WELDING PROCEDURE SPECIFICATION (ASME Section IX, ASME VIII Div. 1, ASME B 31.

3)
ESPECIFICAÇÃO DE PROCEDIMENTO DE SOLDAGEM
WPS No. (WPS número): ACA-PIP-WPS-011 Rev. No.(Revisão No.).: 0B1 Date (Data): 28-08-2024
WELDING PROCESS (es) & Type: GTAW/SMAW
Supporting (Apoio) PQR(s): ACA-PIP-SD-PQR-003-1
PROCESSO(S) E TIPO DE SOLDADURA
BASE METALS (Metais básicos) (QW – 403)
P-No. 10H Group No. 1 to P-No. 10H Group No. 1
OR
Specification Type & Grade or UNS Number Specification Type & Grade or UNS Number
Tipo e classe de especificação ou número UNS Tipo e classe de especificação ou número UNS
to
SA 815-WP 31803-S SA 815-WP 31803-S
OR
Chemical Analysis and Mechanical Properties. Chemical Analysis and Mechanical Properties
Análise Química e Propriedades Mecânicas to Análise Química e Propriedades Mecânicas
S31803 S31803
Applicable Piping material Classifications: AL1EN1, BL1EN1 or per Above Groupings
MDMT: -46 °C
Classificações de materiais de tubulação aplicáveis
Thickness Ranges Qualified For : 0.32” (8.18mm) – 0.639” (16.0mm)
Faixas de espessura qualificadas para
Base Metal with Impact Test
0.322” (8.18mm) – 0.630” (16.0mm) Fillet (Filé) : All
Metal base com teste de impacto
Base Metal without Impact Test
Metal base sem teste de impacto
0.322” (8.18mm) – 0.630” (16.0mm) Fillet (Filé): All
Deposited weld metal:
Metal de solda depositado
Diameter range: All Fillet(Filé): All
Maximum Pass Thickness =/< ½”(13mm) (Yes-Sim). (No-Não)
Espessura Máxima de Passagem
Other. (Outra)
JOINTS (QW-402)
Sketches, Production drawings, weld Edge
Refer to
Joint Design symbols, or written description should Preparation
attached show the general arrangement of the
Ground Finish
Projeto Conjunto Preparação de
Sketch parts to be welded where applicable, Borda
Root Spacing the details of the weld groove may be
specified. Backing
Espaçamento Raiz 1 – 4 mm With or Without
Esboços, desenhos de produção, símbolos de apoio
solda ou descrição escrita devem mostrar a
disposição geral das peças a serem soldadas, Metal : N/A
quando aplicável, os detalhes da ranhura de Non metallic : N/A
Backing
solda podem ser especificados Não metálico
Retainers None Material
Lacaios Non fusing Metal : N/A
Material de
Metal não fundível
apoio
Other : N/A
Outra
FILLER METALS (QW – 404) Metal de adição
Process(es) Processo(s) : GTAW SMAW
Specification No (SFA) SFA 5.9 SFA 5.4
Especificações
AWS No. (Classification) ER2209 E2209-15
F No.: 6 5
A No. 8 8
Electrode or Filler wire trade name (Nome BOHLER FOX CN 22/9 THERMANIT 22/09
comercial do eletrodo ou fio de enchimento
Addition / deletion of filler metal (Adição/exclusão N/A N/A
de metal de adição)

-1- Form ACA-C013-WI-F3 Rev 01, 09-2023

Alloy flux (Fluxo de liga) N/A N/A
Supplemental Alloy elements
N/A N/A
Elementos de liga suplementares
Size of Filler metal
2.4 mm 2.5 mm
Tamanho do metal de adição
Diameter > ¼” (6mm) N/A N/A
Diâmetro > ¼” (6mm)
Filler Metal Product form Solid Wire N/A
Formulário de produto de metal de enchimento
Supplemental Filler metal N/A N/A
Metal de adição suplementar
Weld Metal (Metal de solda)
Thickness Grossura
Groove (Sulco) : 6.0 mm max 10.0 mm max
Fillet (File) : All All
Electrode –Flux (Eletrodo – Fluxo) (Class-Aula ) N/A N/A
Flux Type (Tipo de fluxo) N/A N/A
Electrode -Flux Trade Name
N/A N/A
Eletrodo - Nome comercial de fluxo
Consumable Insert
N/A N/A
Inserção Consumível
Re-crushed Slag
N/A N/A
Escória Re-triturada
Other (Outra)
POST WELD HEAT TREATMENT - TRATAMENTO TÉRMICO PÓS
POSITIONS-POSIÇÕES (QW – 405)
SOLDA(QW – 407)(STRESS RELIEVING-ALÍVIO DO STRESS)
Position(s) of Groove: All Temperature Range: N/A
Posição(ões) do Groove Faixa de temperatura
Welding Progression: Uphill for Vertical Time Range: N/A
Progressão de Soldagem Intervalo de tempo:
Position(s) of Fillet: All Heating Rate/Hr.: N/A
Posição(ões) do filé: Taxa de aquecimento/hora
Other. (Outra) Cooling Rate/Hr. N/A
Taxa de resfriamento/hora

PREHEAT- PRÉ-AQUECIMENTO (QW – 406) GAS -GÁS (QW – 408)

Preheat Temp. Repair
(Min.): 50°F Weld: Percent Composition
Temperatura de pré- Solda de reparo Composição percentual
(10°C)
aquecimento (mínima)
Inter-pass Temp (max.): Gas(es) (Mixture) Flow Rate
Temperatura entre passagens 210°F (100°C) -GÁS(s) Mistura Quociente de vazão
(máximo):
Preheat Maintenance: Shielding Argon /
N/A Nitrogen
98% / 2% 10 - 14 L/Min
Manutenção de pré aquecimento: Blindagem
Other (Outra) Trailing
None None N/A
Seguindo
(Continuous or special heating where Backing Argon /
applicable should be specified) (Aquecimento Apoio Nitrogen 98% / 2% 10 - 14 L/Min
contínuo ou especial, quando aplicável, deve ser especificado)
Other(Outra)
TEHNIQUE - TÉCNICA (QW – 410)
String or Weave bead: Oscillation:
Conta de cordão ou trama:
String & Weave Oscilação:
None
Max. Weave Width: 2 x Æ Of Wire Contact tube to work distance: N/A
Máx. Largura da tram Número de eletrodos
Orifice/Gas cup size: 10mm For GTAW Multiple/Single pass (per side) Multiple
-2- Form ACA-C013-WI-F3 Rev 01, 09-2023
 Tamanho do orifício/copo de gás Passagem múltipla/única (por lado):
Initial Cleaning: SS Grinding or Wire Multiple/Single Electrode(s):
Single
Limpeza inicial: Brushing Eletrodo(s) Múltiplo/Único(s):
Inter-pass Cleaning: SS Grinding or Wire Electrode Spacing:
N/A
Limpeza entre passagens Brushing Espaçamento entre eletrodos:
Method of back gouging:
N/A Peening: Not Allowed
Método de goivagem nas costas
Manual / Automatic Use of thermal process:
Manual N/A
Manual / Automático Uso de processo térmico
Closed out chamber Time between R & H. pass :
Câmara fechada N/A Tempo entre a passagem R e H. N/A

ELECTRICAL CHARACTERISTICS (QW-409)

Filler Metal Metal de Current Travel Speed Heat input
preenchimento Atual (Range) (KJ/mm)
Proces Volts
Side mm/min (Max.)
Run# s Amp. (Range)
Lad Type & Velocidade Entrada de
Correr Proces Class Dia Range Volts
o Polarity de calor
so Aula Diâmetro Amplificador. (faixa)
Tipo e deslocament (KJ/mm)
Faixa
polaridade o (alcance) (Máx.)
mm/minuto
A Root GTAW ER2594 2.4 mm DCEN 80 - 87 9 – 10 53.26-57.60 0.750 – 0.980
A Hot GTAW ER2594 2.4 mm DCEN 95 - 105 9 - 10 69.23-72.25 0.710 – 0.910
A Fill SMAW E2594-15 2.5 mm DCEP 73 - 75 20 - 22 108.19-132.72 0.660 – 0.915
A Or Fill SMAW E2594-15 3.2mm DCEP 75 - 80 21 - 23 120.65-143.18 0.660 – 0.915
A Cap SMAW E2594-15 2.5 mm DCEP 73 - 75 20 - 22 108.19-120.00 0.730 – 0.915
A Or Cap SMAW E2594-15 3.2 mm DCEP 75 - 80 21 - 23 120.65-129.45 0.730 – 0.915

Pulsing Current Heat Input (Max)

Corrente pulsante N/A Entrada de calor (Máx.) 0.980 KJ/mm

Mode of metal Transfer for GMAW

Tungsten Electrode Size & Type 2.4mm, SFA 5.12,
Tamanho e tipo do eletrodo de tungstênio (Spray arc, short circuiting arc, etc.) N/A
EWTh-2 Modo de transferência de metal para GMAW
(Arco spray, arco de curto-circuito, etc.)
NOTES: NOTAS:
1. Use stringer bead welding technique for first pass and second pass; Use stringer or weave for remaining passes.
2. Weld preparation and cleaning tools are restricted to stainless steel brushes, grinding wheels etc. that have not been
contaminated on other metals
3. Maintain back purge until Root and Hot pass of weld metal is deposited or 6.0mm, whichever is greater.

Prepared By ACFS: Reviewed & Approved By: Client: Reviewed / Approved By:
Preparado pela ACFS ACFS (Revisado e aprovado Cliente: Revisado/Aprovado por:
por): ACFS

Name: (Nome):

Date: (Data):

Sign: (Assinatura):

-3- Form ACA-C013-WI-F3 Rev 01, 09-2023

 JOINT DESIGNS

max
m (max)
35°
65 ± 5° ± 5° 10° ± 3°

119mm
9
60° ± 5°

T (max)
1.6 mm (max)

1.6 mm (max)
1.0 ~ 5.0 mm 1.6 ~ 4.0mm

1.6 mm (max)
1.0 ~ 5.0 mm

Slip on Flange
O-Let
Socket
± 5°
35°

Pipe Hub
1.6 ~ 4.0 mm

Pipe1 Pipe
Approx. 1.6mm Gap
Before Welding

60° ± 10°
Threaded Coupling
QUALIFICATION IN GROOVE
WELDS QUALIFIES FOR ALL

t (max)
FILLET WELD CONNECTIONS
1.6mm (max)

Threaded Pipe 30 (max)

)

1.6 ~ 4.0mm

t (max) 3 5°
60° ± 10° 60° ± 10° ±5
°
t (max)

t (max)

5mm
t (max)
1.6mm (max)

1.6mm (max)
1.6mm (max)

1.6 ~ 4.0mm 1.0 ~ 5.0mm

1.0 ~ 5.0mm
 Welding Procedure Qualification Record (ASME IX-ASME VIII Div. 1)
PQR No.: ACA-PIP-SD-PQR-003-1 Date: 28-08-2024 Rev. No. 0B1
Welding Process(es): GTAW/SMAW Type/Mode: Manual WPS No: ACA-PIP-WPS-011
Joint Design (QW-402)

Coupon Thickness: 8.18 mm

Base Metal (QW-403) Pre Heat (QW-406)

Material Specification: SA790 ASTM A790 Preheat Temperature: 10 °C
Type or Grade, or UNS Number: ASTM UNS 32750
P No. 10H Group No. 1 to P No. 10H Group No. 1

Thickness of Test Coupon : 8.18 mm Inter-pass Temp: £ 100 °C

Diameter of Test Coupon: 219.1 mm (8”)
Measurement Method: Digital Thermometer

Heat No.: 60177 Heat No.: 60177

Filler Metal (QW-404) GTAW SMAW PWHT (QW-407)

SFA Specification (SFA): 5.9 5.4 Heating Rate °C/Hr: N/A

AWS Classification: ER2594 E2954-15 Soak Temperature °C: N/A
Flux Class and Type: N/A N/A Holding Time Hrs: N/A
Filler F No: 6 5 Cooling Rate °C/Hr: N/A
Weld metal Analysis A No 8 8 Withdrawal Temperature °C: N/A
Filler Metal Size: 2.4 mm 2.5 mm

Filler metal product form Solid N/A

Electrode flux classification N/A N/A

Flux trade Name N/A N/A

ESAB OK
ESAB OK 68.55
Electrode Trade Name: Tigrod 2509
Position (QW-405) Gas (QW-408)
Groove Position : 5G Percent Composition
Weld Progression: Uphill Gases Mixture Flow rate
Argon / 98% /
Shielding 10 - 14 L/Min
Nitrogen 2%
Argon / 98% /
Backing 10 - 14 L/Min
Nitrogen 2%

