Service Manual
Agilent 7890 Series Gas
Chromatograph
Agilent Technologies
Notices
Agilent Technologies, Inc. 2013
Warranty
No part of this manual may be reproduced
in any form or by any means (including
electronic storage and retrieval or
translation into a foreign language)
without prior agreement and written
consent from Agilent Technologies, Inc. as
governed by United States and
international copyright laws.
The material contained in this document is
provided "as is," and is subject to being
changed, without notice, in future editions.
Further, to the maximum extent permitted
by applicable law, Agilent disclaims all
warranties, either express or implied, with
regard to this manual and any information
contained herein, including but not limited
to the implied warranties of
merchantability and fitness for a particular
purpose. Agilent shall not be liable for
errors or for incidental or consequential
damages in connection with the
furnishing, use, or performance of this
document or of any information contained
herein. Should Agilent and the user have a
separate written agreement with warranty
terms covering the material in this
document that conflict with these terms,
the warranty terms in the separate
agreement shall control.
Manual Part Number
G3430-90006
Edition
Ninth edition, August 2013
Eighth edition, May 2013
Seventh edition, November 2011
Printed in USA
Agilent Technologies, Inc.
2850 Centerville Road
Wilmington, DE 19808-1610 USA
Safety Notices
A warning calls attention to a condition
or possible situation that could cause
injury to the user.
A caution calls attention to a condition or
possible situation that could damage or
destroy the product or the user's work.
Contents
1
Before Servicing the Instrument
Safety
20
Hand tools
20
Specialized tools for GC support
24
Electronic tools for GC support
26
Pneumatic tools for GC support
For Checking Inlet Pressure
28
30
Inlets
Inlet overview
34
Split/Splitless Inlet 35
Replacing the split/splitless inlet 35
Replacing the split/splitless inlet top weldment assembly 38
Replacing the split/splitless inlet split vent line 39
Replacing the split/splitless inlet split vent filter canister and valve
assembly 40
Reinstalling the split/splitless inlet 42
Multimode Inlet 43
Replacing the multimode inlet 44
Replacing the multimode inlet top weldment assembly 46
Replacing the multimode inlet split vent line 47
Replacing the multimode inlet split vent filter canister and valve
assembly 48
Replacing a Multimode CO2 cryo valve 50
Replacing the Multimode N2 cryo valve 52
Removing the MMI cryo/PC board bracket 54
Replacing the MMI heater/cryo PC board 56
Cool On-Column Inlet 58
Replacing the COC inlet 58
Replacing the COC heater/sensor assembly
Replacing an inlet cryo cooling tube 62
Purged Packed Inlet 65
Replacing the Purged Packed inlet 65
Replacing the Purged Packed inlet heater
60
70
Programmed Temperature Vaporization Inlet (PTV)
Replacing the PTV inlet 74
Replacing the PTV inlet cryo jacket 77
Service Manual
73
Replacing the PTV CO2 or LN2 inlet cryo assembly
Replacing a PTV CO2 cryo valve 80
Replacing the PTV N2 cryo valve 81
Removing the PTV cryo/PC board bracket 83
Replacing the PTV heater/cryo PC board 85
79
Volatiles Interface 87
Replacing or cleaning the volatiles interface 87
Replacing the volatiles interface heater/sensor assembly
Calibrating the interface 92
90
Solvent Vapor Exit Accessory 93
Replacing the SVE valve/fitting assembly 94
Replacing the SVE bleed restrictor column 96
Replacing the SVE tri-column assembly 97
Replacing the SVE pre-column assembly 98
Detectors
Detector overview
100
About the detector signal boards
100
Accessing detector signal boards
103
Replacing detector signal boards
104
Detector signal board, bad checksum error
107
Flame Ionization Detector (FID) 113
Selecting an FID jet 113
Replacing the FID interconnect assembly or spring
To replace the interconnect spring only 117
To replace the interconnect (and spring) 117
Replacing the heater 118
Replacing the FID signal board 122
Replacing the FID electrometer 123
Replacing the FID glow plug (ignitor) 125
Replacing the entire FID 127
Ultrasonic cleaning the FID 130
115
Nitrogen Phosphorus Detector (NPD) 132
Selecting an NPD jet 132
Removing the NPD electrometer
134
Removing the NPD electrometer 134
Replacing the entire NPD 136
Replacing an NPD signal board 138
Replacing the NPD heater 140
Replacing the NPD electrometer
142
Service Manual
Cleaning the NPD jet and collector
Cleaning the NPD 146
144
Thermal Conductivity Detector (TCD) 148
Replacing the TCD detector cell 148
Replacing the TCD switching valve 150
Micro-cell Electron Capture Detector (uECD) 152
Replacing the uECD heater/sensor assembly 152
Replacing the uECD makeup gas adapter 154
Frequency test 156
Leak test 158
Performing a radioactivity leak test (wipe test) 159
Flame Photometric Detector (FPD) 7890A 160
Preparing for maintenance 160
Disassembling the FPD 161
Rebuilding the FPD optics assembly 171
Reassembling the FPD 178
Replacing the FPD 186
Bake out and run checkout test 188
Replacing the heater/sensor assemblies 189
Replacing the FPD signal board 194
EPC modules
EPC overview
196
Repairing EPC modules
197
Accessing EPC modules
199
Replacing the EPC modules
200
Replacing EPC module proportional valves
203
Inlet modules 205
Inlet modules 206
Proportional valves 207
Detector modules 208
Detector modules 209
Proportional valves 210
Pneumatics Control Module (PCM) 211
Calibrating the PCM interface 212
Changing the PCM pressure channel frit
Correcting PCM leaks 215
Potential PCM leak areas 216
Aux EPCs
Service Manual
213
217
Frits for auxiliary pressure control channels
Procedure for replacing frit 220
218
Updating PID Constants 221
Updating PID constants 222
No positive feedback on reconnect 226
Updating PID constants available for use by Instrument Utilities
Performance Verification
About Chromatographic Checkout
229
To Prepare for Chromatographic Checkout
To Check FID Performance
Typical values 237
230
232
To Check NPD Performance
Typical values 243
238
To Check TCD Performance
Typical values 249
244
To Check uECD Performance
Typical values 255
250
To Check FPD Performance (Sample 5188-5953)
Preparation 256
Phosphorus performance 257
Typical values 261
Sulfur performance 262
Typical values 263
256
To Check FPD Performance (Sample 5188-5245, Japan)
Preparation 264
Phosphorus performance 265
Typical values 269
Sulfur performance 270
Typical values 271
227
264
Configuration
Configuration overview 273
Inlet example 274
Detector example 275
PCM example 276
AUX example 277
Heater assignments 278
GC modules and the communications buss
280
Service Manual
To configure an MSD transfer line
To configure a valve box 286
MSD transfer line heater error
Initial steps 286
If that doesn't work 287
Replacing a GC module
288
Removing a GC module
289
283
286
Changing the GC configuration 290
Agilent data system methods 290
Methods stored in GC 290
Configuration locks
291
Installing new devices
Configuring time
292
294
External Cabling
Connectors on the back of the GC
296
Remote Start/Stop 297
APG Remote Control 297
Electrical specifications 297
Suggested Drive Circuits 298
The Remote Connector 298
Signal Descriptions 299
Timing Diagram 299
Cable pinouts, remote start/stop, general use 300
Cable pinouts, GC to 3395B/3396C Integrator 301
Cable pinouts, GC to 35900C, D, E/MSD/Sampler, 2 meters
Cable pinouts, GC to Headspace Sampler 303
Cable pinouts, APG Remote Y-cable 304
External event
302
305
Automatic sampler for GC 306
Cable pinouts, GC to G2613A Injector 306
Cable pinouts, GC to G4513A and 7650 Injector
Cable pinouts, GC to G2614A Tray 308
Cable pinouts, GC to G4514A Tray 309
307
Analog signal outputs 310
Analog cable: GC to 3395A/B or 3396B/C Integrators and 35900 C/D/E
Analog to Digital Interface instrument 310
Analog cable: general use 311
Service Manual
Analog signal inputs 312
General purpose AIB cable 312
XCD Chemiluminescence detector AIB cable
312
Internal Cabling
Internal cabling overview
314
MSD transfer line heater cable
315
Third detector heated zone cable
316
Communication harness 317
Power connection table 318
Data communication table 319
Motor Harness & AC Control Assembly
320
Keyboard and display connection board (original style only)
AC power inlet assemblies 323
Keyboard and display connection board (original style only)
AC power inlet assemblies
Inlet/Detector harness
326
328
Third detector EPC communication cable
Keyboard/Display harness
Keyboard interconnect board
332
Heated zone extension cable
333
Ignitor cable, FID
334
Ignitor cable, FPD
335
PTV thermocouple cable
330
331
RS-232 cable, ALS controller
336
337
339
Mainframe
Mainframe overview
341
Covers and Fans 342
Removing and replacing the covers 343
Detector top cover 343
The pneumatics top cover 343
Replacing the pneumatics top cover buttons
The electronics top cover 343
The side covers 343
324
325
Auxiliary zone/Valve box harness
NPD power cable
322
343
Service Manual
The rear covers 344
The side cover on the third detector assembly
Replacing the inlet cooling fan 345
Replacing the EPC cooling fan 346
Replacing the oven bezel
348
Replacing the oven door
349
Replacing the oven door button
344
350
Replacing the keypad assembly and display board 351
Replacing the keypad assembly (original style) 351
Replacing only the display board (original style) 354
Replacing the keypad assembly (new style) 356
Replacing only the display board (new style) 357
Replacing the original keypad assembly with the new assembly
Oven temperature control
359
362
Oven temperature troubleshooting
Oven does not heat up 363
Oven not cooling or never cools
363
364
Testing resistance of the heater coil
365
Cryo valve installation/replacement 366
Installing a new cryo valve 366
Replacing an existing cryo valve 368
Replacing the oven sensor
371
Replacing the oven door sensor
372
Replacing the oven shroud, oven fan, and oven fan motor
Replacing the oven flapper assembly
Replacing the flapper or flapper motor
375
381
383
Replacing Components Inside the Electronics Panel 385
Accessing the analog and power board 385
Replacing the ALS board 386
Replacing the fuse on the ALS controller board 389
Troubleshooting 390
Removing the valve bracket 391
Replacing the logic board 392
Check GC configuration 395
Replacing the analog and power board 396
Replacing Components Inside the Lower Rear Metal Cover
Replacing AC board fuse sets 401
Replacing the AC board 402
Service Manual
400
Replacing the oven triac 404
Replacing the power transformer
10
406
Valves
Valves 409
Introduction 410
Valco W-series minivalves 411
Valve bodies 411
Valve rotors 412
Preload assembly (not shown) 412
Valco W-series minivalve 413
Valve bodies 413
Valve rotors 414
General purpose valves 415
Gas sample valves 415
Gas sample loops 415
Adjustable restrictor valves 415
Liquid sample valves 416
Valve Box 417
Installing the valve box 417
Removing the valve box assembly
422
Actuators 423
Installing the actuators 423
Installing the actuator on a heated valve box
426
Installing the actuator on a side mount bracket 429
Valve actuator alignment 430
Valve actuator drivers 431
Solenoid differences 431
Which solenoid valve is installed?
431
Replacing an original solenoid valve 431
Installing a new valve stack assembly 432
Original style 432
Assemble the valve driver block 432
Install the bracket and cabling (original style) 433
Installing the valve driver block 434
New style 436
Replacing a solenoid valve (new style) 436
Installing the valve driver (solenoid) bracket, cabling, and elbow fitting
(new style) 441
Typical Valve Configurations 442
Option numbers 443
Custom Plumbing (diagram required), Option 700 or 730
10
443
Service Manual
Gas Sampling Option, Option 701 or 731 443
Column Isolation, Option 702 or 732 444
Two Stream Selection (Requires Gas Sampling), Option 703 or 733 444
Backflush to Detector, Option 704 or 734 445
Backflush a Precolumn to Vent, Option 705 or 735 445
Column Selection (Unused Column Isolated), Option 706 or 736 446
Sequence Reverse, Option 707 or 737 446
Sequence Reverse with Backflush of Column 1, Option 708 or 738 447
Custom Plumbing (Diagram Required), Option 800 or 830 447
Gas Sampling with Backflush of Precolumn to Vent, Option 801 or
831 448
Gas Sampling with Backflush to Detector, Option 802 or 832 448
Gas Sampling of Alternate Streams, Option 803 or 833 449
Gas Sampling with Sequence Reverse, Option 804 or 834 449
Gas Sampling with Sequence Reverse and Backflush of Column 1, Option
805 or 835 450
Column Selection with Backflush to Vent, Option 806 or 836 450
Liquid Sampling, Options 850, 852, 854, and 856 451
Troubleshooting 452
Chromatographic symptoms 452
Loss of sensitivity or excessive drift 453
Loss of peaks in specific areas of the chromatogram
Extraneous peaks 453
Peak broadening and tailing 454
Baseline shifts 454
Baseline upsets 454
Variation in peak area and retention time 455
Pressure check 455
11
453
Capillary flow technology (CFT) devices
CFT overview
458
Ultimate union 460
Tools and kits 460
Metal ferrules and nuts 461
Assembling nut, ferrule and swaging nut 461
Connecting and disconnecting columns 464
Mounting the union 464
Service Manual
11
12
Electrical
Power options 466
Regular oven 466
Fast oven 467
Converting the power option
Procedure 469
469
Remote start/stop connection
Remote control
470
471
Measuring inlet and detector heater and PRT resistance
Sensor resistance 474
Temperature sensor resistance
Oven heater coil resistance
475
476
Setting the instrument power configuration
Line voltage configuration plug
Ceramic and glass fuses
AC power board schematic
Oven shroud
13
472
477
478
479
480
481
Firmware
Firmware overview
483
To Update GC Firmware 484
Troubleshooting problems 486
Firmware history 487
7890 A.01.10.2 488
7890 A.01.10.1 489
7890 A.01.10 490
7890 A.01.09.2 490
7890 A.01.09.1 491
7890 A.01.09 491
7890 A.01.08 492
7890 A.01.07 492
7890A.01.04 492
7890A.01.03 494
7890A.01.02.581 494
Confirm firmware update
495
Problems and solutions 496
Possible solutions to unusual behaviors
12
496
Service Manual
Clearing battery-backed PF-RAM (7890A only)
Partial clear 497
Total clear 497
14
Set the default method
500
Default method listing
501
497
Firmware Instructions for Channel Partner Devices
Firmware overview for channel partners
Tuning a small heated zone
508
509
Thermal Aux Configuration 510
Heater and cryo connection locations 510
Connections assigned to a thermal zone 511
Auxiliary Type Selection 512
User Configurable Heater 513
Custom heater parameters 513
Programmable temperature zones 514
Cryo control model 515
Configuring the thermal Aux zone (Firmware A.01.07) 516
Configuring the thermal Aux zone (Firmware A.01.08 and A.01.09)
519
Valve Box Configuration 521
Heater connection locations 522
Custom heater parameters 523
Custom Heater Conf. 523
View Custom Heater Conf. 523
The PID and Mass fields 523
The Power field 523
Configuring the Valve Box Zone 524
Inlet configuration 525
Hardware configuration 526
EPC module installation 527
Heater and Cryo installation 528
The Inlet configuration display 529
Gas type 529
Cryo Parameters 529
Cryo type 529
Cryo 529
Use Cryo temperature 529
Cryo timeout 529
Cryo fault 529
Custom heater parameters 530
Configured hardware 531
Service Manual
13
Configuring a custom inlet (Firmware A.01.05) 532
Configuring a custom inlet (Firmware A.01.07) 534
Configuration procedure 537
Configuring a custom inlet (Firmware A.01.08 and A.01.09)
538
Cryo focus valve configuration 540
Operation 540
Assigned connections 540
Cryo trap configuration
541
Detector configuration 543
FID Signal 1 Detector Hardware Connections
AIB Signal 1 Detector Hardware Connections
Aux Detector Hardware Connections 548
EPC module installation 548
Detector Board Installation 549
Heater installation 549
Configuring a custom detector 550
15
Service Mode Diagnostics
Service mode overview
Detector diagnostics
553
554
Signal board diagnostics
Multiplexed ADC
Pneumatics
16
Accessories and options
17
Printed circuit boards
555
556
557
Power diagnostics
558
Summary of PCB Part Numbers
AC power board
568
569
Analog and power board
570
Logic and communications board (7890A)
572
Logic and communications board (7890B)
573
FID signal board
TCD signal board
uECD signal board
FPD signal board
14
544
546
574
575
576
577
Service Manual
NPD signal board
578
FID electrometer board
uECD electrometer board
NPD electrometer board
Analog input board
18
579
580
581
582
Illustrated Parts Breakdown
Inlets 584
Split/Splitless Inlet (SSL) 585
Split/Splitless Inlet, Top 586
SSL Split Vent Trap 587
Split Splitless Inlet Body 588
Split Splitless Inlet Warmer 590
Multimode Inlet (MMI) 591
Multimode Inlet Body 594
MMI Top Insert Assembly 596
MMI Split Vent Trap 598
7890A MMI Temperature controller 599
7890B MMI Temperature controller 600
7890A MMI Cryo assemblies 601
7890B MMI Cryo assemblies 602
Purged Packed Inlet (PP) 603
Purged Packed Inlet Upper Body 604
Purged Packed Inlet Lower Parts 606
Cool on-column inlet (COC) 608
Cool on-column inlet body 609
Programmed Temperature Vaporization Inlet (PTV)
PTV Inlet Body 613
PTV Septumless head 615
PTV Split vent 616
PTV Temperature controller 617
PTV CO2 cryo assembly 618
PTV LN2 cryo assembly, 7890A 619
PTV LN2 cryo assembly, 7890B 620
Volatiles Interface (VI) 622
Volatiles Interface (VI) 623
Volatiles Interface Trap 625
Detectors 627
Flame Ionization Detector (FID)
FID detector 629
FID Base Assembly 631
Service Manual
611
628
15
PM kits for the FID 633
Flame Photometric Detector (FPD) 634
FPD inert transfer line parts 636
FPD ignitor and heat shield assembly 638
PMT and bracket assemblies 640
FPD lens assembly 643
FPD Covers 644
FPD+ (High Temperature FPD) 646
FPD+ Assemblies 648
Microcell Electron Capture Detector (uECD) 654
Microcell Electron Capture Detector (uECD) parts
uECD Side Mount (3rd Detector) Parts 657
Nitrogen Phosphorus Detector (NPD) 659
Nitrogen Phosphorus Detector (NPD) parts 660
Thermal Conductivity Detector (TCD) 662
Thermal Conductivity Detector (TCD) parts 665
655
EPC Module Parts 669
Lookup table 669
Inlet modules 670
Detector modules 671
PCM modules 672
Aux EPCs 673
Nickel Catalyst Accessory
674
Oven 676
Oven assembly 677
Oven flapper assembly 680
CO2 cryogenic cooling 682
Liquid nitrogen (LN2) cryogenic cooling
684
Valves 685
Valve box assembly 686
Valve driver assembly 688
Valve driver assembly (original style) 689
Valve driver assembly (new style) 691
Valve actuator assembly (1 of 2) 694
Valve actuator assembly (2 of 2) 696
Miscellaneous Valve Parts 698
16
Service Manual
Electronics and Fans 700
Electronics carrier 701
Keyboard Assemblies 705
7890A Keyboard and Display (original style) 705
7890A Keyboard and Display (new style) 707
7890B Keyboard and Display 709
AC circuit board components 711
AC power 713
Power cords 715
Main transformer 716
Analog input board (G1556A accessory) 718
Chassis fans 719
Covers 720
Plastic covers 721
Back covers 723
Auto-injector mounting and parking posts
7890A Side Carrier 726
7890B Side Carrier 727
Mainframe 728
724
Tools 729
Shipping Crates 729
Hand tools 730
Specialized tools for GC support 734
Electronic tools for GC support 736
Pneumatic tools for GC support 738
For Checking Inlet Pressure 740
Service Manual
17
18
Service Manual
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
1 Before Servicing the Instrument
Safety 20
Hand tools 20
Specialized tools for GC support 24
Electronic tools for GC support 26
Pneumatic tools for GC support 28
Agilent Technologies
19
Before Servicing the Instrument
Safety
Before servicing the GC, observe the safety precautions in the
7890 Series GC Safety Manual.
Hand tools
We assume you have a well-equipped toolbox, but some of the
special tools listed here will be helpful.
Table 1
20
7890 Series GC tool bag, 5182-3456
Description
Part no.
Wrench, 1/4-inch to 5/16-inch
8710-0510
Wrench, open-end, 7/16-inch and 9/16-inch
8710-0803
Wrench, open-end, 1/2-inch and 7/16-inch
8710-0806
Wrench, open-end, 7/16-inch and 3/8-inch
8710-0972
Driver, nut, 7-mm
8710-1217
Cutter, tube
8710-1709
Screwdriver, Torx T-20
8710-1615
Screwdriver, Torx T-10
8710-1623
Tool bag
9222-3253
Tool, ferrule, .25.32 mm, 2 x 3 x 3/4-inch
RFT-2500
Tool, ferrule, .53 mm
RFT-5300
Lens, magnifying
G2855-40001
Septum tool, knurled handle
450-1000
7890 Series GC IPB
Before Servicing the Instrument
Drivers
T-20 Torx Driver 5182-3465
T-20 Torx Key (for close-quarters work) 8710-1807
T-10 Torx Driver 5182-3466
7890 Series GC IPB
21
Before Servicing the Instrument
T-10 Torx Key (for close-quarters work) 8710-2140
#1 Pozidriv screwdriver 8710-0899
#2 Pozidriv screwdriver 8710-0900
Flat-blade screwdriver 8730-0008
1/4-inch Nut Driver 8710-1561 (FID Jets)
7-mm Nut Driver 8710-1217
Wrenches
Wrench, 1/4-inch to 5/16-inch 8710-0510
Wrench, open-end, 7/16-inch and 9/16-inch 8710-0803
Wrench, open-end, 1/2-inch and 7/16-inch 8710-0806
Wrench, open-end, 7/16-inch and 3/8-inch 8710-0972
Wrench, adjustable, 12-inch 8710-1712
Wrench, open-end, 3/16-inch x 1/4-inch 8710-2618
Wrench, open-end, 9/16-inch x 5/8-inch 8720-0010
Wrench, 7-mm x 8-mm 1340407010
Wrench, 6-mm x 7-mm 1340407011
Wrench, 8-mm x 10-mm 1340407012
Wrench, 6-mm x 6-mm 8710-2156
Wrench, 5-mm x 5-mm 8710-2157
Cutters/Crimpers/Strippers
Diagonal Cutters
Crimper/Wire Strippers
Tubing Cutters
Restek #20193 http://www.restekcorp.com
Agilent 8710-1709
Agilent precision tubing cutter for 1/16-in. SS tubing
5190-1442
Alternate for Europe:
HICHROM Ltd - Part No: HI-196
Description: Tubing Cutters - Price: 17.00
1 The Markham Centre Station Road Theale, Berkshire
RG7 4PE, UK Telephone: +44 (0) 118 930 3660
mailto:
[email protected]22
7890 Series GC IPB
Before Servicing the Instrument
Pliers
Channel lock pliers
Slip-joint pliers
Needle nose pliers
Agilent needle nose pliers 8710-0004
Agilent Truarc pliers 8710-0018
7890 Series GC IPB
23
Before Servicing the Instrument
Specialized tools for GC support
FID Flow Tool 19301-60660
FID Cleaning Kit 9301-0985, (.010-inch Guitar String)
Injection Port Cleaning Kit 480-0003
24
7890 Series GC IPB
Before Servicing the Instrument
12 Piece File Kit RSF-1200
(Ferrule Removal tool, not shown 440-1000)
Fiberglass Tape 0460-0186
PTFE Tape 0460-0016
White Gloves 8650-0030
NPT Adapter 0100-0118
5/16-inch by #20 Thread Chaser (Die), to clean 1/8-inch
Swagelok threads Other Supplier
On/Off Valve, 1/8-inch Ball Valve 0100-2144
Exacto Knife
Metric (8710-0641) and English Allen Wrench Hex Keys
Pin Vise and small drill bit
Tweezers 8710-0007
Micro Probes (Sharp Object) RMP-5005 Qty 5
Inspection Mirror 707-0027
1.25-inch socket and ratchet for removing FID brass
retaining nut
Column cutter wafer, 4/pk 5181-8836
6890 inlet wrench 19251-00100
7890 inlet wrench (for SSL and MMI) G3452-20512
7890 Series GC IPB
25
Before Servicing the Instrument
Electronic tools for GC support
Digital Multimeter (Agilent U1231A True RMS shown)
Power Outlet Test Tool (Radio Shack/Sears/Electrical
Supply)
Static Strap 9300-0969 (small) or 9300-0970 (large), 5 ft
cord/clip 9300-0980
Wrist strap, disposable, 4-LG 1-W 9300-1408
Various jumpers and clip leads electronic supply
ESD mat 9300-1484
Useful Cables not shown:
Crossover LAN Cable 5183-4649
9 Pin RS-232 Null Modem Cable G1530-60600
USB/RS-232 adapter cable 8121-1013
Sensor pin extractor 8710-1542
26
7890 Series GC IPB
Before Servicing the Instrument
7890 Series GC IPB
27
Before Servicing the Instrument
Pneumatic tools for GC support
28
7890 Series GC IPB
Before Servicing the Instrument
Electronic Leak Detector
G3388B (or G3388A)
5182-9646, 120 VAC
5182-9648, 220 VAC (Agilent)
Rotameter, Porter Model 65
Tube 1: 10-70 cc/min He, Tube 2: 85850 cc/min Air
http://www.porterinstrument.com/indust_21.php
Electronic Flow Meter
Preferred flow meter: Precision gas flow meter, flow range
5500 mL/min 5067-0223
ADM 1000 220-1170
ADM 2000 220-1171-U (Mass Flow Version)
Electronic "Mass" Flow Meter Flow Tracker
Model 1000 Flow Only 5183-4779
Model 2000 with Leak Detector 5183-4780
Universal Power Adapter 5183-4781
White Silicone Tubing:
4 meters 701-0016
7 cm 220-1179
PTFE tubing, 1/8-inch, 1 m long G1290-80050
7890 Series GC IPB
29
Before Servicing the Instrument
For Checking Inlet Pressure
Quality Analog Pressure Gauge (0-100 or 0-60 PSIG) adapted
with a Headspace Probe (301-013-HSP) need NPT adapter
0100-0118 and TCD Ferrules Set 5180-4103, 5182-9673,
5182-3477
Digital Pressure Gauge (0-100 PSIG) Omega Model
HHP-201 Adapted with 1/8-inch NPT adapter 0100-0111, SS
Capillary 5021-1831, Reducing Ferrule 0100-1342 and 530
uM Column Ferrule 5080-8773
NPD Flow adapter - G1534-60640
G1530-20610 - FID/NPD Jet Plug
"No-Hole" Column Ferrules 5181-7458
30
7890 Series GC IPB
Before Servicing the Instrument
FID Flow adapter - 19301-60660
5060-9055 uECD/TCD Detector Plug
Plastic 1/8-inch Swagelok Cap P/N 0100-2414 Qty 3
Replacement Septum Purge Fitting for EPC Module P/N
G2630-61720 (Not included in kit)
7890 Series GC IPB
31
Before Servicing the Instrument
Blanking plug, finger tight, 5020-8294. (Can be used with any
ferrule to duplicate using a no-hole ferrule.)
