Date.
Espt. No.: Page No.
T7TRAT1ONKMoO, Vh £AS
ttutng
i agofnst o'r Mstandosud:
Salution af' FuO ammonum guphate
Patneiple -8-A kown Value o tandauc fAS Golut Pon
Cmohu's silt solutfor) is ttsoted gafut KMnO, soßutfon
Po aidie edium.
D eat for Fuous Sulphate qta oridise to
Fesuie Bulphate and t*Mano, qets edued to colounleu
Manqanou solut or
Molecula Poum equatPon8
|8%MnO +8 H, 5o, +Lo Fe Sok, So, +5fsoat Mnóot
Reduetiãn ho HLact lon
Ozidotion holl eaetion
Oveall Ponic equation
MnO +8 + 5 Mot +6fe'H;
|By rawing thi volume o< EMnOu solut ien autoed to
Osidise f so. Arom the titsatfon, h molowity e<
CS CamScanner
Cbun voion:
Buette olutionknDy
Contcat taak omr kemeois ammorlum tùlphate aolutin
1 tut tube tull of dilute H, 6a,
Thicatox -*Mna l&lyndicatou)
End pofnt ’ Cosouulws to pumañid. pÉn k'
aia Ftral bunctesadfng
No.
tal tbusutte vodta ladded
vokum ay*Mno,
o Cm.
Cal ealoion:
Foumua ?- MV,a,
(PMAO.) CPAs
M, Molout ty D FMnO e ?
volume
Moloty a fAS =[Link]
voume a PAG oml
Numbu o loA e le ctaons' te
H,. . M, Vas
V,ar
M : O02 M
O Scanned with OKEN Scanner
Dats
Expt No,: Page No..
Puocedwe -
1O cno pipete is wauhtd with wate andt then
vinsd with the qivLn fAS sOlut Ton, A butee te Ta
washed with unteu and then einst with the KMnOu
solut on Ond Aix ed to a stond
S 4 a l buwette steodirg ia notd to the utp Meniseu
Ccotouued solution)
Exatly tomt o OM FAs ts pipeted out ftoa clean
conial losk and abot one teut tuube ful! al diute
aeld A added.
gulphwie
DTe soution fn the conical Hak A 41tuatd against
KMnOy token io the buette unt a pumanent pale
pink colou la obtaned
eodïng is noted, Ttnotfor Ps epratd
oo! bueette
Pon ConcoHdant value. Th ia ttotfor, kMnO aeta
sl! inditot a.
Repot
Date ...
Page No....s
TeTTON (KMa0, vls Guo.)
Atng o dettumlo the- concentuatiorrnoloty ol
potauium pumongarate solution by tatq f
OtM otandat soutfon iDxale aerd
Peiociple 3- A koown value ol gtandud oxatle aeA aidi
in alde mdiuin ond fn hot tornditfon.
and tMhg qota edud do cololua mongprous sulphot
Pecucttn hall steoetfon
Didotion haly otfon
Ovesatt Tonte cqueton
Enawtrg the voure aj *MnOr aolutfen, molatay g
#MaO saluton on b Caleulot d
A piptte Ts wahed with uotu and losed wth the
warhd wih
Otolfe asd so lution . The buwette fs
BveHe ’ k n , solution
Conial lank : toc ' calie acid + ttuttube ful af Hso.
Tniat o KMnO, (sll Pndioto)
Erd poit Colouil to puahed polelolowr'
atifrat buette HAnding nttal busettereodrgoiime a} *MN o,
Sotin odddn´Cm
Colutoion
foumula ; mN, a, : m a
m,
Lo, * 5
Date
Expt. No.:
Page No.
with KMnO 4olution ond
Lh4tal buette suodirq fa notd to he utbo Meniscus
Exoctly tDm O.1 MDxaie ad I4 pipttd ct Pato o
ctean coni cal Plart and tut tube latl of AFauted Haa
A ddd. the 4oution a heatd do t6Ñc , he hotecuton
s 4tattud against kMnO taken in the buntte unttu
pormanet pink olous fa cbtained. -hta Ba the end
point of tttatfon , The buwette eading:
and titatfon fs upatd fon OQMeetevalueu.