1 Form ACA-C013-WI-F5 Rev 01, 09-2023

Electrical Characteristics (QW-409)
Wave
Power or
Process Current Polarity Amps Volts Control Arc Time Weld Bead Length
Energy
Form
GTAW/ REFER TO RECORDS OF VARIABLES
DC EN
SMAW
Mode of Metal Transfer (FCAW) N/A Tungsten Electrode Size Æ2.4mm
Technique (QW-410)
Ref. to
Travel speed Range: String /
Records of String / Weave: Single / Multi pass Multi Pass
mm/min Variables Weave
Cont.Tube/Work
Single / Multiple Electrode Single N/A Oscillation N/A
Dist.
Record of Actual Test Parameters: REFER TO RECORDS OF VARIABLES
Environmental Conditions: Welding Conducted in the day time at ambient temperature of 29 - 33°C
Attachments: Mill Certificates, NDT reports, Mechanical Test Reports, Macro Photos, Hardness Test Report
Visual Inspection: ACCEPTED PWHT: N/A
TENSILE TEST:( QW-150): Report No.: R-AL15-159-04 Rev 03 Sec 2.1, Table 1
Standard: ASTM A370-23
Tensile
Size (mm) Ultimate
Specimen # Area (mm²) Strength Fracture Location % Elongation
Width x Thickness Load, KN
MPa
1 13.05 X 8.28 108.05 88.67 821 Parent Material 26.46
2 13.16 X 8.10 106.60 87.86 824 Parent Material 30.58
Requirements : ASTM A790 S32750
Result : PASSED
Alternate Tension Specimen Specification (QW-462):
Guided Bend Test (QW-160): Report No.: R-AL15-159-04 Rev 03 Sec 2.2, Table 2
Mandrel
Type (Face Bend Width Length Thickness
Specimen # Diameter Result
(mm) / Root / Side Angle (mm) (mm) (mm)
1 40 Face 180° 38 250 9 PASSED
2 40 Face 180° 38 250 9 PASSED
3 40 Root 180° 38 250 9 PASSED
4 40 Root 180° 38 250 9 PASSED
Toughness Test (V-Notch) (QW-170): Report No.: R-AL15-159-04 Rev 03 Sec 2.3, Table 3
Test
Transverse To Weld Standard ASTM E23-24
Direction
Temperature Impact Value (J) Lateral Expansion
Location Percent Shear Fracture
(°C) Individual Avg. (x0.001)
WM 28.7 28.88 30.28 29.14 0.54 0.43 0.43 0 0 10
FL -46 73.90 47.46 44.03 55.13 - 0.85 0.78 - 30 30
FL+2 80.65 88.84 87.51 85.67 - - - - - -
Size : 5 x 10 x 55mm

2 Form ACA-C013-WI-F5 Rev 01, 09-2023

 27J Minimum Average Value
Requirement (J)
20J Minimum Single Value
Result : PASSED
Fillet weld test (QW-180):
Penetration Into Parent
Result-Satisfactory N/A N/A
Metal
Macro Results: Report No.: R-AL15-159-04 Rev 03 Sec 2.5: PASSED
Other Tests
Type of Hardness Test: Vicker Hardness HV10: Report No.: R-AL15-159-04 Rev 03 Sec 2.4, Table 4
Test Standard : ASTM E384-22/E92
PM A HAZ A WM HAZ B PM B
ROOT 264.49 264.79 267.64 274.33 265.46
MID - 276.16 277.95 284.48 -
CAP 263.34 258.77 207.09 260.59 272.08
Maximum Recorded Value : 274.33 HV10
Maximum Requirements : 350 HV 10
Other Tests:
Ferrite Count: Report No. R-AL15-159-04 Rev. 03, Sec. 2.6, Table 5: ASTM E562: Passed
Corrosion Test: Report No. R-AL15-159-04 Rev. 03, Sec. 2.7, Table 6: ASTM G48-11 (Method A): Passed
Microscopic Examination: Report No. R-AL15-159-04 Rev. 03, Sec. 2.8: ASTM A923-A @ 500x: Passed

Welders Name : Employee Number : Stamp No.:

Eduardo Enguito E246 T
Test Conducted by : One Eighty Materials Laboratory Test No.:
Testing (PTY) Ltd. R-AL15-159-04 Rev 03

We certify that the statements in this record are correct and that the test welds were prepared,
welded and tested in requirements of section IX and ASME VIII Div. 1 of the ASME Boiler and Pressure
Vessel Code.

Prepared By ACFS : Certified By ACFS :

Preparado por ACFS: Certificado pela ACFS

Name (Nome):

Signature( Assinatura):
George Digitally signed by
George Lacerna
Jessie Digitally signed by
Jessie Culla
Lacerna Culla Date: 2024.09.11
Date: 2024.09.11
16:51:30 +01'00'
Date (Data): 16:50:18 +01'00'

3 Form ACA-C013-WI-F5 Rev 01, 09-2023

Client : Record Number : ACFS-PIP-SD-PQR-003-1

Fabrication Yard Location: MALEMBO SHOP Date : 20 MAY 2024

Project Title: ACFS SUPER DUPLEX WPS QUALIFICATION Page : 1

Record of Variables for Welding Procedure Qualification

PQR NO.: ACFS-PIP-SD-PQR-003-1 Welder I.D.# T Material Grade: ASTM UNS 32750 Coupon Id: SD-2-1

WPS NO.: Electrode Trade Name: Heat Number : 60177 / 60177 Coupon Dimensions : 8" ∅ X 23.62"(600mm) Long Coupon Thickness : 0.32" (8.18mm)
ACA-PIP-WPS-010-00 ESAB Lot No.: IT31433 / SBX1910834

Heat Input Data Temperature

Type Arc time Gas Flow Ltr
Process Run# Class Dia mm Position Amps Volts Weld Length Weld thickness Flux Pre Heat Inter pass Deg
( Sec.) mm/Minute KJ/mm / Min
(mm) each pass, mm Deg.C C

GTAW 1A ER2594-15 2.4 5G DCEN 80 9,9 183 150 49.2 0.966 - 10-14L 29.4

GTAW 1B ER2594-15 2.4 5G DCEN 80.1 9,8 103 90 52.4 0.898 - 10-14L - 33.4

GTAW 1C ER2594-15 2.4 5G DCEN 80.3 9,6 140 125 53.6 0.863 - 10-14L - 35.1

GTAW 1D ER2594-15 2.4 5G DCEN 80.3 9,4 109 95 52.3 0.866 - 10-14L - 32.3

GTAW 1E ER2594-15 2.4 5G DCEN 85 9,5 89 90 60.7 0.799 - 10-14L - 36.4

GTAW 1F ER2594-15 2.4 5G DCEN 86 9,6 105 105 2 60.0 0.826 - 10-14L - 37.1

Joint Details

Name George M. Lacerna Signature George Lacerna Digitally signed by George Lacerna
Date: 2024.09.03 16:21:22 +01'00'
Date:
Test Witnessed by
Name Sherwin Vere Signature Date:

Form ACA-C013-WI-F7 Rev 0, 06-2023

Client : Record Number : ACFS-PIP-SD-PQR-003-1

Fabrication Yard Location: MALEMBO SHOP Date : 20 MAY 2024

Project Title: ACFS SUPER DUPLEX WPS QUALIFICATION Page : 1

Record of Variables for Welding Procedure Qualification

PQR NO.: ACFS-PIP-SD-PQR-003-1 Welder I.D.# T Material Grade: ASTM UNS 32750 Coupon Id: SD-2-1

WPS NO.: Electrode Trade Name: Heat Number : 60177 / 60177 Coupon Dimensions : 8" ∅ X 23.62"(600mm) Long Coupon Thickness : 0.32" (8.18mm)
ACA-PIP-WPS-010-00 ESAB Lot No.: IT31433 / SBX1910834

Heat Input Data Temperature

Type Arc time Gas Flow Ltr
Process Run# Class Dia mm Position Amps Volts Weld Length Weld thickness Flux Pre Heat Inter pass Deg
( Sec.) mm/Minute KJ/mm / Min
(mm) each pass, mm Deg.C C

GTAW 2A ER2594-15 2.4 5G DCEN 97 9,8 201 210 62.7 0.910 - 10-14L 30.4

GTAW 2B ER2594-15 2.4 5G DCEN 105.1 9,9 234 315 80.8 0.773 - 10-14L - 36.4

GTAW 2C ER2594-15 2.4 5G DCEN 105 9,7 113 160 1.5 85.0 0.719 - 10-14L - 33.5

Joint Details

Digitally signed by George

Name George M. Lacerna Signature George Lacerna Lacerna
Date: 2024.09.03 16:21:39 +01'00'
Date:
Test Witnessed by
Name Sherwin Vere Signature Date:

Form ACA-C013-WI-F7 Rev 0, 06-2023

Client : Record Number : ACFS-PIP-SD-PQR-003-1

Fabrication Yard Location: MALEMBO SHOP Date : 20 MAY 2024

Project Title: ACFS SUPER DUPLEX WPS QUALIFICATION Page : 1

Record of Variables for Welding Procedure Qualification

PQR NO.: ACFS-PIP-SD-PQR-003-1 Welder I.D.# T Material Grade: ASTM UNS 32750 Coupon Id: SD-2-1

WPS NO.: Electrode Trade Name: Heat Number : 60177 / 60177 Coupon Dimensions : 8" ∅ X 23.62"(600mm) Long Coupon Thickness : 0.32" (8.18mm)
ACA-PIP-WPS-010-00 ESAB Lot No.: IT31433 / SBX1910834

Heat Input Data Temperature

Type Arc time Gas Flow Ltr
Process Run# Class Dia mm Position Amps Volts Weld Length Weld thickness Flux Pre Heat Inter pass Deg
( Sec.) mm/Minute KJ/mm / Min
(mm) each pass, mm Deg.C C

SMAW 3A E2954-15 2.5 5G DCEN 75 21,4 32 60 112.5 0.856 - - 37.1

SMAW 3B E2954-15 2.5 5G DCEN 75 21,3 33 60 109.1 0.879 - - - 48

SMAW 3C E2954-15 2.5 5G DCEN 75 21,3 30 55 110.0 0.871 - - - 47.9

SMAW 3D E2954-15 2.5 5G DCEN 75.1 21,3 25 45 108.0 0.889 - - - 49

SMAW 3E E2954-15 2.5 5G DCEN 75.2 21,2 31 55 106.5 0.899 - - - 50

SMAW 3F E2954-15 2.5 5G DCEN 75.3 21,4 29 55 113.8 0.850 - - - 49.3

SMAW 3G E2954-15 2.5 5G DCEN 75.6 21,6 24 45 112.5 0.871 - - - 48

SMAW 3H E2954-15 2.5 5G DCEN 75.5 20,9 30 60 120.0 0.789 - - - 48.2

SMAW 3I E2954-15 2.5 5G DCEN 75.4 21 25 45 108.0 0.880 - - - 47.8

SMAW 3J E2954-15 2.5 5G DCEN 75 21 31 60 116.1 0.814 - - - 49.2

SMAW 3K E2954-15 2.5 5G DCEN 75 21,2 26 50 115.4 0.827 - - - 46

SMAW 3L E2954-15 2.5 5G DCEN 75 21,1 44 85 2 115.9 0.819 - - - 48.5

Joint Details

Name George M. Lacerna Signature George Lacerna Digitally signed by George Lacerna
Date: 2024.09.03 16:21:55 +01'00' Date:
Test Witnessed by
Name Sherwin Vere Signature Date:

Form ACA-C013-WI-F7 Rev 0, 06-2023

Client : Record Number : ACFS-PIP-SD-PQR-003-1
Fabrication Yard Location: MALEMBO SHOP Date : 20 MAY 2024

Project Title: ACFS SUPER DUPLEX WPS QUALIFICATION Page : 1

Record of Variables for Welding Procedure Qualification

PQR NO.: ACFS-PIP-SD-PQR-003-1 Welder I.D.# T Material Grade: ASTM UNS 32750 Coupon Id: SD-2-1

WPS NO.: Electrode Trade Name: Heat Number : 60177 / 60177 Coupon Dimensions : 8" ∅ X 23.62"(600mm) Long Coupon Thickness : 0.32" (8.18mm)
ACA-PIP-WPS-010-00 ESAB Lot No.: IT31433 / SBX1910834

Heat Input Data Temperature

Type Arc time Gas Flow Ltr
Process Run# Class Dia mm Position Amps Volts Flux
( Sec.) Weld Length Weld thickness / Min Pre Heat Inter pass Deg
mm/Minute KJ/mm
(mm) each pass, mm Deg.C C

SMAW 4A E2954-15 2.5 5G DCEN 75.4 21,1 37 90 145.9 0.654 - - 39

SMAW 4B E2954-15 2.5 5G DCEN 77 21,6 35 65 111.4 0.896 - - - 50

SMAW 4C E2954-15 2.5 5G DCEN 75 21,1 39 90 138.5 0.686 - - - 48.7

SMAW 4D E2954-15 2.5 5G DCEN 75 21,5 34 65 114.7 0.843 - - - 49

SMAW 4E E2954-15 2.5 5G DCEN 75.2 21,4 37 80 129.7 0.744 - - - 50

SMAW 4F E2954-15 2.5 5G DCEN 75 22 34 65 114.7 0.863 - - - 50.4

SMAW 4G E2954-15 2.5 5G DCEN 75.2 21,3 40 90 135.0 0.712 - - - 48.8

SMAW 4H E2954-15 2.5 5G DCEN 75 21,5 35 80 137.1 0.705 - - - 51

SMAW 4I E2954-15 2.5 5G DCEN 74.6 21,6 34 65 2 114.7 0.843 - - - 51.4

Joint Details

Name George M. Lacerna Signature George Lacerna Digitally signed by George Lacerna
Date: 2024.09.03 16:22:11 +01'00' Date:
Test Witnessed by
Name Sherwin Vere Signature Date:

Form ACA-C013-WI-F7 Rev 0, 06-2023

Client : Record Number : ACFS-PIP-SD-PQR-003-1

Fabrication Yard Location: MALEMBO SHOP Date : 20 MAY 2024

Project Title: ACFS SUPER DUPLEX WPS QUALIFICATION Page : 1

Record of Variables for Welding Procedure Qualification

PQR NO.: ACFS-PIP-SD-PQR-003-1 Welder I.D.# T Material Grade: ASTM UNS 32750 Coupon Id: SD-2-1

WPS NO.: Electrode Trade Name: Heat Number : 60177 / 60177 Coupon Dimensions : 8" ∅ X 23.62"(600mm) Long Coupon Thickness : 0.32" (8.18mm)
ACA-PIP-WPS-010-00 ESAB Lot No.: IT31433 / SBX1910834

Heat Input Data Temperature

Type Arc time Gas Flow Ltr
Process Run# Class Dia mm Position Amps Volts Weld Length Weld thickness Flux Pre Heat Inter pass Deg
( Sec.) mm/Minute KJ/mm / Min
(mm) each pass, mm Deg.C C

SMAW 5A E2954-15 2.5 5G DCEN 74.5 21,2 30 60 120.0 0.790 - - 32.3

SMAW 5B E2954-15 2.5 5G DCEN 74.6 21,3 26 45 103.8 0.918 - - - 48.5

SMAW 5C E2954-15 2.5 5G DCEN 73 21,4 31 60 116.1 0.807 - - - 50.1

SMAW 5D E2954-15 2.5 5G DCEN 73 21,6 33 60 109.1 0.867 - - - 47.8

SMAW 5E E2954-15 2.5 5G DCEN 73 21,6 35 65 111.4 0.849 - - - 49.4

SMAW 5F E2954-15 2.5 5G DCEN 73 21,5 31 55 106.5 0.885 - - - 51.2

SMAW 5G E2954-15 2.5 5G DCEN 73 21,6 37 65 105.4 0.898 - - - 51.4

SMAW 5H E2954-15 2.5 5G DCEN 73 21,6 13 25 115.4 0.820 - - - 51.8

SMAW 5I E2954-15 2.5 5G DCEN 73 21,6 32 60 112.5 0.841 - - - 49

SMAW 5J E2954-15 2.5 5G DCEN 73 21,4 35 65 111.4 0.841 - - - 50

SMAW 5K E2954-15 2.5 5G DCEN 73 21,6 32 60 112.5 0.841 - - - 51.5

SMAW 5L E2954-15 2.5 5G DCEN 73 21,4 36 70 2 116.7 0.803 - - - 49.8

Joint Details

Name George M. Lacerna Signature George Lacerna Digitally signed by George Lacerna
Date: 2024.09.03 16:22:26 +01'00' Date:
Test Witnessed by
Name Sherwin Vere Signature Date:

Form ACA-C013-WI-F7 Rev 0, 06-2023

Client : Record Number : ACFS-PIP-SD-PQR-003-1
Fabrication Yard Location: MALEMBO SHOP Date : 20 MAY 2024

Project Title: ACFS SUPER DUPLEX WPS QUALIFICATION Page : 1

Record of Variables for Welding Procedure Qualification

PQR NO.: ACFS-PIP-SD-PQR-003-1 Welder I.D.# T Material Grade: ASTM UNS 32750 Coupon Id: SD-2-1

WPS NO.: Electrode Trade Name: Heat Number : 60177 / 60177 Coupon Dimensions : 8" ∅ X 23.62"(600mm) Long Coupon Thickness : 0.32" (8.18mm)
ACA-PIP-WPS-010-00 ESAB Lot No.: IT31433 / SBX1910834

Heat Input Data Temperature

Type Arc time Gas Flow Ltr
Process Run# Class Dia mm Position Amps Volts Flux
( Sec.) Weld Length Weld thickness / Min Pre Heat Inter pass Deg
mm/Minute KJ/mm
(mm) each pass, mm Deg.C C

SMAW 6A E2954-15 2.5 5G DCEN 75.4 21,3 40 80 120.0 0.803 - - 33

SMAW 6B E2954-15 2.5 5G DCEN 75.3 21,6 33 60 109.1 0.895 - - - 51

SMAW 6C E2954-15 2.5 5G DCEN 75 21,6 35 70 120.0 0.810 - - - 48.9

SMAW 6D E2954-15 2.5 5G DCEN 75 21,5 35 65 111.4 0.868 - - - 47.5

SMAW 6E E2954-15 2.5 5G DCEN 75.1 21,6 33 60 109.1 0.892 - - - 51

SMAW 6F E2954-15 2.5 5G DCEN 75.2 21,8 37 70 113.5 0.867 - - - 52.1

SMAW 6G E2954-15 2.5 5G DCEN 75 21,3 36 70 116.7 0.822 - - - 50.5

SMAW 6H E2954-15 2.5 5G DCEN 75 21,5 39 80 123.1 0.786 - - - 49.8

SMAW 6I E2954-15 2.5 5G DCEN 75.3 21,7 35 70 120.0 0.817 - - - 47.6

SMAW 6J E2954-15 2.5 5G DCEN 75.5 21,4 34 70 1.5 123.5 0.785 - - - 52

Joint Details

Digitally signed by George

Name George M. Lacerna Signature George Lacerna Lacerna
Date: 2024.09.03 16:22:43 +01'00'
Date:
Test Witnessed by
Name Sherwin Vere Signature Date:

Form ACA-C013-WI-F7 Rev 0, 06-2023

Client : Record Number : ACFS-PIP-SD-PQR-003-1

Fabrication Yard Location: MALEMBO SHOP Date : 20 MAY 2024

Project Title: ACFS SUPER DUPLEX WPS QUALIFICATION Page : 1

Record of Variables for Welding Procedure Qualification

PQR NO.: ACFS-PIP-SD-PQR-003-1 Welder I.D.# T Material Grade: ASTM UNS 32750 Coupon Id: SD-2-1

WPS NO.: Electrode Trade Name: Heat Number : 60177 / 60177 Coupon Dimensions : 8" ∅ X 23.62"(600mm) Long Coupon Thickness : 0.32" (8.18mm)
ACA-PIP-WPS-010-00 ESAB Lot No.: IT31433 / SBX1910834

Heat Input Data Temperature

Type Arc time Gas Flow Ltr
Process Run# Class Dia mm Position Amps Volts Flux
( Sec.) Weld Length Weld thickness / Min Pre Heat Inter pass Deg
mm/Minute KJ/mm
(mm) each pass, mm Deg.C C

SMAW 7A E2954-15 2.5 5G DCEN 75 21,6 41 90 131.7 0.738 - - 32.8

SMAW 7B E2954-15 2.5 5G DCEN 75.3 21,8 39 70 107.7 0.915 - - - 48.7

SMAW 7C E2954-15 2.5 5G DCEN 75 21,8 37 80 129.7 0.756 - - - 50.4

SMAW 7D E2954-15 2.5 5G DCEN 75 21,5 38 70 110.5 0.875 - - - 51.2

SMAW 7E E2954-15 2.5 5G DCEN 75 21,4 37 70 113.5 0.848 - - - 51

SMAW 7F E2954-15 2.5 5G DCEN 75.5 21,8 34 70 123.5 0.799 - - - 47.4

SMAW 7G E2954-15 2.5 5G DCEN 75.3 21,7 36 75 125.0 0.784 - - - 49.1

SMAW 7H E2954-15 2.5 5G DCEN 75.2 21,5 39 80 123.1 0.788 - - - 50.4

SMAW 7I E2954-15 2.5 5G DCEN 75 21,8 38 85 1.5 134.2 0.731 - - - 52.4

Joint Details

Name George M. Lacerna Signature George Lacerna Digitally signed by George Lacerna
Date: 2024.09.03 16:23:00 +01'00'
Date:
Test Witnessed by
Name Sherwin Vere Signature Date:

Form ACA-C013-WI-F7 Rev 0, 06-2023

 DYE PENETRANT INSPECTION REPORT

CLIENT LOCATION INSPECTION DATE

ALGOA MALEMBO 3 May 2024
OCEANEERING JOB NO. REPORT NO.
CABGOC 171092 PT-PQT-ACFS-PIP-SD-PQR-003-1-0524
CLIENT ORDER NO.
PAGE 1 OF 3
1564567
EQUIPMENT DETAILS:
COMPONENT ALGOA PQT
DESCRIPTION ACFS PQT COUPON
DRAWING / P&ID No. ACFS-PIP-SD-PQR-003-1
AFE No. N/A WO / VWR # N/A REQUEST / IT No. 207D
MATERIAL MATERIAL THICKNESS SURFACE CONDITION TEMPERATURE
Stainless Steel 8.18mm As Cleaned 27 Degrees C
PROCEDURE/WORK INSTRUCTION/TECHNIQUE ACCEPTANCE STANDARD
NDT-OPR-041 Rev 8 / NDT-TEC-P100 Rev 4 ASME IX / 2021Edition
PENETRANT AND SOAK TIME CLEANER DEVELOPER AND SOAK TIME
ARDROX 996PB (10-30 Mins.) ARDROX 9PR5 ARDROX 9D1B (10-15 Mins.)
BATCH NO. C232475103 BATCH NO. C232432160 BATCH NO. C232461743
LIGHTING EQUIPMENT LIGHT METER (WHITE / UV) READING AT TEST SURFACE
Head Lamp RS PRO ILM 1337 - S/N-221004226 1750 Lux
RESTRICTIONS TO INTENDED SCOPE / N/A
TEST COVERAGE
SCOPE OF WORK:
Dye Penetrant Inspection was carried out on the weld bevel preparation listed below.

RESULTS:
JOINT NO WELDER ID DIMENSIONS DRAWING NUMBER RESULT
SD-2-1 N/A 8" X 0.32" ACFS-PIP-SD-PQR-003-1 Accepted

Note:

OCEANEERING INSPECTOR OCEANEERING SUPERVISOR CLIENT

Joaquim Digitally signed by Joaquim

Jude Digitally signed by

Viegas

SIGN Viegas
Date: 2024.05.13 16:13:49
+01'00' Jude Rassie
QUALS. ASNT LII
NAME Joaquim Viegas NAME
Rassie Date: 2024.05.13
16:14:11 +01'00' NAME
This report signifies acceptance or otherwise with regard only to the acceptance criteria of the applicable standard. Such compliance, or otherwise, does not infer or imply
suitability and/or fitness for any particular use or purpose. No other communication by Oceaneering, whether oral or written, shall be construed as an option as to whether
the weld or other work inspected should be accepted or rejected.

113059-ANG-IMDS-FRM-0004 Rev 1 Uncontrolled copy when printed.

 DYE PENETRANT INSPECTION REPORT

CLIENT LOCATION INSPECTION DATE

ALGOA MALEMBO 22 May 2024
OCEANEERING JOB NO. REPORT NO.
CABGOC 171092 PT-ACFS-PIP-SD-PQR-003-1-0524
CLIENT ORDER NO.
PAGE 1 OF 2
1564567
EQUIPMENT DETAILS:
COMPONENT ALGOA PQT
DESCRIPTION ACFS PQT COUPON
DRAWING / P&ID No. ACFS-PIP-SD-PQR-003-1- 5G
AFE No. N/A WO / VWR # N/A REQUEST / IT No. 244B
MATERIAL MATERIAL THICKNESS SURFACE CONDITION TEMPERATURE
Super Duplex 0.32" (8.18mm) As Cleaned 27 Degrees C
PROCEDURE/WORK INSTRUCTION/TECHNIQUE ACCEPTANCE STANDARD
NDT-OPR-041 Rev 8 / NDT-TEC-P100 Rev 4 ASME IX / 2021Edition
PENETRANT AND SOAK TIME CLEANER DEVELOPER AND SOAK TIME
ARDROX 996PB (10-30 Mins.) ARDROX 9PR5 ARDROX 9D1B (10-15 Mins.)
BATCH NO. C232475103 BATCH NO. C232432160 BATCH NO. C232461743
LIGHTING EQUIPMENT LIGHT METER (WHITE / UV) READING AT TEST SURFACE
Head Lamp RS PRO ILM 1337 - S/N-221004226 1750 Lux
RESTRICTIONS TO INTENDED SCOPE / N/A
TEST COVERAGE
SCOPE OF WORK:
Dye Penetrant Inspection was carried out on the weld listed below.

RESULTS:
JOINT NO WELDER ID DIMENSIONS DRAWING NUMBER RESULT
SD-2-1 T 8" x 0.32" (8.18mm) ACFS-PIP-SD-PQR-003-1 Accepted

Note:

OCEANEERING INSPECTOR OCEANEERING SUPERVISOR CLIENT

Joaquim Digitally signed by Joaquim

SIGN Viegas
Viegas
Date: 2024.05.29 11:11:02
+01'00'
Jude Digitally signed
by Jude Rassie
QUALS. ASNT LII
NAME Joaquim Viegas
Rassie
NAME
Date: 2024.05.29
11:11:19 +01'00'
NAME
This report signifies acceptance or otherwise with regard only to the acceptance criteria of the applicable standard. Such compliance, or otherwise, does not infer or imply
suitability and/or fitness for any particular use or purpose. No other communication by Oceaneering, whether oral or written, shall be construed as an option as to whether
the weld or other work inspected should be accepted or rejected.