32
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
2 Inlets
Split/Splitless Inlet 35
Multimode Inlet 43
Cool On-Column Inlet 58
Purged Packed Inlet 65
Programmed Temperature Vaporization Inlet (PTV) 73
Volatiles Interface 87
Solvent Vapor Exit Accessory 93
Agilent Technologies
33
Inlets
Inlet overview
Inlets are a means of introducing a sample into the carrier gas
stream and then into the analyzing column. The term "Inlets"
includes:
Injection ports, for use with a syringe
Sampling valves, both liquid and gas, for high sample size
reproducibility
Vapor inlets, in which the sample is vaporized in an external
sampler, then swept into the GC. Headspace and thermal
desorbers are examples.
Solid samplers
and other devices.
34
7890 Series GC IPB
Inlets
Split/Splitless Inlet
This is the general-purpose inlet for use with capillary columns.
It vaporizes the sample in a heated liner, then delivers all
(splitless mode) or a specified fraction (split mode) of the vapor
to the column.
Replacing the split/splitless inlet
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
WA R N I N G
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
3 Inside the oven, remove interferences as needed: column(s),
the inlet insulating cup, and so forth.
4 Remove the split/splitless top weldment assembly. See
Replacing the split/splitless inlet top weldment assembly.
5 At the top of the GC, remove screws from the injection port
top cover and remove the cover to expose the inlet assembly.
7890 Series GC IPB
35
Inlets
6 Disconnect the split vent line.
7 Disconnect the sensor/heater cable and work it back through
any interfering wiring, tubing, and/or GC frame members.
8 Remove 3 screws to release the inlet body assembly with its
insulation and cup and lift the assembly from the GC.
36
7890 Series GC IPB
Inlets
9 Replacing the inlet assembly is the reverse of these steps. Pay
attention to rotational orientations of the inlet body, the
preformed insulation and its cup, and positions of the split
vent connection and the heater/sensor cable as you fit the
assembly into the GC.
7890 Series GC IPB
37
Inlets
Replacing the split/splitless inlet top weldment assembly
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Rotate the locking tab to release the top weldment assembly
from the split/splitless inlet.
4 Disconnect tubing connector blocks at the EPC module
locations (T-10 screwdriver). Take care to make sure sealing
O-rings are not dislodged or damaged.
5 Guide the top weldment assembly carefully through any
interfering wiring and/or tubing to remove it from the GC.
6 Reassembly is the reverse of these steps.
38
7890 Series GC IPB
Inlets
Replacing the split/splitless inlet split vent line
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top EPC module cover and the left side panel on
the GC.
4 Remove the inlet cover.
5 Disconnect the split vent line from the inlet and from the
trap canister. At the trap end, use two wrenches against each
other to prevent the trap body from rotating.
CAUTION
When removing/attaching the split vent line at its trap canister,
always use one wrench to support the canister fitting and one to
tighten the nut. Failure to do this could break the seal within the
canister.
6 Remove the split vent line for cleaning or replacement.
7 Replacement is the reverse of these steps.
7890 Series GC IPB
39
Inlets
Replacing the split/splitless inlet split vent filter canister and valve
assembly
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top EPC module cover.
4 Disconnect the cable to the split valve from the inlet EPC
module. See Replacing the split/splitless inlet split vent
line.
40
7890 Series GC IPB
Inlets
5 Disconnect the split vent line. See Replacing the EPC
modules.
6 Loosen the screw securing the canister retainer enough to
rotate it aside. Loosen 2 screws to release the split valve
assembly.
7 The canister and split valve are removed as a unit. Note that
the split valve is now easily accessible for replacement if
needed.
8 Reassembly is the reverse of these steps.
7890 Series GC IPB
41
Inlets
Reinstalling the split/splitless inlet
1 Make sure the heater/sensor assembly is installed and the
inlet insulation sleeve is in place.
2 Install a column nut and blank ferrule on the bottom of the
inlet to prevent insulation contamination, and place the inlet
into the inlet carrier.
NOTE
Make sure the insulation is properly seated around the inlet and that the
heater/sensor wiring harness insulation sleeve is tucked under the top
inlet plate.
3 Retighten the three screws (Torx T-20) to secure the top inlet
weldment plate to the inlet carrier.
4 Reconnect the split vent flow line.
5 Reinstall the top insert assembly (with septum and carrier
lines attached). Line up the tab on the bottom of the top
insert assembly with the hole on the insert weldment
assembly so that the locking tab is on the left. Push down to
connect. Slide the locking tab to the back.
6 Route the septum purge and carrier gas lines along the oven
side of the inlet carrier and into the chassis slots leading to
the EPC module.
7 Seat the heater/sensor leads into the channel on the inlet
carrier.
8 Reconnect the heater/sensor assembly into the provided
connector (front or back) on the left side of the GC.
9 Reinstall the insulated thermal cup and insulation in the GC
oven.
10 Reinstall the inlet cover.
42
7890 Series GC IPB
Inlets
Multimode Inlet
The multimode inlet (MMI) is a programmable temperature
vaporization inlet based off of the standard split-spitless inlet. It
has six modes of operation: split, splitless, pulsed split, pulsed
splitless, solvent vent, and direct. The inlet has the same
internal configuration and dimensions of the split/splitless
inlet, and uses the same liners, consumables, ferrules, O-rings,
and septa as the split/splitless inlet.
The differences include:
Cooling jacket for CO2, LN2, and air cooling
Free-spinning nut for column connection
No gold seal
Like the PTV, the MMI requires a thermocouple PCB and
additional harness connections.
7890A and 7890A+: Due to space limitations (you can only have
one thermocouple PCB in the GC), only one MMI or PTV is
allowed per GC.
7890B: Two MMIs can be installed.
7890 Series GC IPB
43
Inlets
Replacing the multimode inlet
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
WA R N I N G
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
3 Inside the oven, remove interferences as needed: column(s),
the inlet insulating cup, and so forth.
4 Remove the multimode top weldment assembly. See
Replacing the multimode inlet split vent line.
5 At the top of the GC, remove screws from the injection port
top cover and remove the cover to expose the inlet assembly.
44
7890 Series GC IPB
Inlets
6 Disconnect the split vent line.
7 Disconnect the sensor/heater cable and work it back through
any interfering wiring, tubing, and/or GC frame members.
8 Disconnect the plug labeled PCB from the wiring harness.
9 Disconnect the cryo line (use two wrenches against each
other to prevent rotation).
10 Remove 3 screws to release the inlet body assembly with its
insulation and cup and lift the assembly from the GC.
11 Replacing the inlet assembly is the reverse of these steps. Pay
attention to rotational orientations of the inlet body, the
preformed insulation and its cup, and positions of the split
vent connection and the heater/sensor cable as you fit the
assembly into the GC.
7890 Series GC IPB
45
Inlets
Replacing the multimode inlet top weldment assembly
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Rotate the locking tab to release the top weldment assembly
from the multimode inlet.
4 Disconnect tubing connector blocks at the EPC module
locations (T-10 screwdriver). Take care to make sure sealing
O-rings are not dislodged or damaged.
5 Guide the top weldment assembly carefully through any
interfering wiring and/or tubing to remove it from the GC.
6 Reassembly is the reverse of these steps.
46
7890 Series GC IPB
Inlets
Replacing the multimode inlet split vent line
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top EPC module cover and the left side panel on
the GC.
4 Remove the inlet cover.
5 Disconnect the split vent line from the inlet and from the
trap canister. At the trap end, use two wrenches against each
other to prevent the trap body from rotating.
CAUTION
When removing/attaching the split vent line at its trap canister,
always use one wrench to support the canister fitting and one to
tighten the nut. Failure to do this could break the seal within the
canister.
6 Remove the split vent line for cleaning or replacement.
7 Replacement is the reverse of these steps.
7890 Series GC IPB
47
Inlets
Replacing the multimode inlet split vent filter canister and valve
assembly
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top EPC module cover.
4 Disconnect the cable to the split valve from the inlet EPC
module. See Replacing the multimode inlet split vent line.
5 Disconnect the split vent line. See Replacing the EPC
modules.
48
7890 Series GC IPB
Inlets
6 Loosen the screw securing the canister retainer enough to
rotate it aside. Loosen 2 screws to release the split valve
assembly.
7 The canister and split valve are removed as a unit. Note that
the split valve is now easily accessible for replacement if
needed.
8 Reassembly is the reverse of these steps.
7890 Series GC IPB
49
Inlets
Replacing a Multimode CO2 cryo valve
WA R N I N G
High pressure or extremely cold gas. Before replacing the cryo
valve, turn off the cryo line at the source, and depressurize the
cryo line to the GC.
If changing the GC configuration, see Changing the GC
configuration for important information regarding GC
methods. Then proceed with the steps below.
1 Cool down the oven and all heated zones.
2 Turn off all gas flows at their sources.
3 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
50
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
7890 Series GC IPB
Inlets
4 Remove the valve via its two mounting screws accessible
under the removed bracket assembly. See Removing the
MMI cryo/PC board bracket for details.
5 When reinstalling, make sure the valve is oriented correctly
on the bracket with its cryo feed input connection towards
the rear of the GC and that its cable is reconnected to the
nearby PC board.
7890 Series GC IPB
51
Inlets
Replacing the Multimode N2 cryo valve
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the inlet cover and GC left side panel.
4 Remove the N2 cryo feed tube between the cryo valve and the
multimode inlet.
5 Remove two screws from the multimode N2 cryo feed cover
plate. Remove the cover plate.
6 Disconnect the multimode N2 cryo valve cable. If you intend
to replace this cable with a new one, use the existing cable as
52
7890 Series GC IPB
Inlets
a model while you install the new cable, then remove the old
cable.
7 Remove the valve bracket and cryo valve by removing three
screws.
8 Replace the N2 cryo valve assembly by reversing these steps.
9 Reinstall the N2 cryo tube between the valve and the inlet.
7890 Series GC IPB
53
Inlets
Removing the MMI cryo/PC board bracket
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top EPC module cover.
4 Disconnect cables to the multimode heater/cryo PC board.
See Replacing the MMI heater/cryo PC board.
5 If a multimode CO2 valve is present, disconnect its cryo feed
lines (CO2 in / CO2 out).
6 Remove two screws securing the bracket to the GC.
54
7890 Series GC IPB
Inlets
7 Lift the bracket assembly out of the GC working it around
any interfering wiring and/or tubing.
NOTE
The multimode CO2 cryo valve, if present, is also mounted on this bracket.
8 Reassembly is the reverse of these steps.
7890 Series GC IPB
55
Inlets
Replacing the MMI heater/cryo PC board
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top EPC module cover.
56
7890 Series GC IPB
Inlets
4 To remove the heater/cryo PC board, first remove its three
cables: from left-to-right, respectively, the LN2 (liquid
nitrogen) cryo valve cable (if present), the thermocouple
cable, and the heater/sensor cable.
5 Next, remove two T-20 screws securing the board onto its
bracket.
6 Lift the board straight up and out of the GC.
7 Installing the new board is the reverse of these steps.
7890 Series GC IPB
57
Inlets
Cool On-Column Inlet
Cool On-Column (COC) inlets allow the injection syringe to
deposit the liquid sample directly into the capillary column.
This is accomplished by the use of an insert which aligns the
syringe with the capillary column and the syringe needle.
Replacing the COC inlet
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 From inside the oven, remove the column from the inlet
fitting.
4 From the top of the GC, remove the inlet carrier cover (or the
tray/tray bracket, if installed) and the left side cover.
5 Unclip the heater/sensor leads from the connector to the left
of the inlet carrier.
6 Disconnect the inlet plumbing and remove from the chassis
slot leading to the EPC flow module.
7 Disconnect the inlet plumbing pneumatics blocks from the
EPC flow module (Torx T-10).
8 Use a Torx T-20 screwdriver to loosen the three captive
screws that attach the inlet weldment to the top of the inlet
carrier.
9 Slide the inlet up out of the inlet carrier. If necessary, you
can also slide the insulation sleeve off the bottom of the inlet.
10 Reinstallation is the reverse of these steps. Use new O-rings
when reconnecting the pneumatic tubing to the EPC flow
module.
58
7890 Series GC IPB
Inlets
7890 Series GC IPB
59
Inlets
Replacing the COC heater/sensor assembly
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
WA R N I N G
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 If necessary, remove the septum nut, cooling tower and/or
needle guide to provide access to the two screws in the top of
the cooling fin.
NOTE
If desired, you can remove the entire inlet for better access.
4 Remove the screws securing the cooling fin to the inlet
weldment and remove the fin.
5 Lift the heater/sensor leads out of the weldment channel and
lift the assembly out of the inlet.
6 Install the new heater/sensor assembly and reassemble the
inlet. You may need to use tweezers to seat the cable back in
the channel and fully seat the heater/sensor in the weldment.
60
7890 Series GC IPB
Inlets
7890 Series GC IPB
61
Inlets
Replacing an inlet cryo cooling tube
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
NOTE
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
Unless otherwise noted, the installation process is the same for both
LCO2 and LN2 oven cryo valves, and for front or back inlet locations.
Preparation of the inlet
1 Remove the septum retaining nut carefully: there is a small
septum and very small coil spring held in place by the nut.
NOTE
These parts, especially the coil spring, are easily lost. For their safety, it is
recommended that the spring, septum, and septum retainer nut be kept
together in a safe place for later reassembly.
2 Next, remove the heat sink by removing its two screws.
3 If the inlet is secured into the inlet chassis, release its three
mounting screws and pull it straight upwards enough to
expose the full length of the inlet body.
4 If, as you raise the inlet body, there is a large insulation pad
either on the inlet body or in the inlet's mounting hole, it
must be carefully removed to preserve its integrity.
5 Carefully inspect both the inlet mounting flange and the
existing end of the inlet cryo cooling tube to be replaced:
Note the large, round hole in the flange - this is the pass
through for the nozzle end of the inlet cryo cooling tube.
62
7890 Series GC IPB
Inlets
Also note the smaller, square hole with a raised metal tab
adjacent to the round hole - this is a location and
alignment guide. The double right-angle bent portion of
the inlet cryo cooling tube must be routed over the square
hole and against the tab when installation is complete.
6 Remove the old tube from the inlet and entirely from the GC.
Use two wrenches against each other at the T-fitting to avoid
twisting tube.
7 Install the new inlet cryo cooling tube into the opening in the
mounting flange, as noted in step 5.
8 Carefully work the insulation pad onto both the inlet body
and inlet cryo cooling nozzle such that you end with both the
inlet cryo cooling tube and the tube on the inlet body in the
slit provided in the insulation pad (if two precut slits are
present, use one for each tube). Work the pad upwards until
it contacts the inlet mounting flange.
NOTE
In the next step, maintain control over the inlet cryo cooling tube as you
insert and secure the inlet: the tube must not be allowed to slip deeper
into the inlet cavity than as described in the inspection detail item in
steps 3-8: basically, the tube's double right-angle bend must remain in its
described position at all times.
9 Lower the inlet into its prepared location with its three
screws aligned with the holes in the inlet chassis and its
heater/sensor cable sitting in the trough in the inlet chassis.
While doing so, mark where to bend the inlet cryo cooling
tube into its channel across the inlet chassis.
10 Remove the inlet and bend the cryo tube at the marked
location to pass between the inlet chassis and the GC frame.
11 Reinsert the inlet while guiding the inlet cryo cooling tube
through the channel between the inlet chassis and the GC
frame. Again, maintain control over the inlet cryo cooling
tube inside the inlet, as noted above.
12 Start each mounting screw one at a time to insure the inlet is
aligned and screws are properly threaded. Then tighten each
screw in turn evenly until snug and the inlet secured.
13 From the left side of the GC, locate the inlet's heater/sensor
cable and its corresponding connector plug. Tuck the
heater/sensor cable underneath the routing tabs at the side
of the GC and connect it to the heater connector.
7890 Series GC IPB
63
Inlets
14 In the following order, replace the heat sink, coil spring,
septum, and septum retaining nut on the inlet. Route the
inlet cryo cooling tube to the tee attached to the cryo valve.
15 Tighten the swage fitting where the inlet cryo cooling tube
connects to the T-fitting at the oven cryo valve. Use two
wrenches against each other to avoid twisting tubing.
This completes replacement of a inlet cryo cooling tube for a
cool on-column capillary inlet.
64
7890 Series GC IPB
Inlets
Purged Packed Inlet
The purged packed column inlet controls column flow by means
of a forward pressure/flow, electronic proportional control
valve. A forward pressure regulator controls flow out the
septum purge vent. The inlet can be used for packed or capillary
columns. Based on the column you have configured, the inlet
can be operated in either a mass flow controlled mode or a
pressure controlled mode.
Replacing the Purged Packed inlet
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off all gas flows at their sources.
WA R N I N G
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
4 Remove the insulating cup and insulation from inside the
oven.
5 Disconnect the column from the inlet and cap the column to
minimize contamination.
6 Remove the inlet cover.
7890 Series GC IPB
65
Inlets
7 Note and record plumbing and wiring layouts and
connectivity.
8 Remove the assembly stepwise. You will need Torx T-10 and
T-20 drivers.
9 Disconnect the heater/sensor cable.
10 Disconnect the 1/16-inch tubing pair from the EPC module.
11 Remove the three top screws retaining the inlet to the GC.
12 Gently lift the assembly up and out.
13 Insert replacement inlet.
14 Reassembly is the reverse of these steps.
15 Use new O-rings during EPC reconnection.
16 Refer to the figures and photos in this section for guidance.
66
7890 Series GC IPB
Inlets
If the EPC module is disconnected, the inlet can be removed and
replaced.
7890 Series GC IPB
67
Inlets
This housing is designed to accommodate a variety of Agilent
inlets.
Note fibrous insulation within housing. See earlier warning.
68
7890 Series GC IPB
Inlets
7890 Series GC IPB
69
Inlets
Replacing the Purged Packed inlet heater
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
WA R N I N G
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
Heater replacement requires removal of the inlet. Refer to
Replacing the Purged Packed inlet for removal instructions.
70
7890 Series GC IPB
Inlets
With the inlet removed:
1 Remove the tubing nut and column adapter.
2 Remove the bottom nut holding the thermal block.
3 Slide the thermal block off the inlet weldment.
4 Carefully remove the heater and sensor from the thermal
(heater) block.
7890 Series GC IPB
71
Inlets
5 Replace heater/sensor cable assembly with a new unit.
6 Reassembly is the reverse of these steps.
72
7890 Series GC IPB
Inlets
Programmed Temperature Vaporization Inlet (PTV)
In addition to the PTV consumables (inlet adapters, columns,
PTFE ferrules, and septa), the replacement parts in the PTV
inlet assembly are:
The PTV inlet
PTV weldment and front trap assemblies
The filter
The head assembly (septum or septumless)
The cryo shroud on the inlet body (CO2 or liquid nitrogen)
The PTV thermocouple board
The O-rings and restrictors in the gas fitting assembly.
7890 Series GC IPB
73
Inlets
Replacing the PTV inlet
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
The PTV inlet system is removed and replaced as a single unit
consisting of the inlet and split vent trap assemblies connected
via its split vent line.
WA R N I N G
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
1 Remove the top EPC module cover.
2 Remove the inlet cover and GC left side panel.
3 At the inlet, if present, disconnect the cryo line (use two
wrenches against each other to prevent rotation).
74
7890 Series GC IPB
Inlets
CAUTION
When removing/attaching the cryo line use two wrenches: one
wrench to support one fitting and the other to loosen/tighten the
nut. Failure to do this could damage the fitting/tubing.
4 At the inlet, also disconnect the carrier gas line. If equipped
with septum purge, disconnect the purge line from the inlet.
5 At the PTV EPC module, disconnect the split vent valve cable
from the lower right corner of the PC board underneath the
module exposed by lifting the module.
6 Disconnect inlet thermocouple and heater/sensor cables at
the PTV heater/cryo PC board and work them back through
other wiring and tubing to the inlet. Disconnect any
additional cables at the inlet. Note that, if fitted, the PTV LN2
cryo feed tube from the LN2 cryo valve to the inlet may need
to be entirely removed from the GC to provide room for cable
connectors.
7 Release the inlet assembly by removing three screws and
lifting the entire assembly from the GC.
7890 Series GC IPB
75
Inlets
8 In reassembly, pay attention to the following:
Maintain correct orientations of insulation and the inlet
body.
Ensure that the inlet's insulation aligns properly with the
tube for the cryo attachment, if present.
9 Reconnect PTV inlet cables.
10 As necessary, reconnect the split vent line, cryo line, carrier
gas line, and septum purge (if present). Use new O-rings as
needed.
76
7890 Series GC IPB
Inlets
Replacing the PTV inlet cryo jacket
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
WA R N I N G
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
3 Remove the PTV inlet assembly. See Replacing the PTV
inlet.
7890 Series GC IPB
77
Inlets
4 Remove three screws from the underside of the inlet body
assembly securing the cryo jacket to the inlet body.
NOTE
The CO2 cryo jacket (marked "CO2" on its inlet fitting) is different from
the LN2 jacket (marked "N2" on its inlet fitting).
5 Reassembly is the reverse of these steps.
NOTE
78
The inlet body with its heater and sensor are not individually replaceable
parts.
7890 Series GC IPB
Inlets
Replacing the PTV CO2 or LN2 inlet cryo assembly
1 Once the PTV with cooling assembly is removed, the cryo
assembly on the inlet can be replaced.
2 Remove the PTV inlet as described under Replacing the PTV
inlet.
3 Remove the three screws on the cryo assembly from the PTV
inlet, and remove the cryo assembly.
4 Install the new cryo assembly over the inlet body. Be sure to
align the assembly so that the fitting is closest to the wires.
5 Reassembly is the reverse of these steps.
6 Check for leaks.
7890 Series GC IPB
79
Inlets
Replacing a PTV CO2 cryo valve
If changing the GC configuration, see Changing the GC
configuration for important information regarding GC
methods. Then proceed with the steps below.
1 Cool down the oven and all heated zones.
2 Turn off all gas flows at their sources.
3 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
4 Remove the valve via its two mounting screws accessible
under the removed bracket assembly. See Removing the PTV
cryo/PC board bracket for details.
5 In reinstallation, make sure the valve is oriented correctly on
the bracket with its cryo feed input connection towards the
rear of the GC and that its cable is reconnected to the nearby
PC board.
80
7890 Series GC IPB
Inlets
Replacing the PTV N2 cryo valve
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the inlet cover and GC left side panel.
7890 Series GC IPB
81
Inlets
4 Remove the N2 cryo feed tube between the cryo valve and the
PTV inlet.
5 Remove two screws from the PTV N2 cryo feed cover plate.
Remove the cover plate.
6 Disconnect the PTV N2 cryo valve cable. If you intend to
replace this cable with a new one, use the existing cable as a
model while you install the new cable, then remove the old
cable.
7 Remove the valve bracket and cryo valve by three screws.
8 Replace the N2 cryo valve assembly by reversing these steps.
9 Reinstall the N2 cryo tube between the valve and the inlet.
82
7890 Series GC IPB
Inlets
Removing the PTV cryo/PC board bracket
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top EPC module cover.
4 Disconnect cables to the PTV heater/cryo PC board. See
Replacing the PTV heater/cryo PC board.
5 If a PTV CO2 valve is present, disconnect its cryo feed lines
(CO2 in / CO2 out).
6 Remove two screws securing the bracket to the GC.
7 Lift the bracket assembly out of the GC working it around
any interfering wiring and/or tubing.
7890 Series GC IPB
83
Inlets
NOTE
The PTV CO2 cryo valve, if present, is also mounted on this bracket.
8 Reassembly is the reverse of these steps.
84
7890 Series GC IPB
Inlets
Replacing the PTV heater/cryo PC board
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top EPC module cover.
7890 Series GC IPB
85
Inlets
4 To remove the heater/cryo PC board, first remove its three
cables: from left-to-right, respectively, the LN2 (liquid
nitrogen) cryo valve cable (if present), the thermocouple
cable, and the heater/sensor cable.
5 Next, remove two T-20 screws securing the board onto its
bracket.
6 Lift the board straight up and out of the GC.
7 Installing the new board is the reverse of these steps.
86
7890 Series GC IPB
Inlets
Volatiles Interface
The Volatiles Interface (VI) uses a controlled stream of gas to
transfer a vaporized sample from an external sampler
(headspace, purge and trap, thermal desorber, etc.) to a
capillary column.
Replacing or cleaning the volatiles interface
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Disconnect the transfer line. Loosen the nut with a 1/4-inch
wrench and remove the line. Remove the clamping plate from
the interface by loosening the captive screw with a T-20 Torx
screwdriver. Put the plate in a safe place.
4 Lift the interface out of the heater block.
5 If a column is installed, remove it.
6 Remove the split and pressure sensing lines by loosening the
hex nuts with the wrench.
7 Clean or replace the interface. If cleaning the interface,
sonicate it twice and then rinse.
8 Reinstall the split line and pressure sensing lines and finger
tighten the hex nuts. Tighten the hex nuts an additional 1/4
turn with the wrench.
9 Reinstall the column in the interface.
10 Place the interface in the heater block. Replace the clamping
plate and tighten the screw until snug. Do not overtighten.
11 Reinstall the transfer line. Finger tighten the nut and then
tighten an additional 1/4 turn with the wrench.
NOTE
7890 Series GC IPB
If the transfer line is from a TMR-8900 Purge and Trap, install the transfer
line support nut assembly up and inside the metal sleeve of the heated
line assembly to prevent damage to the fused silica line.
87
Inlets
12 After the column is installed at both the interface and the
detector, establish a flow of carrier gas through the interface
and maintain it for 10 to 15 minutes. Check for leaks. Heat
the interface to operating temperatures and retighten the
fittings, if necessary.
88
7890 Series GC IPB
Inlets
7890 Series GC IPB
89
Inlets
Replacing the volatiles interface heater/sensor assembly
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Disconnect the transfer line. Loosen the nut with a 1/4-inch
wrench and remove the line.
4 Remove the heater/sensor wire connector from the GC
connection.
5 Remove the three screws in the top plate of the volatiles
assembly which mount it in the GC using a T-20 Torx
screwdriver. Loosen each screw a little at a time.
6 Remove the top plate and the top insulation from the GC.
7 Remove the heater/sensor assembly and replace.
8 Reinstall the top insulation and the top plate. Align the
volatiles interface with the mounting holes.
9 Reinstall the three Torx screws. Tighten each screw once
with the T-20 Torx screwdriver until the interface is properly
aligned. Tighten each screw again until snug.
10 Reinstall the heater/sensor wire connector in the GC. Route
the wire as shown.
11 Reinstall the transfer line using a 1/4-inch wrench and check
for leaks.
90
7890 Series GC IPB
Inlets
Figure 1
7890 Series GC IPB
Cable routing
91
Inlets
Calibrating the interface
The interface's flow module contains a pressure sensor that
must be zeroed after it is installed on your GC. This calibration
procedure ensures an accurate interface pressure display.
Do not connect the carrier gas to the flow module until you have
zeroed the interface's pressure sensor.
1 Plug in the GC and turn it on, if you haven't already done so.
2 Wait 15 minutes. This allows the GC to reach thermal
equilibrium.
