.00

CL A0002 Clean water based 20.00 1

MS M8501 nD manual 20.00

MS M8502 Brix manual 20.00

MS M8503 Brix w. SPR200 20.00

Back New

3 Tap Start (1). A0002: Clean water based Tasks

Line Method function

Title

Configuration

Clean

Back Print Delete method Insert Start

1

4 Tap Start (1). Start analysis Tasks

ð The method window with the list of the method Type Method
functions opens. Method ID A0002

ð A message prompts you to rinse the measuring cell Method type Clean

with deionized water.

AddToHome Start 1

Refractometer Excellence Maintenance​​ 79

 Rinse the measuring cell with deionized water
1 Fill a clean plastic pipette with deionized water.
2 Open the lid.
3 Place the pipette tip on the prism (1) and move it in
circles over the prism while you empty it into the
measuring cell.

4 Place the pipette tip on the prism (1) and aspirate the
content of the measuring cell.
5 Repeat the steps above two or three times.
6 Tap OK.
ð A message prompts you to dry the measuring cell.

Dry the measuring cell

CAUTION
Slight burns due to hot surface
The measuring cell can become hot enough to cause slight burns.
1 Do not touch the measuring cell without gloves before the measuring cell has cooled
down.
2 Wear gloves that protect from contact heat if you need to touch the hot measuring cell.

1 Wipe the measuring cell with a dry, clean and lint-free tissue.
2 Tap OK.
ð The home screen opens.
3 Wait a few seconds until any remaining residue of the deionized water has evaporated.
4 Close the lid.
ð The measuring cell is clean and dry.

9.4 Check the measurement accuracy

9.4.1 Typical phases of checking the measurement accuracy

Checking the measurement accuracy usually includes three phases:
• Fill the measuring cell and measure the refractive index.
• Rinse the measuring cell to remove residue of the sample.
• Dry the measuring cell.

80 Maintenance​​ Refractometer Excellence

 See also
2 Fill the measuring cell } Page 67
2 Rinse the measuring cell } Page 67
2 Dry the measuring cell } Page 68

9.4.2 Example: test with a water standard

The following chapters show you how to configure and perform a refractive-index determination for a water
standard at 20 °C.
You can find more information about the configuration of methods in the chapter .

9.4.2.1 Create the test method

§ The home screen is open. Home Administrator 08/15/2018 Tasks

R5
1 Go to Methods / Products (1) > Methods. 1 Methods /
Products 20.00

ð The Methods window opens. Series

Results

Setup

Manual

Log out User data Barcode start Start

2 Tap New (1). Methods Tasks

Type ID Title °C

MS M8501 nD manual 20.00

MS M8502 Brix manual 20.00

MS M8503 Brix w. SPR200 20.00

MS M8504 Brix & pH (S220) w. InMotion 20.00

MS M8505 Clean&Park electrode InMotion 20.00

Back New
1

3 Select the template TEST (1). Method templates Tasks

Type ID Title

MS T001 MEASURE

ADJ T002 ADJUSTMENT

TE T003 TEST 1
CL T004 CLEAN

Cancel

Configuration Tasks

Cell mode R

Automation None
1

Cancel OK
2

Refractometer Excellence Maintenance​​ 81

 4 For Automation select None (1) and tap OK (2).
ð The method window with the list of the method U8001: TEST Tasks

functions opens.
Line Method function

Title

Configuration

Sample

Fill

Measure

Cancel Print Insert Save

9.4.2.2 Configure the test method

§ A test set for water at 20°C is configured.
1 Select the Title (1) method function. U8001: TEST Tasks

Line Method function

Title
1
Configuration

Sample

Fill

Measure

Cancel Print Insert Save

2 Change Method ID (1) as needed. The following Title Tasks

format is reserved for METTLER TOLEDO predefined

Method type Test
methods: "M" followed by a number.
Method ID A0003 1
3 Change Title (2) as needed and tap OK (3). Title Test water 20° 2
ð The method window with the list of the method Author Administrator

functions opens. Created on 08/15/2018

4 Move your finger upward on the touch screen to scroll Modified on 08/15/2018

down. Cancel OK 3

5 Select the Test method function. Test Tasks

6 Set Tolerance nD to a value in the range listed for your Tolerance nD 0.00002 1
instrument type.
- R4: 0.0002
- R5: 0.00002…0.00008