Molaulty ol ¢MnO, iA O-o1q M
Date ..
Ept. No.:
Page No.m
5
SyTEMAtIc QaITATTVE ANALYEI9 OE
TrogGANI
eeimïoauy Analyata
stote Gyatollne
6 tolou g- white
Deteetion,Ad Hadlol
Dteetlon a T quoup ad actia!
ExpulmLnt ObavatPon Trtenee
Galt + dilute HcL No buiAk
veucenie .Hodseal co abaut
Deteetfon Taoup aid nadat. .
Ex puiinnt obuvation DoBountet
Galt + Conc. Ha60, colouulutpungut T quaup chlouide
Ro a duy tuttube amell qs whiehaive Ton may be puesut
dense whiterfene i
koth qla Kod dipped
to thMonth. a +he
tut tbe
CS CamScanner
Lonjumotouy tut Aox chlotde Pon Cr):
(Chuomyt ehloutde tut)
Expaimen obsuvat ion
|foli +tfiycu,Oy Ceuystats Ororged vao
- w s aue evolved
Ino duy tut tub +
Conc. H, S0,
ike above vopouu aue obtand
ipo4sd ato a teut tub ..
itontainig NaH Aoto
Totte above ylo Bight yutow ppt Chloide oni Ceudi
Oution+ actic acid + ton ftayined
kead acetote Aoution
aue added.
5ivu [Link] chlouefoo ( )
Ez puiment obawator Tnjuance
Sot &outfon + chlonids for ler)ts
AgNo, vodtin wheh iagotudein langisind:
quoup oud wodial chloetde Cer) is puuent and confirmd
Pupotton af autgfrol sottonCòs)
A satuotd aolutfon oqfuensatt ?4
Afmowirq the Salt wtt tle exe o wote.
Date.
Expt. No.:
Page No...
3 Dtection al Basie a a
Deteetton guoqoup tatl¡ (baste odscal)
Ammonium fon(MH)
Expulment obsatio La7uune
Salt + dilute Nao purqunt rmll o Ammonium fon (te
kotut Pon AH qa ia wowdmas be pesent
which qius dene
white kunu t th
|Conc HHe A0uti
Confisumatouy tut fom Arnonumn ion
Nessle's yuagnt Tuti
Expuimnt obsuwation Trluunee
OMatiral aoudian Boun ppt ia Ammonfun tonCNH)
Conllumtd
baste Odial ammoniu lon (NH) Ps
pHuent ond con fumed
Ruult
Baute od tal NHe
Ompntun
Hence, the qiver Bo ouQcnie satt ta
chtortde (NHa)
O Scanng
Date,
Expt. No.:
Page No
5y5TEMATI¢ ALITATTVE ANALySIS OF
TNORG ANIe SALT -09.
(. Petiminauy Anatyeisg
state 2- ceystalline
) tolouu - white
Golub+¯ty' the qiven solutin is'-4olubleifointu
2 Dteetion a AA nodial3
Dt eetio o 2qoup ald nadlal::
Ex pufmind öbsuiin Iokuene
Salt t dilute HCt No bsk
euevecnce
Dtetiona T quoup oeld odfiat
Ea puimtnt ObsiuatSon Tnluenee
Solt +lonc. HhGOuahte fumes' kotlad quoup basie sotieal
taken fn a day by ReddAh ban Bcom td Ceer) fon nay
tut t u b e ; * punqunt kumun bepuunt...
Conflsumotasiy test tou Buonida fon (B] 3
LGlobute tut!. i
Expuimñtt bavwatton!
Salt t uoty shakiAniovoriqe, d. Buomide .ion (Bx)
to diuolve+uatex+9obule ts dosned s Lon4nd
3dveps af cela, the
mizteTa chakenwetl
Expt.