3 Zero the interface's pressure sensor:
a Press [Options], scroll to Calibration and press [Enter].
b Scroll to the module to be zeroed and press [Enter].
c Scroll to a zero line and press [Info]. The GC will remind
you of the conditions necessary for zeroing that specific
sensor.
Flow sensors. Verify that the gas is connected and flowing
(turned on).
Pressure sensors. Disconnect the gas supply line at the back of
the GC. Turning it off is not adequate; the valve may leak.
d Press [On/Yes] to zero or [Clear] to cancel.
4 Turn off the GC.
5 Plumb the carrier gas to the flow module. If you need help
with this step, see the GC site preparation and installation
manuals.
6 Turn on the GC.
7 Configure the column and carrier gas.
92
7890 Series GC IPB
Inlets
Solvent Vapor Exit Accessory
This accessory vents the carrier gas and solvent vapor to waste
for a controlled time after injection. This greatly reduces the
size of the solvent peak.
7890 Series GC IPB
93
Inlets
Replacing the SVE valve/fitting assembly
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is plugged in. Avoid a potentially dangerous shock
hazard by unplugging the power cord before removing the side
panels.
Prevent electrostatic voltages from damaging the GC by using an
ESD wriststrap.
1 Turn off the GC and unplug the power cord. Allow time for
all heated zones to cool and then turn off supply gases at
their sources.
2 Remove the top cover, the pneumatics cover, the electronics
carrier cover, and the right side cover.
3 Remove the bleed restrictor column and the solvent vent
waste line from the valve fitting assembly.
4 Inside the oven, disconnect the transfer line from the
stainless union on the 1/16-inch stainless steel tubing.
Carefully remove the tubing from the oven through the
cutout in the top of the oven.
5 Disconnect the valve driver cable from the valve jumper cable
or valve driver assembly, as applicable.
6 Remove the mounting screw in the valve/fitting assembly and
remove the assembly from the GC.
7 Install the new valve/fitting assembly and mount it to the GC
oven with the screw. Cover the open end of the union to
avoid contamination and route the 1/16-inch stainless steel
tubing and union into the oven. Repack the insulation
around the cabling. Connect the valve driver cable to the
valve jumper cable or valve driver assembly, as applicable.
8 Use a new graphite/Vespel ferrule to reconnect the transfer
line to the union.
9 Examine the bleed restrictor column. If the column is
damaged, replace it with a new 0.5 m length of 0.050 mm
column, installing a new fitting and ferrule. Be sure to trim 5
to 10 mm off the end of the new column after installing the
new fitting and ferrule.
10 Reattach the solvent waste vent line.
94
7890 Series GC IPB
Inlets
WA R N I N G
Because a significant amount of solvent is vented through the
SVE valve assembly, it is important that the bleed restrictor and
the solvent vent are connected to an appropriate laboratory
ventilation system.
11 Check for leaks.
7890 Series GC IPB
95
Inlets
Replacing the SVE bleed restrictor column
1 Turn off the GC and unplug the power cord. Allow time for
all heated zones to cool and then turn off supply gases at
their sources.
2 Remove the top cover and the right side cover. If necessary,
also remove the pneumatics cover and the electronics carrier
cover.
3 Using a wrench, remove the old bleed restrictor column.
4 Cut a 0.5 m section off of the new 50 m bleed column for use
as the restrictor.
5 Attach a male fitting and ferrule to the restrictor column,
then trim 5 to 10 mm from that end of the column.
6 Connect the 0.5 m x 50 m bleed restrictor to the SVE valve.
7 Make a loop (or loops) in the excess column protruding from
the valve and move it to an unobstructive position.
Coil it in a loose coil (approximately 6 inch diameter).
Secure the coil with heat resistant tape or equivalent.
96
7890 Series GC IPB
Inlets
Replacing the SVE tri-column assembly
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Disconnect the Tri-column assembly from the COC inlet,
detector and (SS) union and remove the column assembly
from the GC oven.
4 Install the new SVE Tri-column assembly onto a column
hanger and hang the assembly inside the GC oven. Position
the column assembly so that the end of the retention gap
(530 m) is located under the COC inlet and the end of the
analytical column (250 m) is under the detector.
5 Connect the retention gap to the COC inlet using a graphite
ferrule and a column nut.
6 If using a MSD, connect the analytical column (HP-5MS) to
the MSD using a column nut (part no. 05988-20066) and a
graphite/Vespel ferrule (part no. 5062-3508). If using any
other type of detector, connect the analytical column
(HP-5MS) to the GC detector using a column nut (part no.
5181-8830) and a graphite/Vespel ferrule (part no.
5062-9527).
7 Remove the stainless ferrules from the union. Use a
graphite/Vespel ferrule to connect the 0.5 m 320 m
transfer line from the quartz Y-splitter of the Tri-column
assembly to the unused end of the stainless union located
inside the GC oven.
8 Check all of the connections for leaks using an electronic
leak detector.
7890 Series GC IPB
97
Inlets
Replacing the SVE pre-column assembly
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Disconnect the Tri-column assembly from the COC inlet, the
detector and the stainless steel union and remove the
column assembly from the GC oven.
4 Using a column cutter, cut the transfer column and the
analytical columns as close to the quartz Y-splitter as
possible. Be sure to cut the columns straight.
5 Using the column cutter, trim the ends of the tri-column
assembly ensuring that the cuts are straight. Then use a lint
free wipe and methanol to clean any dirt and finger prints
from approximately three to four centimeters from each of
the five column ends.
6 Being careful not to touch the ends of the columns, insert
them into the quartz splitter as far as possible, making sure
that the column ends are making contact with the inside
walls of the splitter. Sufficient pressure should be applied to
give a good seal. Too much pressure, on the other hand, can
damage the polyimide layer or even the column and result in
leakage. Test to see that the column has been installed
correctly by trying to pull the column out of the splitter using
medium force. If the column comes out easily, trim the end
and insert again.
NOTE
A concentric circle inside the splitter should result if the column is
installed correctly.
7 After connecting the column ends into the quartz splitter,
reconnect the tri-column assembly inside the GC oven and
increase the column head pressure incrementally to the
desired pressure. An incremental increase is better than
immediately applying the total column head pressure to
avoid a "shock" that can loosen the connection.
98
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
3 Detectors
Detector overview 100
About the detector signal boards 100
Accessing detector signal boards 103
Replacing detector signal boards 104
Detector signal board, bad checksum error 107
Flame Ionization Detector (FID) 113
Nitrogen Phosphorus Detector (NPD) 132
Thermal Conductivity Detector (TCD) 148
Micro-cell Electron Capture Detector (uECD) 152
Flame Photometric Detector (FPD) 7890A 160
Agilent Technologies
99
Detectors
Detector overview
A detector monitors the gas stream exiting from the analyzing
column. Its electrical output changes when the composition of
the gas does. This section deals with the most widely used
detectors.
About the detector signal boards
The GC can control up to 4 detector signal boards and
simultaneously process their digital signals. Except for a TCD,
all detector boards are mounted in the electronics carrier on the
right-hand side of the GC. A TCD signal board can be mounted
in the optional 3rd detector carrier.
Sometimes other problems seem like a signal board failure.
Replace a signal board only after ruling out other possible
causes as follows:
1 Verify the signal board is receiving 24 VDC power, the green
LED is ON, and the board appears configured in the GC
display.
2 Check diagnostics for faults caused by components
connected to the signal board, such as, ignitors,
electrometers, filaments, and PMTs.
3 Replace the signal board only after eliminating the possible
causes listed in steps 1 and 2.
Repairs should be verified by the following:
Typical detector signal baseline output and noise.
There are 6 types of detector signal boards. Their part numbers
and possible locations are listed in the table below.
100
7890 Series GC IPB
Detectors
7890 Series GC IPB
101
Detectors
Table 2
Table 3
Detector signal boards
Description
Part number
Slot
AIB
G3456-60010
Aux DET1
uECD
G3433-61020
F-DET or B-DET
FID
G3431-60020
F-DET or B-DET
FPD
G3435-60010
F-DET or B-DET or Aux
DET2
NPD
G3434-60020
F-DET or B-DET
TCD
G3432-60010
F-DET or B-DET or Aux
DET1
Detector signal electrical connectors
Description
P1
AIB
Communication buss
uECD
Communication buss
Electrometer
FID
Communication buss
Ignitor
Electrometer
FPD
Communication buss
Ignitor
Signal input
NPD
Communication buss
Bead current
Electrometer
TCD
Communication buss
102
P2
P3
Switching valve
P4
Other
J1 Signal input
P5
P7
S11 High voltage
source for PMT
J4 Filaments
7890 Series GC IPB
Detectors
Accessing detector signal boards
The front and back detector signal boards are located under the
right-hand side panel.
1 Loosen the T-20 captured screws until they do not engage the
electronics carrier.
2 Slide the panel toward the back of the GC and lift off. Place
the tip of the driver in one of the top ventilation slots and
push back.
The 3rd detector signal board is located in the 3rd detector
carrier on the left side of the GC.
1 Remove the 2 T-20 screws from the side panel.
2 Lift the panel (both side and top) off of the carrier.
3 Remove the screw from the detector signal board cover.
Remove the cover.
7890 Series GC IPB
103
Detectors
Replacing detector signal boards
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the right-hand side panel for the electronics carrier.
104
7890 Series GC IPB
Detectors
4 Disconnect the electrical cables to the board.
5 Turn the thumb screw counter-clockwise and lift the screw
to disengage it from the sheet metal.
6 Slide the board down and lift it out.
7890 Series GC IPB
105
Detectors
7 When replacing the signal board, short boards, such as the
FID and uECD, slide into 3 slots. Long boards, such as NPD
and FPD, slide into 4 slots.
8 Push in on the thumbscrew to engage the threads. Turn the
screw clockwise until it is tight.
CAUTION
The grounding point for the signal board is the thumbscrew. If this
screw is not secured, the detector signal will be noisy and may
cause damage to the board.
9 Connect the electrical cables to the board.
10 Turn ON the GC and reconfigure the detector signal board.
See Replacing a GC module for details.
106
7890 Series GC IPB
Detectors
Detector signal board, bad checksum error
It is very possible that you will get error messages at power on.
The messages can be a fault or exception. They are often due to
a checksum error with the detector signal boards. Use the
following instructions to add a serial number and
manufacturing date to the signal board eeprom.
Detector signal boards are programmed and labelled with a
unique ID number along with a manufacturing date. The
following is an example of an FPD signal board. The serial
number is STI190698769.
In some rare occasions, the board ID number or manufacturing
date is not programmed into the board's EEPROM. In these
cases, the GC will post an exception or a "bad checksum error."
In this state, the detector is not usable.
Before you start, you can confirm the problem by trying to view
the information. Navigate to Service Mode > Diagnostics >
Front Detector > Signal board. At the bottom of the table, you
will see the manufacturing date and ID number.
You can perform the following procedure to insert the ID
number and/or date into the EEPROM of the board. You will
need:
PC with a telnet program, such as, HyperTerminal.
LAN cable or cross-over cable.
LAN connection to the GC and IP address for this GC.
The ID number of the board.
Procedure
1 Power off the GC, remove the detector signal board, and
record the serial number.
2 Reinstall the detector signal board and power ON the GC.
7890 Series GC IPB
107
Detectors
3 If necessary, configure the GC and the PC for a LAN
connection.
4 Unlock the keyboard.
5 Launch HyperTerminal or other telnet program.
6 Name the connection and click OK.
7 Select TCP/IP (Winsock) for the connection.
8 Enter the IP address of the instrument and a Port number of
9101.
9 Under the Connection properties select ASCII Setup. Check
the items shown below.
108
7890 Series GC IPB
Detectors
10 The GC will automatically reply with this prompt. Enter go
and press Enter.
7890 Series GC IPB
109
Detectors
11 Type go and press Enter.
12 For an ID number, enter the following string and press enter.
The memory location is 1.
dvcLES<space>< 9 or 8 or 7or 6
><space>1<space>(string)<serial number>
9 for FRONT DET
8 for BACK DET
7 for AUX DET2
6 for AUX DET1 or 3rd detector
13 For a manufacturing date, enter the following string and
press enter. The memory location is 7.
dvcLES<space><9 or 8 or 7 or
6><space>7<space>(int)1134699051
If the process is successful, the GC will respond with a 0.
110
7890 Series GC IPB
Detectors
14 After writing the information to the eeprom, confirm the ID
number and date by entering these strings and pressing
enter.
dvcRES<space>< 9 or 8 or 6 ><space>1<space>(string) and
dvcRES<space><9 or 8 or 7 or 6><space>7<space>(int)
The next steps reconfigure the detector signal board.
15 Press [Config] [Front Det] or [Back Det].
16 Press [Mode/Type] and press [Enter].
17 The GC displays a message prompting to power cycle. Do not
power cycle.
18 Press [Mode/Type] again and press [Enter].
19 Power cycle the GC. Your detector is reconfigured.
7890 Series GC IPB
111
Detectors
If you do not perform steps 14 through 18, the GC will display
the following messages at power ON.
and
112
7890 Series GC IPB
Detectors
Flame Ionization Detector (FID)
The FID is the most widely used of the GC detectors. It responds
to almost all organic compounds (there are a few exceptions),
has good sensitivity and a wide linear range, and is easy to use.
Selecting an FID jet
Open the oven door and locate the column connection fitting at
the base of the detector. It will look like either a capillary
optimized fitting or an adaptable fitting.
If you have an application that tends to clog the jet, select a
jet with a wider tip id.
When using packed columns in high column-bleed
applications, the jet tends to clog with silicon dioxide.
In simulated distillation applications, the high-boiling
hydrocarbons tend to clog the jet.
7890 Series GC IPB
113
Detectors
For capillary optimized fittings, select a jet from the table below,
Jets for capillary optimized fittings.
Table 4
Jets for capillary optimized fittings
Figure 2 ID
Jet type
Part number
Jet tip id
Length
Capillary
G1531-80560
0.29 mm (0.011 inch)
48 mm
High-temperature
(use with simulated distillation)
G1531-80620
0.47 mm (0.018 inch)
48 mm
Figure 2
Capillary optimized jets
For adaptable fittings, select a jet from the table below, Jets for
capillary adaptable fittings.
Table 5
Jets for capillary adaptable fittings
Capillary
adaptable jets ID
Jet type
Part number
Jet tip id
Capillary
19244-80560
0.29 mm (0.011 inch) 61.5 mm
Capillary, high- temperature
(use with simulated distillation)
19244-80620
0.47 mm (0.018 inch) 61.5 mm
Packed
18710-20119
0.46 mm (0.018 inch) 63.6 mm
Packed, wide-bore
(use with high-bleed applications)
18789-80070
0.76 mm (0.030 inch) 63.6 mm
Figure 3
114
Length
Capillary adaptable jets
7890 Series GC IPB
Detectors
Replacing the FID interconnect assembly or spring
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Gather the following:
New FID collector assembly. (See PM kits for the FID.)
T-20 Torx screwdriver
1/4-inch nut driver
Tweezers
Lint-free gloves
4 Shut off the detector and the detector gases and let the
detector cool.
CAUTION
7890 Series GC IPB
To avoid contaminating the FID, wear clean, lint-free gloves when
handling the collector assembly.
115
Detectors
5 Disconnect the ignitor cable assembly.
6 Remove the three screws holding the collector assembly to
the mounting pallet.
CAUTION
116
The next step exposes the interconnect spring. Be careful not to
touch or disfigure the spring while working on the FID. Any dirt or
bending will reduce the sensitivity of your detector.
7890 Series GC IPB
Detectors
7 Lift and remove the assembly from the pallet.
To replace the interconnect spring only
1 Pull the spring off the end of the interconnect. Push a new
spring on.
2 Reassemble the detector.
To replace the interconnect (and spring)
1 Remove the screws at each end of the electrometer body. DO
NOT loosen the screw in the center of the electrometer cover.
2 The interconnect is held by a small spring clip. Remove the
screw holding this clip.
3 Disconnect the ribbon cable that connects the electrometer
to the signal board. Remove the electrometer.
4 There is a hex section where the interconnect enters the
electrometer. Use a wrench to losen and remove the
interconnect.
5 Insert a new interconnect and tighten it firmly (do not
overtighten!).
6 Reassemble the detector.
7890 Series GC IPB
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Detectors
Replacing the heater
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off all gas flows at their sources.
WA R N I N G
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
4 Disconnect the column from the bottom of the detector.
5 Remove the right side electronics panel.
6 Access the FID module by unscrewing the single T-20 screw
holding the GC cover over the detector(s).
7 Raise it out of the way or remove it temporarily.
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8 Disconnect the heater/sensor cable from the heater/sensor
connector.
9 Disconnect the ignitor cable from the FID signal board to the
ignitor castle.
10 Disconnect the electrometer cable from the FID signal board.
7890 Series GC IPB
119
Detectors
11 Unscrew the three captive T-10 screws retaining the FID flow
blocks to the EPC module.
12 Remove the four T-20 screws retaining the FID assembly to
the GC.
13 Lift the entire FID assembly up and off.
14 Lay the assembly down on a clean flat surface.
15 Examine the underside of the detector assembly.
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7890 Series GC IPB
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16 Remove the insulated cover over the heater block.
17 Loosen the heater/sensor cable sufficiently to allow for the
lifting and removal of the heater from the heater block.
18 Carefully remove the defective heater/sensor cable and
replace it with a new heater/sensor cable.
19 Reassembly is the reverse of these steps.
7890 Series GC IPB
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Detectors
Replacing the FID signal board
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off all gas flows at their sources.
WA R N I N G
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
4 Remove the right side electronics panel from the GC.
5 Lift up the GC detector cover to access the FID.
6 Disconnect all electrical connections between the FID and
the signal board.
7 Rotate the FID board thumbscrew counterclockwise, lift the
board up and then downward to remove it from the GC.
8 Replace the defective board with a new FID board.
9 Restore the FID electrical connections.
10 Reassembly is the reverse of these steps.
11 Reconfigure the GC using the front panel keypad, supplying
the requested information.
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7890 Series GC IPB
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Replacing the FID electrometer
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off all gas flows at their sources.
WA R N I N G
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
4 Remove the right side electronics cover.
5 Disconnect the electrometer ribbon cable from the FID signal
board.
6 Remove the Torx T-20 screw and clamp over the interconnect
tube.
7 Remove the two Torx T-20 screws from each end of the
electrometer.
8 Lift the electrometer up and away.
7890 Series GC IPB
123
Detectors
9 Replace the defective electrometer with a new one, making
sure that there is firm contact between the interconnect
spring and the collector.
10 Reassembly is the reverse of these steps.
11 After reassembly, turn the GC power on and reconfigure the
modified detector using the front panel keypad, supplying
the requested information.
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Detectors
Replacing the FID glow plug (ignitor)
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
WA R N I N G
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
3 Remove the right side electronics panel and identify the FID
signal board.
4 Disconnect the ignitor cable from the FID signal board.
7890 Series GC IPB
125
Detectors
5 Lift up or remove the GC detector cover to access the FID.
6 Unclip the ignitor cable from the cable extension to the FID
board.
7 From the top, unscrew the defective ignitor cable from the
ignitor castle.
8 Replace the defective cable with a new ignitor cable.
9 Reassembly is the reverse of these steps.
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7890 Series GC IPB
Detectors
Replacing the entire FID
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off all gas flows at their sources.
WA R N I N G
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
4 Disconnect the column from the bottom of the detector.
5 Remove the right side electronics panel.
6 Access the FID module by unscrewing the single T-20 screw
holding the GC cover over the detector(s).
7 Raise the cover out of the way or remove it temporarily.
8 Disconnect the heater/sensor cable to the FID.
9 Disconnect the ignitor cable from the FID signal board.
10 Disconnect the electrometer cable from the FID signal board.
7890 Series GC IPB
127
Detectors
11 Unscrew the three captive T-10 screws retaining the tubing
connection blocks to the EPC module.
128
7890 Series GC IPB
Detectors
12 Remove the four T-20 screws retaining the FID assembly to
the mounting pallet.
13 Lift the entire FID assembly up and off.
14 At this point the entire unit can be replaced with a new or
repaired unit.
15 Reassembly is the reverse of these steps.
16 After completing the reassembly turn the power on and
reconfigure the GC from the front panel keypad.
7890 Series GC IPB
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Detectors
Ultrasonic cleaning the FID
The collector requires occasional cleaning to remove deposits
(usually white silica from column bleed, or black, carbonaceous
soot). Deposits reduce sensitivity and cause chromatographic
noise and spikes. The cleaning procedure presented here
suggests you use an ultrasonic bath to clean the collector and
other parts of the detector. However, if your collector is not too
dirty, it may be sufficient to scrub it with a nylon brush and
then use a burst of compressed air or nitrogen to blow stray
particles away.
WA R N I N G
This procedure summarizes the general steps for cleaning the
parts. You need to follow the standard safety practices of your
laboratory for handling chemicals. For example, wear the
appropriate safety eye glasses, lab coat, and gloves.
CAUTION
Scratches on the FID jet affects its performance. If you choose to
clean the jet, be sure not to scratch or bend the jet.
CAUTION
The FID castle is coated with a layer of PTFE. Ultrasonic cleaning of
this part for more than 5 to 10 seconds will damage this coating.
It is often more convenient to replace dirty jets with new ones
than to clean them, especially jets that have been badly
contaminated.
1 Gather the following:
Small ultrasonic cleaning bath
Aqueous detergent
GC-grade methanol in a PTFE wash bottle. Wash bottles
made of other materials usually contain plasticizer
contaminants
Dry, filtered, compressed air or nitrogen
Clean cloth
2 If you are cleaning the jet, run the cleaning wire through the
tip of the jet. Run it back and forth a few times until it moves
smoothly. Be careful not to scratch the jet.
130
7890 Series GC IPB
Detectors
3 Place the parts in your glassware, cover them with the
aqueous detergent, and place them in the ultrasonic bath.
4 If you are cleaning the castle, sonicate for only 5 to 10
seconds. Push the wire brush through the collector.
For other parts, sonicate for 1 to 5 minutes.
5 Remove the parts from the bath.
6 Push the wire brush through the collector.
7 Rinse the parts in tap water or distilled water.
8 Rinse all surfaces of the parts in methanol; inside and
outside surfaces. To insure good rinsing use either a PTFE
wash bottle or a beaker.
9 From this point on, handle the parts only with forceps (or
tweezers). Remove the jet from the bath and rinse it
thoroughly with hot tap water and then with a small amount
of methanol.
10 Blow the jet dry with a burst of compressed air or nitrogen
and then place the jet on a clean cloth to air dry.
7890 Series GC IPB
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Detectors
Nitrogen Phosphorus Detector (NPD)
The NPD is a variation on the FID, in that the sample is burned
and the resulting ions are collected. However, the hydrogen/air
ratio is set to suppress carbon ionization and an alkali salt
enhances nitrogen and phosphorus ionization.
Selecting an NPD jet
Open the oven door and locate the column connection fitting at
the base of the detector. It will look like either a capillary
optimized fitting or an adaptable fitting.
If you have an application that tends to clog the jet, select a
jet with a wider tip id.
When using packed columns in high column-bleed
applications, the jet tends to clog with silicon dioxide.
For capillary optimized fittings, select one of the following from
the table below, Jets for capillary optimized fittings.
Table 6
Jets for capillary optimized fittings
Capillary optimized NPD jets ID
Jet type
Part number
Jet tip id
Length
Capillary with extended
jet (recommended)
G1534-80580
0.29 mm (0.011
inch)
51.5 mm
Capillary
G1531-80560
0.29 mm (0.011
inch)
43 mm
High-temperature
G1531-80620
0.47 mm (0.018
inch)
43 mm
132
7890 Series GC IPB
Detectors
Figure 4
Capillary optimized NPD jets
For adaptable fittings, select one of the following from the table
below, Jets for adaptable fittings.
Table 7
Jets for adaptable fittings
Adaptable NPD jets ID
Jet type
Part number
Jet tip id
Length
Capillary with extended jet
(recommended)
G1534-80590
0.29 mm (0.11
inch)
70.5 mm
Capillary
19244-80560
0.29 mm (0.011
inch)
61.5 mm
Capillary, high- temperature
19244-80620
0.47 mm (0.018
inch)
61.5 mm
Packed
18710-20119
0.46 mm (0.018
inch)
63.6 mm
Figure 5
Adaptable NPD jets
7890 Series GC IPB
133
Detectors
Removing the NPD electrometer
Removing the NPD electrometer
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
NOTE
NOTE
Hazardous voltages are present in the mainframe when the GC power
cord is connected. Avoid a potentially dangerous shock hazard by
disconnecting the power cord before removing any GC panels.
Components can be damaged by static electricity: be sure to wear an ESD
strap grounded to the GC chassis while performing this procedure.
3 Remove both the electronics top cover and the right side
cover.
4 Lift up the hinged detector tower cover and remove the Torx
T-20 screw and the clamp on the electrical interconnect.
134
7890 Series GC IPB
Detectors
5 Loosen the three Torx T-10 screws on the lid weldment and
remove the lid.
6 Remove one Torx T-20 screw from each end of the
electrometer. (You do not need to remove the screw on the
top of the electrometer that holds the cover on.)
7 Unlock and detach the electrometer's ribbon cable from the
detector's interface board and lift the electrometer from the
detector pallet.
8 Reassembly is the reverse of these steps.
7890 Series GC IPB
135
Detectors
Replacing the entire NPD
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
WA R N I N G
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
3 Remove the right side electronics panel.
4 Disconnect the column from the bottom of the detector.
5 To access the NPD module unscrew the single T-20 screw
holding the GC cover over the detector(s).
6 Raise it out of the way or remove it temporarily.
7 Disconnect the power/sensor cable to the NPD.
8 Disconnect the electrometer cable from the NPD signal
board.
9 Remove the three T-10 screws fastening the NPD pneumatic
tubing assembly to the EPC module.
10 Remove the four T-20 screws retaining the NPD pallet.
11 Lift the entire NPD unit up and off.
12 At this point the entire unit can be replaced.
13 Reassembly is the reverse of these steps.
136
7890 Series GC IPB
Detectors
14 Restore power and reconfigure the GC using the keypad,
supplying the requested information.
15 Note that the replacement of some NPD components does not
require the complete removal of this detector.
7890 Series GC IPB
137
Detectors
Replacing an NPD signal board
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off all gas flows at their sources.
WA R N I N G
CAUTION
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
Wear lint-free gloves to minimize source contamination when
servicing the bead assembly.
4 Disconnect three electrical connections (to electrometer, to
heater, and the 4-wire communication buss).
5 Turn thumb screw counterclockwise, lift screw to disengage,
slide board down, and then lift out. (Note that the grounding
point for the board is at the thumbscrew.)
6 Insert the replacement board.
7 Reassembly is the reverse of these steps.
8 Reconfigure the modified GC from the front panel keypad,
supplying requested information.
138
7890 Series GC IPB
Detectors
7890 Series GC IPB
139
Detectors
Replacing the NPD heater
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off the oven and all heated zones and let them cool.
4 Turn off all gas flows at their sources.
5 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
6 Disconnect the column from the bottom of the detector.
7 Remove the right side mainframe panel.
8 Access the NPD module by unscrewing the single T-20 screw
holding the GC cover over the detector(s).