Back

7 Select the Clean method function. Clean Tasks

8 Deactivate Rinse cycle 1 (1) and tap OK (2). Automation None

Drain

Rinse cycle 1 1
Dry

Condition

Cancel OK
2

82 Maintenance​​ Refractometer Excellence

 9 Select the Report method function. Report Tasks

10 Deactivate Print / USB-RS232 data export (1) and tap Export to USB stick None

OK (2). Export to network None

Print / USB-RS232 data export 1

Condition

Cancel Delete OK 2

11 Tap Save (1). U8001: TEST Tasks

Line Method function

Measure

Calculation

Clean

Online display

Report

Cancel Print Insert Save

1

9.4.2.3 Perform the test

Material
• METTLER TOLEDO water standard
• Plastic pipettes
• Waste container
• Lint-free tissues

Start the method and configure the standard

§ The home screen is open. Home Administrator 08/15/2018 Tasks

§ The lid is closed. 1 Methods /

Products
R5
20.00

§ The measuring cell is clean and dry. Series

1 Go to Methods / Products (1) > Methods. Results

ð The Methods window opens. Setup

Manual

Log out User data Barcode start Start

2 Select the test method that you configured (1). Methods Tasks

Type ID Title °C

MS A0001 Water 20°C 20.00

CL A0002 Clean water based 20.00

TE A0003 Test water 20°C 20.00

1
MS M8501 nD manual 20.00

MS M8502 Brix manual 20.00

Back New

3 Tap Start (1). A0003: Test water 20°C Tasks

Line Method function

Title

Configuration

Sample

Fill

Measure

Back Print Delete method Insert Start 1

Refractometer Excellence Maintenance​​ 83

 4 Tap Standard (1). Start analysis Tasks

Type Method

Method ID A0003

Method type Test

Standard 1
Comment

AddToHome Start

5 Enter the information Lot number (1), Date of certifi- Standard data Tasks

cation (2), Expiry date Std (3) and Uncertainty

Standard name Water
nD (4) as printed on the certificate and tap OK (5).
Lot number 171118 1
6 Tap Start (2). Date of certification 08/15/2018
2
ð The temperature of the measuring cell is brought to Expiry date Std 08/15/2020
3
the temperature defined in the method. nD nominal 1.33299

ð A message prompts you to add the sample. Uncertainty nD 0.00002 4

Cancel OK
5

Fill the measuring cell

1 Open the standard bottle.
2 Fill a clean plastic pipette with 0.5 mL of the water standard.
3 Open the lid.
4 Place the pipette tip on the prism (1) and move it in
circles over the prism while you empty it into the
measuring cell.
5 Close the lid.

6 Tap OK (1). A0003: Test water20°C

Info

Add sample.

OK
1

ð The temperature of the measuring cell (2) is A0003: Test water 20°C Tasks

brought to the temperature defined in the

Measuring
method (1).
10 s
ð The currently measured value is displayed (3).
ð The measured value is saved as result when the
3 1.33298 1.33298
1
20.00
criteria for measurement reliability are met. 2
ð A message prompts you to drain the measuring cell.
Stop

84 Maintenance​​ Refractometer Excellence

 Drain the measuring cell
1 Open the lid.
2 Place the pipette tip on the prism (1) and aspirate the
content of the measuring cell.
3 Empty the pipette into a suitable waste container.
4 Tap OK.
ð A message prompts you to dry the measuring cell.

Dry the measuring cell

1 Wipe the measuring cell with a dry, clean and lint-free tissue.
2 Tap OK.
ð The home screen opens.
3 Wait a few seconds until any remaining residue of the deionized water has evaporated.
4 Close the lid.
ð The measuring cell is clean and dry.