113059-ANG-IMDS-FRM-0004 Rev 1 Uncontrolled copy when printed.

 RADIOGRAPHIC INSPECTION REPORT

CLIENT LOCATION INSPECTION DATE

ALGOA MALEMBO 22 May 2024
OCEANEERING JOB NO. REPORT NO.
CABGOC 171092 RT-ACFS-PIP--SD-PQR-003-1-0524
CLIENT ORDER NO.
PAGE 1 OF 2
1068046
EQUIPMENT DETAILS:
COMPONENT ALGOA PQT
DESCRIPTION ACFS PQT COUPON
DRAWING / P&ID No. ACFS-PIP-SD-PQR-003-1 - 5G
AFE No. N/A WO / VWR # N/A REQUEST / IT No. 244B
Surface Condition Material Welding Process Heat Treat (If Applicable)
As Welded Super Duplex GTAW/SMAW N/A
OCEANEERING Procedure No: OCEANEERING Technique No: Standard / Code: Acceptance Standard
NDT-OPR-011 NDT-TEC-R103 ASME IX ASME IX
Rev 8 Rev 4 2021 EDITION 2021 EDITION
732.6 Gbq Source Dims Effective Focal Spot
Source Type Iridium-192 Source Activity 0.079" X 0.049" 0.093"
19.8 Ci (Inch) Dimension
Source To Film Distance Technique Density Required No. Films in Cassette
Min Req 8.6" D.W.S.I. 2.0 - 4.0 1
IQI Type IQI Range Location Of IQI Geometric Unsharpness (in) Thickness
FE EN 10 - 16 Film Side 0.004 8''Ø X8.18mm
Screen Type Number of Exposures No. of Radiographs Utilized Film Type Film Size
Lead 3 3 AGFA D7 10 x 40cm

RESULTS

Accept

Reject
Weld ID / Area of Density Sensitivity Location of
Welder ID Dia / Size Type Of Indication
Test Item Interest Range (Essential Wire) Indication

SD-2-1 T 8" 0 - 23 2.4 -2.8 W13 N/A Y

23 - 46 2.5 -2.7 W13 N/A Y
46 - 0 2.5 -2.7 W13 N/A Y

Total Welds Rejected:

Test Restrictions or necessary Deviations from Technique:
Comments: None

TECHNICIAN INTERPRETER SUPERVISOR CLIENT REP

Digitally signed by Digitally signed by
Arif Arif Kayamkhani
Kayamkhani Date: 2024.05.29
10:15:03 +01'00'
SIRAJUDEE
N HAMEED
SIRAJUDEEN
HAMEED
Date: 2024.05.29
Jude Digitally signed
by Jude Rassie
QUALS: PCN LII QUALS:
10:15:33 +01'00'
PCN LII Rassie Date: 2024.05.29
10:15:51 +01'00'
NAME: A. KHAN NAME: Sirajudeen

This report signifies acceptance or otherwise with regard only to the acceptance criteria of the applicable standard. Such compliance, or otherwise, does not infer or imply
suitability and/or fitness for any particular use or purpose. No other communication by Oceaneering, whether oral or written, shall be construed as an option as to whether the
weld or other work inspected should be accepted or rejected.

113059-ANG-IMDS-FRM-0005 Rev 1 Uncontrolled copy when printed.

 ONE EIGHTY MATERIALS TESTING (PTY) LTD - WPQR Testing According to: ASME IX, ASME VIII DIV. 1
Report Information Company Information
Report Number R-AL15-159-04
Director JA Cotton BSc (Eng) PhD (Mat Eng UCT), PrEng
Revision 03 Postal: Postnet Suite 78, Private Bag X11 Mowbray 7705, Cape Town
Physical: Building 23B, Unit 15, The Waverley Business Park, Kotzee Rd, Mowbray
Report Author Lisa Kumadiro
7700, Cape Town.
SOW Number SOW-AL15-156-03 (NG) Tel: +27 21 447 5258/4643 | Fax: +27 86 617 1047
Customer PO Number 819226 www.one-eighty-degrees.com
Reg No 2007/007050/07 | VAT No 4410261889
Technical Signatory Murendeni Munyai OE-MSP-02 SF61 Rev 03
Witnessed By N/A
Disclaimer
Sonwabile, Boitumelo, Declan, Lisa, Daniel,
Tested By Test results only relate to items tested. Test results apply to the sample as received.
Matthew
Samples will be kept for 1 month from this report date unless otherwise requested.
Customer Name Algoa Cabinda Fabrication Services LDA Opinions and interpretations expressed herein are outside the scope of SANAS
accreditation.
Customer Contact Details +244225001000

Customer Address Rua Nacional N100, Malembo, Cabinda, Angola Accreditation

Date of issue of the report 2024/08/26

WPQR Inspection Report

1. Identification of the item

Figure 1: Sample as Received (marked)

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Company Name Algoa Cabinda Fabrication Services LDA Welder's Name T

Welding Process 1 GTAW/SMAW Welding Process 2 GTAW/SMAW

Supporting WPS Number ACA-WPS-011-00 Weld Joint Type SINGLE V 60 DEGREE

Supporting PQR Number ACFS-PIP-SD-PQR-003-1 Position 5G

Base Metal 1 ASTM UNS 32750 / 60177 Base Metal 2 ASTM UNS 32750 / 60177
ER2594 / E2954-15 ER2594 / E2954-15
Filler Metal (GTAW) Filler Metal (SMAW)
SFA 5.9 / 5.4 SFA 5.9 / 5.4

Requirements as per (ASME IX & ASME VIII DIV.1)

Tensile Test results ☒ Pass ☐ Fail
Bend Test results ☒ Pass ☐ Fail
Impact Test results ☒ Pass ☐ Fail
Macro examination ☒ Pass ☐ Fail
Micro examination ☒ Pass ☐ Fail
Hardness test results ☒ Pass ☐ Fail
Corrosion Test ☒ Pass ☐ Fail
Ferrite count ☒ Pass ☐ Fail

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2. Results
2.1 Tensile Test
Table 1: Tensile Test Results

TENSILE TEST
Standard ASTM A370-24
Specimens Direction Width Thickness Area Gauge Yield Load RT0.2 Yield Max Load Rm UTS Elongation RIA Fracture
No. Trans. / Long. mm mm mm 2
mm kN MPa kN MPa % % Location
1 Longitudinal 13.05 8.28 108.05 50 71.52 662 88.67 821 26.46 64.85
Within gauge, PM
2 Longitudinal 13.16 8.10 106.60 50 69.15 649 87.86 824 30.58 60.58
550 min - 800 min
Requirements: ASTM A790 S32750
PASS - PASS

2.2 Bend Test

Table 2: Bend Test Results

180° BEND TEST

Standard ASME IX-23

Specimens Type Result Width Length Thickness
Comment
No. Face/Root/Side Pass/Fail mm mm mm
1 Face Pass 38 250 9
2 Face Pass 38 250 9
No cracks or inclusions greater than 3 mm
3 Root Pass 38 250 9
4 Root Pass 38 250 9
Bend Mandrel Diameter 40 mm

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Figure 2: Samples Post-Bending

2.3 Impact Test

Table 3: Charpy V-Notched Impact Test Results

CHARPY V-NOTCHED IMPACT TEST Size: 5 x 10 x 55 mm

Machine Used MTS Sans ZBC2302 300J Impact, 21210016 Calibration date 13/02/2024
Test Direction Transverse to Weld Standard ASTM E23-24
Temperature Impact Value (J)
Location Lateral Expansion (x0.001) Percent Shear Fracture
(°C) Individual Avg.
WM 28.27 28.88 30.28 29.14 0.54 0.43 0.43 0 0 10
FL -46 73.90 47.46 44.03 55.13 - 0.85 0.78 - 30 30
FL+2 80.65 88.84 87.51 85.67 - - - - - -
Note: Absorbed energy values > 240J must be reported as an approximation as 80% of the equipment capacity is exceeded (300J = 100%) acc. to ASTM E23.

OEMT does not fulfil the NIST requirements as per ASTM E23 A2.4.1.1. All Unbroken specimens (If any) are used in average calculation
27 min Average
Requirements (J)
20 min Sin

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2.4 Vicker’s Hardness Test

Table 4: Vicker’s Hardness Test Results

VICKERS HARDNESS
TH 720, S/N:
Machine Used Calibration Date 13/02/2024
107
Test Standard ASTM E384-22/E92
PM A HAZ A WM HAZ B PM B
CAP 264.49 264.79 267.64 274.33 265.46
MID 276.16 277.95 284.48
ROOT 263.34 258.77 207.09 260.59 272.08
Maximum Recorded Value 274.33 HV10
Maximum Requirements: 350 HV10

2.5 Macroscopic Examination

Figure 3: Hardness Locations Figure 4: Macroscopic Image of Weld Cross Section

Macroscopic examination of weld, sample etched with 40% NaOH (electrolytic) at 7V for 5 seconds as per client specification. As per the ASME IX
requirements, no flaw or crack should appear on the picture. Based on these requirements, the macroscopic image analysis on is a pass.

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2.6 ASTM E562 Ferrite Count and Ferrite Percentage

Table 5: ASTM E562 Ferrite Count Results

ASTM E562-20 FERRITE COUNT

Location Average (%) Readings Acceptance Criteria 30-65%
WM Cap 35.85 31.50, 35.00, 39.50, 43.00, 37.00, 43.50, 21.00, 36.00, 37.50, 34.50
WM Mid 39.45 43.50, 40.00, 36.00, 30.50, 46.50, 42.00, 36.00, 36.00, 42.50, 41.50
WM Root 34.35 41.50, 38.00, 29.00, 35.00, 34.00, 41.50, 34.50, 30.50, 31.50 28.00
Haz 1 Root 49.40 52.00, 51.00, 60.00, 44.00, 48.50, 55.00, 49.50, 37.00, 49.50, 47.50 PASS
Haz 2 Root 49.30 52.50, 46.50, 49.50, 66.00, 40.00, 53.50, 51.50, 55.00, 41.50, 37.00
PM 1 Mid 51.05 45.00, 46.50, 61.50, 47.00, 37.00, 48.50, 53.00, 49.00, 62.50, 60.50
PM 2 Mid 51.05 55.00, 54.00, 51.00, 42.50, 66.00, 38.00, 53.00, 49.50, 56.50, 45.00

2.7 Corrosion Testing

Table 6: ASTM G48 Corrosion Test Results

CORROSION RESISTANCE - ASTM G48-11 (2020) - Method A

Location of test sample: 6 O'clock
Nature of test sample (Surface Preparation): Grit 120
Sample size: 25x50xt
Passivation test: 15 min pickling and 24hr passivation
Test duration: 24 hours
Composition of corrosion solution: 6 % FeCl3 by mass
Test temperature: 40°C
Date of calibration for thermostatic bath: 10/5/2024
Surface Area (cm²) Initial Mass (g) Mass after 24h (g) Corrosion Rate (g/m²/day) Presence of pitting at 20x magnification
31.338 72.17938 72.17784 0.4914211 No pitting at a magnification of x20 after the test
Acceptance Criteria: 4 No pitting at a magnification of x20 after the test
Result: Pass Pass

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2.8 Microscopic Examinations according to ASTM 923-A @ 500x

Figure 5: Parent Metal 1 Figure 6: Parent Metal 2

Figure 7: HAZ 1 Figure 8: HAZ 2

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Figure 9: WM CAP Figure 10: WM MID Figure 11: WM ROOT

All regions are unaffected. The ferrite has been etched without revelation of intermetallic phase. The interphase boundaries are smooth.

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3. Appendices
3.1 Sample, Testing, and Client Information

Sample Information
Date received 2024/06/05
Sampling method As per SOP OE-TSP-03 SOP21
Testing Information
Date Testing Commenced: 2024/07/08
Room Temperature before Test commences: 22.8
Location of Testing: (Including any subcontracting work location) OEMT
Deviations, Additions, or Exclusions from the Test Method, if any: N/A
Customer Data or Deviations Requested, if applicable: N/A
Statement of Conformity Requests or Deviations, and Decision Rules, if applicable: N/A
Measurement of uncertainty Available on request.
Note: The machining of samples is carried out by an approved subcontractor.

3.2 Revision History

Rev. Date Reason for the Revision Affected Pages Originator

Addition of Charpy V-Notched Impact
02 2024/08/26 6 Lisa Kumadiro
Test Requirements
Addition of Hardness Values and Mid
03 2024/08/12 6 Matthew Sassman
Hardness Locations

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3.3 Test Specifications

One Eighty Materials Testing (Pty) Ltd is SANAS 17025 accredited for the test methods indicated below. Mechanical testing that falls under the SANAS accreditation has been
approved by Bureau Veritas.