9 Raise it out of the way or remove it temporarily.
10 Disconnect the power/sensor cable to the NPD detector.
11 Disconnect the electrometer cable from the NPD signal
board.
12 Remove the three T-10 screws fastening the NPD pneumatic
tubing connectors to the EPC module.
140
7890 Series GC IPB
Detectors
13 Remove the four T-20 screws retaining the NPD assembly to
the GC.
14 Remove the NPD detector assembly from the GC.
15 Examine the underside of the detector assembly.
16 Cover or plug the sample inlet tube while servicing this unit
to limit contamination.
17 Remove the insulated cover over the heater/detector block.
18 Loosen the heater cable sufficiently to allow for the lifting off
and removal of the heater from the detector block.
19 Remove and replace the entire heater/cable assembly.
20 Reassembly is the reverse of these steps.
7890 Series GC IPB
141
Detectors
Replacing the NPD electrometer
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off all gas flows at their sources.
WA R N I N G
CAUTION
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
Wear lint-free gloves to minimize source contamination when
servicing the bead assembly.
4 Remove both the electronics top cover and the right side
cover.
5 Lift up the hinged NPD cover and remove the T-20 screw and
J-clamp on the interconnect assembly.
6 Loosen the three Torx T-10 screws on the lid weldment and
remove the lid.
7 Remove one Torx T-20 screw from each end of the
electrometer. Do not remove the screw on the top of the
electrometer that holds the cover on.
8 Disconnect the power/sensor cable from the bead assembly
and from the NPD signal board.
142
7890 Series GC IPB
Detectors
9 Unlock and detach the electrometer's ribbon cable from the
NPD signal board and lift the electrometer up from the pallet.
10 Reassembly is the reverse of these steps.
11 Reconfigure the modified GC from the front panel keypad,
supplying requested information.
7890 Series GC IPB
143
Detectors
Cleaning the NPD jet and collector
The collector requires occasional cleaning to remove deposits
(usually white silica from column bleed, or black, carbonaceous
soot). Deposits reduce sensitivity and cause chromatographic
noise and spikes. The cleaning procedure presented here
suggests you use an ultrasonic bath to clean the collector and
other parts of the detector. However, if your collector is not too
dirty, it may be sufficient to scrub it with a nylon brush and
then use a burst of compressed air or nitrogen to blow stray
particles away.
WA R N I N G
CAUTION
This procedure summarizes the general steps for cleaning the
parts. You need to follow the standard safety practices of your
laboratory for handling chemicals. For example, wear the
appropriate safety eye glasses, lab coat, and gloves.
Scratches on the NPD jet affects its performance. If you choose to
clean the jet, be sure not to scratch or bend the jet.
It is often more convenient to replace dirty jets with new ones
than to clean them, especially jets that have been badly
contaminated.
1 Gather the following:
Small ultrasonic cleaning bath
Aqueous detergent
GC-grade methanol in a PTFE wash bottle. Wash bottles
made of other materials usually contain plasticizer
contaminates.
Dry, filtered, compressed air or nitrogen
Clean cloth
2 If you are cleaning the jet, run the cleaning wire through the
tip of the jet. Run it back and forth a few times until it moves
smoothly. Be careful not to scratch the jet.
144
7890 Series GC IPB
Detectors
3 Place the parts in your glassware, cover them with the
aqueous detergent, and place them in the ultrasonic bath for
1 to 5 minutes.
4 Remove the parts from the bath and push the wire brush
through the collector.
5 Rinse the parts in tap water or distilled water.
6 Rinse all surfaces of the parts in methanol; inside and
outside surfaces. To insure good rinsing use either a PTFE
wash bottle or a beaker.
7 From this point on, handle the parts only with forceps (or
tweezers). Remove the jet from the bath and rinse it
thoroughly with hot tap water and then with a small amount
of methanol.
8 Blow the jet dry with a burst of compressed air or nitrogen
and then place the jet on a clean cloth to air dry.
7890 Series GC IPB
145
Detectors
Cleaning the NPD
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
WA R N I N G
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
Inlets, detectors, and the oven are insulated with fibrous
materials which may cause irritation to skin, eyes, and/or
mucous membranes. Always wear gloves when working with the
insulation. Additionally, if the insulation is flaky/crumbly, wear
protective eyewear and a suitable breathing mask and/or
respirator.
Wear lint-free gloves to minimize source contamination when
servicing the bead assembly.
3 Remove the right side mainframe panel.
4 To access the NPD module unscrew the single T-20 screw
holding the GC cover over the detector(s).
5 Raise it out of the way or remove it temporarily.
6 Disconnect the power/sensor cable to the NPD.
7 Disconnect the electrometer cable from the NPD signal
board.
8 Remove the three T-20 screws fastening the NPD pneumatic
tubing assembly to the EPC module.
9 Remove the four T-20 screws retaining the NPD assembly to
the GC.
10 Lift entire unit up and off.
11 Place unit on a clean surface.
12 Lift up the hinged metal cover over the detector assembly.
13 Remove the three T-10 screws retaining the bead assembly to
the housing and then remove the bead assembly to prevent
accidental damage.
14 Do not touch the ceramic bead.
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7890 Series GC IPB
Detectors
15 Apply protective cap over the bead assembly, if available.
16 Loosen the three captive T-20 screws retaining the lid.
17 Lift the lid up and off.
18 Using a pair of tweezers, carefully remove the three O-rings,
two alumina insulators, and the collector assembly.
19 At this point one can choose to clean only the parts removed
or continue the disassembly to remove, clean, or replace the
jet.
20 Use a 1/4-inch deep-socket nut driver to unscrew the jet.
21 Use slight side pressure on the nut driver to drag the jet up
out of the detector weldment and then use tweezers to grasp
and remove the jet.
22 Reassembly is the reverse of these steps.
7890 Series GC IPB
147
Detectors
Thermal Conductivity Detector (TCD)
The TCD is sometimes called the "universal" detector because it
responds to anything that is not the carrier gas.
Replacing the TCD detector cell
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Turn off any detector gases at their supply.
4 Shut off the detector and the detector gases and let the
detector cool.
5 Remove the detector cover, the electronics cover, the right
side cover, and the rear top panel.
6 Disconnect the TCD filament leads which run from the
detector to the detector interface card. Disconnect the wires
from the detector interface card using a small flat blade
screwdriver to push down on the connector tabs while you
pull out the wires.
7 Remove the cover and the insulation.
8 Use a T-20 Torx screwdriver to remove the two screws
securing the detector cell to the aluminum detector carrier
bracket and lift the cell from the bracket.
9 Slide the heater/sensor assembly from the detector cell.
10 Slide the PRT out of the detector cell.
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7890 Series GC IPB
Detectors
11 Install the new cell and reassemble the detector. Reassembly
is the reverse of these steps with the following additional
considerations:
Before replacing the insulation, place the cap that came
with your detector over the detector vent to prevent
plugging the vent with insulation. Remove the cap once
the insulation is in place.
12 When replacing the detector cover, make sure that the hole in
the top of the cover is positioned over the detector vent and
that the filaments, plumbing and heater/sensor leads
including the PRT leads are positioned under the
appropriate cut-outs on the sides of the cover.
Make sure that only the filament wire is inserted into the
connector, not the insulation sleeve. Then, check the
filaments by tugging slightly on them.
Check the PRT sensor lead connections to the detector
card by tugging slightly on them.
Replace the heater/sensor and PRT in the sensor holes as
shown below.
CAUTION
7890 Series GC IPB
Make sure the PRT leads are properly installed. If the PRT leads
are not properly installed in the detector card, filament burnout can
occur.
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Detectors
Replacing the TCD switching valve
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the EPC module cover and the module retainer. With
a side-mounted TCD, remove the left side cover.
4 It is possible, but quite difficult, to replace the switching
valve without further disassembly. We recommend raising
the module for better accessibility. With a side-mounted
TCD, remove the module from its bracket.
5 Trace the wires from the valve to the extension cable
connector. Disconnect them.
6 Loosen the screw holding the clamp and slide the old valve
out.
7 Examine the new valve. The plastic part has a flat side with 3
small O-rings. These must be placed over the 3 holes in the
piece to which the screw connects.
8 Slide the new valve into position (flat side against the metal)
and place the clamp over it.
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9 Align the flat end of the valve with the flat metal surface next
to it. Adjust the valve position until it lies flat against the
adjacent metal.
10 Tighten the clamp screw. There should be no gap between the
plastic and the metal. If there is, loosen the clamp screw and
repeat the adjustment.
11 Reconnect the wires and remount the module.
12 Restore the covers.
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Micro-cell Electron Capture Detector (uECD)
This detector simply ignores most compounds, but responds
with enormous sensitivity to electron-accepting species such as
the halogens.
Replacing the uECD heater/sensor assembly
After removing the uECD detector from the GC, you can further
disassemble it to replace the heater/sensor assembly.
WA R N I N G
The ECD micro-cell contains radioactive 63Ni. To reduce the risk
of exposure, wear disposable gloves while handling the ECD
micro-cell. When you are finished, dispose of the gloves and
wash your hands with soap and water.
1 Remove the detector.
2 Loosen the locking tab screw on top of the detector, slide the
locking tab back, and pivot it out of the away.
3 Lift the thermal cover up and carefully slide it off the anode
assembly.
4 Remove the two screws holding the upper heated block onto
the assembly. Lift the block over the anode lead and remove.
5 Slide the heater and sensor out of the lower heated block.
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Replacing the uECD makeup gas adapter
After removing the uECD detector from the GC, you can further
disassemble it to replace the makeup gas adapter. The makeup
gas adapter consists of a line from the detector pneumatics
manifold that carries makeup gas to a weldment that screws
into the bottom of the uECD detector. From there, the makeup
gas sweeps past the end of the column and carries the column
effluent into the uECD cell.
1 Remove the detector.
2 Remove the Torx T-20 screw holding the pneumatics block(s)
to the detector manifold.
3 Slide the makeup gas adapter up and out of the GC.
4 When re-installing the makeup gas adapter, ensure the
following:
Approximately 6 inches of the makeup gas line resides in
the oven after installation.
The makeup gas line is bent into a coil or loop (inside the
oven) that loops around the bottom of the detector
weldment and makeup gas adapter.
The end of the column does not protrude from the top of
the makeup gas adapter. For most columns (outer
diameter > 0.20 mm), insert the column as far as it will go
into the gigabore liner. If using a microbore column (id <
0.20 mm) that passes completely through the liner,
position the column so that the total length from the back
of the capillary nut to the end of the column is about 69 to
71 mm.
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Frequency test
Perform this test to make sure that the base frequency for the
uECD during a blank run indicates a relatively
contaminant-free system. See also the related troubleshooting
manual topic on uECD Life Cycle.
NOTE
It may take 24 hours for the uECD baseline to completely stabilize,
especially if you are starting with a cold system and want to assure
high-sensitivity operation. Therefore, for the most accurate results, run
the detector at normal operating conditions for as long as possible (at
least 2 hours and up to 24 hours) before running the frequency test. If you
will be injecting into an unused inlet, you must use low-bleed septa. Make
sure to condition new septa before use in an inlet for several hours with 1
to 5 mL/min carrier flow.
1 Make sure you are using normal operating conditions and
that at least 2 hours have elapsed since the last run.
2 Turn on the uECD and the corresponding signal.
3 Check the displayed "Output":
< 25 = uECD frequency is acceptable
1000 = Contaminants in system
NOTE
Each display count equals a frequency of 1 Hertz (e.g., a display reading of
100 = 100 Hz.).
4 If the uECD frequency indicates contamination ( 1000)
check for the following:
Contaminated carrier gas trap(s) and or supplyreplace
carrier gas supply tank and any traps on the carrier
supply line.
Insufficient column conditioningfully condition the
column.
Contaminated detectorbake out the detector.
Column, inlet and/or septum bleedclean the
inlet/replace the septum with a conditioned, low bleed
septum.
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Leaksperform leak tests on both the inlet and detector
systems.
Anode current leakagemake sure the anode contacts are
clean. Make sure the anode nut is tight.
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Leak test
NOTE
Once you have determined that the flow system components upstream
from the detector (gas supply tubing, inlet, column fittings) are leak free,
perform the following uECD detector leak test.
1 With the GC on and operating normally, set the oven,
detector, and inlet temperatures to ambient.
2 Turn off the uECD and then turn off the inlet pressure.
3 Turn off the anode and makeup gas flows.
4 Cap the uECD exhaust vent with a vent plug (part no.
5060-9055).
5 Set carrier gas pressure at the inlet corresponding to the
uECD to 15 psi (103 kPa).
6 Wait until the system reaches the setpoint pressure and then
turn off the pressure and monitor the actual pressure value
for at least 10 minutes.
7 Check for pressure drop:
If the pressure stays stable or drops only 0.5 psi, you can
consider the uECD leakfree.
If the pressure drops more than 0.5 psi, you have a leak.
If you are sure none of the upstream flow system components
are leaking, check for leaks at the column fitting and plugged
inlet. If you find leaks, tighten the fittings and repeat the leak
test.
NOTE
158
If you can find no other leaks, the uECD itself is probably leaking. The
uECD cannot be disassembled without special license from the Nuclear
Regulatory Commission or Agreement State Licensing Agency (USA only).
Return the leaking uECD to Agilent for disposal.
7890 Series GC IPB
Detectors
Performing a radioactivity leak test (wipe test)
Micro-cell ECDs must be tested for radioactive leakage at least
every 6 months. Records of tests and results must be
maintained for possible inspection by the Nuclear Regulatory
Commission and/or responsible state agency. More frequent
tests may be conducted when necessary.
The procedure used is the wipe test. A Wipe Test Kit (part no.
18713-60050) is supplied with each new uECD. Refer to the
information card supplied in the Wipe Test Kit for instructions
on performing the wipe test.
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Flame Photometric Detector (FPD) 7890A
The sample is burned in a hydrogen-rich flame. Excited species
rise into a cooler zone above the flame, decay, and give off
characteristic radiation. This is filtered and measured by a
high-gain photomultiplier.
The intense yellow carbon radiation is blocked by a shield
around the flame. Filters select either sulfur or phosphorus
radiation.
Preparing for maintenance
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
To prevent damage to the column or columns, remove the columns
from the GC.
Additional tasks in preparation include:
If you are replacing the transfer line, turn off the source
gases to the FPD detector.
If you are not replacing the transfer line, plug base of
transfer line with a 1/8-inch Swagelok nut to keep it clean.
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Disassembling the FPD
Our objective is to disassemble the detector and prevent it from
getting dirty. We recommend using lint free gloves during most
of these steps.
1 Disconnect the spring and remove the photomultiplier tube
(PMT). Place it in a safe place away from the light. (For a dual
FPD, repeat for the second PMT.)
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2 Remove and set aside the filter in a lint free cloth. For sulfur,
remove the plastic spacer and then the filter. Try tapping the
side of the detector or using the edge of a cotton swab. The
phosphorus filter sits closer to the end of the housing.
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3 Remove the vent or exhaust tube with a 9/16-inch wrench.
4 Remove the 4 screws and detector cover with a Torx T-20
driver.
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Detectors
5 Loosen one screw and remove the ignitor collar with a Torx
T-10 driver. The collar of your ignitor may have 1 or 2 screws.
6 Remove the heater/sensor assembly from the emission block.
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7 The heater/sensor assembly for the dual FPD attaches with a
screw.
8 Remove one screw and retainer for the heater/sensor
assembly in the transfer line with a Torx T-10 Key.
9 Remove the heater/sensor assembly.
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10 Move the heater/sensor assemblies and ignitor cable to the
front of the oven top.
11 Remove two 7-mm mounting nuts from the base of the
transfer line.
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Detectors
12 Loosen 3 screws that hold the optics assembly to the detector
bracket with a Torx T-10 driver.
13 The objective of this step is to separate the optics from the
transfer line. Do not flex the tubing where it is brazed to the
transfer line weldment. Grasp the transfer line with your left
hand and the optics assembly with your right hand. Lift them
just high enough so that the 3 screws that you loosened in
step 11 are above the bracket.
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14 Twist and lift the optics while holding the transfer line
stationary. Carefully separate the assemblies. The O-ring on
the transfer jet is compressed against the inside of the
emissions chamber. This is the resistance that you feel.
15 Place the optic assembly on a lint free cloth.
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16 If you are not replacing the transfer line, skip to the section
Rebuilding the FPD optics assembly. If you are replacing
the transfer line, continue with the next section.
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Rebuilding the FPD optics assembly
Use lint-free gloves when handling the optics assembly and
O-ring seal.
1 Completely loosen the 4 T-10 screws from the clamp and
coupling.
2 Set the Y-shaped clamp to one side.
3 Carefully separate the lens housing from the stainless steel
coupling. The focusing lens and O-ring usually stick to the
coupling, but could stay with the lens housing. Try to keep
the housing, flange ring, screws and washers in place.
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4 Remove the brown O-ring on the lens housing with a small
pick. Roll the new seal over the edge of the housing until it
sits in the groove.
5 Remove the coupling and heat shield disk from the old
emission chamber with a No 1 Pozidrive or Philips
screwdriver. Try to keep the screws, washers, and parts
together.
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6 Assemble the ignitor parts. Slip the stainless steel spacer
over the glow plug, followed by the O-ring. Do not use the
copper washer.
7 Screw the glow plug into the new emission chamber and
tighten with a 5/16-inch wrench.
8 Assemble the new emission chamber, seal, and window.
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9 Position the heat shield and coupling onto the emission
chamber so the threaded hole is aligned with the threaded
fitting for the exhaust tube.
10 Reconnect the parts using the 4 screws and washers. Tighten
opposite screws, similar to a wheel on an automobile, to
insure a good seal.
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11 Turn the lens housing so that it faces the coupling. Insert the
lens and rust colored O-ring.
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Detectors
12 Place the housing onto the coupling and fasten the top screw
just tight enough to keep the parts together.
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13 Hold the y-shaped clamp and start the remaining screws into
the clamp. Do not tighten until step 7 of Reassembling the
FPD.
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Detectors
Reassembling the FPD
This part of the procedure reassembles the optics assembly with
the transfer line, reconnects both to the detector bracket,
replaces the heater/sensor and ignitor wires, replaces the
covers and PMT.
1 Replace or install the O-ring on the transfer line jet. Remove
the O-ring with a small pick. Place the new O-ring over the
jet. Roll it into the groove below the jet.
2 Reposition the detector optics above the bracket.
3 The objective of this step is to reattach the optics to the
transfer line and insure a good seal between the O-ring and
the emissions chamber. Grasp the transfer line with your left
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hand and the optics assembly with your right hand. Push
them together while twisting back and forth.
4 Before lowering the assemblies into the bracket, make sure
there is no gap between the transfer line and the emission
chamber.
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5 Lower the assemblies into the bracket. Line up the holes in
the transfer line base with the threaded posts in the bracket.
Line up the 3 screws and the clamp with the notches in the
detector bracket.
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6 Reattach the transfer line to the bracket with the 7-mm nuts.
7 Tighten the clamp against the detector bracket. Tighten the 3
bottom screws on the optics assembly.
8 Insert the heater/sensor assembly into the transfer line.
Make sure the sensor is at the bottom of the hole.
9 Reinstall the retainer and screw.
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182
Detectors
7890 Series GC IPB
Detectors
10 Insert the heater/sensor assembly into the emission
chamber.
11 Reconnect the ignitor wire to the glow plug.
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12 Replace the cover. First, start the 2 screws on the right-hand
side of the cover. Second, start and tighten the screws at the
base on the left-hand side. Third, tighten the screws on the
right-hand side.
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13 Replace the filter. If you are doing the Agilent checkout, run
the phosphorus filter before the sulfur filter with spacer.
14 Replace the photomultiplier tube (PMT). Connect the spring.
15 Install the new vent tube. Make sure it is tight to prevent light
leaks.
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Detectors
Replacing the FPD
1 Before this can be done you must first disconnect some
cables originating from the FPD board in the electronics
panel.
2 From the side panel side, disconnect heater sensors to the
Aux heater and to the back detector, the ignitor cable, the
high voltage connector, and the PMT signal cable.
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3 Remove the top four T-20 screws retaining the PMT
assembly.
4 Lift up the entire assembly and lay it down on the top GC
surface.
5 Loosen the one screw holding the adjacent cover and pivot
the cover up and off.
6 The FPD is now ready for replacement, if required.
If not, reassembly is the reverse of these steps.
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Detectors
Bake out and run checkout test
This part of the procedure bakes out the detector and restores
conditions. The detector output will level off in about 1 hour
after you restore the conditions. The detector output will
continue to drift down slowly for about 24 hours.
1 Reinstall the column or columns.
2 Reinstall the drain tube to the FPD exhaust tube.
3 Restore the gases to the GC.
4 Restore the power to the GC.
5 Restore the conditions to the inlets and detectors, but turn
off the flame of the FPD to prevent condensation.
6 After the FPD is at temperature for about 10 minutes, light
the flame.
7 Bake out the detector. Set the oven and detector
temperatures to 250C for 15 minutes. Insure there is
adequate gas flows through the column.
8 After the bakeout, restore the oven and FPD conditions.
9 Allow the output to level off.
10 Run a checkout and compare the results.
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Replacing the heater/sensor assemblies
Replacing the heater/sensor assemblies takes about 30 minutes.
It requires you to turn off the GC, remove the vent, and the
detector cover. (If using a dual-wavelength FPD--not available
on all GC models--also remove the left PMT assembly.)
CAUTION
When turning the GC off, turn off the flame first to prevent
condensation from dripping into the jet and column.
You may wish to replace or check the FPD heater/sensor
assemblies for the following reasons:
One or both of the heaters or sensors are defective.
The actual temperature reading on the display of the heaters
is cycling more than 1 C.
Materials needed
G1535-60610 Heater/Sensor assembly with short lead for the
emissions block assembly.
G1535-60620 Heater/Sensor assembly with long lead for the
transfer line.
Procedure
1 Turn off the flame.
2 Turn off the GC.
3 Remove the vent assembly and cover.
4 Put on an ESD wrist strap. Remove the right-side cover to
access the GC electronics. Disconnect the heater/sensor
leads from the auxiliary heater board and the connectors
above the main board.
5 Carefully pull the cables up onto the top of the GC.
Transfer line
1 Use a Torx T-10 driver to remove the screw and retainer clip
holding the lower heater/sensor assembly. Remove the
heater and sensor from the transfer line.
2 Remove the protective cap from the temperature sensor of
the heater/sensor assembly with the short cable.
3 Insert the heater and sensor into the transfer line. Make sure
the sensor is seated at the bottom of the hole. If not, the AUX
temperature will wander above and below the detector
setpoint.
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4 Position the retainer clip over the heater/sensor assembly
and install the screw.
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Emissions block assembly
1 Remove the upper heater and temperature sensor from the
emissions block assembly.
2 Remove the protective cap from the sensor of the
heater/sensor assembly with the long cable.
3 Install the upper heater and sensor in the emissions block
assembly.
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Detectors
Closing up
1 Route the heater/sensor cables out of the bracket as shown.
2 Replace the cover, vent assembly, and, on the
dual-wavelength detector, the left PMT assembly. Refer to
Accessing Heaters and Ignitor.
3 Carefully thread the heater/sensor cables into the electronics
compartment.
4 Put on an ESD wrist strap. Connect the short cable as shown
in Back-top panel cutouts. Connect the long cable to the
auxiliary heater board as shown in Long cable connectors
and leads.
5 Replace the right-side cover to the GC electronics
compartment.
6 Turn on the GC. Confirm that the flame is off.
7 Restore the operating conditions.
8 Wait 20 minutes for the detector to heat up, then ignite the
flame.
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Table 8
7890 Series GC IPB
Long cable connectors and leads
Detector type
Location
Connector
Single-wavelength
Front
A1
Single-wavelength
Back
A2
Dual-wavelength
Back
A2
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Detectors
Replacing the FPD signal board
If changing the GC configuration, see Changing the GC
configuration for important information regarding GC
methods. Then proceed with the steps below.
1 Cool down the oven and all heated zones.
2 Turn off all gas flows at their sources.
3 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
4 Disconnect all attached electrical connections to the FPD
board.
5 Turn thumb screw counterclockwise, lift screw to disengage,
slide board down, and then lift out. (Note that the grounding
point for the board is at the thumbscrew).
6 Replace board if required. (Note that the FPD board is longer
than the FID board and is attached to the full length of the
GC board receptacle.)
7 Replace connections in reverse order of disassembly.
8 Reconfigure the modified GC from the front panel keypad
supplying requested information.
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Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
4 EPC modules
EPC overview 196
Repairing EPC modules 197
Accessing EPC modules 199
Replacing the EPC modules 200
Replacing EPC module proportional valves 203
Inlet modules 205
Detector modules 208
Pneumatics Control Module (PCM) 211
Calibrating the PCM interface 212
Changing the PCM pressure channel frit 213
Correcting PCM leaks 215
Aux EPCs 217
Frits for auxiliary pressure control channels 218
Updating PID Constants 221
Agilent Technologies
195
EPC modules
EPC overview
An Electronic Pneumatic Controller (EPC) module senses gas
pressure or mass flow and controls that pressure or flow.
There are four kinds of EPC modules:
Inlet flow modules
Detector flow modules
Pneumatic control modules (PCM)
Aux EPCs
Inlet and detector modules are each designed for specific inlets
and detectors.
A PCM has two control channels. One is intended for carrier
gas. The other may function as either a forward- or
back-pressure regulator, depending on the external plumbing.
An Aux EPC provides three independent forward-pressure
regulation channels.
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7890 Series GC IPB
EPC modules
Repairing EPC modules
The 7890 Series GC can control up to 6 EPC modules. Each has
a particular purpose and is limited to a particular location in
the EPC carrier. A TCD or AUX EPC module can be located in
the optional 3rd detector carrier.
Repairs on EPC modules should be in this order:
1 Verify the EPC module is receiving 24 VDC power, the green
LED is ON, and the EPC appears configured in the GC
display.
2 Compare the Communication buss connection with an
adjacent module that has a good power and signal
connection.
3 Replace proportional valve or valves for flow or pressure
problems.
4 Replace the module only after 1 and 2 (when dealing with
power issues).
Repairs should be verified by the following:
Zero the pressure channels before performing any
verification tests.
Inlets: With the inlet capped, perform pressure decay test.
With column installed, compare calculated flow reading from
the display with measured flow for column, septum purge,
and split vent.
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EPC modules
Detectors: With the detector capped, compare calculated
flow readings from the display with measured flow for each
gas.
Failure modes for a proportional valve include:
Sticking solenoid plunger causing variable flows.
Electronic open causing no flow. Valve fail in a closed
position.
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7890 Series GC IPB
EPC modules
Accessing EPC modules
1 Turn off all gas flows at their sources.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top rear cover by pressing in the two black side
tabs and lifting the cover up and off.
4 Disconnect the gas plumbing to the module that is being
replaced. If the module is towards the back (slots 2, 4, or 6),
the gas plumbing on the front module may need to be
removed.
NOTE
7890 Series GC IPB
In some cases, it may be necessary to remove the upper rear cover plate.
Do this by first loosening the three retaining T-20 screws along the
bottom and then lifting the cover plate up and off.