9.5 Replace the protection plate

9.5.1 Remove the protection plate

§ The measuring cell is clean and dry.
1 Hold the protection plate (1) by the back of the lid (2)
with one hand.
2 Pull the back of the lid up to overcome the force of the
magnets that hold the protection plate in place. 2
1

3 Hold one of the edges (1) of the protection plate with

your free hand, let go of the lid and hold the protection
plate with both hands.
1
4 Remove the protection plate with both hands.

Refractometer Excellence Maintenance​​ 85

 9.5.2 Install the protection plate
1 Open the lid (2).
2 Hold the protection plate by its edges (1) with both 1
hands.
3 Align the front edge of protection plate with the front
edge (3) of the refractometer. 2
4 Let go with one hand and use it to hold the protection 1
cover by the open lid.
5 CAUTION Bruising of fingers due to strong magnet. 3
Hold the protection plate by the open lid and not by its
edge when you lower it.

6 Lower the protection plate and make sure that the

opening (2) in the protection plate is aligned with the
rim (1) of the measuring cell.
ð When the protection plate is close to the top of the 1
refractometer, strong magnets pull it down and hold
it in place. 2

See also
2 Accessories } Page 96

9.6 Replace the lid

9.6.1 Remove the lid

1 Open the lid (1) completely.
2 Pull one side of the lid (2) up until it slides off its axle.
1

3 Pull the other side of the lid (1) off the axle (2).

4 Remove the lid.

86 Maintenance​​ Refractometer Excellence

 9.6.2 Install the lid
1 Align the back of the upright lid (3) with the axle (4).
2 Make sure that the spring (1) is in front of the lid.
1 2
3 Push one side of the lid (2) down until it clicks into
place.

3
4

4 Push the other side of the lid down until it clicks into
place.

See also
2 Accessories } Page 96

9.7 Replace the measuring-cell cover

9.7.1 Remove the measuring-cell cover

1 Remove the lid.
2 Insert the tip of a flat screwdriver (3) in the slit between
the measuring-cell cover (1) and the lid (2).
3 Use the screwdriver to lift the measuring-cell cover
partially out of the lid.
1

2
3

4 Remove the measuring-cell cover (1).

See also
2 Remove the lid } Page 86
1

Refractometer Excellence Maintenance​​ 87

 9.7.2 Install the measuring-cell cover
1 Lower the measuring-cell cover (1) into its support on
the lid (2). 1

2 Push the measuring-cell cover into its support until it

clicks into place.
3 Install the lid.

See also
2 Install the lid } Page 87
2 Accessories } Page 96

9.8 Replace the measuring-cell O-ring

9.8.1 Remove the measuring-cell O-ring

1 Remove the protection plate.
2 Insert the tip of a flat screwdriver (3) in the slit between
the O-ring (2) and the measuring cell (1).

3 Use the screwdriver to lift the O-ring (1) over the rim of
the groove.

88 Maintenance​​ Refractometer Excellence

 4 Lift the O-ring (1) completely out of the groove (2).
1
See also
2 Remove the protection plate } Page 85

9.8.2 Install the measuring-cell O-ring

1 Place the one side of the O-ring (1) in the groove (2)
on the measuring cell. 1

2 Push the other side of the O-ring (1) over the rim into
the groove.
3 Install the protection plate.

See also 1
2 Install the protection plate } Page 86
2 Accessories } Page 96

9.9 Replace the O-ring of the measuring-cell cover

9.9.1 Remove the O-ring of the measuring-cell cover

1 Remove the lid.
2 Insert the tip of a flat screwdriver (3) in the slit between
the O-ring (2) and the measuring-cell cover (1). 1

Refractometer Excellence Maintenance​​ 89

 3 Use the screwdriver to lift the O-ring (1) over the rim of
the groove.

4 Lift the O-ring (1) completely out of the groove (2).

See also 1
2 Remove the lid } Page 86
2

9.9.2 Install the O-ring of the measuring-cell cover

1 Place the one side of the O-ring (1) in the groove (2)
on the measuring-cell cover. 1

2 Push the other side of the O-ring (1) over the rim into
the groove.
3 Install the lid.

See also 1
2 Accessories } Page 96
2 Install the lid } Page 87

9.10 View the firmware version

1 Press the Info key.
2 The firmware version and other system information is displayed.

9.11 Update the firmware

It is possible to update the firmware of your refractometer. If you want to update the firmware of your refrac-
tometer, contact your authorized METTLER TOLEDO dealer or service representative.
u www.mt.com/contact

