(Done) Appendix A Neraca Massa
(Done) Appendix A Neraca Massa
NERACA MASSA
Kapasitas
Waktu Operasi
Basis waktu
Satuan
F1
Absorber
F3
1
F4
APENDIKS A
Dalam absorber terdapat dua reaksi penghilangan gas asam (CO 2
dan H2s) :
a) Reaksi penyerapan H2S
Konversi reaksi 0.95 (kirk othmer) :
2(C2H5O)5NH + H2S
((C2H5O)2NH2)2S
Mula-mula:
19.308
10.162
Bereaksi :
19.308
9.654
Sisa
:
0
0.508
9.654
b) Reaksi penyerapan CO2
Konversi reaksi 0.95 (kirk othmer) :
2(C2H5O)5NH + 2CO2 + 4H2O 2((C2H5O)2COONH+ 4H2O
Mula-mula:
63.512
66.855
Bereaksi :
63.512
63.512
Sisa
:
0
3.343
63.512
Larutan DEA yang digunakan adalah dengan konsentrasi
optimalnya yaitu 35 %:
Dari reaksi diatas maka jumlah larutan DEA yang dibutuhkan
adalah:
Larutan DEA 35 %
: 82.819 Kmol/jam
Menghitung BM Campuran DEA :
BM Campuran : (0.35 x 105.18) + (0.65 x 18)
: 48.513 Kg/Kmol
Berat DEA Sol. Yang dibutuhkan : 4017.8 Kg/jam
Komposisi
:
a) DEA 35 %
: 1406.238 Kg/jam :28.987 kmol/jam
b) Air 65 %
: 2611.585 Kg/jam
: 53.833 kmol/jam
82.819 K mol/jam
Neraca Massa Masuk Absorber
F1
F2
Komposisi
Laju
laju
Laju
Laju
Kmol/jam Kg/jam Kmol/jam kg/jam
CH4
344.59548
5520
0
0
C2H6
30.218291
908.7
0
0
C3H8
21.767866
959.7
0
0
n-C4H10
4.813533
279.8
0
0
n-C5H12
2.674185
192.5
0
0
2
APENDIKS A
F1
Komposisi
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C4H11NO2
TOTAL
Komposisi
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C4H11NO2
F2
Laju
laju
Laju
Laju
Kmol/jam Kg/jam Kmol/jam kg/jam
1.7114784
147.2
0
0
0.8022555
81.83
0
0
1.9788969
154.4
0
0
66.854625
2942
0
0
10.161903
345.5
0
0
49.258488
886.7 53.832681 1406.238
0
0 28.986828 2611.584
534.837
12418 82.81951 4017.823
Neraca Massa keluar Absorber
F3
F4
Laju
laju
Laju
Laju
Kmol/ja
Kg/ja
Kmol/ja
m
m
m
kg/jam
0
0 344.59548 5520.42
0
0 30.218291 908.664
959.745
0
0 21.767866
2
279.762
0
0 4.813533
5
192.541
0
0 2.674185
3
147.187
0
0 1.7114784
1
81.8300
0
0 0.8022555
6
0
0 1.9788969 154.354
147.080
63.511894
2795 3.3427313
2
17.2752
9.6538079
328.2 0.5080952
4
886.652
0
0 49.258488
8
0
0
0
0
3
APENDIKS A
((C2H5O2)2NH)2S
(C2H5O2)2COONH
19.3076
63.5119
TOTAL
155.985
936.7
3081
7140.5
8
461.6713
9295.51
HEAT EXCHANGER
F5
F 11
Neraca Massa masuk Heat Exchanger
F3
F 10
Komposisi
Laju
laju
Laju
Laju
Kmol/jam Kg/jam Kmol/jam kg/jam
CH4
0
0
0
0
C2H6
0
0
0
0
C3H8
0
0
0
0
n-C4H10
0
0
0
0
n-C5H12
0
0
0
0
n-C6H14
0
0
0
0
n-C7H18
0
0
0
0
C6H6
0
0
0
0
CO2
63.511894
2795
0
0
H2S
9.6538079
328.2
0
0
H2O
0
0 53.832681 1406.238
C4H11NO2
0
0 28.986828 2611.584
((C2H5O2)2NH)2S
19.3076
936.7
0