199
EPC modules
Replacing the EPC modules
1 Access the EPC module. See Accessing EPC modules.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
2 EPC modules are secured by one or two clamps on the top
edge. Remove the one or two retaining clamps holding the
EPC module in place.
3 Remove the 1/8 inch Swagelok gas supply tubing connections
(1, 2, or 3) from the EPC module.
4 Lift the EPC module up and remove the communication buss
connector. The SSL, PTV, and VI EPC modules also require
removal of an electrical connector to their split vent valves.
This illustration (a split/splitless module) shows these
features.
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7890 Series GC IPB
EPC modules
5 Remove the 1, 2, or 3 tubing block using a T-10 driver. This is
the EPC module for an FID detector.
6 Remove the EPC module by lifting straight up.
7 Install the new EPC module. Remember to plug in the
Communication buss. If a SSL, PTV, or VI inlet module, plug
in the split vent valve.
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EPC modules
8 Remove the O-rings for the pneumatic tubing blocks. Clean
the sealing surface under the O-rings with a lint-free cloth.
Install new O-rings.
9 Install the new pneumatic tubing blocks and tighten the
screws.
10 Turn ON the GC and configure the EPC module. See
Replacing a GC module for details.
11 Zero the flow and/or pressure sensors (Options / Calibration).
12 Verify the flow or pressure control.
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EPC modules
Replacing EPC module proportional valves
This is a generalized procedure for replacing all G3440A and
G3440B EPC proportional valves. Select the valve and valve
part number from EPC Module Parts. Valves come in a kit with
spare O-rings and screws.
1 To protect the column and inlet liner, place the instrument
into Inlet or GC maintenance mode. Let instrument go ready.
2 Turn off instrument.
3 If you need to lift the EPC module to access the wire
connectors, remove 1 or 2 retaining brackets.
4 Lift the EPC module and disconnect the 2-wire connector
from the printed circuit board. The figure shows an Aux EPC
module, which has three proportional valves.
5 Using a T-10 driver, remove the two retaining screws holding
the proportional valve to the EPC module. Save and reuse the
screws if you did not get them in the kit.
6 Remove the valve and the O-rings. Clean the seat of the
O-ring on the flow block with a lint free cloth.
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EPC modules
7 Insert 2 new O-rings.
8 Except for the split vent valve, tie a loose knot in the
proportional valve wire to shorten the wire.
9 Attach the new proportional valve, the electrical connector,
the EPC retaining clamps, and body panels.
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7890 Series GC IPB
EPC modules
Inlet modules
These modules are essentially carrier gas regulators. The SSL,
MMI, VI, and PTV modules have a split vent valve that sits next
to the module..
This is a split/splitless inlet module:
It consists of
One or more proportional valves
Gas tubing connections
A printed circuit board
A connection to the communications buss in the lower left
corner
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EPC modules
Inlet modules
Description
Part number
O-rings
Slot
COC
G3454-60554
1 or 2
PP
G3451-60551
1 or 2
PTV
G3500-60500
1 or 2
S/SL 100 PSI
G3452-60552
1 or 2
S/SL 150 PSI
G3452-60510
1 or 2
VI
G3504-60501
1 or 2
MMI
G3510-60500
1 or 2
The type of proportional valve varies with the module.
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7890 Series GC IPB
EPC modules
Proportional valves
Description
Carrier
Septum purge
Split vent
COC
G3430-67013
G3430-67014
PP
G3430-67013
G3430-67014
PTV
G3430-67013
G3430-67014
G3430-67015
S/SL 100 PSI
G3430-67013
G3430-67014
G3430-67015
S/SL 150 PSI
G3430-67013
G3430-67014
G3430-67015
VI
G3430-67013
G3430-67014
G3430-67015
MMI
G3430-67013
G3430-67014
G3430-67015
Valves require 2 O-rings each (5180-4181, 12/pkg).
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EPC modules
Detector modules
Detector modules often supply multiple detector gases and a
makeup gas. They always control flow by controlling pressure
through a fixed restrictor. This is a typical FID module. FID,
NPD and FPD modules control Air, Hydrogen, and column
makeup. The Hydrogen and makeup are tied together and
mixed. The Air has a separate connection.
The TCD module supplies both carrier and reference gases and
has a switching valve in the reference gas supply.
208
7890 Series GC IPB
EPC modules
Detector modules
7890 Series GC IPB
Description
Part number
Slot
uECD
G3433-60533
3 or 4
FID
G3431-60531
3 or 4
FPD
G3435-60535
3 or 4
NPD
G3434-60502
3 or 4
TCD
G3432-60532
3 or 4 or AUX Det 2
209
EPC modules
Proportional valves
Description
Air
uECD
Makeup
Hydrogen
Reference
G3430-67013
FID
G3430-67013
G3430-67014
G3430-67014
FPD
G3430-67013
G3430-67013
G3430-67013
NPD
G3430-67013
G3430-67014
G3430-67014
TCD
G3430-67013
G3430-67013
Valves require 2 O-rings each (5180-4181, 12/pkg).
210
7890 Series GC IPB
EPC modules
Pneumatics Control Module (PCM)
This module contains two channels.
The PCM carrier channel has both pressure and flow sensors.
It is functionally identical to the Purged Packed inlet flow
module.
The PCM auxiliary channel has only a pressure sensor. When
plumbed normally (gas in at the threaded connector, out via
the tubing), it provides forward pressure regulation. If the
plumbing is reversed, it operates as a back-pressure
regulator.
Table 9
PCM module
Description
Part number
O-rings
Slot
PCM
G3476-60501
1, 2, 5, or 6
Table 10 Proportional valves
7890 Series GC IPB
Description
Carrier
AUX
PCM
G3430-67013
G3430-67016
211
EPC modules
Calibrating the PCM interface
The interface's flow module contains a pressure sensor that
must be zeroed after it is installed on the GC. Calibration
ensures an accurate interface pressure display.
Do not connect the carrier gas to the flow module until you have
zeroed the interface's pressure sensor. For more information on
zeroing the pressure sensor, refer to the 7890A Advanced User
Guide or 7890B Operation Manual.
1 If the gas supply is connected to the GC, turn off the supply
at the source, then disconnect the supply line from the PCM
inlet fitting.
2 Turn on the GC and wait 15 minutes to allow it to reach
thermal equilibrium.
3 When the GC has reached thermal equilibrium, press
[Options], scroll to Calibration and press [Enter].
4 Scroll to the module to be zeroed and press [Enter].
5 Scroll to a zero line and press [Info]. The GC will remind you
of the conditions necessary for zeroing that specific sensor.
Flow sensors. Verify that the gas is connected and flowing
(turned on).
Pressure sensors. Disconnect the gas supply line at the back of
the GC. Turning it off is not adequate; the valve may leak.
6 Press [On/Yes] to zero or [Clear] to cancel.
7 Turn off the GC.
8 Plumb the carrier gas to the flow module.
9 Turn on the GC.
If you were calibrating the flow sensor after replacing the PCM,
check for leaks.
212
7890 Series GC IPB
EPC modules
Changing the PCM pressure channel frit
To change a frit:
1 Gather the following:
O-rings, package of 12, 5180-4181
Restrictor
2 Turn off the gas supply to the channel.
3 Remove the screw holding the tubing block with the output
tubing.
4 Remove the tubing block. Remove the frit and O-ring. Be
careful to avoid scratching the metal surfaces.
5 Remove the other O-ring as well. Replace it with a new
O-ring.
7890 Series GC IPB
213
EPC modules
6 Place a new O-ring on the new frit and press it down into the
block.
7 Place the block on the module and tighten the screw firmly.
8 Restore the gas supply.
214
7890 Series GC IPB
EPC modules
Correcting PCM leaks
1 Use the electronic leak detector to check all areas of the PCM
that are potential sources of a leak.
2 Tighten any connections which are leaking and retest.
NOTE
If the pressure drop is now 0.05 psi/min or less, you can consider the
interface system leakfree.
3 If the interface still leaks, continue to check for and correct
leaks.
7890 Series GC IPB
215
EPC modules
Potential PCM leak areas
Check the following areas when checking for leaks in the PCM.
Flow channel
Two O-rings behind the block where the pneumatic lines
enter the PCM
Two O-rings for the valve in the PCM
Pressure channel
Flatness of tubing block fitting
Two O-rings behind the block where the pneumatic lines
enter the PCM
Two O-rings for the valve in the PCM
Forward pressure valve leaks
Occasionally an increase in pressure, rather than a decrease,
may be observed. This is usually due to slight leakage into the
module across the forward pressure control proportional valve.
Although slight leaks of this nature do not create
chromatographic problems, they may obscure other small leaks
that do cause problems by allowing air into the system. The
valves can leak at about 0.2 mL/min and be within specification.
To check for internal valve leakage (when leak testing the PCM
only):
1 Remove the supply pressure at the carrier inlet fitting, and
quickly cap the fitting with a solid 1/8-inch Vespel plug and a
Swagelok nut.
2 Check the actual pressure on the display and monitor it for 5
minutes. Pressure loss should not be greater than 0.5 psi.
216
7890 Series GC IPB
EPC modules
Aux EPCs
Up to three of these modules can be installed, for a possible
total of 9 pressure-regulated channels. Each channel has a block
connector covering a frit with O-ring for the gas output via the
block connector.
The module is shipped with a brown (low resistance) frit in each
channel.
Table 11 Module
Description
Part number
Slot
AUX
G3470-60501
5 or 6 or AUX
Proportional valves
Table 12 Proportional valves
Description
Air, Makeup, Hydrogen
AUX EPC
G3430-67013
Table 13 Tubing weldment
7890 Series GC IPB
Description
Part number
Pneumatic tubing with block
connector and captive screw
G3430-60550
217
EPC modules
Frits for auxiliary pressure control channels
The auxiliary pressure control channels in the Aux EPC module
are used to provide a flow to various devices including a purged
splitter or a QuickSwap or a headspace sampler. The PCM Aux
channel can be used to provide a flow in forward pressure
control mode.
A replaceable frit is used in these auxiliary channels to optimize
control for the range of flows. The image below shows one of the
three channels.
NOTE
218
Different frits may require different PID constants. See Updating PID
Constants.
7890 Series GC IPB
EPC modules
This table lists the 4 types of frits, their flow characteristics,
and common uses.
Kit
Component
Marking
Flow characteristic
Resistance Often used with
No
G3430-80061
1 ring Brown
Low
Yes
G3430-80062
2 rings Red
Yes
G3430-80063
3 rings Blue
Yes
G3430-20011
None
400 +/- 30 SCCM AIR @ 40
PSIG
30 +/- 1.5 SCCM H2 @ 15
PSIG
3.33 +/- 0.3 SCCM H2 @ 15
PSIG
No restriction
Medium
FID Air, QuickSwap, Splitter, Deans
Switch
FID Hydrogen
High
NPD Hydrogen
Zero
Headspace vial pressurization
Notes for this table
The Air frit, G3430-80061, ships in each channel in the AUX
EPC module. No frit ships in the PCM Aux channel.
Yes indicates this part is included in the AUX module ship kit
and the PCM ship kit.
Always use a new O-ring. 5180-4181, O-rings 12/pk
7890 Series GC IPB
219
EPC modules
Procedure for replacing frit
1 Select the appropriate frit.
2 Gather a new O-ring, a T-10 Torx driver, and a tweezer.
3 Loosen the captured screw for the channel that you want to
change.
4 Lift up the pneumatic tubing block.
5 Replace the O-ring and frit.
6 Replace the pneumatic block and tight the screw.
220
7890 Series GC IPB
EPC modules
Updating PID Constants
Pneumatic PID constants are the coefficients used by the EPC
modules to control flows and pressures. Certain gases or special
applications (such as QuickSwap, Headspace vial
pressurization, or splitter and backflush applications) require
different PIDs than provided at the factory. For the Agilent 7890
Series GC, you must use G4600AA Agilent Instrument Utilities
software to download new PIDs to the EPC modules.
The table below summarizes custom PID values required for
selected applications. Note that if updating an Aux EPC module,
you will need to change the frit for the channel used.
NOTE
7890 Series GC IPB
Application
Module
AUX Frit
Select Available
PID Values
QuickSwap
AUX EPC
G3430-80061
brown or 1 ring
Quickswap
AUX EPC
Purged Splitter
and Deans Switch
when using
Backflush
G3430-20011 no
color or no rings
Quickswap
Purged Splitter
AUX EPC
and Deans Switch
G3430-80061
brown or 1 ring
Standard
Headspace vial
pressurization
AUX EPC
G3430-20011 no
color or no rings
AUX_EPC_Heads
pace
Headspace
sampling loop
PCM in
backpressure
control
NA
PCM_Headspace
The driver for the 7890Series GC will calculate backflush conditions. The
calculation of Hold Times assumes that a zero restrictor is installed in the
AUX EPC channel. If you use an FID Air restrictor the actual hold time will
be less than what the software displays.
221
EPC modules
Updating PID constants
Follow these steps to update the PID constants for any EPC
module (inlet, detector, AUX, or PCM). Use these same
directions to apply special PIDs for use with QuickSwap,
Capillary Flow Technology devices, and Headspace samplers, or
to restore factory defaults.
The PID Constants screen displays (for the selected
instrument):
Currentlists devices (and the associated Module for each)
installed on the selected GC
Versionversion number of the currently-installed PID values
for the selected module
AvailablePID files available for upload to the selected
module
Selected Versionversion number of the Available PID values
selected for update
Statusindicates (after an update) whether or not the PID
values were uploaded to the module successfully
To set your PID values:
1 Close any online data system session for this instrument.
2 Open Instrument Utilities.
3 Select Firmware Update from the software explorer pane.
4 Select the PID Constants tab.
222
7890 Series GC IPB
EPC modules
5 From the Instruments list, select the GC with the module(s)
you wish to update, and click Connect. The list of modules
for this GC will display. The list may not appear immediately.
6 Locate the Module you wish to update. If updating an EPC
AUX or PCM module, determine the specific channel to be
updated.
If you are unsure of the channel to be updated, remove the
pneumatics cover and trace the wiring from the device to
the EPC module. Use the figure below to determine the
module's EPC location.
7890 Series GC IPB
223
EPC modules
7 Select the row of the EPC module (and channel) that you
need to update. This is most often an AUX_EPC module.
8 From the Available selection box, select the appropriate set of
values to download. Note the Selected Version number that
appears. In the example below, we are updating Aux 1 with
QuickSwap PIDs.
9 When finished specifying your desired values, click Update in
the row(s) of the module(s) you wish to update. This will
download the PIDs to the appropriate EPC modules.
224
7890 Series GC IPB
EPC modules
10 If the download is successful, the status will read Values Set
(see below). If the file is not accepted by Instrument Utilities,
the status will read Invalid File. Note that these Status
messages are the only feedback on the success of the PID
update.
The following screen capture illustrates updating PIDs for
QuickSwap.
11 The software writes a log entry for the instrument.
12 Power cycle the GC to activate the new PIDs.
13 If using Instrument Utilities, close the software to remove
your CE key from the customer's system.
7890 Series GC IPB
225
EPC modules
No positive feedback on reconnect
NOTE
The ChemStation driver for the 7890A will calculate backflush conditions.
The calculation of Hold Times assumes that a zero restrictor is installed in
the AUX EPC channel. If you use an FID Air restrictor the actual hold time
will be less than what the software displays.The only feedback on the
success of the update is the message Values Set and an entry in the
software log file.
If you reconnect, you will not see any confirmation that you
updated a PID. For example, if you update one or more AUX
EPC channels to QuickSwap PID values, the screen does not tell
you that the channel has QuickSwap values.
However, the Version number may have changed for all channels.
This number is read from the EPC module. There is only one
version number in each EPC module. If you update one channel
of an AUX EPC module, the version number will be the latest
update. Because there are not a version number for each
channel, it will look like you updated all channels. This is not
correct. The current version does not provide you positive
feedback that you updated one channel. Here is an example
screen after the update of one channel to QuickSwap.
The Selected Version is read from the eeprom file on your PC.
226
7890 Series GC IPB
EPC modules
Updating PID constants available for use by Instrument Utilities
If at any time the PID constant values are updated, follow the
procedure below to update the files within the Instrument
Utilities directory. Perform this procedure before accessing the
PID Constants interface.
1 Obtain the latest EEPROM files.
Browse to where the Instrument Utilities is installed (default is
C:\Program Files\Agilent\Lab Monitor).
1 In this Instrument Utilities directory, browse to
firmware\pneumatic-eeprom.
2 If the latest EEPROM file dates are newer than the files in
this directory:
a Delete the old .xml files.
b Copy the new .xml files into the
firmware\pneumatic-eeprom directory. The directory will
look similar to the one below.
c See "Updating PID Constants" to download these values
to the EPC modules.
7890 Series GC IPB
227
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
5 Performance Verification
About Chromatographic Checkout 229
To Prepare for Chromatographic Checkout 230
To Check FID Performance 232
To Check NPD Performance 238
To Check TCD Performance 244
To Check uECD Performance 250
To Check FPD Performance (Sample 5188-5953) 256
To Check FPD Performance (Sample 5188-5245, Japan) 264
Agilent Technologies
228
Performance Verification
About Chromatographic Checkout
The tests described in this section provide basic confirmation
that the GC and detector can perform comparably to factory
condition. However, as detectors and the other parts of the GC
age, detector performance can change. The results presented
here represent typical outputs for typical operating conditions
and are not specifications.
The tests assume the following:
Use of an automatic liquid sampler. If not available, use a
suitable manual syringe instead of the syringe listed.
Use of a 10-L syringe in most cases. However, a 5-L syringe
is an acceptable substitute for the 1-L injections described
here.
Use of the septa and other hardware (liners, jets, adapters,
and so forth) described. If you substitute other hardware,
performance can vary.
7890 Series GC IPB
229
Performance Verification
To Prepare for Chromatographic Checkout
Because of the differences in chromatographic performance
associated with different consumables, Agilent strongly
recommends using the parts listed here for all checkout tests.
Agilent also recommends installing new consumable parts
whenever the quality of the installed ones is not known. For
example, installing a new liner and septum ensures that they
will not contribute any contamination to the results.
1 Check the indicators/dates on any gas supply traps.
Replace/recondition expended traps.
2 Install new consumable parts for the inlet and prepare the
correct injector syringe (and needle, as needed).
Table 14 Recommended parts for checkout
Recommended part for checkout
Part number
Split splitless inlet
Syringe, 10-L
5181-1267
O-ring
5188-5365
Septum
5183-4757
Liner
5062-3587 or 5181-3316
Multimode inlet
Syringe, 10-L
5181-1267
O-ring
5188-6405
Septum
5183-4757
Liner
5188-6568
Packed column inlet
Syringe, 10-L
5181-1267
O-ring
5080-8898
Septum
5183-4757
Cool on-column inlet
230
Septum
5183-4758
Septum nut
19245-80521
Syringe, 5-L on-column
5182-0836
0.32 mm needle for 5-L syringe
5182-0831
7890 Series GC IPB
Performance Verification
Recommended part for checkout
Part number
7683B Needle support assembly for
.250/.320 mm injections
G2913-60977
Insert, fused silica, 0.32-mm id
19245-20525
PTV inlet
7890 Series GC IPB
Syringe, 10-L -- for septum head
Syringe, 10-uL, 23/42/HP -- for
septumless head
5181-1267
5181-8809
Inlet adapter, Graphpak-2M
5182-9761
Silver seal for Graphpak-2M
5182-9763
Glass liner, multibaffle
5183-2037
PTFE ferrule (septumless head)
5182-9748
Microseal replacement (if installed)
5182-3444
Ferrule, Graphpak-3D
5182-9749
231
Performance Verification
To Check FID Performance
1 Gather the following:
Evaluation column, HP-5 30 m 0.32 mm 0.25 m
(19091J-413)
FID performance evaluation (checkout) sample
(5188-5372)
Chromatographic-grade isooctane (wash solvent)
4-mL solvent and waste bottles or equivalent for
autoinjector
2-mL sample vials or equivalent for sample
Inlet and injector hardware
2 Verify the following:
Capillary column jet installed. If not, select and install a
capillary column jet.
Capillary column adapter installed (adaptable FID only).
If not, install it.
Chromatographic-grade gases plumbed and configured:
helium as carrier gas, nitrogen, hydrogen, and air.
Empty waste vials loaded in sample turret.
4-mL solvent vial with diffusion cap filled with isooctane
and inserted in Solvent A injector position.
3 Replace consumable parts (liner, septum, traps, syringe, and
so forth) as needed for the checkout.
4 Install the evaluation column. (See the procedure for the SS,
MMI, PP, COC, or PTV in the Maintenance manual.)
Bake out the evaluation column for at least 30 min at 180
C. (See the procedure for the SS, MMI, PP, COC, or PTV in
the Maintenance manual.)
Be sure to configure the column.
5 Check the FID baseline output. The output should be
between 5 pA and 20 pA and relatively stable. (If using a gas
generator or ultra pure gas, the signal may stabilize below 5
pA.) If the output is outside this range or unstable, resolve
this problem before continuing.
6 If the output is too low:
Check that the electrometer is on.
Check that the flame is lit.
7 Create or load a method with these parameter values.
232
7890 Series GC IPB
Performance Verification
Table 15 FID checkout conditions
Column and sample
Type
HP-5, 30 m x 0.32 mm x 0.25 m
(19091J-413)
Sample
FID checkout 5188-5372
Column flow
6.5 mL/min
Column mode
Constant flow
Split/splitless inlet
Temperature
250 C
Mode
Splitless
Purge flow
40 mL/min
Purge time
0.5 min
Septum purge
3 mL/min
Gas saver
Off
Multimode inlet
Mode
Splitless
Inlet temperature
75 C
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
250C
Final time 1
5.0 min
Purge time
1.0 min
Purge flow
40 mL/min
Septum purge
3 mL/min
Purged packed inlet
Temperature
250 C
Septum purge
3 mL/min
Cool on-column inlet
Temperature
Oven Track
Septum purge
15 mL/min
PTV inlet
7890 Series GC IPB
Mode
Splitless
Inlet temperature
75 C
233
Performance Verification
Column and sample
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
350 C
Final time 1
2 min
Rate 2
100 C/min
Final temp 2
250 C
Final time 2
0 min
Purge time
0.5 min
Purge flow
40 mL/min
Septum purge
3 mL/min
Detector
Temperature
300 C
H2 flow
30 mL/min
Air flow
400 mL/min
Makeup flow (N2)
25 mL/min
Lit offset
Typically 2 pA
Oven
Initial temp
75 C
Initial time
0.5 min
Rate 1
20 C/min
Final temp
190 C
Final time
0 min
ALS settings (if installed)
234
Sample washes
Sample pumps
Sample wash volume
Injection volume
1 L
Syringe size
10 L
Solvent A pre washes
Solvent A pre washes
Solvent A wash volume
7890 Series GC IPB
Performance Verification
Column and sample
Solvent B pre washes
Solvent B post washes
Solvent B wash volume
Injection mode (7693A)
Normal
Airgap volume (7693A)
0.20
Viscosity delay
0s
Inject dispense speed (7693A)
6000
Plunger speed
Fast (Slow for cool on-column inlet)
PreInjection dwell
PostInjection dwell
Manual injection
Injection volume
1 L
Data system
Path
Setting
Method and Run Control View:
Instrument>Edit
Parameters>Options
Keep instrument keyboard locked
after method is loaded? = No
Method and Run Control View:
Instrument>Edit
Parameters>Signals
Assign Signal 1 to the detector
Choose Save Data All
Data Rate = 5 Hz
8 If using a data system, prepare the system to perform one
run using the loaded checkout method. Make sure that the
data system will output a chromatogram.
9 Start the run.
If performing an injection using an autosampler, start the
run using the data system or press [Start] on the GC.
If performing a manual injection (with or without a data
system):
a Press [Prep Run] to prepare the inlet for splitless injection.
b When the GC becomes ready, inject 1 L of the checkout
sample and press [Start] on the GC.
10 The following chromatogram shows typical results for a new
detector with new consumable parts installed and nitrogen
makeup gas.
7890 Series GC IPB
235
236
Performance Verification
7890 Series GC IPB
Performance Verification
Typical values
The following are typical values for the detector results. The
results for a detector depend on site preparation related
factors. These are not pass/fail criteria.
Components
Typical area counts
C13 and C14
46 pA-sec (area counts)
C15 and C16
460 pA-sec
FID ASTM noise <= .0382 pA
Repeatability (6 runs, first deleted to avoid first run anomalies):
RSD% of RT = 0.01%; <0.0008 m of area <1%.
Split: C13/C16 and C14/C16 sensitivity ratios: >0.95 and <1.05
7890 Series GC IPB
237
Performance Verification
To Check NPD Performance
1 Gather the following:
Evaluation column, HP-5 30 m 0.32 mm 0.25 m
(19091J-413)
NPD performance evaluation (checkout) sample
(18789-60060)
4-mL solvent and waste bottles or equivalent for
autoinjector
Chromatographic-grade isooctane
2-mL sample vials or equivalent for sample
Inlet and injector hardware
2 Verify the following:
Capillary column jet installed. If not, select and install a
capillary column jet.
Capillary column adapter installed. If not, install it.
Chromatographic-grade gases plumbed and configured:
helium as carrier gas, nitrogen, hydrogen, and air.
Empty waste vials loaded in sample turret.
4-mL vial with diffusion cap filled with isooctane and
inserted in Solvent A injector position.
3 If present, remove any protective caps from the inlet
manifold vents.
4 Replace consumable parts (liner, septum, traps, syringe, and
so forth) as needed for the checkout.
5 Install the evaluation column. (See the procedure for the SS,
MMI, PP, COC, or PTV in the Maintenance manual.)
Bake out the evaluation column for at least 30 min at 180
C. (See the procedure for the SS, MMI, PP, COC, or PTV in
the Maintenance manual.)
Be sure to configure the column.
6 Create or load a method with these parameter values.
238
7890 Series GC IPB
Performance Verification
Table 16 NPD checkout conditions
Column and sample
Type
HP-5, 30 m x 0.32 mm x 0.25 m
(19091J-413)
Sample
NPD checkout 18789-60060
Column mode
Constant flow
Column pressure
6.5 mL/min (helium)
Split/splitless inlet
Temperature
200 C
Mode
Splitless
Purge flow
60 mL/min
Purge time
0.75 min
Septum purge
3 mL/min
Multimode inlet
Mode
Splitless
Inlet temperature
60 C
Initial time
0.75 min
Rate 1
720 C/min
Final temp 1
350 C
Final time 1
2 min
Purge time
1.0 min
Purge flow
60 mL/min
Septum purge
3 mL/min
Packed column inlet
Temperature
200 C
Septum purge
3 mL/min
Cool on-column inlet
Temperature
Oven track
Septum purge
15 mL/min
PTV inlet
7890 Series GC IPB
Mode
Splitless
Inlet temperature
60 C
Initial time
0.1 min
239
Performance Verification
Column and sample
Rate 1
720 C/min
Final temp 1
350 C
Final time 1
2 min
Rate 2
100 C/min
Final temp 2
250 C
Final time 2
0 min
Purge time
0.75 min
Purge flow
60 mL/min
Septum purge
3 mL/min
Detector
Temperature
300 C
H2 flow
3 mL/min
Air flow
60 mL/min
Makeup flow (N2)
Makeup + column = 10 mL/min
Output
30 display units (30 pA)
Oven
Initial temp
60 C
Initial time
0 min
Rate 1
20 C/min
Final temp
200 C
Final time
3 min
ALS settings (if installed)
240
Sample washes
Sample pumps
Injection volume
1 L
Syringe size
10 L
PreInj Solvent A Washes
PreInj Solvent B Washes
PostInj Solvent A Washes
PostInj Solvent B Washes
Viscosity delay
7890 Series GC IPB
Performance Verification
Column and sample
Plunger speed
Fast (Slow for cool on-column inlet)
PreInjection dwell
PostInjection dwell
Manual injection
Injection volume
1 L
Data system
Path
Setting
Method and Run Control View:
Instrument>Edit
Parameters>Options
Keep instrument keyboard locked
after method is loaded? = No
Method and Run Control View:
Instrument>Edit
Parameters>Signals
Assign Signal 1 to the detector
Choose Save Data All
Data Rate = 5 Hz
7 If using a data system, prepare the system to perform one
run using the loaded checkout method. Make sure that the
data system will output a chromatogram.