90 Maintenance​​ Refractometer Excellence

 9.12 Prepare the refractometer for storage
1 Shut down the refractometer.
2 Disconnect the refractometer from the power supply.
3 Disconnect and remove any accessories from the refractometer.
4 Disconnect the terminal.
5 Clean the refractometer.
6 Protect the refractometer from dust.
7 Store the refractometer and the terminal in a dry and clean place.

9.13 Transport the refractometer

If you have questions about transporting your refractometer, contact your authorized METTLER TOLEDO dealer
or service representative.
u www.mt.com/contact

1 Shut down the refractometer.

2 Disconnect the refractometer from the power supply.
3 Disconnect any accessories from the refractometer.
4 Disconnect the terminal.
5 Clean the refractometer.
6 If you transport the refractometer and the terminal over long distances, use the original packaging.
7 Move the refractometer and the terminal to the new location.

9.14 Dispose of the refractometer

In conformance with the European Directive 2012/19/EU on Waste Electrical and Electronic
Equipment (WEEE) this device may not be disposed of in domestic waste. This also applies
to countries outside the EU, per their specific requirements.
Please dispose of this product in accordance with local regulations at the collecting point
specified for electrical and electronic equipment. If you have any questions, please contact
the responsible authority or the distributor from which you purchased this device. Should this
device be passed on to other parties, the content of this regulation must also be related.

Refractometer Excellence Maintenance​​ 91

 10 Troubleshooting
10.1 View and export system information

10.1.1 View system information of the refractometer

Info key: System information and current firmware
Home > Setup > maintenance & service > Firmware: Firmware history

10.1.2 View system information of connected accessories

Info key: System information and current firmware
Home > Setup > maintenance & service > Firmware: Firmware history

92 Troubleshooting​​ Refractometer Excellence

 11 Technical data
11.1 Refractometer
Characteristic Value
Power rating instrument Input values 24 V DC, 5 A
Socket 4-pin, power Mini-DIN female
Power rating AC adapter Input values 100...240 V AC ±10%, 1.8 A
Input frequency 50 - 60 Hz
Output values 24 V DC, 5 A
Dimensions Width 208 mm
Depth 226 mm
Height 193 mm
Weight 4.8 kg
Materials Housing PP HCT540
Lid PBT-CRASTIN SO653
Measuring-cell cover PTFE C25
O-ring of measuring-cell cover EPDM
Measuring cell Sapphire prism, stainless steel SUS316, perfluo-
roelastomer
Ambient conditions Ambient temperature +5 °C…+40 °C
Relative humidity 20…80 % (not condensing)
Altitude ≤5000 m above sea level
Pressure range Atmospheric pressure
Use In interior spaces
Overvoltage category II
Pollution degree 2
Storage Temperature range -20…70 °C
Relative humitidy 10…90 %
Connections
The power consumption of all connected and active devices must be ≤2.4 A.
Characteristic Value
ErgoSens Socket 3.5 mm jack socket
Voltage 12 V DC pulsed ±5 % (max. 100 mA)
LevelSens Socket 5-pin mini-DIN
Voltage 24 V DC ±5 % (max. 100 mA)
Aux Socket 5-pin mini-DIN
Voltage 24 V DC ±5 % (max. 500 mA)
DryPro Socket 5-pin mini-DIN
Voltage 24 V DC ±5 % (max. 500 mA)
SPR200 Socket 6-pin mini-DIN
Voltage 24 V DC ±5 % (max. 500 mA)