0
4
APENDIKS A
(C2H5O2)2COONH
63.5119
TOTAL
155.985
3081
7140.5
8
82.81951
4017.823
APENDIKS A
3. Stripper
F6
F5
O
c 2 H 5 2 NH
Stripper
F9
O
2 (
c 2 H 5 5 NH + H 2 S
O
C2 H 5
O
Asumsi Reaksi terkonversi 100 %:
C2 H 5
Neraca Massa Masuk Stripper
F5
2
Laju
Laju
Komposisi
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C4H11NO2
Kmol/ja
m
0
0
0
0
0
0
0
0
63.5118
94
9.65380
79
0
0
6
Kg/jam
0
0
0
0
0
0
0
0
2795
328.2
0
0
APENDIKS A
((C2H5O2)2NH)2
S
(C2H5O2)2COO
NH
TOTAL
19.3076
936.7
63.5119
155.985
3081
7140.58
F 11
COOLER
F2
Neraca Massa
Masuk
Komponen
Jumlah (kg)
F 11:
Keluar
Komponen
Jumlah (kg)
F 2:
7
APENDIKS A
H2O
C4H11NO2
Jumlah
2611.585 H2O
1406.238 C4H11NO2
4017.8229 Jumlah
2611.585
1406.238
4017.8229
F4
Absorber
F13
F12
Triethylene Glycol (C6H14O4) :
a) Densitas TEG
: 1.1255 Kg/L
b) BM TEG
: 150
c) Sirkulasi rate glycol
: 3 L TEG/jam (yang paling
umum digunakan)
d) 1 gal TEG/ lbm H2O
: 8.345 L TEG/ Kg H2O
e) Jumlah air dlm sweet gas : 886.6528 Kg/jam
Sirkulasi rate glycol yang dibutuhkan : (sirkulasi rate glycol x air
yang akan diserap x 1gal
TEG/lbm H2O)
: 22198.418 L TEG/jam
TEG yang dibutuhkan (Kg/jam)
: 24984.32 Kg/Jam
Air untuk TEG Sol.
: 125.549 Kg/Jam
Asumsi Konsentrasi TEG (N=2)
APENDIKS A
Dari
diatas didapatkan persamaan :
grafik
( W W out )
0.96=
Maka dapat dihitung pula air yang
W diserap:
Win
Wout
W loss/ serap
Komposis
i
CH4
C2H6
C3H8
n-C4H10
: 886.6528 Kg/jam
: 35.4661 Kg/jam
: 851.1867 Kg/jam
0
0
0
0
APENDIKS A
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C6H14O4
TOTAL
Komposis
i
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C6H14O4
TOTAL
2.674185
1.7114784
0.8022555
1.9788969
3.34273125
0.50809515
49.258488
0
461.671298
192.54132
147.1871424
81.830061
154.3539582
147.080175
17.2752351
886.6527786
0
9295.511986
0
0
0
0
0
0
6.974963
166.56213
173.53709
0
0
0
0
0
0
125.54934
24984.319
25109.868
6. Reboiler
F 12
Reboiler
10
F 14
APENDIKS A
Komposis
i
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C6H14O4
TOTAL
F 14
FLASH TANK
F 16
11
APENDIKS A
Neraca Massa Flash Tank
Komposisi
F14
F15
F16
kmol/jam
kg/jam
Kmol/jam
Kg/jam
Kmol/jam
Kg/jam
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
34.44
551.71
4.53
72.51
29.91
479.20
3.02
90.81
0.03
1.05
2.99
89.77
2.18
95.92
0.02
0.80
2.16
95.12
0.48
27.96
0.00
0.05
0.48
27.91
0.27
19.24
0.00
0.02
0.27
19.22
0.17
14.71
0.00
0.01
0.17
14.70
0.08
8.18
0.00
0.00
0.08
8.18
0.20
15.43
0.00
0.01
0.20
15.41
0.33
14.70
0.00
0.02
0.33
14.68
0.05
1.73
0.00
0.00
0.05
1.73
54.26
11.24
202.26