8 Start the run.
If performing an injection using an autosampler, start the
run using the data system or press [Start] on the GC.
If performing a manual injection (with or without a data
system):
a Press [Prep Run] to prepare the inlet for splitless injection.
b When the GC becomes ready, inject 1 L of the checkout
sample and press [Start] on the GC.
9 The following chromatogram shows typical results for a new
detector with new consumable parts installed.
7890 Series GC IPB
241
242
Performance Verification
7890 Series GC IPB
Performance Verification
Typical values
The following are typical values for the detector results. The
results for a detector depend on site preparation related
factors. These are not pass/fail criteria.
Agilent ChemStation
SS/MMI/COC/PTV/PP
Sensitivity
Azobenzene area counts
38
Malathion area counts
71
Agilent ChemstationASTM noise
Measured with GC isothermal @ 100C
10 minute blank run, noise range(s) >1 minute
Performance + noise report
NPD ASTM noise .0765 pA
3396B or 3396C or 3397A integrator sample conditions with
analog input [GC Analog output, Range 0]
>>Set DATE and TIME<<
Zero
10
Pk wd
0.04
Att 2^
Thresh
Cht sp
[Stop time 12.0]
Ar Rej
1000
SS/MMI/COC/PTV/PP
Sensitivity
7890 Series GC IPB
Azobenzene area counts
306,000
Malathion area counts
575,000
243
Performance Verification
To Check TCD Performance
1 Gather the following:
Evaluation column, HP-5 30 m x 0.32 mm x 0.25 m
(19091J-413)
FID/TCD performance evaluation (checkout) sample
(18710-60170)
4-mL solvent and waste bottles or equivalent for
autoinjector
Chromatographic-grade hexane
2-mL sample vials or equivalent for sample
Chromatographic-grade helium as carrier, makeup, and
reference gas
Inlet and injector hardware
2 Verify the following:
Chromatographic-grade gases plumbed and configured:
helium as carrier gas, nitrogen, hydrogen, and air.
Empty waste vials loaded in sample turret.
4-mL solvent vial with diffusion cap filled with isooctane
and inserted in Solvent A injector position.
3 Replace consumable parts (liner, septum, traps, syringe, and
so forth) as needed for the checkout.
4 Install the evaluation column. (See the procedure for the SS,
MMI, PP, COC, or PTV in the Maintenance manual.)
Bake out the evaluation column for at least 30 min at 180
C. (See the procedure for the SS, MMI, PP, COC, or PTV in
the Maintenance manual.)
Be sure to configure the column.
5 Create or load a method with these parameter values.
244
7890 Series GC IPB
Performance Verification
Table 17 TCD Checkout Conditions
Column and sample
Type
HP-5, 30 m 0.32 mm 0.25 m
(19091J-413)
Sample
FID/TCD checkout 18710-60170
Column flow
6.5 mL/min
Column mode
Constant flow
Split/splitless inlet
Temperature
250 C
Mode
Splitless
Purge flow
60 mL/min
Purge time
0.75 min
Septum purge
3 mL/min
Multimode inlet
Mode
Splitless
Inlet temperature
40 C
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
350 C
Final time 1
2 min
Purge time
1.0 min
Purge flow
40 mL/min
Septum purge
3 mL/min
Purged packed inlet
Temperature
250 C
Septum purge
3 mL/min
Cool on-column inlet
Temperature
Oven track
Septum purge
15 mL/min
PTV inlet
7890 Series GC IPB
Mode
Splitless
Inlet temperature
40 C
Initial time
0.1 min
245
Performance Verification
Column and sample
Rate 1
720 C/min
Final temp 1
350 C
Final time 1
2 min
Rate 2
100 C/min
Final temp 2
250 C
Final time 2
0 min
Purge time
0.5 min
Purge flow
40 mL/min
Septum purge
3 mL/min
Detector
Temperature
300 C
Reference flow (He)
20 mL/min
Makeup flow (He)
2 mL/min
Baseline output
< 30 display counts on Agilent
ChemStation (< 750 V)
Oven
Initial temp
40 C
Initial time
0 min
Rate 1
25 C/min
Final temp
90 C
Final time
0 min
Rate 2
15 C/min
Final temp
170 C
Final time
2 min
ALS settings (if installed)
246
Sample washes
Sample pumps
Injection volume
1 L
Syringe size
10 L
PreInj Solvent A Washes
PreInj Solvent B Washes
7890 Series GC IPB
Performance Verification
Column and sample
PostInj Solvent A Washes
PostInj Solvent B Washes
Viscosity delay
Plunger speed
Fast (Slow for cool on-column
inlet)
PreInjection dwell
PostInjection dwell
Manual injection
Injection volume
1 L
Data system
Path
Setting
Method and Run Control View:
Instrument>Edit Parameters>Options
Keep instrument keyboard locked
after method is loaded? = No
Method and Run Control View:
Instrument>Edit Parameters>Signals
Assign Signal 1 to the detector
Choose Save Data All
Data Rate = 5 Hz
6 Display the signal output. A stable output at any value
between 12.5 and 750 V (inclusive) is acceptable.
If the baseline output is < 0.5 display units (< 12.5 V),
verify that the detector filament is on. If the offset is still
<0.5 display units (< 12.5 V), your detector requires
service.
If baseline output is > 30 display units (> 750 V), there
may be chemical contamination contributing to the signal.
Bakeout the TCD. If repeated cleanings do not give an
acceptable signal, check gas purity. Use higher purity
gases and/or install traps.
7 If using a data system, prepare the system to perform one
run using the loaded checkout method. Make sure that the
data system will output a chromatogram.
8 Start the run.
If performing an injection using an autosampler, start the
run using the data system or press [Start] on the GC.
7890 Series GC IPB
247
Performance Verification
If performing a manual injection (with or without a data
system):
a Press [Prep Run] to prepare the inlet for splitless injection.
b When the GC becomes ready, inject 1 L of the checkout
sample and press [Start] on the GC.
9 The following chromatogram shows typical results for a new
detector with new consumable parts installed.
248
7890 Series GC IPB
Performance Verification
Typical values
The following are typical values for the detector results. The
results for a detector depend on site preparation related
factors. These are not pass/fail criteria.
Agilent ChemStation
Sensitivity
C14, C15, C16 area
counts
SS/MMI/COC/PTV
PP
73
65
Discrimination C14/C16 area ratio 1.00 0.10
1.00 0.10
Agilent ChemStationASTM noise
Measured with GC isothermal at 100 C
10 minute blank run, noise range(s) > 1 minute
Performance + noise report
TCD ASTM noise 0.05733 display units (25 V/display unit)
Detector signal set to 5 Hertz
3396B or 3396C or 3397A integrator sample conditions with
analog input (GC Analog output, Range 0)
>>Set DATE and TIME<<
Zero
10
Pk wd
0.04
Att^2
Thresh
Cht sp
Stop time
8.75
Ar Rej
1000
Sensitivity
C14, C15, C16 area
counts
SS/MMI/COC/PTV
PP
585,000
515,000
Discrimination C14/C16 area ratio 1.000.10
7890 Series GC IPB
1.000.10
249
Performance Verification
To Check uECD Performance
1 Gather the following:
Evaluation column, HP-5 30 m x 0.32 mm x 0.25 m
(19091J-413)
uECD performance evaluation (checkout) sample
(18713-60040, Japan: 5183-0379)
4-mL solvent and waste bottles or equivalent for
autoinjector
Chromatographic-grade isooctane
2-mL sample vials or equivalent for sample
Inlet and injector hardware
2 Verify the following:
Clean fused silica indented mixing liner installed. If not,
install it.
Chromatographic-grade gases plumbed and configured:
helium.
Empty waste vials loaded in sample turret.
4-mL vial with diffusion cap filled with hexane and
inserted in Solvent A injector position.
3 Replace consumable parts (liner, septum, traps, syringe, and
so forth) as needed for the checkout.
4 Install the evaluation column. (See the procedure for the SS,
MMI, PP, COC, or PTV in the Maintenance manual.)
Bake out the evaluation column for at least 30 minutes at
180 C. (See the procedure for the SS, MMI, PP, COC, or
PTV in the Maintenance manual.)
Be sure to configure the column.
5 Display the signal output to determine baseline output. A
stable baseline output at any value between 0.5 and 1000 Hz
(ChemStation display units) (inclusive) is acceptable.
If the baseline output is < 0.5 Hz, verify that the
electrometer is on. If the offset is still < 0.5 Hz, your
detector requires service.
If the baseline output is > 1000 Hz, there may be chemical
contamination contributing to the signal. Bakeout the
uECD. If repeated cleanings do not give an acceptable
signal, check gas purity. Use higher purity gases and/or
install traps.
6 Create or load a method with the parameter values listed in
the table below.
250
7890 Series GC IPB
Performance Verification
Table 18 uECD checkout conditions
Column and sample
Type
HP-5, 30 m 0.32 mm 0.25 m
(19091J-413)
Sample
ECD checkout (18713-60040 or
Japan: 5183-0379)
Column mode
Constant flow
Column pressure
6.5 mL/min (helium)
Split/splitless inlet
Temperature
200 C
Mode
Splitless
Purge flow
60 mL/min
Purge time
0.75 min
Septum purge
3 mL/min
Multimode inlet
Mode
Splitless
Inlet temperature
80 C
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
250 C
Final time 1
5 min
Purge time
1.0 min
Purge flow
60 mL/min
Septum purge
3 mL/min
Purged packed inlet
Temperature
200 C
Septum purge
3 mL/min
Cool on-column inlet
Temperature
Oven track
Septum purge
15 mL/min
PTV inlet
7890 Series GC IPB
Mode
Splitless
Inlet temperature
80 C
251
Performance Verification
Column and sample
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
350 C
Final time 1
2 min
Rate 2
100 C/min
Final temp 2
250 C
Final time 2
0 min
Purge time
0.75 min
Purge flow
60 mL/min
Septum purge
3 mL/min
Detector
Temperature
300 C
Makeup flow (N2)
30 mL/min (constant + makeup)
Baseline output
Should be < 1000 display counts in
Agilent ChemStation (< 1000 Hz)
Oven
Initial temp
80 C
Initial time
0 min
Rate 1
15 C/min
Final temp
180 C
Final time
10 min
ALS settings (if installed)
252
Sample washes
Sample pumps
Injection volume
1 L
Syringe size
10 L
PreInj Solvent A Washes
PreInj Solvent B Washes
PostInj Solvent A Washes
PostInj Solvent B Washes
Viscosity delay
Plunger speed
Fast (Slow for cool on-column inlet)
7890 Series GC IPB
Performance Verification
Column and sample
PreInjection dwell
PostInjection dwell
Manual injection
Injection volume
1 L
Data system
Path
Setting
Method and Run Control View:
Instrument>Edit
Parameters>Options
Keep instrument keyboard locked
after method is loaded? = No
Method and Run Control View:
Instrument>Edit
Parameters>Signals
Assign Signal 1 to the detector
Choose Save Data All
Data Rate = 5 Hz
7 If using a data system, prepare the system to perform one
run using the loaded checkout method. Make sure that the
data system will output a chromatogram.
8 Start the run.
If performing an injection using an autosampler, start the
run using the data system or press [Start] on the GC.
If performing a manual injection (with or without a data
system):
a Press [Prep Run] to prepare the inlet for splitless injection.
b When the GC becomes ready, inject 1 L of the checkout
sample and press [Start] on the GC.
9 The following chromatogram shows typical results for a new
detector with new consumable parts installed.
7890 Series GC IPB
253
254
Performance Verification
7890 Series GC IPB
Performance Verification
Typical values
The following are typical values for the detector results. The
results for a detector depend on site preparation related
factors. These are not pass/fail criteria.
Agilent ChemStation Noise ([N3])
Measured by ChemStation, ASTM [N3]
< 3 Hz
Signal
Area, Lindane peak
7500 [N3]
3396B or 3396C or 3397A integrator sample conditions with
analog input [GC Analog output, Range 0]
>>Set DATE and TIME<<
GC Analog output
Noise ([N1])
Measured at [GC Range 0],
[3396 Attn. 3, Chart speed 1, zero 50]
<37 mm for 1 min. measurement
Signal
GC Range 6
3396
Zero
10
Pk wd
0.04
Att 2^
Thresh
Cht sp
Stop time
11.0
Ar Rej
100000
Area, Lindane peak
7890 Series GC IPB
47,950 [N1]
255
Performance Verification
To Check FPD Performance (Sample 5188-5953)
If sample FPD checkout sample 5188-5953 is available, use it to
test FPD performance.
To check FPD performance, first check the phosphorus
performance, then the sulfur performance.
Preparation
1 Gather the following:
Evaluation column, HP-5 30 m x 0.32 mm x 0.25 m
(19091J-413)
FPD performance evaluation (checkout) sample
(5188-5953)
Phosphorus filter
Sulfur filter and filter spacer
4-mL solvent and waste bottles or equivalent for
autoinjector
2-mL sample vials or equivalent for sample
Chromatographic-grade isooctane for syringe wash
solvent
Inlet and injector hardware
2 Verify the following:
Capillary column adapter installed. If not, install it.
Chromatographic-grade gases plumbed and configured:
helium as carrier gas, nitrogen, hydrogen, and air.
Empty waste vials loaded in sample turret.
4-mL vial with diffusion cap filled with isooctane and
inserted in Solvent A injector position.
3 Verify that the Lit Offset is set appropriately. Typically, it
should be about 2.0 pA for the checkout method.
4 Replace consumable parts (liner, septum, traps, syringe, and
so forth) as needed for the checkout.
5 Install the evaluation column. (See the procedure for the SS,
MMI, PP, COC, or PTV in the Maintenance manual.)
Set the oven, inlet, and detector to 250 C and bake out for
at 15 min. (See the procedure for the SS, MMI, PP, COC, or
PTV in the Maintenance manual.)
Be sure to configure the column.
256
7890 Series GC IPB
Performance Verification
Phosphorus performance
1 If it is not already installed, install the phosphorus filter.
2 Create or load a method with the parameter values listed in
the table below.
Table 19 FPD Checkout Conditions (P)
Column and sample
Type
HP-5, 30 m x 0.32 mm x 0.25 m
(19091J-413)
Sample
FPD checkout (5188-5953)
Column mode
Constant pressure
Column pressure
25 psi
Split/splitless inlet
Temperature
200 C Split/splitless
Mode
Splitless
Purge flow
60 mL/min
Purge time
0.75 min
Septum purge
3 mL/min
Multimode
Mode
Splitless
Inlet temperature
75 C
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
250 C
Final time 1
5.0 min
Purge time
1.0 min
Purge flow
60 mL/min
Septum purge
3 mL/min
Purged packed inlet
Temperature
200 C
Septum purge
3 mL/min
Cool on-column inlet
Temperature
7890 Series GC IPB
Oven track (cool on-column)
257
Performance Verification
Column and sample
Septum purge
15 mL/min
PTV inlet
Mode
Splitless
Inlet temperature
75 C
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
350 C
Final time 1
2 min
Rate 2
100 C/min
Final temp 2
250 C
Final time 2
0 min
Purge time
0.75 min
Purge flow
60 mL/min
Septum purge
3 mL/min
Detector
Temperature
200 C (On)
Hydrogen flow
75 mL/min (On)
Air (Oxidizer) flow
100 mL/min (On)
Mode
Constant makeup flow OFF
Makeup flow
60 mL/min (On)
Makeup gas type
Nitrogen
Flame
On
Lit offset
Typically 2 pA
Electrometer
On
Oven
258
Initial temp
70 C
Initial time
0 min
Rate 1
25 C/min
Final temp 1
150 C
Final time 1
0 min
Rate 2
5 C/min
7890 Series GC IPB
Performance Verification
Column and sample
Final temp 2
190 C
Final time 2
4 min
ALS settings (if installed)
Sample washes
Sample pumps
Injection volume
1 L
Syringe size
10 L
PreInj Solvent A Washes
PreInj Solvent B Washes
PostInj Solvent A Washes
PostInj Solvent B Washes
Viscosity delay
Plunger speed
Fast (Slow for cool on-column inlet)
PreInjection dwell
PostInjection dwell
Manual injection
Injection volume
1 L
Path
Setting
Method and Run Control View:
Instrument>Edit
Parameters>Options
Keep instrument keyboard locked
after method is loaded? = No
Method and Run Control View:
Instrument>Edit
Parameters>Signals
Assign Signal 1 to the detector
Choose Save Data All
Data Rate = 5 Hz
3 Ignite the FPD flame, if not lit.
7890 Series GC IPB
259
Performance Verification
4 Display the signal output and monitor. This output typically
runs between 40 and 55 but can be as high as 70. Wait for the
output to level off. This takes approximately 1 hour.
If the baseline output is too high:
Check column installation. If installed high, the stationery
phase burns out and increases measured output.
Check for leaks.
Bake out the detector and column at 250 C.
Wrong flows set for installed filter.
If the baseline output is zero, verify the electrometer is on
and the flame is lit.
5 If using a data system, prepare the system to perform one
run using the loaded checkout method. Make sure that the
data system will output a chromatogram.
6 Start the run.
If performing an injection using an autosampler, start the
run using the data system or press [Start] on the GC.
If performing a manual injection (with or without a data
system):
a Press [ Run] to prepare the inlet for splitless injection.
b When the GC Prepbecomes ready, inject 1 L of the
checkout sample and press [Start] on the GC.
7 The following chromatogram shows typical results for a new
detector with new consumable parts installed.
260
7890 Series GC IPB
Performance Verification
Typical values
The following are typical values for the detector results. The
results for a detector depend on site preparation related
factors. These are not pass/fail criteria.
7890 Series GC IPB
FPD P filter
Typical range after 24
hours
Limits at installation
MDL (pg/sec)
0.06 to 0.08
0.10
Peak area
19000 to 32000
19000
Signal height
5000 to 11000
--
Noise
1.6 to 3.0
Half-width (min)
0.05 to 0.07
--
Output
34 to 80
80
261
Performance Verification
Sulfur performance
1 Install the sulfur filter and filter spacer.
2 Make the following method parameter changes.
Sulfur method parameters (S)
Parameter
Value ( mL/min)
H2 flow
50
Air flow
60
3 Display the signal output and monitor. This output typically
runs between 50 and 60 but can be as high as 70. Wait for the
output to level off. This takes approximately 1 hour.
If the baseline output is too high:
Check column installation. If installed high, the stationery
phase burns out and increases measured output.
Check for leaks.
Bake out the detector and column at 250 C.
Wrong flows set for installed filter.
If the baseline output is zero, verify the electrometer is on
and the flame is lit.
4 If using a data system, prepare the system to perform one
run using the loaded checkout method. Make sure that the
data system will output a chromatogram.
5 Start the run.
If performing an injection using an autosampler, start the
run using the data system or press [Start] on the GC.
If performing a manual injection (with or without a data
system):
a Press [Prep Run] to prepare the inlet for splitless injection.
b When the GC becomes ready, inject 1 L of the checkout
sample and press [Start] on the GC.
6 The following chromatogram shows typical results for a new
detector with new consumable parts installed.
262
7890 Series GC IPB
Performance Verification
Typical values
The following are typical values for the detector results. The
results for a detector depend on site preparation related
factors. These are not pass/fail criteria.
7890 Series GC IPB
FPD S filter
Typical range after 24
hours
Limits at installation
MDL (pg/sec)
3.8 to 5
Peak area
8000 to 19000
8000
Signal height
2500 to 6000
--
Noise
2 to 4
Half-width (min)
0.06 to 0.08
--
Output
34 to 65
70
263
Performance Verification
To Check FPD Performance (Sample 5188-5245, Japan)
To verify FPD performance, first check the phosphorus
performance, then the sulfur performance.
Preparation
1 Gather the following:
Evaluation column, DB5 15 m x 0.32 mm x 1.0 m
(123-5513)
FPD performance evaluation (checkout) sample
(5188-5245)
Phosphorus filter
Sulfur filter and filter spacer
4-mL solvent and waste bottles or equivalent for
autoinjector
2-mL sample vials or equivalent for sample.
Chromatographic-grade isooctane for syringe wash
solvent.
Inlet and injector hardware
2 Verify the following:
Capillary column adapter installed. If not, install it.
Chromatographic-grade gases plumbed and configured:
helium as carrier gas, nitrogen, hydrogen, and air.
Empty waste vials loaded in sample turret.
4-mL vial with diffusion cap filled with isooctane and
inserted in Solvent A injector position.
3 Verify the lit offset is set appropriately. Typically, it should
be about 2.0 pA for the checkout method.
4 Replace consumable parts (liner, septum, traps, syringe, and
so forth) as needed for the checkout.
5 Install the evaluation column. (See the procedure for the SS,
MMI, PP, COC, or PTV in the Maintenance manual.)
Set the oven, inlet, and detector to 250 C and bake out for
at 15 min. (See the procedure for the SS, MMI, PP, COC, or
PTV in the Maintenance manual.)
Configure the column.
264
7890 Series GC IPB
Performance Verification
Phosphorus performance
1 If it is not already installed, install the phosphorus filter.
2 Create or load a method with these parameter values.
Table 20 FPD Phosphorus Checkout Conditions
Column and sample
Type
DB-5MS, 15 m x 0.320 m x 1.0 m
(123-5513)
Sample
FPD checkout (5188-5245)
Column mode
Constant flow
Column pressure
7.5 mL/min
Split/splitless inlet
Temperature
250 C Split/splitless
Mode
Splitless
Total purge flow
69.5 mL/min
Purge flow
60 mL/min
Purge time
0.75 min
Septum purge
3 mL/min
Multimode
Mode
Splitless
Inlet temperature
75 C
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
250 C
Final time 1
5.0 min
Purge time
1.0 min
Purge flow
60 mL/min
Septum purge
3 mL/min
Purged packed inlet
7890 Series GC IPB
Temperature
250 C
Septum purge
3 mL/min
265
Performance Verification
Column and sample
Cool on-column inlet
Temperature
Oven track
Septum purge
15 mL/min
PTV inlet
Mode
Splitless
Inlet temperature
80 C
Initial time
0.1 min
Rate 1
720 C/min
Final temp 1
350 C
Final time 1
2 min
Rate 2
100 C/min
Final temp 2
250 C
Final time 2
0 min
Purge time
0.75 min
Purge flow
60 mL/min
Septum purge
3 mL/min
Detector
Temperature
200 C (On)
Hydrogen flow
75.0 mL/min (On)
Air (oxidizer) flow
100.0 mL/min (On)
Mode
Constant makeup flow Off
Makeup flow
60.0 mL/min (On)
Makeup gas type
Nitrogen
Flame
On
Lit offset
Typically 2 pA
Electrometer
On
Oven
266
Initial temp
70 C
Initial time
0 min
Rate 1
10 C/min
Final temp
105 C
7890 Series GC IPB
Performance Verification
Column and sample
Final time
0 min
Rate 2
20 C/min
Final temp 2
190 C
Final time 2
7.25 min for sulfur
12.25 min for phosphorus
ALS settings (if installed)
Sample washes
Sample pumps
Injection volume
1 L
Syringe size
10 L
PreInj Solvent A Washes
PreInj Solvent B Washes
PostInj Solvent A Washes
PostInj Solvent B Washes
Viscosity delay
Plunger speed
Fast (Slow for cool on-column
inlet)
PreInjection dwell
PostInjection dwell
Manual injection
Injection volume
1 L
Data System
Path
Setting
Method and Run Control View:
Instrument>Edit
Parameters>Options
Keep instrument keyboard locked
after method is loaded? = No
Method and Run Control View:
Instrument>Edit
Parameters>Signals
Assign Signal 1 to the detector
Choose Save Data All
Data Rate = 5 Hz
3 Ignite the FPD flame, if not lit.
7890 Series GC IPB
267
Performance Verification
4 Display the signal output and monitor. This output typically
runs between 40 and 55 but can be as high as 70. Wait for the
output to level off. This takes approximately 1 hour.
If the baseline output is too high:
Check column installation. If installed high, the stationery
phase burns out and increases measured output.
Check for leaks.
Bake out the detector and column at 250 C.
Wrong flows set for installed filter.
If the baseline output is zero, verify the electrometer is on
and the flame is lit.
5 If using a data system, prepare the system to perform one
run using the loaded checkout method. Make sure that the
data system will output a chromatogram.
If performing an injection using an autosampler, start the
run using the data system or press [Start] on the GC.
If performing a manual injection (with or without a data
system):
a Press [Prep Run] to prepare the inlet for splitless
injection.
b When the GC becomes ready, inject 1 L of the checkout
sample and press [Start] on the GC.
6 Start the run.
If performing an injection using an autosampler, start the
run using the data system or press [Start] on the GC.
If performing a manual injection (with or without a data
system):
a Press [Prep Run] to prepare the inlet for splitless injection.
b When the GC becomes ready, inject 1 L of the checkout
sample and press [Start] on the GC.
7 The following chromatogram shows typical results for a new
detector with new consumable parts installed.
268
7890 Series GC IPB
Performance Verification
Typical values
The following are typical values for the detector results. The
results for a detector depend on site preparation related
factors. These are not pass/fail criteria.
7890 Series GC IPB
FPD P filter
Typical range after 24
hours
Limits at installation
MDL (pg/sec)
0.06 to 0.08
0.10
Peak area
19000 to 32000
19000
Signal height
5000 to 11000
--
Noise
1.6 to 3.0
Half-width (min)
0.05 to 0.07
--
Output
34 to 80
80
269
Performance Verification
Sulfur performance
1 Install the sulfur filter.
2 Make the following method parameter changes.
Sulfur method parameters
Parameter
Value ( mL/min)
H2 flow
50
Air flow
60
3 Ignite the FPD flame, if not lit.
4 Display the signal output and monitor. This output typically
runs between 50 and 60 but can be as high as 70. Wait for the
output to level off. This takes approximately 2 hours.
If the baseline output is too high:
Check column installation. If installed high, the stationery
phase burns out and increases measured output.
Check for leaks.
Bake out the detector and column at 250 C.
Wrong flows set for installed filter.
If the baseline output is zero, verify the electrometer is on
and the flame is lit.
5 If using a data system, prepare the data system to perform
one run using the loaded checkout method. Make sure the
data system will output a chromatogram.
6 Start the run.
If performing an injection using an autosampler, start the
run using the system or press [Start] on the GC.