Refractometer Excellence Technical data​​ 93

 Characteristic Value
Automation Socket 9-pin male D-sub
Configuration Full-duplex
Baud rate 4800
Handshake X-On / X-Off
Galvanic isolation No
ESD stability Min. 1000 V
Short-circuit protection Yes
Ethernet Socket RJ45
Speed 10/100 MBit/s
Cable length Max. 10 m
Terminal Socket 19-pin Mettler-HDMI with non-standard pin
assignment
PC Socket Device, USB B 2.0, full speed
Cable length Max. 3 m
USB 1 / USB 2 / USB Socket Host, USB A 2.0 , full speed
terminal Current Max. 500 mA
Cable length Max. 3 m
CAN out Socket RJ12
Speed 500 kBit/s
Voltage 24 V DC ±5 % (max. 1 A)
Directives, standards and REACH regulation
The instrument complies with the directives and standards that are listed on the declaration of conformity.
SVHC candidate substances according to REACH (Article 33)
Material CAS No.
1,2-dimethoxyethane 110-71-4

11.2 Terminal
Characteristic Value
Dimensions Width 194 mm
Depth 129.5 mm
Height 56.7 mm
Weight 638.4 g
Materials Top housing EN ZL-ZnAl4Cu1 (EN Zl-0410)
Lower housing Crastin SO653
Cover glass Gorilla glass
Display Technology Color TFT
Size 7"
Resolution WVGA 800 x 480 pixels
Backlighting LED backlight
Brightness control Per software 50–100%
Input Technology Full-coverage capacitive touchscreen

94 Technical data​​ Refractometer Excellence

 Characteristic Value
Connections Cables 1m (standard)
Connector 19-pin Mettler-HDMI with non-standard pin
assignment
USB 2.0
Angle adjustment Mechanical 2-stage

11.3 Measurement
Characteristic R4 R5
Refractive index Measuring range 1.32…1.70 1.32…1.58
1)
Accuracy ±0.0001 ±0.000022)
Repeatability1) ±0.00005 ±0.00001
Resolution1) 0.0001 0.00001
Wavelength 589 nm 589 nm
3)
Measuring temperature Range 5…100 °C 5…75 °C
Accuracy (5…15 °C) ±0.1 °C ±0.05 °C
Accuracy (15…50 °C) ±0.1 °C ±0.03 °C
Accuracy (50…75 °C) ±0.1 °C ±0.05 °C
Accuracy (75…100 °C) ±0.1 °C –
1)
Resolution 0.01 °C 0.01 °C
Min. sample volume Syringe 1 mL 1 mL
Application Max. number of methods 120 120
Max. number of products 100 100
Stored results 200 200
1)
R4: for temperature range 15…70 °C, R5: for temperature range 15…50 °C
2)
R5: 0.00002 (around the adjustment point), 0.00004 (entire range)
3)
Minimal temperature not more than 12 °C below ambient temperature
International standards and norms
International standards and norms complied with are listed on the internet.
u www.mt.com/dere-norms

Refractometer Excellence Technical data​​ 95

 12 Accessories
The following accessories and parts are available for the refractometers R4 and R5.
All parts and accessories are specified with their ordering number and quantity in cases where more than one
part is included. When ordering, some parts are only available in a minimum order quantity. In such cases, the
corresponding minimum order quantity is quoted.
If you have any questions, contact your authorized METTLER TOLEDO dealer.

12.1 Standards
Combined density / refractive index standard water 51338010
9mL, 0.99… g/cm3, nD 1.33…

Combined density / refractive index standard dodecane 51338012

9 mL, 0.75... g/cm3, nD 1.42…

Combined density / refractive index standard 2,4-dichloro- 51338013

toluene
9 mL, 1.25... g/cm3, nD 1.55…

Combined density / refractive index standard 1-bromonaph- 51338014

thalene
9 mL, 1.48... g/cm3, nD 1.66…

12.2 Sensors
LevelSens 51109863
• Fluid level sensor
• Attachment strap
• Cable (2 m)

Extension cable for LevelSens 51108308

1m

Motion sensor ErgoSens 11132601

12.3 Sample changers and pumps

DryPro drying pump 30474899
• Desiccator
• Silicon tube (500 mm)
• Silica gel

96 Accessories​​ Refractometer Excellence

 Desiccator tower 51337180

Silica gel bag 51337241

170 g

3-way valve SV3 30474898

Pump SPR200 Peristaltic Reversible 30094285

• Silicone tubing
• Connectors

Connecting Kit SPR200 DxRx 30474908

• Adapter M8 M / M8x1 F
• Sampling Tube DM/DX
• Tube (connectors M8/M8, length 280) mm