☒ OE-TSP-03 TM01 Tensile Test Metals

☒ OE-TSP-03 TM03 Impact Test Metals

☒ OE-TSP-03 TM05 Vickers Hardness Test

☐ OE-TSP-03 TM06 Spectrographic Analysis

☒ OE-TSP-03 TM08 Microstructural Analysis

☒ OE-TSP-03 TM011 Bend Test

☐ OE-TSP-03 TM19 Portable Hardness Test

☒ OE-TSP-03 TM13 Ferrite Count and Ferrite Percentage

☐ OE-TSP-03 SOP 13 Micro Examination Determination of microstructure in the field

☐ OE-TSP-03 TM15 Determination of Resistance to Intergranular Corrosion of Duplex Stainless Steels

☒ OE-TSP-03 TM16 Intermetallic Phase Detection

☐ OE-TSP-03 TM18 Detection of Susceptibility of Austenitic Stainless Steels to Intergranular Corrosion

☒ OE-TSP-03 TM22- ASTM G48 Corrosion Testing

☒ OE-TSP-03 TM24 Macro Examination Determination of Weld Defects and Fillet Weld Size

☐ OE-TSP-03 TM26- PMI (Handheld XRF) X-MET 8000

☐ OE-TSP-03 TM27- ASTM G28 Corrosion Testing

Non-accredited tests: None
Subcontracted work: None

Note on subcontracted work: A portion of this test has been outsourced to an approved and accredited subcontractor as per section 0E-MSP04 SF07 and OE- MSP SF01 of the
quality management system.

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Page 2 / 2
Certificate number: SMS.LAB.320/103910/02/B.0
THE SCHEDULE OF RECOGNITION
1. RANGE OF THE RECOGNITION
Type of test Test standard Test witnessing requirements
☒ Bend Test ASME IX, AWS D1 ASTM A370, ABS Rules and BS EN ISO Tests to be witnessed -as practicable at each periodical audit
☐ Chemical Analysis ASTM E415 and A751 Tests to be witnessed -as practicable at each periodical audit
☐ Chemical Analysis using X-MET 8000 ASTM A 751 and ASTM E1085 Tests to be witnessed -as practicable at each periodical audit
☒ Corrosion Test ISO 3651-2 & ASTM A262C & ASTM G48 & ASTM A923C Tests to be witnessed -as practicable at each periodical audit
☒ Hardness Testing ASTM E384 & ASTM E140 Tests to be witnessed -as practicable at each periodical audit
☒ Impact Testing ASTM E23, ISO 148-1 Tests to be witnessed -as practicable at each periodical audit
☒ Macro Examination ASTM E340, ISO 5817 Tests to be witnessed -as practicable at each periodical audit
☒ Micro Examination ASTM E1351 Tests to be witnessed -as practicable at each periodical audit
☒ Microstructural Analysis ASTM E3 & ASTM E562 and ASTM E1245 Tests to be witnessed -as practicable at each periodical audit
☐ Portable Hardness Test ASTM A956 and ASTM E110 Tests to be witnessed -as practicable at each periodical audit
☒ Tensile Testing ASTM E8, BS EN ISO 6892-1 BS EN ISO 10002-1 and ASTM A370 Tests to be witnessed -as practicable at each periodical audit

2. LIMITATIONS

Bureau Veritas Marine & Offshore is to be informed immediately of any modification to testing facilities and associated quality procedures in order to agree on appropriate
actions.

ONE EIGHTY MATERIALS TESTING (PTY) LTD. has to carry out and report the tests in compliance with the relevant testing standard(s) and has to make the necessary
arrangements to comply with the witnessing requirements agreed with Bureau Veritas Marine & Offshore.

ONE EIGHTY MATERIALS TESTING (PTY) LTD. has to apply for the periodical audits as agreed with Bureau Veritas Marine & Offshore.

3. REMARKS
Nil.
*** END OF CERTIFICATE ***

Document: R-AL15-159-04 rev 03 Page 13 of 13 2024/08/26

ACFS-PIP-SD-PQR-003-1 Algoa Cabinda Fabrication Services LDA
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 1 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

TTI - TUBACEX TUBOS INOXIDABLES

Registro Mercantil de Alava, Tomo 587, Folio 189, Hoja VI 2885 - N.I.F. A-01140227
Tres cruces, 8 TL: 946721350
01400 Llodio (Alava) FAX: 946725062
SPAIN E-MAIL:

CUSTOMER DESCRIPTION/DESCRIPCIÓN DEL CLIENTE/KUNDENBEZEICHNUNG/COMMETTANT

CLIENT SOLD TO/SOLICITANTE/AUFTRAGGEBER/COMMETTANT
TSS SOLD TO:WITTE TUBE & PIPE SYSTEMS GMBH
TUBACEX SERVICE SOLUTIONS, S.A.U SOLD P.O. REF.:EB0008835
POLIGONO INDUSTRIAL SARATXO SOLD ORDER REF.:388105
01470 AMURRIO COPY NUMBER: 001

CLIENT ORDER/PEDIDO CLIENTE/KUNDEN AUFTRAGSNUMMER/NO.DE COMMANDE: I010988

SALES ORDER/PEDIDO VENTAS/AUFTRAGSNUMMER/NO.DE COMMANDE D'USINE:

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 2 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

MATERIAL:SEAML. STAINL. STEEL TUBES/PIPES/TUBOS INOXIDABLES SIN SOLDADURA/TUBES INOX SANS SOUDURE/NAHTLOSE
EDELSTAHLROHRE
HEAT-TREATED, PICKLED / TRATADO, DECAPADO / HYPERTREMPE, DECAPE / WÄRMEBEHANDELT, GEBEIZT, PASSIVATED AS PER
ASTM A380 / PASIVADO SEGUN ASTM A380 / PASSIVÉ (ASTM A380) / PASSIVIERT (ASTM A380)
GRADE / ACERO / GRADE / WERKSTOFF: S32750,1.4410,
STANDARD / NORMA / STANDARD / LIEFERUNG NACH: ASME SECT.II PART.A SA790/SA790M-2021 ED.
ASTM A790/A790M-22
EN 10216-5:2021 TC2
EN 10297-2:2005
NORSOK M650 QTR. 4
NORSOK M630:2020 MDS D51 REV.6
CHECK ANALYSIS
CORROSION TESTED ACC. TO ASTM A262 PRACTICE E
CORROSION TESTED ACC. TO ASTM A923-22 TEST METHOD C
CORROSION TESTED ACC. TO ASTM G48 TEST METHOD A
CORROSION TESTED ACC. TO EN ISO 3651-2 PRACTICE B
SHELL ES/247 REV.2 EXCEPT DPI (TABLE 1) AND SURFACE REQUIREMENTS (POINT
9.1)
HYDROTEST
ANSI/NACE MR0103/ISO 17945:2015
ANSI/NACE MR0175/ISO15156-3:2015
QAD 68 REV.0
RTX_D51S REV.6
SHELL MESC SPE 74/014 FEBRUARY 2021 EXCEPT:
NO LIQUID PENETRANT TEST (POINT 14.12.1),
TENSILE TEST ONLY IN LONGITUDINAL DIRECTION.
ULTRASONIC TEST ONLY FOR LONGITUDINAL DEFECTS.
IMPACT TEST (if applicable): Lateral expansion 0.38 mm. minimum.
ULTRASONIC TEST ACC. TO ASTM A999/A999M / ASTM E213
TOLERANCES / TOLERANCIAS / TOLERANCES / TOLERANZEN NACH: ASME SECT.II PART.A SA999/SA999M-2021 ED.
ASTM A999/A999M-18
EN ISO 1127/03.2019 D2/T2
RANDOM LENGTHS / LARGOS VARIABLES / LONGUEUR COURANTE / EINGEENGTE LÄNGE 6.000/7.000 MM
PLAIN ENDS / LISOS / EXTRÉMITÉ D'EQUERRE / GLATTE ENDEN,
DIMENSIONS/DIMENSIONES/DIMENSIONS/DIMENSIONS: 219,08 X 8,18 MM - 8" SCH 40S
HOT FINISHED/ACABADOS EN CALIENTE/WARMGEFORMT/FINIS A CHAUD

Sales Item Client Item Delivery No Lot No. Heat No Pieces Weight Tot Lgth Un Lgth
Pos Ped. Pos Clnt Nº Entrega Nº lote Colada Piezas Peso Long. Tot Long. Un
AuftrgPos Kunde Pos Lieferung Los Nr. Schmelze Stück Gewicht Gesamtlänge Längentyp
Usine Pos Com. Pos Avis. d'exp Lot d`inspection Coulée Pcs Poids Tolength Long. Un
60 8110077955 P2303407 60177 4 1.147 KG 26,30 M 6000-7000 MM

RAW MATERIAL/DATOS MATERIAL/VORMATERIAL/MATIERE PREMIERE

Heat Nr: Supplier Method
60177 ACERALAVA (SPAIN) Electric furnace+AOD

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 3 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

CHEMICAL COMPOSITION (%)/COMPOSICIÓN QUÍMICA (%)/CHEMISCHE ZUSAMMENSETZUNG (%)/COMPOSITION CHIMIQUE(%)

*L: Ladle C:Products
* Heat Seq C Mn Si P S Ni Cr Mo Al Cu
L 60177 1 0,010 0,68 0,310 0,026 0,0004 6,70 25,60 3,64 0,011 0,14
C 60177 2 0,010 0,68 0,330 0,027 0,0004 6,66 25,42 3,66 0,010 0,14
C 60177 3 0,010 0,69 0,310 0,026 0,0004 6,66 25,49 3,65 0,010 0,14

* Heat Seq V Nb W Co N Pren

L 60177 1 0,071 0,004 0,040 0,085 0,2795 42,0840
C 60177 2 0,070 0,003 0,042 0,087 0,2795 41,9700
C 60177 3 0,070 0,003 0,042 0,087 0,2795 42,0070

HEAT TREATMENT/TRATAMIENTO TÉRMICO/WÄRMEBEHANDLUNG/TRAITEMENT THERMIQUE

HIPERTEMPLADOS A 1100 °C , ENFRIADO DIRECTO AL AGUA
SOLUTION ANNEALED AT 1100 °C , Direct water quenched
HYPERTREMPES 1100 °C , REFROIDISSEMENT À L#EAU P
LOESUNGSGEGLUEHT 1100 °C , Direkt in Wasser abgeschr

TENSILE TEST/TEST DE TENSIÓN/ESSAI TRACTION/ZUGVERSUCH

Lot No. Sample T Rp0.2 Rp1.0 Rm A2" A5 Type Spc.Type Spc.Dim
°C MPa MPa MPa % % mm
P2303407 1 20 603 663 804 40 36 L S 20,15
2 20 605 675 802 41 39 L S 20,09
3 20 579 664 804 40 38 L S 20,13

IMPACT TEST/TEST DE IMPACTO/RESILIENCE/KERBSCHLAGVERSUCH

Lot No. Sample T Wspec Ecv 1 Ecv 2 Ecv 3 Ecv AVG Type Le1 Le2 Le3 Shear 1 Shear 2 Shear 3
°C mm J J J J mm mm mm % % %
P2303407 1 -51 7,50 226 214 216 218 L 2,53 2,44 2,49 80 70 70

CORROSION ACCORDING TO ASTM A923 C/CORROSION DE ACUERDO ASTM A923 C/CORROSION SUIVANT ASTM A923 C/CORROSION
ACCORDING TO ASTM A923 C
Lot No. Sample T Pits-20x Wloss time
°C MDD Horas
P2303407 1 50 N 5,8320 24,0

Corrosion test ASTM G48 practice A/Corrosión ASTM G48 práctica A/TEST DE CORROSION ASTM G48 practice A/LOCHFRASSTEST ASTM G 48
PR.A
Lot No. Sample T Pits-20x W.loss time
°C g/m2 Horas
P2303407 1 50 N 0,5832 24,0

HARDNESS TEST/TEST DE DUREZA/DUREE/HÄRTEPRÜFUNG

Lot No. Sample 0ºExt1 0ºExt2 0ºExt3 0ºInt1 0ºInt2 0ºInt3 90ºExt1 90ºExt2 90ºExt3 90ºInt1 90ºInt2 90ºInt3 180ºExt1
HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC
P2303407 1 20,2 20,6 21,6 21,3 21,3 21,4 20,1 21,8 18,0 20,9 20,3 21,1 18,0
Lot No. Sample 180ºExt 180ºExt3 180ºInt1 180ºInt2 180ºInt3 270ºExt1 270ºExt2 270ºExt3 270ºInt1 270ºInt2 270ºInt3
2
HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC
P2303407 1 20,4 21,0 21,5 21,3 22,3 21,1 21,6 22,6 23,0 23,9 23,9

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 4 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

FERRITE ACCORDING TO ASTM E 562/Contenido de Ferrita según ASTM E562/FERRITE SUIVANT ASTM E562/FERRIT ENTSPRECHEND
ASTM E562
Lot No. Sample %Fer Dev.Ferr
% %
P2303407 1 44,60 8,90