If performing a manual injection (with or without a data
system):
Press [Prep Run] to prepare the inlet for splitless injection.
When the GC becomes ready, inject 1 L of the checkout
sample and press [Start] on the GC.
7 The following chromatogram shows typical results for a new
detector with new consumable parts installed.
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7890 Series GC IPB
Performance Verification
Typical values
The following are typical values for the detector results. The
results for a detector depend on site preparation related
factors. These are not pass/fail criteria.
7890 Series GC IPB
FPD S filter
Typical range after 24
hours
Limits at installation
MDL (pg/s)
3.8 to 5
Peak area
8000 to 19000
8000
Signal height
2500 to 6000
--
Noise
2 to 4
Half-width (min)
0.06 to 0.08
--
Output
34 to 65
70
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Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
6 Configuration
Configuration overview 273
GC modules and the communications buss
To configure an MSD transfer line 283
To configure a valve box 286
Replacing a GC module 288
Removing a GC module 289
Changing the GC configuration 290
Configuration locks 291
Installing new devices 292
Configuring time
280
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272
Configuration
Configuration overview
There are 2 kinds of configuration information: hard and soft.
Hard configuration includes what hardware options are
installed on the GC: the type of inlets and detectors, where
they are located, and what auxiliary heaters are connected.
Soft configuration includes application specific information:
carrier gas type, make up gas type, inlet control modes,
column dimensions.
The GC modules that make up an instrument (i.e., EPC modules,
detector boards, and heaters) are initially configured during
manufacturing. This information is stored in the signal board
memory.
An inlet is configured as an EPC module and a heater.
A detector is configured as an EPC module, a detector signal
board, and a heater.
A pneumatic control module (PCM) is configured as an EPC
module and can be associated with a heater.
An Aux EPC module (AUX) is configured as 3 channels of
auxiliary pressure control and can be associated with a
heater.
A valve box is configured with one or two heaters.
An AUX thermal zone is configured with a heater. For
example, an MSD transfer line or a nickel-catalyst accessory.
There are many custom configuration options available. Most
are explained in G3430-90024, Firmware A.01.05 Instructions
For Channel Partner Devices.
You can configure the GC modules by pressing [Config] and
then pressing the key for the GC module, for example, [Config]
[Front Det]. Under the configuration menu, you will find these
features:
Install or remove the module.
If you wish to ignore a ready or not ready status.
The type of gas that the EPC module is controlling.
The baseline output to use for reigniting the flame.
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273
Configuration
Inlet example
The configuration control table for a front SSL Inlet includes 5
items.
CONFIGURE FRONT INLET
Configured:
Ignore Ready =
Makeup gas type
[ EPC1 ] = (INLET)
FINLET (OK) 68 watts
Split/Splitless
FALSE
He
(SS)
250.0
This list interprets each line of the control table.
Configured: The type of module configured as a front inlet is
an split/splitless capillary inlet.
Ignore Ready: If TRUE, the GC will ignore a Not Ready status.
If the inlet actuals do not match their setpoints, the GC will
go ready. The ignored items are displayed under Status.
This line indicates the EPC module. In this case, it is plugged
into the 4-wire connector labeled EPC1 and is an inlet EPC
module for an split/splitless inlet.
This line describes the heater and sensor. In this case, there
is a 64 watt heater cartridge associated with the front inlet
and the sensor is reading 250.0C.
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7890 Series GC IPB
Configuration
Detector example
The configuration control table for a front FID detector includes
7 items.
CONFIGURE FRONT DETECTOR
Configured:
Ignore Ready =
Makeup gas type
Lit offset
[ F-DET ] = (SIGNAL)
[ EPC3] = (DET_EPC)
F-DET (OK) 64 watts
(FID)
FALSE
N2
2.0
(FID)
(FID)
300.0
This list interprets each line of the control table.
Configured: The type of module configured as a front
detector is an FID.
Ignore Ready: If TRUE, the GC will ignore a Not Ready status.
If the detector actuals do not match their setpoints, the GC
will go ready. The ignored items are displayed under Status.
Lit offset: The detector will try to reignite if the output drops
to this level.
This line indicates the signal board. In this case, it is plugged
into the 4-wire communication buss connector labelled
F-DET and is an FID signal board.
This line indicates the EPC module. In this case, it is plugged
into the 4-wire connector labeled EPC3 and is a detector EPC
module for an FID.
This line describes the heater and sensor. In this case, there
is a 64 watt heater cartridge associated with the front
detector and the sensor is reading 300.0C.
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Configuration
PCM example
The configuration control table for an pneumatic control
Module (PCM) module includes 6 items. For custom hardware,
the configuration could include a heater.
CONFIGURE PCM C
Configured:
Ignore Ready =
Gas type
Aux Gas type
Aux Mode
[ EPC6 ] = (AUX_EPC)
PCM
FALSE
N2
N2
Forward Pressure
(PCM)
This list interprets each line of the control table.
Configured: The type of module configured as a pneumatic
control module or PCM.
Ignore Ready: If TRUE, the GC will ignore a Not Ready status.
If the PCM actuals do not match their setpoints, the GC will
go ready. The ignored items are displayed under Status.
The next two lines indicate what gas type is associated with
each channel. The Gas type refers to channel one. The
options for an both channels are: Helium, Hydrogen,
Nitrogen, Argon methane 5%, and Air.
This line indicates the Aux Mode for the pressure control
channel. This can be Forward Pressure or Back Pressure
control.
This line indicates the EPC module. In this case, it is plugged
into the 4-wire connector labelled EPC6 and is an AUX EPC
module for a PCM.
There are no heaters configured in this example. However,
you can associate a PCM with a front or back inlet heater.
CONFIGURE PCM C
Install EPC6
Install EPC6
Install EPC6
276
Htr = NONE
Htr = FINLET
Htr = BINLET
7890 Series GC IPB
Configuration
AUX example
The configuration control table for an Aux EPC module includes
6 items. For custom hardware, the configuration could include a
heater.
CONFIGURE APC 1,2,3
Configured:
Ignore Ready =
Chan 1 Gas type
Chan 2 Gas type
Chan 3 Gas type
[ EPC6 ] = (AUX_EPC)
Aux Pressure
FALSE
N2
N2
N2
(AUX)
This list interprets each line of the control table.
Configured: The type of module configured as Aux EPC
channels 1, 2 and 3 is Aux Pressure module.
Ignore Ready: If TRUE, the GC will ignore a Not Ready status.
If the AUX actuals do not match their setpoints, the GC will
go ready. The ignored items are displayed under Status.
The next three lines indicate what gas type is associated with
each channel. The options for an AUX channel are: Helium,
Hydrogen, Nitrogen, Argon methane 5%, and Air
This line indicates the EPC module. In this case, it is plugged
into the 4-wire connector labeled EPC6 and is an AUX EPC
module labeled AUX.
There are no heaters associated with an AUX module in this
position.
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277
Configuration
Heater assignments
There are 4 standard connection for heaters and sensors. With a
valve bracket and harness, you add 2 more for a total of 6. The
following picture and table describe the harness labels and
typical uses.
Number
Label
Typical uses
FI
Front inlet
BI
Back inlet
FD
Front detector
BD
Back detector
A1
Valve box, 3rd detector,
Front FPD
A2
MSD transfer line, Valve
box. Back FPD
For our specials group and for our channel partners, there are
many options for configuring the heaters. These options are
based on connecting a heater and configuring it to a type of
module to enable a certain type of behavior. See the
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7890 Series GC IPB
Configuration
configuration topics in Firmware Instructions for Channel
Partner Devices.
As an Inlet or detector, a small zone is isothermal.
As an Thermal Aux, a small zone can be programmed.
This table describes this flexibility available in firmware.
Controlling
Number
Heater type
Configuration Setpoints
Front inlet
Inlet
[Config][Front [Front Inlet]
Inlet]
Back inlet
Inlet Nickel
catalyst
[Config][Back [Back Inlet]
[Aux Temp]
Inlet]
[Config][Ther
mal Aux 1]
Front detector 3
Detector
[Config][Front [Front Det]
Det]
Back detector 4
Detector
Custom
heater
[Config][Back [Back Det]
[Aux Temp]
Det]
[Config][Ther
mal Aux 2]
Thermal Aux
1
3rd Detector
Front FPD
[Config][Aux [Aux Det]
[Back Det]
Det]
[Config][Back
Det]
Thermal Aux
2
MSD transfer [Config][Aux [Aux Temp]
[Back Det]
line Back FPD Temp]
[Config][Back
Det]
Valve box
5 6 5 and 6
Valve box
Valve box
Valve box
[Config][Ther [Aux Temp]
[Back Det]
mal Aux 2]
[Config][Back [Valve Box]
Det]
[Config][Valve
Box]
Notes:
1 You can only configure 6 heaters. Each heater can only be
configured to one component type.
2 Front FPD uses heaters 3 and 5.
3 Back FPD uses heaters 4 and 6.
4 FPDs can be configured for one or two heater versions.
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279
Configuration
GC modules and the communications buss
This GC provides a flexible architecture. Along with the
flexibility, the configuration of the GC can be more complex.
The flexible architecture is represented in this schematic.
Above each arrow is a label that represents an address on a
communications buss.
The 4-wire communications buss is the nervous system of the
GC. It connects to up to 6 EPC modules and up to 4 detector
signal boards. On each of the 10 connectors, there is a label to
help identify what can be plugged in.
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7890 Series GC IPB
Configuration
The red and black wires on the buss provide power to the
module. The black wire is ground. The red wire is switched,
unregulated +24 VDC. All of these wires plug into the Analog
and Power Board. The white and colored wires provide serial
communications between the signal board and the module.
7890 Series GC IPB
281
Configuration
There are 2 extension cables for the GC modules of the 3rd
detector:
For the GC modules, there is an extension cable for both the
EPC module and the signal board; G3432-60505.
For the heater, there is an extension heater cable to connect
to the AUX 2 heater; G3432-60506.
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7890 Series GC IPB
Configuration
To configure an MSD transfer line
The factory does NOT configure any MSD transfer line. Thus you
may find, on installation, that the MSD heater will not heat, that
you cannot set a temperature, and that the transfer line is not
seen by the software. The transfer line heater may be configured
as a valve box heater or other device.
These instructions explain how to go from the configuration
shipped to you which may look like this (the valve box case)
to the configuration that you need for the transfer line.
To set up the MSD transfer line requires the user to
un-configure where the aux heater has been configured.
1 Press Config Aux Temp #. Scroll to the Valve Box and press
Enter. CONFIGURE VALVE BOX will be displayed.
7890 Series GC IPB
283
Configuration
2 Press Mode/Type. This will display the Remove module
message.
3 Press Enter. This displays the following message.
4 While a power cycle is required for the change to take effect,
it does not need to be done until the MSD transfer line
configuration is complete. Press Clear to return to
CONFIGURE VALVE BOX. Return to Configure Aux Temp
and select the Thermal Aux zone corresponding to the MSD
transfer line connection.
Thermal Aux 1 if the heater cable is connected to
connector 5.
Thermal Aux 2 if the heater cable is connected to
connector 6.
5 Using Thermal Aux 1 as the example, CONFIGURE AUX
HEATER 1 is displayed after selecting Thermal Aux 1 and
pressing Enter.
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7890 Series GC IPB
Configuration
6 Press Mode/Type. The following is displayed.
7 Press Enter. The Caution message appears again. Press Clear.
This displays the following.
8 Scroll to Auxiliary type and press Mode/ Type. Scroll to MSD
transfer line.
9 Press Enter to select. This shows the Caution message again.
Now power cycle the instrument.
10 Press Thermal Aux # and the appropriate number if
necessary. This shows the thermal aux that was configured.
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285
Configuration
To configure a valve box
The common approach is to configure the valve box heater to
Valve Box. Alternates are to use Thermal Aux 2 or Thermal Aux
1. A valve box can house one or two heaters.
MSD transfer line heater error
If you are updating a GC with an MSD transfer line heater, you
may observe a heater fault or error associated with Thermal
Aux 2.
Objective: Configure the Thermal Aux 2 heater, plugged into the
Aux 2 position, as an MSD transfer line heater. This may be
difficult because the heater may be configured as something
else. You may have to unconfigure it first.
Assumptions: The heater cable is plugged into the 5975A MSD
and into the Aux 2 position of the GC. Firmware is version
A.01.04 or higher.
Initial steps
1 Press Options. Scroll to Keyboard & Display and press Enter.
2 Turn Hard configuration lock off.
3 Press Config. Scroll to Thermal Aux 2 and press Enter.
4 You should see Configured Aux Heater on line 2 and
Auxiliary type: MSD transfer line on line 5.
5 If line 2 is correct, scroll to line 5. If the type is wrong, press
Mode/Type and select MSD transfer line. Confirm the change
by pressing Aux Temp.
6 If line 2 indicates that nothing is configured, press
Mode/Type to see if anything is available for configuration. If
nothing is, go to the next steps. If Thermal Aux 2 is available,
press Enter to select it, then power cycle the GC.
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7890 Series GC IPB
Configuration
If that doesn't work
Examine the other heaters that could be configured as Thermal
Aux 2. These are Valve Box or Thermal Aux 1.
1 Press Config. Scroll to Valve Box and examine line 2.
2 If it is configured, press Mode/Type and then Enter to Remove
the module.
3 Navigate back to Thermal Aux 2 to see if you can configure it
as Aux 2.
4 Continue in this way until you find where Aux 2 is
configured and unconfigure it.
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Configuration
Replacing a GC module
When replacing an EPC module or a detector signal board, you
will have to update the configuration of the GC. This is because
the configuration information includes the unique ID# and
manufacturing date for these parts.
To configure the new GC module
1 Replace the module and power on the GC. The GC will list
the Exceptions to the configuration and indicate that these
modules are broken or missing.
2 Unlock the Configuration locks.
3 Press [Config] and select the GC module that you replaced.
4 Press [Mode/Type]. The GC displays Remove module. Press
[Enter].
5 A Caution message tells you to reboot the GC.
6 Press [Mode/Type]. The GC displays Install module. Press
[Enter].
CAUTION
Be sure that you select the correct module configuration. Incorrect
selections can cause operation problems. For example, for an FPD
select the 2 heater version.
7 A Caution message tells you to reboot the GC.
8 Press [Options]. Scroll to Communications and press [Enter].
9 Scroll to Reboot the GC. Press [Yes/On] twice.
10 Navigate to the configuration table for the GC module.
11 Verify that the configuration is correct. Modify any
additional configuration items, such as, Gas type or Lit
offset.
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7890 Series GC IPB
Configuration
Removing a GC module
It is easy to unconfigure a module and make it appear to be
uninstalled without disconnecting any cables. This is useful if a
module fails and the customer still wants to use the other
modules. For example, if the back inlet fails, the customer can
unconfigure the back inlet and continue to use the front inlet
and detectors.
1 Press [Options] and select Keyboard & Display.
2 Press [Off / No] to turn the Configuration Lock off.
3 Press [Config] and the key for the GC module to remove.
4 From the line labeled Configure, press [Mode/Type].
5 Press [Enter]. The GC will display a message requesting you to
power cycle the instrument.
6 Power cycle the instrument.
7 Verify the removal by pressing the key for the GC module.
The GC should display an uninstalled message.
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289
Configuration
Changing the GC configuration
The GC configuration is changed when you do any of the
following:
Add or replace a detector signal board.
Add or replace an EPC module.
Replace the GC logic board.
Add or remove a tray or auto-injector.
Add or remove a heater.
Change any soft configuration items, such as, gas types,
heater types, and Lit offset.
Changing the GC configuration impacts data system methods
and methods stored in the GC.
Agilent data system methods
During the first connection and when loading any of the
methods created with the old configuration, the data system
will note the change in configuration and force you to resolve
the differences. If you do not resolve differences in both the
configuration and method parameter screens the method will
not load. Run method or run sequence will not start the run.
Use the GC Configuration Connection screen to get the new
configuration. Review and update any configuration
setpoints.
Use the Edit parameters screen to review and update any
method setpoints.
Methods stored in GC
Methods stored in the GC that do not match the new
configuration must be updated. Make the necessary additions or
modifications. Store this method over the old method.
When you load a method, the GC compares the method against
the current hardware it detects (inlet types, detector types,
PCM, heaters, valves, and so forth). A method which does not
match is not loaded. Default setpoints for this configuration are
loaded. Before adding new hardware or changing the installed
hardware type, verify that any methods stored in the GC have
been documented.
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7890 Series GC IPB
Configuration
Configuration locks
When trying to change the GC configurationas by adding,
removing, or changing an Inlet moduleyou may encounter this
or a similar message:
Configuration is Locked
Go to keyboard options to unlock
To unlock the configuration
1 Press [Options].
2 Select Keyboard and Display.
3 Select Hard Configuration lock, then press [No/Off].
When you power cycle the GC, the configuration lock is
automatically set to On.
When you use the Reboot GC feature under Options |
Communications, the configuration lock is not changed.
7890 Series GC IPB
291
Configuration
Installing new devices
When a new device is added to the GC, it must be described so
that the GC knows what it is and how to use it.
This procedure, using a PCM module as an example, illustrates
the process.
1 Replace all instrument covers in the reverse order in which
they were removed.
2 Plug in the GC and turn on the power.
3 Unlock the GC keypad.
a Press [Options].
b Select Keyboard & Display.
c Select Hard Configuration lock, then press [No/Off].
4 Press [Configure].
5 Scroll to select the entry for the new PCM module (PCM A,
PCM B, or PCM C) and press [Enter].
6 On the GC keypad, press [Mode/Type].
7 The GC presents available configuration options.
If using the PCM for something other than an inlet (for
example, to provide carrier gas to a splitter), scroll to
Install EPC# Htr = None (where # indicated the slot chosen).
If using the PCM for inlet carrier gas supply, refer to the
inlet manufacturer's documentation for the correct
configuration choice.
8 Press [Enter]. A caution message appears instructing you to
reboot.
9 Reboot the GC.
a Press [Options].
b Scroll to Communications and press [Enter].
c Scroll to Reboot the GC? and press [Yes/On] twice to reboot
the GC and have the changes take effect. This also resets
the Hard Configuration lock.
10 Zero the pressure sensors.
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7890 Series GC IPB
Configuration
11 Configure the gas types and control mode.
a Press [Config], then scroll to the correct PCM entry (PCM
A,PCM B, or PCM C).
b Scroll to Gas type and use the [Mode/Type] key to set the
gas type connected to the PCM's Channel 1.
c Scroll to Aux Gas type and use the [Mode/Type] key to set
the gas type connected to the PCM's Channel 2.
d Scroll to Aux Mode and use the [Mode/Type] key to set the
pressure control mode (forward or backward) for the
PCM's Channel 2.
7890 Series GC IPB
293
Configuration
Configuring time
To localize the date/time stamp in the Run and Event logs, use
this procedure.
1 Press [Config][Time].
2 Enter the offset from Greenwich Mean Time using 24-hour
format. Press [Enter].
3 Enter the local time (24 hour format). Press [Enter].
4 Enter the date, in ddmmyy format. Press [Enter].
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Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
7 External Cabling
Connectors on the back of the GC
Remote Start/Stop 297
External event 305
Automatic sampler for GC 306
Analog signal outputs 310
Analog signal inputs 312
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Agilent Technologies
295
External Cabling
Connectors on the back of the GC
296
7890 Series GC IPB
External Cabling
Remote Start/Stop
These cables are used to link multiple instruments together, so
that they start and stop together.
APG Remote Control
Remote control allows easy connection between single
instruments or systems to ensure coordinated analysis with
simple coupling requirements. For example, you might have an
integrator, automatic sampler, and a gas chromatograph
connected with Remote cables.
You can synchronize a maximum of ten instruments using
Remote cables. Control of analysis is maintained by instrument
readiness - READY for next analysis, followed by START of run
and optional STOP of run triggered on the respective lines. In
addition, PREPARE may be issued to initiate pre-run activities.
All devices connected to APG remote are connected in parallel.
For example, if one device is NOT READY then all devices on the
bus are also NOT READY.
Electrical specifications
The APG signals are a modified open collector type. The signal
levels are generally TTL levels (low voltage is logic zero, high
voltage is logic one) but the open circuit voltage will be between
2.5 to 3.7 Volts. The typical voltage is 3 Volts. A voltage over 2.2
volts will be interpreted as a high logic state while a voltage
below 0.4 volts will be interpreted as a low logic state. These
levels provide some margin over the specifications of the
devices used.
The pull-up resistance, connected to the open-circuit voltage, is
in the range of about 1K ohms to 1.5K ohms. For a logic-low
state, for a single device on the bus, the minimum current you
must be able to sink is 3.3 milliamps. Since devices are
connected in parallel, when you have multiple devices this
minimum current must be multiplied by the number of devices
attached on the bus. The maximum voltage for a low-input state
= 0.4V.
The bus is passively pulled high. Leakage current out of a port
must be less than 0.2 milliamps to keep the voltage from being
pulled lower than 2.2 volts. Higher leakage current may cause
the state to be interpreted as a low.
7890 Series GC IPB
297
External Cabling
Over-voltage protection - APG Remote connections are clamped
by a zener diode to 5.6 Volts. Exceeding this voltage will damage
the circuit (main board).
Suggested Drive Circuits
A signal on the APG bus may be driven by another APG device
or by one of the following circuits.
A relay, with one side connected to ground, when closed will set
a logic-low state.
An NPN transistor, with the emitter connected to ground and
the collector connected to the signal line will set a logic-low
state if proper base current is supplied.
An open-collector logic gate will perform this same function.
A low-side drive IC will also work, but Darlington-type drivers
should be avoided as they will not meet the low-side voltage
requirement of less than 0.4V.
The Remote Connector
298
7890 Series GC IPB
External Cabling
Signal Descriptions
Prepare (Low True)Request to prepare for analysis. Receiver
is any module performing pre-analysis activities. For example,
shorting pin 2 to ground will put the GC into "Prep-Run" state.
This is useful for Splitless Mode to prepare the inlet for
injection or when using "Gas Saver Mode." This function is not
needed by Agilent autosampler systems.
Ready (High True) If The Ready Line is high (> 2.2 VDC) then
the system is ready for next analysis. Receiver is any sequence
controller.
Start (Low True)Request to start run/timetable. Receiver is
any module performing runtime-controlled activities.
Stop (Low True)Request to reach system ready state as soon
as possible (for example, stop run, abort or finish, and stop
injection). Receiver is any module performing
runtime-controlled activities. Normally this line is not
connected, if the GC oven program is used to control the
method "Stop" time.
Timing Diagram
7890 Series GC IPB
299
External Cabling
Cable pinouts, remote start/stop, general use
Part number 35900-60670
300
Connector 1 9 pin
(male)
Signal name
Connector 2 (spade
lugs)
GND
Black
Prepare (low true)
White
Start (low true)
Red
Start relay
Green
Start relay
Brown
No connection
Blue
Ready (high true input)
Orange
Stop (low true)
Yellow
No connection
Violet
7890 Series GC IPB
External Cabling
Cable pinouts, GC to 3395B/3396C Integrator
Part number 03396-61010
7890 Series GC IPB
Connector 1 9 pin
(male)
Signal name
Connector 2 15 pin
(male)
GND
9 Ground
Prepare
No connection
Start
3 Start in
Start relay
No connection
Start relay
No connection
No connection
No connection
Ready
14 Ready out
Stop
4 STOP2 In
No connection
No connection
301
External Cabling
Cable pinouts, GC to 35900C, D, E/MSD/Sampler, 2 meters
Part number G1530-60930
302
Connector 1 (male)
Signal name
Connector 2 (male)
GND
Prepare
Start
Start relay
Start relay
No connection
Ready
Stop
No connection
7890 Series GC IPB
External Cabling
Cable pinouts, GC to Headspace Sampler
Part number G1290-60575
7890 Series GC IPB
Connector 1 3-pin male
Signal name
Connector 4-pin male
GND
4, 5
Start
Ready
303
External Cabling
Cable pinouts, APG Remote Y-cable
Part number 31530-61020
304
All connectors 9 pin (male)
Signal name
GND
Prepare
Start
Start relay
Start relay
No connection
Ready
Stop
No connection
7890 Series GC IPB
External Cabling
External event
Two passive relay contact closures and two 24-volt control
outputs are available for controlling external devices. Devices
connected to the passive contact closures must be connected to
their own power source.
CAUTION
The external event connector is similar to the BCD connector.
Plugging an external event cable into the BCD connector can
damage the A&P board.
Part number G1530-60590
Connector
Signal name
24 volt control output
1
24 volt output 1
2
24 volt output 2
3
Ground
4
Ground
Relay contact closures (Normally open)
5
Contact closure 1
6
Contact closure 1
7
8
Contact closure 2
Contact closure 2
7890 Series GC IPB
Maximum rating
Wire terminations
Corresponds to
valve #
150 mA
150 mA
Yellow
Black
Red
White
5
6
48V ac/dc, 250 mA
Orange
Green
7
7
48 V ac/dc, 250 mA
Brown or Violet
Blue
8
8
305
External Cabling
Automatic sampler for GC
There are three connectors, Sampler 1, Sampler 2, and Tray, for
the 7683 Autosampler system.
Cable pinouts, GC to G2613A Injector
Part no. G2613-60590
306
Connector 1 16 pin (female)
Connector 2 16 pin (female)
A1
RXD
A1
TXD
A2
CTS
A2
RTS
A3
DSR
A3
DTR
A4
NCTL Reset
A4
NCTL Reset
A5
GND
A5
GND
A6
VAC 1
A6
VAC 1
A7
GND
A7
GND
A8
VAC 2
A8
VAC 2
B1
TXD
B1
RXD
B2
RTS
B2
CTS
B3
DTR
B3
DSR
B4
GND
B4
GND
B5
GND
B5
GND
B6
VAC 1
B6
VAC 1
B7
GND
B7
GND
B8
VAC 2
B8
VAC 2
7890 Series GC IPB
External Cabling
Cable pinouts, GC to G4513A and 7650 Injector
Part no. G4514-60610
7890 Series GC IPB
Connector 1 16 pin (female)
Connector 2 16 pin (female)
A1
RXD
A1
TXD
A2
CTS
A2
RTS
A3
DSR
A3
DTR
A4
NCTL Reset
A4
NCTL Reset
A5
GND
A5
GND
A6
VAC 1
A6
VAC 1
A7
GND
A7
GND
A8
VAC 2
A8
VAC 2
B1
TXD
B1
RXD
B2
RTS
B2
CTS
B3
DTR
B3
DSR
B4
GND
B4
GND
B5
GND
B5
GND
B6
VAC 1
B6
VAC 1
B7
GND
B7
GND
B8
VAC 2
B8
VAC 2
307
External Cabling
Cable pinouts, GC to G2614A Tray
Part no. G2614-60610
308
Connector 1 16 pin (female)
Connector 2 16 pin (female)
A1
RXD
A1
TXD
A2
CTS
A2
RTS
A3
DSR
A3
DTR
A4
M Reset
A4
M Reset
A5
GND
A5
GND
A6
VAC 1
A6
VAC 1
A7
GND
A7
GND
A8
VAC 2
A8
VAC 2
B1
TXD
B1
RXD
B2
RTS
B2
CTS
B3
DTR
B3
DSR
B4
GND
B4
GND
B5
GND
B5
GND
B6
VAC 1
B6
VAC 1
B7
GND
B7
GND
B8
VAC 2
B8
VAC 2
7890 Series GC IPB
External Cabling
Cable pinouts, GC to G4514A Tray
Part no. G4514-60610
7890 Series GC IPB
Connector 1 16 pin (female)
Connector 2 16 pin (female)
A1
RXD
A1
TXD
A2
CTS
A2
RTS
A3
DSR
A3
DTR
A4
M Reset
A4
M Reset
A5
GND
A5
GND
A6
VAC 1
A6
VAC 1
A7
GND
A7
GND
A8
VAC 2
A8
VAC 2
B1
TXD
B1
RXD
B2
RTS
B2
CTS
B3
DTR
B3
DSR
B4
GND
B4
GND
B5
GND
B5
GND
B6
VAC 1
B6
VAC 1
B7
GND
B7
GND
B8
VAC 2
B8
VAC 2
309
External Cabling
Analog signal outputs
There are two channels of analog output available on the back
panel, labeled Sig 1 and Sig 2. Two cables are available one for
3395/6 series integrators and one for general use.