43.03
774.47
C6H14O4
166.56
105.87
15880.61
60.69
9103.70
TOTAL
262.04
976.74
24984.3
2
26801.4
4
121.69
16157.34
140.35
10644.09
HEAT EXCHANGER
F 21
Neraca Massa masuk Heat Exchanger
12
F 17
APENDIKS A
Komposis
i
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C6H14O4
TOTAL
Komposis
i
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C6H14O4
TOTAL
F 16
kmol/jam
29.91267
2.98521
2.157419
0.480181
0.266985
0.170934
0.080153
0.197622
0.333647
0.050769
43.02623
60.69137
140.3532
F 20
Kmol/jam Kg/jam
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
kg/jam
479.2009274
89.76526143
95.12061736
27.90813836
19.22295358
14.70028113
8.175593989
15.41449182
14.68045264
1.726152428
774.4722098
2.1513
9103.704946
60.69
10644.09203 62.8426
38.7236
9103.69
9142.42
774.4722098
2.1513
9103.704946
60.69
10644.09203 62.8426
13
38.7236
9103.69
9142.42
APENDIKS A
9. Regenerator (D-220)
Masuk
Komposisi
Keluar
Aliran 1
kmol/jam
kg/jam
29.91
479.20
2.99
89.77
2.16
95.12
0.48
27.91
0.27
19.22
0.17
14.70
0.08
8.18
0.20
15.41
0.33
14.68
0.05
1.73
43.03
774.47
60.69
9103.70
140.35
10644.09
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
C6H14O4
TOTAL
Aliran 2
Kmol/jam Kg/jam
29.91
479.20
2.99
89.77
2.16
95.12
0.48
27.91
0.27
19.22
0.17
14.70
0.08
8.18
0.20
15.41
0.33
14.68
0.05
1.73
40.87
735.75
0.00
0.01
77.51
1501.68
Aliran 3
Kmol/jam Kg/jam
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
2.15
38.72
60.69
9103.69
62.84
9142.42
Komponen
Surge drum
(F-225)
F 20
APENDIKS A
H2O
C6H14O4
2.1513117
60.691276
8
Total
62.842589
38.7236104
9
9103.69152
5
9142.41513
5
2.151312
60.69128
62.84259
38.7236104
9
9103.69152
5
9142.41513
5
11.Cooler (E-211)
F 23
F 22
COOLER
F 24
DE-ETHANIZER
15
F 26
APENDIKS A
CH4
Boiling
Point (K)
111.16
C2H6
184.60
C3H8
231.10
n-C4H10
272.70
n-C5H12
309.20
n-C6H14
n-C7H18
341.90
371.60
C6H6
353.20
CO2
H2S
H2O
213.50
373.20
Komponen
Antoine coefficients
A
B
C
13.584 958.13
-3.72
13.879
7
1582.2 -13.762
13.709
7
1872.8 -25.101
13.983
6
2292.4 -27.862
13.977
8
2554.6 -36.253
14.056
8
2825.4 -42.709
14.56 3096.2 -49.165
15.063
2
3367.1 -55.621
15.376
8 1956.3
-2.117
15.5
3500
-30
16.53 3985.4 -38.997
Laju
Kg/jam
4968.708843
817.8521156
863.8282715
251.8030699
173.2987405
132.4772594
73.6519647
138.9278236
132.3809823
16
Xf
0.831147791
0.072885069
0.05250305
0.011610011
0.006450006
0.004128004
0.001935002
0.004773005
0.008062508
APENDIKS A
H2S
H2O
TOTAL
0.46
1.97
373.1666139
15.5487481
35.46611114
7603.94393
0.001225501
0.005280053
1
.Xf
yi
4921.19
4090.