SV3 SPR200 Bundle 30474907

• 3 Way Valve SV3
• Connecting Kit SPR200 DxRx
• Pump SPR200 Peristaltic Reversible

Silicon tube 51337228

500 mm

ChemSure tube for SPR 200 30094297

120 mm

Novoprene tubes (1x1 m + 10x118 mm) 51190969

Refractometer Excellence Accessories​​ 97

 Silicone tubes (5x118 mm) 51108149

SC1 Sample changer and cleaning unit 51326000

METTLER
TOLEDO

SC1

Reset

Setup

Enter

Step

SC30 Sample delivery and cleaning unit 51327000

METTLER
TOLEDO

SC30

Reset

Setup

Enter
Step

SC1H Sample Delivery and Cleaning Unit with Heating Option 51326400
including 1 control box
METTLER
TOLEDO

SC1

Reset

Setup

Enter

Step

SC30H (heated version of SC30) 51327500

METTLER
TOLEDO

SC30

Reset

Setup

Enter
Step

Stand SC1H SC30H 30474896

Autosampler InMotion Flex 100mL 30094290

• Base InMotion Flex
• Rack Kit InMotion Flex 100mL

Base InMotion Flex 30094291

Rack Kit InMotion Flex 25 mL 30094124

50 samples

98 Accessories​​ Refractometer Excellence

 Rack Kit InMotion Flex 80 mL 30094125
27 samples

Rack Kit InMotion Flex 100 mL 30094126

18 samples

Base InMotion Pro 30094292

Rack Kit InMotion Pro 25 mL 30094129

182 samples

Rack Kit InMotion Pro 80 mL 30094130

69 samples

Rack Kit InMotion Pro 100 mL 30094131

34 samples

Base InMotion Max 30094293

Rack Kit InMotion Max 25 mL 30094134

303 samples

Rack Kit InMotion Max 80 mL 30094135

113 samples

Refractometer Excellence Accessories​​ 99

 Rack Kit InMotion Max 100 mL 30094136
55 samples

12.4 External measuring cells

RX5 30474906

RX4 30474905

Connecting kit - Refractive Index Cell 51337024

SC1/SC30/InMotion automation or multiparameter system
• Tube (connectors M8/M8, length 400 mm)
• Tube (connectors M8/M8, length 800 mm)
• Waste tube (connector M8, length 600 mm)
• O-ring for flow cell
• Protection plate

12.5 External instruments

SevenCompact S220 pH/Ion 30019028
pH connecting kit complete with 51337023
• Tube (connectors M8/M8, length 400 mm)
• Tube (connectors M8/M8, length 550 mm)
• Cable for pH electrode
• USB/RS adaptor for SevenEasy™ / SevenCompact™ pH
meter
• RS-232C cable
• pH electrode
• External flow cell
• Holding plate for pH / Conductivity flow cell

pH electrode InLab Flow 59902917

InLab cable S7-BNC 30281915

1.2 m

SevenCompact S230 Conductivity 30019033

100 Accessories​​ Refractometer Excellence

 Conductivity connecting kit complete with 51337022
• Tube (connectors M8/M8, length 400 mm)
• Tube (connectors M8/M8, length 550 mm)
• USB/RS adaptor for SevenEasy™ / SevenCompact™ pH
meter
• RS-232C cable
• Conductivity sensor
• External flow cell
• Holding plate for pH / Conductivity flow cell

Conductivity sensor InLab 715 51302885

External Flow Cell Complete 51337190

Holding plate for pH / conductivity flow cell 51337197

USB-RS Adapter Conduct. Meter SevenEasy 51105852

RS-232C cable 51190589

RS9-RS9

Coupling piece for M8 screws (2 pcs) 51337179

Colorimeter
Color connecting kit UV5 30474868
• Flow cell (quarz, 10 mm)
• Tubing set polarimeter/colorimeter
• Syringe adapter
• USB A-B cable (1.8 m)