METALURGICAL TESTS/ENSAYOS METALÚRGICOS/METALLURGISCHE PRÜFUNGEN/ESSAIS

METALLURGIQUES
ETCH STRUCTURE ACC. ASTM A923 MET.A: UNAFFECTED STRUCTURE. MATERIAL FREE
FROM INTERMETALLIC PHASES AND PRECIPITATES. UNIFORM STRUCTURE ACROSS
FULL WALL THICKNESS
EXAMEN DE MICROESTRUCUTRA DE ACUERDO A ASTM A923 MET.A: ESTRUCTURA NO
AFECTADA. MATERIAL LIBRE DE FASES INTERMETALICAS Y PRECIPITADOS.
ESTRUCTURA UNIFORME A TRAVES DEL ESPESOR.
ETCH STRUCTURE ACC. ASTM A923 MET.A: UNAFFECTED STRUCTURE. MATERIAL FREE
FROM INTERMETALLIC PHASES AND PRECIPITATES. UNIFORM STRUCTURE ACROSS
FULL WALL THICKNESS

INTERGRANULAR CORROSION TEST ACC. TO ASTM A262 PRACT."E": SATISFACTORY

ENSAYO DE CORROSION INTERGRANULAR DE ACUERDO A ASTM A262 PRACT.E:
SATISFACTORIO
BESTÄNDIGKEIT GEGEN INTERKRISTALLINE KORROSION ENTSPRECHEND ASTM A262
PRACT.E: IN ORDNUNG
ESSAI DE CORR. INTERGR. SELON ASTM A262 PRACT.E:SATISFAISANT
INTERGRANULAR CORROSION TEST ACC.TO DIN EN ISO 3651-2 MET.B:
SATISFACTORY
ENSAYO DE CORROSION INTERGRANULAR DE ACUERDO A ISO 3651-2 MET.B:
SATISFACTORIO
BESTÄNDIGKEIT GEGEN INTERKRISTALLINE KORROSION ENTSPRECHEND ISO 3651-2
MET."B": IN ORDNUNG
ESSAI DE CORR. INTERGR. SELON ASTM ISO 3651-2 MET."B":SATISFAISANT

NON-DESTRUCTIVE TESTS/ENSAYOS NO DESTRUCTIVOS/ZERSTÖRUNGSFREIE

PRÜFUNGEN/ESSAIS NON DESTRUCTIFS
FERRITE CONTENT DETERMINED BY FISCHER FERRITOSCOPE TO 100% OF PRODUCTS
CONTENIDO EN FERRITA MEDIDO CON FERRITOSCOPIO SOBRE EL 100% DEL
MATERIAL.
Ferritescope-Test auf 100% des Materials.

100% ULTRASONIC TEST ACC. TO ASTM A999 / E213: SATISFACTORY

100% ENSAYO DE ULTRASONIDOS DE ACUERDO A ASTM A999 / E213: SATISFACTORIO
100% ULTRASCHALLPRÜFUNG NACH ASTM A999 / E.213:IN ORDNUNG
100% ESSAI D´ULTRASON D'ACCORD A ASTM A999 / E.213: SATISFAISANTE

100% ULTRASONIC TEST ACC. TO EN 10246-7, U2C: SATISFACTORY

100% ENSAYO DE ULTRASONIDOS DE ACUERDO A EN 10246-7, U2C: SATISFACTORIO
100% ULTRASCHALLPRÜFUNG NACH EN 10246-7, U2C:

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 5 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

IN ORDNUNG
100% ESSAI D´ULTRASON D'ACCORD A EN 10246-7, U2C: SATISFAISANTE
POSITIVE MATERIAL IDENTIFICATION TEST ON EACH TUBE/PIPE BY
"X-RAY-FLUORESCENCE-ANALYZER": SATISFACTORY
VERIFICACION DEL GRADO DE ACERO EN CADA TUBO MEDIANTE "ANALIZADOR DE
FLUORESCENCIA DE RAYOS X": SATISFACTORIO
VERWECHSLUNGSPRUEFUNG AN JEDEM ROHR MIT
"RÖNTGEN-FLUORESZENZ-ANALYSATOR": IN ORDNUNG
VERIFICATION DE LA NUANCE SUR CHAQUE TUBE PAR
"X-RAY-FLUORESCENCE-ANALYZER": SATISFAISANT

HYDROSTATIC PRESSURE TESTED AT 168 bar, 2400 PSI DURING 5 SEC ON EACH
TUBE/PIPE: SATISFACTORY
ENSAYO HIDROSTÁTICO A 168 bar, 2400 PSI DURANTE 5 SEC EN CADA TUBO:
SATISFACTORIO
WASSERDRUCKPRÜFUNG BEI 168 bar, 2400 PSI HALTEZEIT 5 SEC JE ROHR: IN
ORDNUNG
ESSAI DE PRESSION HYDROSTATIQUE À 168 bar, 2400 PSI PENDANT 5 SEC SUR
CHAQUE TUBE: SATISFAISANT

DIMENSIONAL CHECKING ON EACH TUBE: SATISFACTORY

INSPECCION DIMENSIONAL AL 100% DE LOS TUBOS SATISFACTORIA
100% MASSKONTROLLE: O.B.
VERIFICATION DIMENTIONNELLE AU 100% DES TUBES, SATISFAISANTE

VISUAL INSPECTION ON EACH TUBE: SATISFACTORY

INSPECCION VISUAL AL 100% DE LOS TUBOS, SATISFACTORIA
100% BESIGCHTIGUNG: O.B.
EXAMEN VISUEL AU 100% DES TUBES, SATISFAISANT

TECHNOLOGICAL TESTS/ENSAYOS TECNOLÓGICOS/TECHNOLOGISCHE

PRÜFUNGEN/TECHNOLOGICAL TESTS

FLATTENING TEST: SATISFACTORY

APLASTADO S.NORMA: SATISFACTORIO
RINGFALTVERSUCH: IN ORDNUNG
ESSAI D'APLATISSEMENT: SATISFAISANT

RING TENSILE TEST: SATISFACTORY

TRACCION DE ANILLO: SATISFACTORIO

RINGZUGVERSUCH: IN ORDNUNG
ESSAI DE TRACTION A L'ANNEAU: SATISFAISANT

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 6 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

MARKING/ETIQUETADO/KENNZEICHNUNG/MARKSTEXT
TX2 TX1 TUBACEX 219,08 X 8,18 MM - 8" SCH 40S ASME SA790 ASTM A790 EN 10216-5 TC2 EN 10297-2 S32750 1.4410
HFD HF SMLS HEAT/ PMI-AV LOT NO/MADE IN SPAIN

REMARKS/OBSERVACIONES/ANMERKUNG/REMARQUES

NO MERCURY, MERCURY COMPOUNDS OR MERCURY BEARING INSTRUMENTS AND/OR EQUIPMENT HAVE BEEN USED ALONG
MANUFACTURING AND INSPECTION PROCESS.
DURANTE LOS PROCESOS DE FABRICACIÓN E INSPECCIÓN NO SE HA USADO MERCURIO NI INSTRUMENTOS Y/O EQUIPOS
CONTENIENDO MERCURIO O CON COMPONENTES DE MERCURIO.
KEINE QUEKSILBER, BZW. QUECKSILBERVERUNREINIGTES KOMPONENTEN ODER KUGELLAGERINSTRUMENTE UND/ODER GERÄTE SIND
BENUTZT WORDEN PRODUKTIONS UND BESICHTIGUNGSPROZESS.
IL N'A PAS ÉTÉ FAIT USAGE DE MERCURE, DE COMPOSÉS CONTENANT DU MERCURE OU DE MATÉRIAUX ET/OU D'INSTRUMENT
CONTENANT DU MERCURE TOUT AU LONG DES ÉTAPES DE FABRICATION ET DU PROCESSUS D'INSPECTION ET DE CONTRÔLE.

NO WELDING OR WELD REPAIRS WERE MADE

SIN REPARACION POR SOLDADURA
KEINE SCHWEISSBEARBEITUNG WURDE VORGENOMMEN
SANS RÉPARATION AVEC SOUDURE
MATERIAL MANUFACTURER APPROVED BY TÜV SÜD Industrie Service GmbH
(NOTIFIED BODY 036)TO ISSUE CERTIFICATES OF SPECIFIC PRODUCT CONTROL IN
ACCORDING TO PRESSURE EQUIPMENT DIRECTIVE 2014/68/EU ANNEX 1 POINT 4.3.
FABRICANTE DE MATERIALES APROBADO POR TÜV SÜD Industrie Service GmbH (ORGANISMO NOTIFICADO 0036) PARA LA
EMISION DE CERTIFICADOS ESPECIFICOS DE CONTROL DE PRODUCTO DE ACUERDO AL ANEXO 1, PUNTO 4.3 DE LA DIRECTIVADE
EQUIPOS A PRESION 2014/68/EU.
WERKSTOFFHERSTELLER MIT BERECHTIUNG ZUR AUSSTELLUNG VON BESCHEINIGUNGEN ÜBER SPEZIFISCHE PRÜFUNGEN AN DEN
WERKSTOFFEN IM GELTUNGSBEREICH DER ZERTIFIZIERUNG UND IN ÜBEREINSTINSTIMMUNG MIT DER DRUCKGERÄTERICHTLINIE
2014/68/EU UND DEN ZUGRUNDE LIEGENDEN SPEZIFIKATIONEN ENTSPR. DER BENANNTEN STELLE NR.0036, TÜV SÜD Industrie
Service GmbH
PRODUCTEUR DU MATERIEL APPROUVE PAR TÜV SÜD Industrie Service GmbH N.B. 0036) POUR EMISSION DES CERTIFICATS
SPECIFIQUE DE CONTROLE DE PRODUIT SELON LA DIRECTIVE DES EQUIPES A PRESION 2014/68/EU ANNEXE 1 POINT 4.3.

MATERIAL CHARACTERISTICS COMPLY WITH POINT 7.5 OF ANNEX I TO PED BY HAVING AN ELONGATION AFTER RUPTURE AT
TENSILE TEST NO LESS THAN 14% AND A BENDING RUPTURE ENERGY AT IMPACT TEST NO LESS THAN 27J AT 20ºC.
LAS CARACTERISTICAS DEL MATERIAL CUMPLEN CON LOS REQUISITOS DEL PUNTO 7.5 DE LA DIRECTIVA PED POR TENER UN
ALARGAMIENTO TRAS ROTURA EN EL ENSAYO DE TRACCION NO INFERIOR AL 14% Y PO DE TRACCION NO INFERIOR AL 14% Y POR
TENER UNA RESISTENCIA AL IMPACTO NO INFERIOR A 27 J A 20º C.
DIE WERKSTOFF-WERTE ENTSPRECHEN PUNKT 7.5. DER DGRL, ANHANG 1, MIT EINERBRUCHDEHNUNG = 14% IM NORMGEMÄSS
DURCHGEFÜHRTEN ZUGVERSUCH UND DER KERBSCHLAGARBEIT = 27J AN EINER ISO - v PRO PROBE BEI EINER TEMPERATUR VON
HÖCHSTENS 20ºC
LES CARACTERISTIQUES DU MATERIEL, AYANT UN ALLONGEMENT APRES RUPTURE A L'ESSAI DE TRACTION NON INFERIEUR DU
14% ET UNE RESISTENCE A LA FLEXION PAR CHOC A 20ºC NON INFERIEUR A 27J, SONT CONFORMES AUX PRESCIPTIONS DU
PONT 7.5 DE L'ANNEXE I DE PED.

MATERIAL IS FREE OF RADIATION CONTAMINATION

EL MATERIAL ESTA LIBRE DE CONTAMINACION POR RADIACIONES
MATERIAL IS FREI VON RADIOAKTIVITÄT
MATÉRIEL LIBRE DE POLUTION RADIOACTIVE

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 MTC / Certificate
STRUCTURE EXAMINATION 745903

MATERIAL IDENTIFICATION / IDENTIFICACIÓN DEL MATERIAL

Lot No. / Num Lote P2303407 Dimension / Dimensión 219,08 x 8,18 mm - 8'SCH 40

Heat / Colada 60177 Grado de acero / Steel grade S32750

Type Of test / Tipo de Ensayo: MICROSTRUCTURE EVALUATION

RESULTS / RESULTADO

Result: The microestructure is formed by austenite and ferrite. The presence of intermetallic phases or precipitates is not observed. Uniform structure
across full wall thickness Etching method according to ASTM E-407.

Resultado: la microestructura está compuesta por austenita y ferrita. No se observa la presencia de fases intermetálicas y precipitados. Estructura uniforme a
través de todo el espesor. Método de ataque según ASTM E-407.

GRAPHICS RECORDS / REGISTROS FOTOGRÁFICOS:

Dir: LONGITUDINAL / MAG: 500X / Dir: TRANSVERSAL / MAG: 500X /

María Cano
Responsable del Laboratorio
Laboratory Manager
 INSPECTION CERTIFICATE (3.1) - Chemical analysis
TEST REPORT (2.2) - Mechanical properties

Issued Date: 2024-04-18 Certificate number: EC27495675 rev. 0

Our order: 0100931309 Your order:

Our reference: Your reference:
Customer number: NLB00168 Your fax number:
Customer order date: Your e-mail:

Invoice address Receiver of certificate Delivery address

EUROWELD B.V.

