WORK INSTRUCTION FOR SPECTROSCOPIC ANALYSIS OF METALS AND ALLOYS
Unit:-Kangaro Tools.
1 ) PRODUCT TO BE TESTED:- Metals and alloys based on Fe, Al, Zn and Cu
2) PURPOSE/SCOPE:- To analyze complete chemical Composition of metals and alloys.
3 ) EQUIPMENT: - SPECTROMETER (SPECTROMAXX)
4 ) MODEL NO.:- SPECTROMETER LMX09
5 ) PROCEDURE:-
a. It is ensured that the outlet pressure of the Argon gas regulator connected to the machine is maintained between 4.8 to 5 bar.
a. The equipment is switched ON.
b.The tungsten electrode is cleaned, copper block is placed on sample stand and the sample clamp is pressed down .
c. The Plasma source button is switched ON, after 2-3 minutes software is started.
d. Before taking the spark it is ensured that the sample is free of any sample injury or defect.
e. The prepared sample is placed on the spark stand and clamped (Adapter is used as per the requirement) .
f. The green light on the power button ensures the completion of the circuit.
g. Then spark is started by either pressing the power button on machine, F2 button on keyboard or by clicking the start button on the
screen.
h. Distance is kept from the machine as the spark starts, the results displays on the screen after the completion of the spark.
i. If any issue is being observed while taking the spark, it is aborted by switching off the power source or by clicking on the stop butto
the screen.
j. Atleast 3 to 4 sparks are taken on each sample to ensure the consistency in test results.
k. The equipment is turned OFF after the completion of the testing.
7 ) RECORD: All the results are recorded on format as applicable.
Prepared by Checked by Approved by
Name Vikas Singh Ishan Raina Vivek Garg
Date 17/06/2022 17/06/2022 17/06/2022
Last Revision Details:-
Doc. No: WI/QA/176
Issue Date :17/06/2022
Rev. No: 00
Page: _1_ of _1_
ned between 4.8 to 5 bar.
essed down .
ent) .
icking the start button on the
mpletion of the spark.
by clicking on the stop button on
Approved by
Vivek Garg
17/06/2022
FM/MR/15, Issue Date:- 27/11/2021, Rev. No. 00
5 ) PROCEDURE:-
a. It is ensured that the outlet pressure of the Argon gas regulator connected to the machine is maintained between 4.8 to 5 bar.
a. The equipment is switched ON.
b.The tungsten electrode is cleaned, copper block is placed on sample stand and the sample clamp is pressed down .
c. The Plasma source button is switched ON, after 2-3 minutes software is started.
d. Before taking the spark it is ensured that the sample is free of any sample injury or defect.
e. The prepared sample is placed on the spark stand and clamped (Adapter is used as per the requirement) .
f. The green light on the power button ensures the completion of the circuit.
g. Then spark is started by either pressing the power button on machine, F2 button on keyboard or by clicking the start button on the
h. Distance is kept from the machine as the spark starts, the results displays on the screen after the completion of the spark.
i. If any issue is being observed while taking the spark, it is aborted by switching off the power source or by clicking on the stop butto
j. Atleast 3 to 4 sparks are taken on each sample to ensure the consistency in test results.
k. The equipment is turned OFF after the completion of the testing.
7 ) RECORD: All the results are recorded on format as applicable.
UCTION FOR SPECTROSCOPIC ANALYSIS OF METALS AND ALLOYS
n on the screen.