Color connecting kit Konica Minolta 30025477

• Flow cell
• USB A-B cable

Connecting kit - Color Lovibond PFXi-195 30395922

Color connecting kit Lovibond 51337021

• Connection kit for colorimeter
• USB-RS adaptor for Lovibond colorimeter

Flow cell 30258741

Quartz glass, 10 mm

Tubing set polarimetrie/colorimeter 30251100

Refractometer Excellence Accessories​​ 101

 DM tube / syringe adaptor 51337154

USB cable A-B (for PC or printer) 51191926

180 cm

Adapter Auxiliary Instruments (USB-RS232 convertor) 51105856

If you want to use two auxiliary instrument RS232-USB
adapters, contact METTLER TOLEDO for a customized solution.

12.6 Peripheral instruments

Lab equip acc data writer USB-P25/01 11124301

Lab equip access. data writer P-58RUE 30094674

Lab equip access. data writer P-56RUE 30094673

USB data export box 51105855

Handheld barcode reader with USB interface 21901297

Barcode Reader ScanStraight for SC30 51337185

102 Accessories​​ Refractometer Excellence

 Fingerprint reader with USB interface 51192107

12.7 Software
Starter Pack LabX Server for Density Refractometry 11153131
• 1 instrument license for Density Refractometry
• Network installation for up to 30 total instrument licenses
• User Management and Auot Import/Export

Starter Pack LabX Express for Density Refractometry 11153130

• 1 instrument license for Density Refractometry
• Single PC installation for up to 3 total instrument licenses

1 instrument license for Density Refractometry 11153250

12.8 Miscellaneous accessories

Press for paste-like products 51337155

RM / Rx foil stamp 30097047

Terminal protection cover 30125377

USB Keyboard 51192111

O-Ring Lid Flow Cell RM/RX 51192079

Size 63.22 mm x 1.78 mm

O-Ring DI 53.25x2.62 51192051

inserted in lid

Insert for lid of measuring cell 51337159

RM / RX protection plate incl. lid 51337166

Lid incl. magnets Rx 30474909

Extern. Power Supply 120W 30298362

Refractometer Excellence Accessories​​ 103

104 Accessories​​ Refractometer Excellence
Index
Numerics Cell parameters 17
Cell test, method function 54
24V Output 26
Cell update 36
A Cell, method function "Measure"
Accessories 96 Method type "Adjustment" 49
Adjustment Method type "Measure" 48
Method function 55 Method type "Test" 49
Method syntax 41 Clean
MF sample 46 Housing 76
Adjustment data Lid 76
Export 37 Method syntax 42
Adjustment parameters Clean, method function 51
Setup, Cell 18 Color scales 21
Adjustment sets Formula editor 43
Create 16 Condition, method function 43
Delete 17 Configuration dialog 38
AtmoSens Configuration, method function 45
Verify availability 25 Configure barcode reader 22
Audio-Signal Configure USB stick 23
Setting 27 Control type
Automation Output 24 V 57
Manual operation 73 USB-RS-232 57
Automation units
D
>Delete 20
Data storage 28
Create 19
Date and time 28
Types 18
Define account policies 29
Auxiliary Instrument 56
Disposal 91
Auxiliary Instruments
Drain 74
24V Output 26
Dry 74
USB-RS-232 26
Drying 52
Auxiliary values
Create 33 E
Method function 56 Emergency
AuxInst Shut down 67
Variable auxiliary instrument 58 End user license agreement 5
B ErgoSens
Activate 25
Beep
Error detection, method function "Measure"
Setting 27
Method type "Adjustment / Test" 50
Bubble Check 49
Expired Resources 16
C Export
Calculation, method function 51 Adjustment, test, measurement history 37
Calculations in products 63 External devices
Cell Delete 20
Maintenance & Service 37 External instruments