Save Attatt tut
Ez pument
cbtwation Trkuunce 8
(Bu)
Galt <olution ipale yllow ppt, cohicikBuomide ion
Aq No, «outio conyBumd
. T quoup aetd sdial Buomide Pon ia peett and tontimid
.
Asatotfon 4olution gin kalt i pepod: loy diuolw.
-Grg theirsganie kalt with te txe u atu
3. Detetion af Basie walfea!
Ammonfua fon (NH)
Expuimnt Obsuatiav Tnfpence
Annoniun fon CuH
4oluson aeucludwhiehqtuudur may be pesen.
Aippd t'tone Hcd eourto
Confemat ouy tu fon ammonfumlor CNH)
Nuluk tut (ueoqn:
Ezputinnt obiuato. Tnkoen c
NHTon:i4 ir',
tosimd Conhiscmdi
Daut The quen ialt con tointrg
Aud wodi cal Ba
Bauie odial NH
Hene,+he qiven inaqanic Aolt iu Amnonia Buomide CNH,B)
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7
Date ...
Expt. No.:.
Page No.
- GysTAMETIC QUAL0TATENE ANAlysrs
OF TNoRG ANC SAttT- 03
Petimtnay Ara luyata
stote Cystat>ne
bcotoe white.
2. Deteetion el AcRd Rodial:
|Dteetton o î qOUp aid Moal
Eapuumint.? obyuatian
Solt diute Hct No budak llACeni Tquouip autd
Modia to ia absent
Dteeticn Dqoup Actd nadal
Expuumtnt obAwoion Tåliunee
Salt + Conc. H,SO
in a duy tut tube KetondB)iabint
Tut fo No
Epatncnt coimvation
tuttutbe t-tu turninga °apou:
Deteetia o qHoupndial ?*
Expuuiment obiatio
4 hiek whie ppt
Bael, solutia Obtaind so may be peuen
9
Conlinnatouy tet fou So
Expuimentd
obsuat fon Tatuene
fnuallbleis
To the above'ishite ppt hte ppt con blsmed
Leocd acetate tut
Expuaiment obAuvotion iTnhuunci
To a pat q aqous A whtte Ppt ia bpumt
scution ol the aaltht eh ia 4ouble in
add lead aretote exct ol hot ommonium
sout aceetate Aoutia :
.
[Link] qiver kott cont
puuent ond ton6iy md
Paepuasion a o Pnal Aolutlon Cos)
A satusotd oluton iot quen inonganie solt4. :
pepad b4 dimowrg the yalt with Hte exce Dhuatu
a. Detuetion ol Baaie odleal -
Aralysia Buoqoup baute asea:
Ammaum fon CNH
Expscment obAuuotlo
Satt + NoDH solution No punqint Amel oy Buio #Houp iasi.
lootl
Hodieal RHiabsent
Exputmid obiuwatlo Totuenee
Worwhite ppf Z quoup baievaoScal
alosent
Date ..
Expt. No.: 9
Page No.
Deteet ion ol î qMoup bafe cocsal
Eapuimtnt ObAuwat on
oMleinalsoueto+ di No whtte ppt
Cchaoader gti) odfau abscnt
Duteetfon o quoup bale nadleal
Expuument obsuation
Uq4oup Allumtni
NHyc+eytu ol white Ppt i4 Cet*)ay be
AH¡oOH 4outlon foumed Puent
|Con4iumatouy tut fos Auminium Ton (a
Expuimunt obsuvation Totuunce
Daenal kolutond A white qutetatinou Auminfue ton
Srallquorntity tolloo O, NaoH qfulng
-ed by ecUs above a cleas Solutin
elas solutn+ sotid white qlutaniouup
AHct, boil and tool 2eappOu
udutop watu
D.6 + blus limes Aluminium ion CA
Solutantopt ol Wit mas i4 foumd fa tonumed
ke qiven salt ontaintg bauie Madlcal A
aluminium Pon CA3) a punt and con me
4alt contcin,
the qtven
Baute soteal;- Ar
inauqonie
EAl, Csa)]