DELIVERY Lot number: SBX1910834 Quantity:

PRODUCT CHEMICAL ANALYSIS

Brand: ESAB Actual results: acc to EN 10204 - 3.1
Description: OK 68.55 2.5x300mm 1/4 VP
Item number: 68552520L0 All weld metal
C 0.02%
Si 0.6%
Mn 0.8%
P 0.021%
S 0.004%
Cr 25.7%
CLASSIFICATIONS
Ni 9.6%
EN ISO 3581-A: E 25 9 4 N L B 4 2 Mo 4.0%
SFA/AWS A5.4: E2594-15 Cu 0.10%
Werkstoffnummer: (1.4410) N 0.24%

MECHANICAL PROPERTIES
Typical data: acc to EN 10204 – 2.2
A4, A5 = Elongation
Tensile ReH = Upper Yield Point
ReL = Lower Yield Point
Rp0.2 [MPa/ksi] Rm [MPa/ksi] A5 [%]
Rm = Ultimate Tensile Strength (UTS)
700/102 900/131 28 Rp0.2 = Yield Strength 0.2 offset
Rp1.0 = Yield Strength 1.0 offset
Impact
Temp [°C/°F] KV[J/ft-lb]
-60/-76 45/33

COMMENTS

Product supplied under a QA Programme fulfilling the EN ISO 9001 standard.

This certificate is produced electronically.
Please refer any queries to:
Esab Nederland BV - P.O. Box 2236 , 3800 CE Amersfoort , Nederland

Validation
Ellen Bjorgan Quality Manager Tapio Huhtala Product Manager
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 1 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

TTI - TUBACEX TUBOS INOXIDABLES

Registro Mercantil de Alava, Tomo 587, Folio 189, Hoja VI 2885 - N.I.F. A-01140227
Tres cruces, 8 TL: 946721350
01400 Llodio (Alava) FAX: 946725062
SPAIN E-MAIL:

CUSTOMER DESCRIPTION/DESCRIPCIÓN DEL CLIENTE/KUNDENBEZEICHNUNG/COMMETTANT

CLIENT SOLD TO/SOLICITANTE/AUFTRAGGEBER/COMMETTANT
TSS SOLD TO:WITTE TUBE & PIPE SYSTEMS GMBH
TUBACEX SERVICE SOLUTIONS, S.A.U SOLD P.O. REF.:EB0008835
POLIGONO INDUSTRIAL SARATXO SOLD ORDER REF.:388105
01470 AMURRIO COPY NUMBER: 001

CLIENT ORDER/PEDIDO CLIENTE/KUNDEN AUFTRAGSNUMMER/NO.DE COMMANDE: I010988

SALES ORDER/PEDIDO VENTAS/AUFTRAGSNUMMER/NO.DE COMMANDE D'USINE:

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 2 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

MATERIAL:SEAML. STAINL. STEEL TUBES/PIPES/TUBOS INOXIDABLES SIN SOLDADURA/TUBES INOX SANS SOUDURE/NAHTLOSE
EDELSTAHLROHRE
HEAT-TREATED, PICKLED / TRATADO, DECAPADO / HYPERTREMPE, DECAPE / WÄRMEBEHANDELT, GEBEIZT, PASSIVATED AS PER
ASTM A380 / PASIVADO SEGUN ASTM A380 / PASSIVÉ (ASTM A380) / PASSIVIERT (ASTM A380)
GRADE / ACERO / GRADE / WERKSTOFF: S32750,1.4410,
STANDARD / NORMA / STANDARD / LIEFERUNG NACH: ASME SECT.II PART.A SA790/SA790M-2021 ED.
ASTM A790/A790M-22
EN 10216-5:2021 TC2
EN 10297-2:2005
NORSOK M650 QTR. 4
NORSOK M630:2020 MDS D51 REV.6
CHECK ANALYSIS
CORROSION TESTED ACC. TO ASTM A262 PRACTICE E
CORROSION TESTED ACC. TO ASTM A923-22 TEST METHOD C
CORROSION TESTED ACC. TO ASTM G48 TEST METHOD A
CORROSION TESTED ACC. TO EN ISO 3651-2 PRACTICE B
SHELL ES/247 REV.2 EXCEPT DPI (TABLE 1) AND SURFACE REQUIREMENTS (POINT
9.1)
HYDROTEST
ANSI/NACE MR0103/ISO 17945:2015
ANSI/NACE MR0175/ISO15156-3:2015
QAD 68 REV.0
RTX_D51S REV.6
SHELL MESC SPE 74/014 FEBRUARY 2021 EXCEPT:
NO LIQUID PENETRANT TEST (POINT 14.12.1),
TENSILE TEST ONLY IN LONGITUDINAL DIRECTION.
ULTRASONIC TEST ONLY FOR LONGITUDINAL DEFECTS.
IMPACT TEST (if applicable): Lateral expansion 0.38 mm. minimum.
ULTRASONIC TEST ACC. TO ASTM A999/A999M / ASTM E213
TOLERANCES / TOLERANCIAS / TOLERANCES / TOLERANZEN NACH: ASME SECT.II PART.A SA999/SA999M-2021 ED.
ASTM A999/A999M-18
EN ISO 1127/03.2019 D2/T2
RANDOM LENGTHS / LARGOS VARIABLES / LONGUEUR COURANTE / EINGEENGTE LÄNGE 6.000/7.000 MM
PLAIN ENDS / LISOS / EXTRÉMITÉ D'EQUERRE / GLATTE ENDEN,
DIMENSIONS/DIMENSIONES/DIMENSIONS/DIMENSIONS: 219,08 X 8,18 MM - 8" SCH 40S
HOT FINISHED/ACABADOS EN CALIENTE/WARMGEFORMT/FINIS A CHAUD

Sales Item Client Item Delivery No Lot No. Heat No Pieces Weight Tot Lgth Un Lgth
Pos Ped. Pos Clnt Nº Entrega Nº lote Colada Piezas Peso Long. Tot Long. Un
AuftrgPos Kunde Pos Lieferung Los Nr. Schmelze Stück Gewicht Gesamtlänge Längentyp
Usine Pos Com. Pos Avis. d'exp Lot d`inspection Coulée Pcs Poids Tolength Long. Un
60 8110077955 P2303407 60177 4 1.147 KG 26,30 M 6000-7000 MM

RAW MATERIAL/DATOS MATERIAL/VORMATERIAL/MATIERE PREMIERE

Heat Nr: Supplier Method
60177 ACERALAVA (SPAIN) Electric furnace+AOD

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 3 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

CHEMICAL COMPOSITION (%)/COMPOSICIÓN QUÍMICA (%)/CHEMISCHE ZUSAMMENSETZUNG (%)/COMPOSITION CHIMIQUE(%)

*L: Ladle C:Products
* Heat Seq C Mn Si P S Ni Cr Mo Al Cu
L 60177 1 0,010 0,68 0,310 0,026 0,0004 6,70 25,60 3,64 0,011 0,14
C 60177 2 0,010 0,68 0,330 0,027 0,0004 6,66 25,42 3,66 0,010 0,14
C 60177 3 0,010 0,69 0,310 0,026 0,0004 6,66 25,49 3,65 0,010 0,14

* Heat Seq V Nb W Co N Pren

L 60177 1 0,071 0,004 0,040 0,085 0,2795 42,0840
C 60177 2 0,070 0,003 0,042 0,087 0,2795 41,9700
C 60177 3 0,070 0,003 0,042 0,087 0,2795 42,0070

HEAT TREATMENT/TRATAMIENTO TÉRMICO/WÄRMEBEHANDLUNG/TRAITEMENT THERMIQUE

HIPERTEMPLADOS A 1100 °C , ENFRIADO DIRECTO AL AGUA
SOLUTION ANNEALED AT 1100 °C , Direct water quenched
HYPERTREMPES 1100 °C , REFROIDISSEMENT À L#EAU P
LOESUNGSGEGLUEHT 1100 °C , Direkt in Wasser abgeschr

TENSILE TEST/TEST DE TENSIÓN/ESSAI TRACTION/ZUGVERSUCH

Lot No. Sample T Rp0.2 Rp1.0 Rm A2" A5 Type Spc.Type Spc.Dim
°C MPa MPa MPa % % mm
P2303407 1 20 603 663 804 40 36 L S 20,15
2 20 605 675 802 41 39 L S 20,09
3 20 579 664 804 40 38 L S 20,13

IMPACT TEST/TEST DE IMPACTO/RESILIENCE/KERBSCHLAGVERSUCH

Lot No. Sample T Wspec Ecv 1 Ecv 2 Ecv 3 Ecv AVG Type Le1 Le2 Le3 Shear 1 Shear 2 Shear 3
°C mm J J J J mm mm mm % % %
P2303407 1 -51 7,50 226 214 216 218 L 2,53 2,44 2,49 80 70 70

CORROSION ACCORDING TO ASTM A923 C/CORROSION DE ACUERDO ASTM A923 C/CORROSION SUIVANT ASTM A923 C/CORROSION
ACCORDING TO ASTM A923 C
Lot No. Sample T Pits-20x Wloss time
°C MDD Horas
P2303407 1 50 N 5,8320 24,0

Corrosion test ASTM G48 practice A/Corrosión ASTM G48 práctica A/TEST DE CORROSION ASTM G48 practice A/LOCHFRASSTEST ASTM G 48
PR.A
Lot No. Sample T Pits-20x W.loss time
°C g/m2 Horas
P2303407 1 50 N 0,5832 24,0

HARDNESS TEST/TEST DE DUREZA/DUREE/HÄRTEPRÜFUNG

Lot No. Sample 0ºExt1 0ºExt2 0ºExt3 0ºInt1 0ºInt2 0ºInt3 90ºExt1 90ºExt2 90ºExt3 90ºInt1 90ºInt2 90ºInt3 180ºExt1
HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC
P2303407 1 20,2 20,6 21,6 21,3 21,3 21,4 20,1 21,8 18,0 20,9 20,3 21,1 18,0
Lot No. Sample 180ºExt 180ºExt3 180ºInt1 180ºInt2 180ºInt3 270ºExt1 270ºExt2 270ºExt3 270ºInt1 270ºInt2 270ºInt3
2
HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC HRC
P2303407 1 20,4 21,0 21,5 21,3 22,3 21,1 21,6 22,6 23,0 23,9 23,9

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 4 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

FERRITE ACCORDING TO ASTM E 562/Contenido de Ferrita según ASTM E562/FERRITE SUIVANT ASTM E562/FERRIT ENTSPRECHEND
ASTM E562
Lot No. Sample %Fer Dev.Ferr
% %
P2303407 1 44,60 8,90

METALURGICAL TESTS/ENSAYOS METALÚRGICOS/METALLURGISCHE PRÜFUNGEN/ESSAIS

METALLURGIQUES
ETCH STRUCTURE ACC. ASTM A923 MET.A: UNAFFECTED STRUCTURE. MATERIAL FREE
FROM INTERMETALLIC PHASES AND PRECIPITATES. UNIFORM STRUCTURE ACROSS
FULL WALL THICKNESS
EXAMEN DE MICROESTRUCUTRA DE ACUERDO A ASTM A923 MET.A: ESTRUCTURA NO
AFECTADA. MATERIAL LIBRE DE FASES INTERMETALICAS Y PRECIPITADOS.
ESTRUCTURA UNIFORME A TRAVES DEL ESPESOR.
ETCH STRUCTURE ACC. ASTM A923 MET.A: UNAFFECTED STRUCTURE. MATERIAL FREE
FROM INTERMETALLIC PHASES AND PRECIPITATES. UNIFORM STRUCTURE ACROSS
FULL WALL THICKNESS

INTERGRANULAR CORROSION TEST ACC. TO ASTM A262 PRACT."E": SATISFACTORY

ENSAYO DE CORROSION INTERGRANULAR DE ACUERDO A ASTM A262 PRACT.E:
SATISFACTORIO
BESTÄNDIGKEIT GEGEN INTERKRISTALLINE KORROSION ENTSPRECHEND ASTM A262
PRACT.E: IN ORDNUNG
ESSAI DE CORR. INTERGR. SELON ASTM A262 PRACT.E:SATISFAISANT
INTERGRANULAR CORROSION TEST ACC.TO DIN EN ISO 3651-2 MET.B:
SATISFACTORY
ENSAYO DE CORROSION INTERGRANULAR DE ACUERDO A ISO 3651-2 MET.B:
SATISFACTORIO
BESTÄNDIGKEIT GEGEN INTERKRISTALLINE KORROSION ENTSPRECHEND ISO 3651-2
MET."B": IN ORDNUNG
ESSAI DE CORR. INTERGR. SELON ASTM ISO 3651-2 MET."B":SATISFAISANT

NON-DESTRUCTIVE TESTS/ENSAYOS NO DESTRUCTIVOS/ZERSTÖRUNGSFREIE

PRÜFUNGEN/ESSAIS NON DESTRUCTIFS
FERRITE CONTENT DETERMINED BY FISCHER FERRITOSCOPE TO 100% OF PRODUCTS
CONTENIDO EN FERRITA MEDIDO CON FERRITOSCOPIO SOBRE EL 100% DEL
MATERIAL.
Ferritescope-Test auf 100% des Materials.

