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Dynamic Shear Rheometer Guide

The dynamic shear rheometer (DSR) is used to measure the viscous and elastic properties of asphalt binders under different conditions. It applies an oscillating shear stress and measures the resulting shear strain to determine the complex shear modulus (G*) and phase angle (δ), which characterize the binder's stiffness and elasticity. Proper specimen preparation and testing procedures are required to ensure accurate results. Minimum G*/sinδ criteria are used to evaluate rutting resistance at high temperatures, while a maximum G*sinδ criteria addresses fatigue cracking at intermediate temperatures. The DSR must be properly calibrated and standardized.

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0% found this document useful (0 votes)
124 views36 pages

Dynamic Shear Rheometer Guide

The dynamic shear rheometer (DSR) is used to measure the viscous and elastic properties of asphalt binders under different conditions. It applies an oscillating shear stress and measures the resulting shear strain to determine the complex shear modulus (G*) and phase angle (δ), which characterize the binder's stiffness and elasticity. Proper specimen preparation and testing procedures are required to ensure accurate results. Minimum G*/sinδ criteria are used to evaluate rutting resistance at high temperatures, while a maximum G*sinδ criteria addresses fatigue cracking at intermediate temperatures. The DSR must be properly calibrated and standardized.

Uploaded by

zain Ishaq
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PPTX, PDF, TXT or read online on Scribd

PAVEMENT DESIGN AND

CONSTRUCTION

Dynamic Shear
Rheometer
Dynamic Shear
Rheometer
• Purpose
 viscous and elastic properties
 effect of temperature
• Output
 Complex Shear Modulus (G*)
 Phase Angle (
Construction Rutting Fatigue Low Temp
Cracking Cracking

[RV] [DSR] [BBR]

Time RTFO - aging


No aging
PAV - aging
Viscous Behavior
(High Temps) G * : stiffness
G*1

G*2

2  : elasticity
1
Elastic Behavior
(Low Temps)
Test Equipment
• Temperature Control
 + 0.1 degrees C
• Two Methods
 circulating water bath
 air oven
Temp
Control
Running the DSR Test
• Need to know
 High or intermediate temperature
 What aging condition
 Unaged
 RTFO aged
 PAV aged
Equipment Preparation
• Select testing geometry
 25 mm plate diameter with 1 mm gap
 original binder
 RTFO residue
 8 mm plate diameter with 2 mm gap
 PAV residue
Equipment Preparation
• Select test temperature
 From PG chart or estimate
 High vs intermediate
 Allow plates to equilibrate to test temperature
• Set “zero” gap
 Point where plates touch
 Automated
 Allows accurate testing gap
 At test temperature or in middle of expected
range (+/- 12C)
Equipment Preparation
 Set test gap:
 high temperature gap = 1000 microns (1
mm)
 intermediate temperature gap = 2000
microns (2 mm)
 Add extra 50 – 100 microns
 Will remove after trimming
 Eliminates edge effects
Equipment Preparation
• Return plates to loading temperature
 Test temperature for 25mm plates
 34 – 46C for 8mm plates
Equipment Preparation
Micrometer
Wheel
1000 or 2000 microns
Spindle + 50 microns (sample shape)

Fixed Base 1050 microns or 2050 microns


Specimen Preparation
• Heat until fluid to pour
• Stir
• Methods of Applying Specimen
 use a silicone mold
 apply binder directly to spindle or fixed base
 direct transfer with glass rod or spatula
 syringe
 take care when removing plates to load sample
Specimen Preparation
• Close plates to test gap +/- 50 microns
• Trim
• Remove excess to create bulge
• Bring sample to test temperature +/- 0.1C and
hold for 10 minutes (or required equilibrium time
for DSR)
• Start test
Specimen Preparation
Spindle
Excess Asphalt

Fixed
Base

17
Specimen Preparation
Spindle
After trimming

Fixed
Base

18
Specimen Preparation
Spindle
Slight bulge
is proper

Fixed
Base

19
Testing
applied constant
stress

Binder Oscillating Spindle


Sample
Fixed
Base
Spindle Begins at A
Start of Spindle
cycle... Position

A Time

B C
A
Spindle Moves from A to B
Spindle
Position B

A Time

B C
A
Spindle Moves from B to A
Spindle
Position
B

A
Time

B C
A
Spindles Moves from A to C
Spindle
Position

A
Time

C
B C
A
Spindle Moves from C to A
Spindle
One cycle Position
is complete...

A
Time

C
B C
A
DSR Frequency of
Oscillation
• 10 radians per
second
• 1.59 Hz 360 degrees per circle = 2 
radians per circle

1 radian  57.3 degrees


Elastic:  = 0 deg Viscous:  = 90 deg
max max
Applied
Shear
Stress time

time lag = 
max
Resulting
Shear
Strain time

max
Viscoelastic: 0 < o
max
Applied
Shear
Stress
time
max
G* = 
max

max 
 = time lag
Resulting
Shear
Strain
time
Shear Stress ()
and Shear Strain (
torque (T)
deflection angle () 2T
= 3
r
height (h)
r
= h
 max
radius (r) G* = max
Testing
• Run Test
 condition specimen for 10 cycles
 obtain data from 10 additional
cycles
• Print Results
 G* and 
Data Analysis and Presentation

• Printout provides
 G*/sinδ or G*sinδ
 Strain level PG Spec
 Frequency
 Temperature
 Pass or fail
Criteria Review
Rutting (high temperature)
G*/sin d on unaged binder > 1.00 kPa
G*/sin d on RTFO aged binder
> 2.20 kPa
Criteria Review
Question: Why a minimum G*/sin d to
address rutting
Answer: We want a stiff, elastic binder
to contribute to mix rutting resistance
How: By increasing G* or decreasing d
Criteria Review
Fatigue cracking (intermediate temperature)
G* (sin d) < 5000 kPa

Fatigue typically occurs in older pavements


Criteria Review
• Question: Why a maximum G* sin d
to address fatigue?

Answer: We want a soft elastic binder (to


sustain many loads without cracking)

How: By decreasing G* or decreasing d


Calibration and Standardization
• Temperature
 dummy specimen
• Load and Strain Transducers
 manufacturer
• Overall Calibration
 reference fluid

Viscosity
Standard

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