23
0.99
89
0.00
08
0.00
01
0.00
00
0.00
00
0.00
00
0.00
00
0.00
00
0.00
02
0.00
00
0.00
00
C2H6
0.07
5390.19
1.80
46.78
3.41
C3H8
0.05
1345.57
0.45
11.68
0.61
n-C4H10
0.01
381.40
0.13
3.31
0.04
n-C5H12
0.01
115.24
0.04
1.00
0.01
n-C6H14
0.00
36.73
0.01
0.32
0.00
n-C7H18
0.00
16.85
0.01
0.15
0.00
C6H6
0.00
7.25
0.00
0.06
0.00
CO2
0.01
8815.26
2.94
76.50
0.62
H2S
0.00
22.93
0.01
0.20
0.00
H2O
0.01
7.28
0.00
0.06
TOTAL
1.00
0.00
4094.
92
1.00
APENDIKS A
Komponen
CH4
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
1.7811 0.00477
CO2
3.0087 0.00806
H2S
H2O
Total
0.4573 0.00123
1.9703 0.00528
373.2
1
0.017811 5E-05
3.00865
9 0.0089
0.45731
6 0.0013
0
0
339.873
1
F 30
kmol/j
1.55078
3
0.13599
1
19.0046
1
4.24581
9
2.38285
8
1.52502
9
0.71485
7
1.76331
5
Xb
0.04658
0.00408
0.57082
0.12753
0.07157
0.04581
0.02147
0.05296
0
2
33.2936
0
0.05918
1
yi/
0.0019
69
Xi
0.149
95
yi
0.908
Psat
30276.
6
Ki
6.055314
18
461.25
APENDIKS A
C2H6
C3H8
n-C4H10
n-C5H12
n-C6H14
n-C7H18
C6H6
CO2
H2S
H2O
0.0796
0.0017
0.0003
7E-05
5E-05
2E-05
5E-05
0.0089
0.0013
0
4006.0
5
919.85
9
237.21
65.640
4
19.106
9
7.9384
4
3.0633
6
6279.1
2
10.980
6
2.9698
7
0.801209
0.183972
0.047442
0.013128
0.003821
0.001588
0.000613
1.255824
0.002196
0.000594
0.0013
05
0.0001
23
7.05E05
7.08E05
0.0001
56
0.0001
76
0.0011
23
9.25E05
0.0080
44
0.099
38
0.009
4
0.005
37
0.005
39
0.011
86
0.013
38
0.085
54
0.007
05
0.612
7
0.0125
0
0.0131
28
0
1.000
02
86.9
12
20.0
02
6.51
68
2.51
37
Xi.
4.0482
94
0.0817
02
3.7199
27
0.3205
65
Yi
0.488
55
0.009
86
0.448
92
0.038
69
61.03
14.014
3.6138
1
0.2911
0.1209
0.0467
95.659
0.1673
Total
Menghitung Temperatur pada bottom (F 29)
Buble point
Ttrial =
108.8 oC
= 455.75 K
P
=
6
Mpa = 6000 Kpa
Komponen
CH4
C2H6
C3H8
n-C4H10
Xw
0.04
66
0.00
41
0.57
08
0.12
75
Psat
62931
.9
14483
.3
4718.
73
1820.
14
Ki
10.488
2.413
0.78645
00.3033
19
APENDIKS A
n-C5H12
n-C6H14
n-C7H18
C6H6
0.07
16
0.04
58
0.02
15
0.05
3
0
CO2
H2S
H2O
0.05
92
724.0
84
306.2
77
190.9
12
114.4
91
27570
.2
257.5
46
134.8
28
0.120
0.05104
0.019
0.1285
10.6426
0.2416
0.1768
1
0.42
3
0.26
37
0.15
81
38.0
76
0.35
57
0.18
62
Total
0.0715
71
0.0193
75
0.0056
61
0.0083
74
0.008
64
0.002
34
0.000
68
0.001
01
0
0.0110
2
8.2864
89
0
0.001
33
1.000
02
13. Kompressor
F 29
Compressor
(G-410)
F 31
APENDIKS A
Jumlah
7603.94 Jumlah
21
7603.94