Refractometer Excellence Index​​ 105

 Colorimeter 21 Instruction, Method function 56
Conductivity meter 20 Instrument update 36
Create 20
L
Edit 20
Language
Install 20
Setting 26
pH meter 20
LevelSens
Types 20
Activate 25
Extinction
Lid
Formula editor 43
Clean 76
F Line rinse 59
Filling, method function 47 Linking of methods with products 61
Fingerprint reader 23 Lovibond 21
Firmware
M
End user license agreement 5
Maintenance
List 36
Schedule 76
Open source attribution files 5
Maintenance & Service
Third party licenses 5
Firmware history 35
Update 90
Functions 33
Firmware history 35
Import / Export of data 34
Formula editor 43
MT Service 34
Formula syntax 44
Reset to factory settings 35
Formulas
update 35
Example 44
Mathematical Functions and Operators 43
in method functions 43
Measure
Initials 44
Subfunction "Cell" 49
G Subfunction "Error detection" 50
Global settings Subfunction "Measurement acquisition" 49
Analysis and resources behavior 30 Measure, method function 48
Physical properties 31 Measured value acquisition, method function "Measure"
System 28 Method types "Measure", "Adjustment", "Test" 49
Types 28 Measurement
User management 28 Method syntax 40
Measurement history
H
Export 37
Hardware
Memory copy 35
Auxiliary Instruments 25
Menu structure 15
List 36
Method function
History
Wait 45
Adjusting, test entries 18
Method functions
Housing
Adjustment 55
Clean 76
Aux. value 56
I Calculation 51
Identification Cell test 54
Define system settings 28 Clean 51
Import/Export of data 34 Condition 43

106 Index​​ Refractometer Excellence

 Configuration 45 PC – settings 24
Filling 47 Printer 23
Instruction 56 USB data export 23
Measure 48 USB stick 23
Online display 53 PowerShower 58
Report 53 Printer
Temperature compensation 54 Setup 23
Test 55 USB data export 23
Title 44 Products
Wait 56 Calculations 63
Method Functions, Parameters Create 61
Auxiliary Instrument 56 Linking with methods 61
Method quantity 38 Parameters 61
Method syntax Pump sample 75
Adjustment 41
Q
Clean 42
Quantity of methods 38
Measurement 40
Test 42 R
Method type Report, method function 53
Adjustment 46 Reset to factory settings 35
Test 47 Rights for users 29
Method types 38 Rinse 74
Methods Rotate turntable 75
Create 38
S
Linking with products 61
Minolta 21 Safety information
MT Service, Maintenance & Service 34 Signal words 6
Warning symbols 6
N
Sample, method function 45
Network – settings 24 Screen
Network - storage 24 Setting 27
O Sensors
Activate 25
Online display, method function 53
Series
Open source attribution files 5
Create, delete 64
Output 24 V 57
Tasks 64
P Setup-Menu 15
Parameters Shortcuts
Products 61 Create 27
Park 59 Shut down
Parts 96 Emergency 67
PC – settings 24 Forced 66
Peripherals Power button 66
Barcode reader 22 Touch screen 66
Device types 21 Signal words 6
Fingerprint reader 23 Standard data 43
Network – settings 24 Stir 59

Refractometer Excellence Index​​ 107

 Symbol 5 V
Syntax, methods 40
Viewing the results 73
System settings
Date and time 28 W
Define 28 Wait, method function 56
Warning symbols 6
T
WasteSens
Tables
Activate 25
Create 32
Temperature compensation, method function 54
Test data
Export 37
Test parameters
Setup, Cell 18
Test sets
Create 17
Delete 17
Test, method function 55
Test, method syntax 42
Test, method type 47
Third party licenses 5
Title, method function 44
Transmission
Formula editor 43
U
Update
Firmware 90
Update, firmware 35
USB compact printer 23
USB data export 23
USB-RS-232 26, 57
USB-RS232 data export box 23
User – settings
Shortcuts 27
User groups 29
User management
Administer users 28
Define account policies 29
User rights 29
User settings
Audio-Signal 27
Beep 27
Keyboards 27
Language 26
Screen 27

108 Index​​ Refractometer Excellence

 www.mt.com/Refractometry-Excellence
For more information

Mettler-Toledo GmbH
Im Langacher 44
8606 Greifensee, Switzerland
www.mt.com/contact

Subject to technical changes.

© Mettler-Toledo GmbH 10/2018
30471974A

30471974