100% ULTRASONIC TEST ACC. TO ASTM A999 / E213: SATISFACTORY

100% ENSAYO DE ULTRASONIDOS DE ACUERDO A ASTM A999 / E213: SATISFACTORIO
100% ULTRASCHALLPRÜFUNG NACH ASTM A999 / E.213:IN ORDNUNG
100% ESSAI D´ULTRASON D'ACCORD A ASTM A999 / E.213: SATISFAISANTE

100% ULTRASONIC TEST ACC. TO EN 10246-7, U2C: SATISFACTORY

100% ENSAYO DE ULTRASONIDOS DE ACUERDO A EN 10246-7, U2C: SATISFACTORIO
100% ULTRASCHALLPRÜFUNG NACH EN 10246-7, U2C:

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 5 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

IN ORDNUNG
100% ESSAI D´ULTRASON D'ACCORD A EN 10246-7, U2C: SATISFAISANTE
POSITIVE MATERIAL IDENTIFICATION TEST ON EACH TUBE/PIPE BY
"X-RAY-FLUORESCENCE-ANALYZER": SATISFACTORY
VERIFICACION DEL GRADO DE ACERO EN CADA TUBO MEDIANTE "ANALIZADOR DE
FLUORESCENCIA DE RAYOS X": SATISFACTORIO
VERWECHSLUNGSPRUEFUNG AN JEDEM ROHR MIT
"RÖNTGEN-FLUORESZENZ-ANALYSATOR": IN ORDNUNG
VERIFICATION DE LA NUANCE SUR CHAQUE TUBE PAR
"X-RAY-FLUORESCENCE-ANALYZER": SATISFAISANT

HYDROSTATIC PRESSURE TESTED AT 168 bar, 2400 PSI DURING 5 SEC ON EACH
TUBE/PIPE: SATISFACTORY
ENSAYO HIDROSTÁTICO A 168 bar, 2400 PSI DURANTE 5 SEC EN CADA TUBO:
SATISFACTORIO
WASSERDRUCKPRÜFUNG BEI 168 bar, 2400 PSI HALTEZEIT 5 SEC JE ROHR: IN
ORDNUNG
ESSAI DE PRESSION HYDROSTATIQUE À 168 bar, 2400 PSI PENDANT 5 SEC SUR
CHAQUE TUBE: SATISFAISANT

DIMENSIONAL CHECKING ON EACH TUBE: SATISFACTORY

INSPECCION DIMENSIONAL AL 100% DE LOS TUBOS SATISFACTORIA
100% MASSKONTROLLE: O.B.
VERIFICATION DIMENTIONNELLE AU 100% DES TUBES, SATISFAISANTE

VISUAL INSPECTION ON EACH TUBE: SATISFACTORY

INSPECCION VISUAL AL 100% DE LOS TUBOS, SATISFACTORIA
100% BESIGCHTIGUNG: O.B.
EXAMEN VISUEL AU 100% DES TUBES, SATISFAISANT

TECHNOLOGICAL TESTS/ENSAYOS TECNOLÓGICOS/TECHNOLOGISCHE

PRÜFUNGEN/TECHNOLOGICAL TESTS

FLATTENING TEST: SATISFACTORY

APLASTADO S.NORMA: SATISFACTORIO
RINGFALTVERSUCH: IN ORDNUNG
ESSAI D'APLATISSEMENT: SATISFAISANT

RING TENSILE TEST: SATISFACTORY

TRACCION DE ANILLO: SATISFACTORIO

RINGZUGVERSUCH: IN ORDNUNG
ESSAI DE TRACTION A L'ANNEAU: SATISFAISANT

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 INSPECTION CERTIFICATE Number: 745903 Rev:
CERTIFICADO DE INSPECCIÓN Page: 6 / 6
CERTIFICAT DE RÉCEPTION
ABNAHMEPRÜFZEUGNIS
EN 10204:2004 / 3.1 Created on: Modified on:
Date: 17.07.2023 21.07.2023

MARKING/ETIQUETADO/KENNZEICHNUNG/MARKSTEXT
TX2 TX1 TUBACEX 219,08 X 8,18 MM - 8" SCH 40S ASME SA790 ASTM A790 EN 10216-5 TC2 EN 10297-2 S32750 1.4410
HFD HF SMLS HEAT/ PMI-AV LOT NO/MADE IN SPAIN

REMARKS/OBSERVACIONES/ANMERKUNG/REMARQUES

NO MERCURY, MERCURY COMPOUNDS OR MERCURY BEARING INSTRUMENTS AND/OR EQUIPMENT HAVE BEEN USED ALONG
MANUFACTURING AND INSPECTION PROCESS.
DURANTE LOS PROCESOS DE FABRICACIÓN E INSPECCIÓN NO SE HA USADO MERCURIO NI INSTRUMENTOS Y/O EQUIPOS
CONTENIENDO MERCURIO O CON COMPONENTES DE MERCURIO.
KEINE QUEKSILBER, BZW. QUECKSILBERVERUNREINIGTES KOMPONENTEN ODER KUGELLAGERINSTRUMENTE UND/ODER GERÄTE SIND
BENUTZT WORDEN PRODUKTIONS UND BESICHTIGUNGSPROZESS.
IL N'A PAS ÉTÉ FAIT USAGE DE MERCURE, DE COMPOSÉS CONTENANT DU MERCURE OU DE MATÉRIAUX ET/OU D'INSTRUMENT
CONTENANT DU MERCURE TOUT AU LONG DES ÉTAPES DE FABRICATION ET DU PROCESSUS D'INSPECTION ET DE CONTRÔLE.

NO WELDING OR WELD REPAIRS WERE MADE

SIN REPARACION POR SOLDADURA
KEINE SCHWEISSBEARBEITUNG WURDE VORGENOMMEN
SANS RÉPARATION AVEC SOUDURE
MATERIAL MANUFACTURER APPROVED BY TÜV SÜD Industrie Service GmbH
(NOTIFIED BODY 036)TO ISSUE CERTIFICATES OF SPECIFIC PRODUCT CONTROL IN
ACCORDING TO PRESSURE EQUIPMENT DIRECTIVE 2014/68/EU ANNEX 1 POINT 4.3.
FABRICANTE DE MATERIALES APROBADO POR TÜV SÜD Industrie Service GmbH (ORGANISMO NOTIFICADO 0036) PARA LA
EMISION DE CERTIFICADOS ESPECIFICOS DE CONTROL DE PRODUCTO DE ACUERDO AL ANEXO 1, PUNTO 4.3 DE LA DIRECTIVADE
EQUIPOS A PRESION 2014/68/EU.
WERKSTOFFHERSTELLER MIT BERECHTIUNG ZUR AUSSTELLUNG VON BESCHEINIGUNGEN ÜBER SPEZIFISCHE PRÜFUNGEN AN DEN
WERKSTOFFEN IM GELTUNGSBEREICH DER ZERTIFIZIERUNG UND IN ÜBEREINSTINSTIMMUNG MIT DER DRUCKGERÄTERICHTLINIE
2014/68/EU UND DEN ZUGRUNDE LIEGENDEN SPEZIFIKATIONEN ENTSPR. DER BENANNTEN STELLE NR.0036, TÜV SÜD Industrie
Service GmbH
PRODUCTEUR DU MATERIEL APPROUVE PAR TÜV SÜD Industrie Service GmbH N.B. 0036) POUR EMISSION DES CERTIFICATS
SPECIFIQUE DE CONTROLE DE PRODUIT SELON LA DIRECTIVE DES EQUIPES A PRESION 2014/68/EU ANNEXE 1 POINT 4.3.

MATERIAL CHARACTERISTICS COMPLY WITH POINT 7.5 OF ANNEX I TO PED BY HAVING AN ELONGATION AFTER RUPTURE AT
TENSILE TEST NO LESS THAN 14% AND A BENDING RUPTURE ENERGY AT IMPACT TEST NO LESS THAN 27J AT 20ºC.
LAS CARACTERISTICAS DEL MATERIAL CUMPLEN CON LOS REQUISITOS DEL PUNTO 7.5 DE LA DIRECTIVA PED POR TENER UN
ALARGAMIENTO TRAS ROTURA EN EL ENSAYO DE TRACCION NO INFERIOR AL 14% Y PO DE TRACCION NO INFERIOR AL 14% Y POR
TENER UNA RESISTENCIA AL IMPACTO NO INFERIOR A 27 J A 20º C.
DIE WERKSTOFF-WERTE ENTSPRECHEN PUNKT 7.5. DER DGRL, ANHANG 1, MIT EINERBRUCHDEHNUNG = 14% IM NORMGEMÄSS
DURCHGEFÜHRTEN ZUGVERSUCH UND DER KERBSCHLAGARBEIT = 27J AN EINER ISO - v PRO PROBE BEI EINER TEMPERATUR VON
HÖCHSTENS 20ºC
LES CARACTERISTIQUES DU MATERIEL, AYANT UN ALLONGEMENT APRES RUPTURE A L'ESSAI DE TRACTION NON INFERIEUR DU
14% ET UNE RESISTENCE A LA FLEXION PAR CHOC A 20ºC NON INFERIEUR A 27J, SONT CONFORMES AUX PRESCIPTIONS DU
PONT 7.5 DE L'ANNEXE I DE PED.

MATERIAL IS FREE OF RADIATION CONTAMINATION

EL MATERIAL ESTA LIBRE DE CONTAMINACION POR RADIACIONES
MATERIAL IS FREI VON RADIOAKTIVITÄT
MATÉRIEL LIBRE DE POLUTION RADIOACTIVE

TUBACEX TUBOS
INOXIDABLES S.A.U.

We hereby certify that the material herein described has been manufactured, sampled, tested, and
inspected in accordance with above standards and specifications and satisfies order#s requirements. This
certificate is issued by a computerized system and it is valid without original signature. In case the owner
of the certificate would release as a copy of it, he must attest its conformity to the issued, assuming the
responsibility for any unlawful or TUBACEX, not allowed use. Any forgery or falsification of this certificate
shall legally prosecuted.

TSS S.A.U as commercial operation intermediary certifies that this certificate is a true copy of the manufacturer original certificate. TSS S.A.U makes a copy of the
original certificate without changing the properties specified in the original purchase order and the product specification referenced.
 MTC / Certificate
STRUCTURE EXAMINATION 745903

MATERIAL IDENTIFICATION / IDENTIFICACIÓN DEL MATERIAL

Lot No. / Num Lote P2303407 Dimension / Dimensión 219,08 x 8,18 mm - 8'SCH 40

Heat / Colada 60177 Grado de acero / Steel grade S32750

Type Of test / Tipo de Ensayo: MICROSTRUCTURE EVALUATION

RESULTS / RESULTADO

Result: The microestructure is formed by austenite and ferrite. The presence of intermetallic phases or precipitates is not observed. Uniform structure
across full wall thickness Etching method according to ASTM E-407.

Resultado: la microestructura está compuesta por austenita y ferrita. No se observa la presencia de fases intermetálicas y precipitados. Estructura uniforme a
través de todo el espesor. Método de ataque según ASTM E-407.

GRAPHICS RECORDS / REGISTROS FOTOGRÁFICOS:

Dir: LONGITUDINAL / MAG: 500X / Dir: TRANSVERSAL / MAG: 500X /

María Cano
Responsable del Laboratorio
Laboratory Manager
 INSPECTION CERTIFICATE (3.1) - Chemical analysis
TEST REPORT (2.2) - Mechanical properties

Issued Date: 2024-04-18 Certificate number: EC27495675 rev. 0

Our order: 0100931309 Your order:

Our reference: Your reference:
Customer number: NLB00168 Your fax number:
Customer order date: Your e-mail:

Invoice address Receiver of certificate Delivery address

EUROWELD B.V.

DELIVERY Lot number: SBX1910834 Quantity:

PRODUCT CHEMICAL ANALYSIS

Brand: ESAB Actual results: acc to EN 10204 - 3.1
Description: OK 68.55 2.5x300mm 1/4 VP
Item number: 68552520L0 All weld metal
C 0.02%
Si 0.6%
Mn 0.8%
P 0.021%
S 0.004%
Cr 25.7%
CLASSIFICATIONS
Ni 9.6%
EN ISO 3581-A: E 25 9 4 N L B 4 2 Mo 4.0%
SFA/AWS A5.4: E2594-15 Cu 0.10%
Werkstoffnummer: (1.4410) N 0.24%

MECHANICAL PROPERTIES
Typical data: acc to EN 10204 – 2.2
A4, A5 = Elongation
Tensile ReH = Upper Yield Point
ReL = Lower Yield Point
Rp0.2 [MPa/ksi] Rm [MPa/ksi] A5 [%]
Rm = Ultimate Tensile Strength (UTS)
700/102 900/131 28 Rp0.2 = Yield Strength 0.2 offset
Rp1.0 = Yield Strength 1.0 offset
Impact
Temp [°C/°F] KV[J/ft-lb]
-60/-76 45/33

COMMENTS

Product supplied under a QA Programme fulfilling the EN ISO 9001 standard.

This certificate is produced electronically.
Please refer any queries to:
Esab Nederland BV - P.O. Box 2236 , 3800 CE Amersfoort , Nederland

Validation
Ellen Bjorgan Quality Manager Tapio Huhtala Product Manager