Analog cable: GC to 3395A/B or 3396B/C Integrators and 35900 C/D/E
Analog to Digital Interface instrument
Part number G1530-60570
310
Connector 1
Signal Name
Color
Connector 2
1V
Black
Common
White
Shell
Ground
Orange
7890 Series GC IPB
External Cabling
Analog cable: general use
Part number G1530-60560
7890 Series GC IPB
Connector 1
Signal name
Connector 2 quick
disconnects
not used
Brown
0 to 1 V, 0 to 10 V()
White
not used
Red
1 V (+)
Black
10 V (+)
Blue
Shell
Ground
Orange
311
External Cabling
Analog signal inputs
The data from external detectors, such as the
chemiluminescence detectors, can be imported into the GC
using the appropriate signal input cable and the analog input
board.
General purpose AIB cable
G1530-60560 Signal cable, general purpose, 6 pins
Connector 1
Signal name
Connector 2 quick
disconnects
not used
Brown
0 to 1 V, 0 to 10 V()
White
not used
Red
1 V (+)
Black
10 V (+)
Blue
Shell
Ground
Orange
XCD Chemiluminescence detector AIB cable
G6600-60800 Recorder Cable
312
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
8 Internal Cabling
Internal cabling overview 314
MSD transfer line heater cable 315
Third detector heated zone cable 316
Communication harness 317
Motor Harness & AC Control Assembly 320
Keyboard and display connection board (original style only)
AC power inlet assemblies 325
Inlet/Detector harness 326
Auxiliary zone/Valve box harness 328
Third detector EPC communication cable 330
Keyboard/Display harness 331
Keyboard interconnect board 332
Heated zone extension cable 333
Ignitor cable, FID 334
Ignitor cable, FPD 335
RS-232 cable, ALS controller 336
PTV thermocouple cable 337
NPD power cable 339
324
This section covers wiring harnesses in the gas chromatograph.
The following wiring harnesses are described:
Communication harness
Motor harness and AC control assembly
Third detector EPC communication cable
Inlet/Detector harness
Aux zone / valve box cable
Third detector heated zone cable
Keyboard/Display harness
Interconnect board, keyboard
Ignitor cable, FID
Ignitor cable, FPD
RS-232 cable, ALS controller
PTV thermocouple cable
NPD power cable
MSD transfer line heater cable
Agilent Technologies
313
Internal Cabling
Internal cabling overview
The various modules that make up the GC are powered and
interconnected by a set of cables and wiring harnesses. These
modules include inlets, detectors, temperature controllers,
printed circuit boards, and power supplies.
314
7890 Series GC IPB
Internal Cabling
MSD transfer line heater cable
Part number G1530-60790
This cable provides heater power and temperature sensing for
an MSD transfer line heater.
7890 Series GC IPB
315
Internal Cabling
Third detector heated zone cable
Part number G3432-60506
This is a 4-conductor cable that provides heater power and
sensor connections for a third detector mounted on the left side
of the GC.
Table 21 Connection table
316
TD1 connector
pin
Wire color
Twisted pair?
TD2 connector
pin
Orange
Yes
Black
Grey
Green
3
Yes
2
4
7890 Series GC IPB
Internal Cabling
Communication harness
Part number G3430-60513
This harness provides 24 VDC from the Analog and Power board
to all EPC modules. It also carries communications between the
EPC modules and the signal board.The harness connector
labeled "power" connects to P1 on the Analog and Power board.
The harness connector labeled "Comm Bus" connects to P7 on
the logic board.
7890 Series GC IPB
317
Internal Cabling
Power connection table
Black wires, that are not part of twisted pairs, are GROUND for
pin 2 of the associated EPC.
Red wires, that are not part of twisted pairs, supply + 24 VDC to
pin 1 of the associated EPC module.
318
Power connector
pin
Wire color
Signal
EPC (pin)
Red
+ 24 VDC
EPC 1 (1)
Red
+ 24 VDC
EPC 2 (1)
Red
+ 24 VDC
EPC 3 (1)
Red
+ 24 VDC
EPC 4 (1)
Red
+ 24 VDC
EPC 5 (1)
Red
+ 24 VDC
EPC 6 (1)
Red
+ 24 VDC
AUX DET 2 (1)
Red
+ 24 VDC
AUX DET 1 (1)
Red
+ 24 VDC
B DET (1)
10
Red
+ 24 VDC
F DET (1)
11
Black
GROUND
EPC 1 (2)
12
Black
GROUND
EPC 2 (2)
13
Black
GROUND
EPC 3 (2)
14
Black
GROUND
EPC 4 (2)
15
Black
GROUND
EPC 5 (2)
16
Black
GROUND
EPC 6 (2)
17
Black
GROUND
AUX DET 2 (2)
18
Black
GROUND
AUX DET 1 (2)
19
Black
GROUND
B DET (2)
20
Black
GROUND
F DET (2)
7890 Series GC IPB
Internal Cabling
Data communication table
Data are transmitted to and from the EPC modules on twisted
pairs of wires.
7890 Series GC IPB
Comm Bus
connector pin
Wire color
White
Black
White
Brown
White
Red
White
Orange
White
10
Yellow
11
White
12
Green
13
White
14
Blue
15
White
16
Violet
17
White
18
Grey
19
White
20
White/Black
Twisted pair?
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
EPC (pin)
EPC 1 (3)
EPC 1 (4)
EPC 2 (3)
EPC 2 (4)
EPC 3 (3)
EPC 3 (4)
EPC 4 (3)
EPC 4 (4)
EPC 5 (3)
EPC 5 (4)
EPC 6 (3)
EPC 6 (4)
AUX DET 2 (3)
AUX DET 2 (4)
AUX DET 1 (3)
AUX DET 1 (4)
B DET (3)
B DET (4)
F DET (3)
F DET (4)
319
Internal Cabling
Motor Harness & AC Control Assembly
Part number G3430-60512
This harness provides 24 VDC power from the Analog and
Power board at P18 for the following functions:
Flapper motor (6 pin, 2 x 3 connector)
Inlet fan motor (3 pin)
Oven sensor (2 pin, shortest)
Pneumatics fan motor (2 pin)
Cryogenic cooling valve for the oven (5 pin)
Shut-off solenoid on the AC board (5 pin, 3 used)
320
7890 Series GC IPB
Internal Cabling
Table 22 Connection table
7890 Series GC IPB
C1 connector pin
Wire color
Destination
Black
Flapper motor 2
White/Nlue
Flapper motor 4
Red
Flapper motor 6
Orange
Inlet fan 2
White/Green
Inlet fan 3
Blue
Pneumatics fan 2
Green
Oven cryovalve 3
Brown
Oven cryovalve 4
White
AC control 3
10
no connection
11
Violet
Oven sensor 2
12
White
Flapper motor 1
13
White/Black
Flapper motor 3
14
Blue
Flapper motor 5
15
Grey
Oven cryovalve 5
16
Yellow
Inlet fan 1
17
Brown
Pneumatics fan 1
18
Violet
Oven cryovalve 2
19
White/Red
Oven cryovalve 5
20
Black
AC control 2
21
Red
AC control 1
22
Black
Oven sensor 1
321
Internal Cabling
Keyboard and display connection board (original style only)
This board combines the oven door sensor (P2) with the
keyboard and display ribbon cable (P1) and connects them to
the keyboard and display harness (P3).
P1 pins are connected to the corresponding pins on P3 (P2-1 to
P3-1, etc.).
P2 pins are connected to P3 pins 33 and 34.
322
7890 Series GC IPB
Internal Cabling
AC power inlet assemblies
These assemblies provide the connection between the external
power cord and the internal AC power board.
C20 assembly (for C19 plug)
Part number G1530-61550
C14 assembly (for C13 plug)
Part number G1530-61560
7890 Series GC IPB
323
Internal Cabling
Keyboard and display connection board (original style only)
This board combines the oven door sensor (P2) with the
keyboard and display ribbon cable (P1) and connects them to
the keyboard and display harness (P3).
P1 pins are connected to the corresponding pins on P3 (P2-1 to
P3-1, etc.).
P2 pins are connected to P3 pins 33 and 34.
324
7890 Series GC IPB
Internal Cabling
AC power inlet assemblies
These assemblies provide the connection between the external
power cord and the internal AC power board.
C20 assembly (for C19 plug)
Part number G1530-61550
C14 assembly (for C13 plug)
Part number G1530-61560
7890 Series GC IPB
325
Internal Cabling
Inlet/Detector harness
Part number G3430-60535
This harness connects the inlet and detector EPCs to the logic
board at P7.
The FI and BI connectors are for inlets; FD and BD are for
detectors. FV and BV are two-conductor connectors mounted on
the top left edge of the GC near the inlets. They supply 24 VDC
to various accessories.
Table 23 Connection table
326
S1 pin
Wire color
Signal name
Destination
(pin)
Black
ADC-GND
F1 (3)
Black
ADC-GND
BI (3)
Black
ADC-GND
FD (3)
Black
ADC-GND
BD (3)
Green
C GROUND
FI (4)
Green
C GROUND
BI (4)
Green
C GROUND
FD (4)
Green
C GROUND
BD (4)
Yellow
+ 24 V
FV (1)
10
Yellow
+ 24 V
BV (1)
11
Violet
INJA-SENSE
FI (2)
7890 Series GC IPB
Internal Cabling
7890 Series GC IPB
S1 pin
Wire color
Signal name
Destination
(pin)
12
Grey
INJB-SENSE
BI (2)
13
Violet
DETA-SENSE
FD (2)
14
Grey
DETB-SENSE
BD (2)
15
Red
INJ-FRONT
FI (1)
16
Orange
INJ-BACK
BI (1)
17
Red
DET-FRONT
FD (1)
18
Orange
DET-BACK
BD (1)
19
Blue
ICRYOSPLT-FRONT
FV (2)
20
White
ICRYOSPLT-BACK
BV (2)
327
Internal Cabling
Auxiliary zone/Valve box harness
Part number G1530-60660
The Auxiliary Zone/Valve Box harness runs from connector P22
on the A&P board to the valve driver bracket screwed on to the
right side of the GC above the A&P board. It powers the valve
actuator drivers and two auxiliary heater/sensors.
The A1 and A2 connectors have a tab which helps ID which wire
is the heater, sense, or ground.
328
7890 Series GC IPB
Internal Cabling
Table 24 Connection table
Wire color
Pin # on S1
Signal name
Destination (and
Pin #)
Violet
Aux 1 Sense
A1 (2)
Aux 2 Sense
A2 (2)
Heater GND
A1 (4)
Heater GND
A2 (4)
+24 Volts
V1 (1)
+24 Volts
V2 (1)
+24 Volts
V3 (1)
+24 Volts
V4 (1)
Sensor GND
A1 (3)
10
Sensor GND
A2 (3)
Red
11
Aux 1 Heater
A1 (1)
Orange
12
Aux 2 Heater
A2 (1)
Brown
13
Valve #1
V1 (2)
Blue
14
Valve #2
V2 (2)
Gray
15
Valve #3
V3 (2)
White
16
Valve #4
V4 (2)
Green
Yellow
Black
7890 Series GC IPB
329
Internal Cabling
Third detector EPC communication cable
Part number G3432-60505
This cable extends the communications harness to a third
detector mounted on the left side of the GC. It connects to the
EPC 6 connector and extends across the top of the GC to the
side mount.
When removing and replacing the third detector cable, note
carefully how it enters the side detector carrier. You may need
to loosen the screws holding the carrier to the GC body.
Figure 6
EPC AreaSide Carrier Area
Table 25 Connection table
330
Connector, EPC
area (pin)
Wire color
Aux Det 1 (1)
Red
Aux Det 1 (2)
Black
Aux Det 1 (3)
White
Aux Det 1 (4)
Blue
EPC 5 (1)
Red
EPC 5 (2)
Black
EPC 5 (3)
White
EPC 5 (4)
Yellow
Twisted pair?
Yes
Yes
Yes
Yes
Connector, side
carrier area (pin)
Aux Det 1 (1)
Aux Det 1 (2)
Aux Det 1 (3)
Aux Det 1 (4)
Third Det EPC (1)
Third Det EPC (2)
Third Det EPC (3)
Third Det EPC (4)
7890 Series GC IPB
Internal Cabling
Keyboard/Display harness
Part number G3430-60514
This harness connects the keyboard and display to the logic
board at P8.
7890 Series GC IPB
331
Internal Cabling
Keyboard interconnect board
Part number G3430-60003
This board, mounted behind the keyboard/display module,
connects the keyboard to the keyboard/display harness.
Flex circuit from keypad attaches to P1.
Oven door sensor attaches to P2.
Ribbon cable from logic board attaches to P3.
332
7890 Series GC IPB
Internal Cabling
Heated zone extension cable
Part number G1530-60790
Table 26 Connection table
7890 Series GC IPB
Connector C1 pin
Wire color
Connector C2 pin
Orange
Violet
Black
Green
333
Internal Cabling
Ignitor cable, FID
Part number G3431-60680
The ignitor cable connects the glow plug ignitor to its power
source.
334
7890 Series GC IPB
Internal Cabling
Ignitor cable, FPD
Part number G3435-60600
This cable connects the glow plug ignitor to its power source.
7890 Series GC IPB
335
Internal Cabling
RS-232 cable, ALS controller
Part number G2612-60510
The ALS controller is driven by the analog and power board.
This cable makes the connection at J8.
336
J8 pin
Signal
+5 V
no connection
+5 V
DSRA
Ground
+5 V
Ground
RSTA
Ground
10
Ground
11
Ground
12
Ground
13
nStart (ALS Start paralleled with APG
Start to FPGA as nAPG_START)
14
Spare.VDSP
15
RxDA
16
Spare.VDSN
17
TxDA
18
DTRA
19
CTSA
20
RTSA
7890 Series GC IPB
Internal Cabling
PTV thermocouple cable
Part number G2617-60505
The Thermocouple Cable connects the PTV thermocouple board
to the PTV inlet heater/sensor cable, and to the valve and power
connectors on the inlet/detector wiring harness.
7890 Series GC IPB
337
Internal Cabling
Table 27 Connection tables
338
PCB pin
Wire color
Signal
Destination (pin)
Blue
ICRYO_SPLT_FRO FV (2)
NT
Violet
INJA_SENSE
FI (2)
No connection
Yellow
+ 24 VDC
FV (1)
Black
ACC-GND
FI (3)
No connection
HTR pin
Wire color
Destination (pin)
Yellow
FI (1)
No connection
Blue
FI (4)
7890 Series GC IPB
Internal Cabling
NPD power cable
Part number G3434-60600
This cable provides power to the heated bead in the NPD.
Table 28 Connection table
7890 Series GC IPB
Connector A pin
Wire color
Connector B pin
Braided shield
Shell
Blue
Female
Clear
Male
339
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
9 Mainframe
Mainframe overview 341
Covers and Fans 342
Replacing the oven bezel 348
Replacing the oven door 349
Replacing the oven door button 350
Replacing the keypad assembly and display board 351
Oven temperature control 362
Oven temperature troubleshooting 363
Testing resistance of the heater coil 365
Cryo valve installation/replacement 366
Replacing the oven sensor 371
Replacing the oven door sensor 372
Replacing the oven shroud, oven fan, and oven fan motor 375
Replacing the oven flapper assembly 381
Replacing the flapper or flapper motor 383
Replacing Components Inside the Electronics Panel 385
Replacing Components Inside the Lower Rear Metal Cover 400
Agilent Technologies
340
Mainframe
Mainframe overview
The GC mainframe consists of the chassis (baseplate) plus the
following:
A set of metal and plastic covers
The oven, oven door, and related parts
Electronic components inside the right side cover. These are
the "mind" of the GC.
Power handling components inside the lower back cover
Wiring cables and harnesses
Inlets, detectors, valves, and other selected components are
mounted on or in the mainframe.
7890 Series GC IPB
341
Mainframe
Covers and Fans
Metal and plastic covers protect the GC components and guard
the user from exposure to heat and electric shock. The covers
also play a part in controlling the flow of cooling air through the
instrument. The GC should not be operated unless all covers are
in place.
Additional cooling is needed in two areas, the inlets and the
EPC pneumatic controllers. The inlet fan is located at the rear
of the inlet cover. The preumatics fan is located on the back of
the GC under the center of the pneumatics slots.
342
7890 Series GC IPB
Mainframe
Removing and replacing the covers
Detector top cover
This cover protects the detectors, valve box, and valve assembly.
To remove it, raise it to a vertical position, lift the right side,
and disengage the pin on the lower left side.
CAUTION
Do not force the cover, either when installing it or closing it. This
could break the plastic parts.
To replace the cover, make certain that the slot in the brass
bushing (lower right corner) is vertical and that the bushing is
fully seated. Installation is then the reverse of removal.
The pneumatics top cover
The large plastic cover over the pneumatics area on the top, rear
of the GC is held by a black button on each end. Press both
buttons and lift the cover off.
Replacing the pneumatics top cover buttons
1 Remove the cover from the GC.
2 Turn the cover over and remove the two screws holding the
button to be replaced.
3 Assemble the plastic button and the metal mount. Position
the assembly over the two nuts and install the screws.
The electronics top cover
1 Raise or remove the top cover.
2 This exposes a screw near the left front side of the
electronics cover. Loosen this screw.
3 Raise the cover to the vertical position.
4 To remove the cover completely after raising it to the vertical
position, Tilt it to the right to disengage the left end, then
slide it to the left and remove it.
The side covers
The left and right side covers are each held by 2 captive screws
at the bottom and a hook at the rear. Unfasten the screws, slide
the panel to the rear, and remove it.
7890 Series GC IPB
343
Mainframe
The rear covers
The upper and lower rear covers are held by several screws
each, but all are visible from behind the GC. Note that some of
the screws are in slots rather than holes; these screws do not
need to be completely removed.
The side cover on the third detector assembly
Remove 2 screws at the bottom of the panel, then lift and
remove the combined side and top panel.
344
7890 Series GC IPB
Mainframe
Replacing the inlet cooling fan
1 Cool down the oven and all heated zones to below 70 C to
avoid the creation of active sites.
2 Turn off the GC main power switch.
CAUTION
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the top rear cover by pressing in on the side
retaining clips and lifting off.
4 Disconnect its cable from the GC wiring harness.
5 Remove the fan from its clips.
6 In reassembly, make sure the label side of the fan faces
upwards (flow must be in the upwards direction). Also, the
cable should exit nearest its connector on the GC wiring
harness.
7890 Series GC IPB
345
Mainframe
Replacing the EPC cooling fan
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the lower rear cover on the GC.
4 The fan is located below the EPC module compartment; begin
by disconnecting the fan's cable.
346
7890 Series GC IPB
Mainframe
5 Remove 4 screws.
6 In replacement, be careful to not overtighten the screws such
that the fan's plastic frame is cracked. Also, in replacing the
screws, it may be easiest to start with the one at the right
forward corner due to interference caused by the nearby
oven fan motor.
NOTE
7890 Series GC IPB
In reassembly, make sure fan orientation is such that air flow is directed
upwards through the EPC modules.
347
Mainframe
Replacing the oven bezel
WA R N I N G
Be careful! The oven and/or bezel may be hot enough to cause
burns. If it is hot, wear gloves to protect your hands.
The bezel consists of a plastic cover over a metal plate. It is held
by two screws that are reached through holes in the top of the
bezel.
1 Unscrew the two mounting screws.
2 Lift the bezel and metal plate off the GC.
3 When reinstalling, note that the lip on the bezel extends
forward over the top of the oven door. Be very certain that
the metal plate is between the plastic part and the top of the
GC.
348
7890 Series GC IPB
Mainframe
Replacing the oven door
WA R N I N G
Be careful! The oven and/or inlet may be hot enough to cause
burns. If the inlet is hot, wear gloves to protect your hands.
1 If an ALS is installed, remove it.
2 Remove the GC pneumatics cover and the top back panel.
3 Remove the six T-20 screws retaining the inlet cover, lift off
and remove the cover.
4 Open the oven door. This exposes the top of the shaft that
attaches the door to the GC.
5 The hinge shaft threads completely through its bracket, so
that the threads cannot engage and loosen during use. To
remove the shaft, use a flat- head screwdriver to lift the shaft
from the bottom until it contacts the threads. Hold in place
while using a T- 20 driver to loosen the shaft. Turn the T- 20
driver a few times to engage the threads on the bottom of the
shaft with the top threaded plate of the bottom door hinge.
6 While supporting the weight of the door, use pliers to pull the
door shaft up and out of the door.
7 Remove the door.
8 Installation of the new door is the reverse of these steps.
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Mainframe
Replacing the oven door button
WA R N I N G
The oven door button mechanism is under the mainframe. To
reach it, you must either tip the GC on its side or slide it part way
off the bench so that the right front corner is accessible. Be very
certain that the GC is stable and cannot fall.
1 Move the GC so that the bottom of the mainframe near the
button is accessible.
2 Open the oven door and operate the button several times.
Note that the operating lever from the button is behind the
vertical lever that moves the latch,
3 To remove the mechanism, remove the two screws that hold
it and pull it down out of the mainframe.
4 Replacement is the reverse of these steps. Be certain that the
button lever is behind the latch lever.
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7890 Series GC IPB
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Replacing the keypad assembly and display board
Replacing the keypad assembly (original style)
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove three screws with -inch nut heads from the
detector electronics panel side. Two of the screws are near
the upper left and lower left corners of the front detector
signal board; the other is on the bottom of the GC in a slotted
hole.
4 Disconnect the large keypad ribbon cable from the inner
connector board.
5 Remove the T-20 screw from the bracket near the top of the
keypad assembly to release it from the GC body.
6 From the front, slide the keypad panel forward.
7 At this point there are two servicing options: replacement of
the entire keypad assembly or just the display. [See next
topic for the replacement of the display only.]
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8 Disconnect the ribbon cable from the display board.
9 Disconnect the large ribbon cable from the inner connector
board.
10 Disconnect the cable (at the lower left of the inner connector
board) from the oven door safety switch.
11 Remove the inner connector board from the GC.
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7890 Series GC IPB
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12 Replace the entire keypad assembly with a new one.
13 Reassembly is the reverse of these steps.
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Mainframe
Replacing only the display board (original style)
If changing the GC configuration, see Changing the GC
configuration for important information regarding GC
methods. Then proceed with the steps below.
1 Cool down the oven and all heated zones.
2 Turn off all gas flows at their sources.
3 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
4 Perform steps 4 through 8 of the Replacing the keypad
assembly (original style) procedure.
5 Disconnect the connector cable from the display board to the
inner connection board.
6 Remove the four screws holding the display assembly to the
keypad panel.
7 Replace the display panel, making sure it is oriented as
shown in the figure, with the connector receptacle on the
right.
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7890 Series GC IPB
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8 Reassemble all screws and cables in the reverse order of
disassembly.
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Mainframe
Replacing the keypad assembly (new style)
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Open the oven door to facilitate the removal of the front
keypad assembly.
4 Raise the detector top cover.
5 Remove three screws with -inch nut heads from the
detector electronics panel side. Two of the screws are near
the upper left and lower left corners of the front detector
signal board; the other is on the bottom of the GC in a slotted
hole.
6 Remove the T-20 screw from the bracket near the top of the
keypad assembly to release it from the GC body.
7 From the front, slide the keypad panel forward.
8 At this point there are two servicing options: replacement of
the entire keypad assembly or just the display. [See next
topic for the replacement of the display only.]
9 Reassembly is the reverse of these steps.
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7890 Series GC IPB
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Replacing only the display board (new style)
If changing the GC configuration, see Changing the GC
configuration for important information regarding GC
methods. Then proceed with the steps below.
1 Cool down the oven and all heated zones.
2 Turn off all gas flows at their sources.
3 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
4 Perform steps 4 through 8 of the Replacing the keypad
assembly (new style) procedure.
5 Disconnect the connector cable from the display board.
6 Remove the four screws holding the display assembly to the
keypad panel.
7 Replace the display panel, making sure it is oriented as
shown in the figure, with the connector receptacle on the
right.
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Mainframe
8 Reassemble all screws and cables in the reverse order of
disassembly.
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7890 Series GC IPB
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Replacing the original keypad assembly with the new assembly
NOTE
When replacing the original assembly with the new assembly, the only
new parts needed are the new Keypad Assembly (G3430-60555) and the
Door Sensor Interconnect Cable (G3430-60561). All other original parts
are reusable.
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove three screws with -inch nut heads from the
detector electronics panel side. Two of the screws are near
the upper left and lower left corners of the front detector
signal board; the other is on the bottom of the GC in a slotted
hole.
4 Disconnect the large keypad ribbon cable from the inner
connector board.
5 Remove the T-20 screw from the bracket near the top of the
keypad assembly to release it from the GC body.
6 From the front, slide the keypad panel forward.
7 Disconnect the ribbon cable from the display board.
8 Disconnect the large ribbon cable from the inner connector
board.
9 Disconnect the cable (at the lower left of the inner connector
board) from the oven door safety switch.
10 Remove the inner connector board from the GC.
11 Remove the inner connector board bracket from the GC.
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12 Connect the door sensor interconnect cable to the door
sensor cable (to extend the cable length).
13 If the new keyboard assembly does not include a display,
remove the display from the old keyboard assembly and
install it onto the new one.
14 Connect the small ribbon cable to the display board.
15 If using the new ribbon cable, connect the grounding nut to
the GC chassis.
16 Connect the large ribbon cable from the the main board to
the new keypad assembly ribbon cable.
17 Set the new keypad panel in place.
18 From the front, slide the keypad panel backward.
19 Install the T-20 screw in the bracket near the top of the
keypad assembly to fasten it to the GC body.
20 Install three screws with 1/4-inch nut heads on the detector
electronics panel side. Two of the screws are located near the
upper left and lower left corners of the front detector signal
board; the other is on the bottom of the GC in a slotted hole.
21 Lower the detector top cover, and close the oven door.
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7890 Series GC IPB
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7890 Series GC IPB
361
Mainframe
Oven temperature control
The oven temperature is controlled by a combination of the
shroud heater, the flapper assembly, and (optionally) a
cryogenic cooling assembly.
CAUTION
362
Temperature control and safety require a tight seal between the
oven door and the oven body. DO NOT place anything (such as
thermocouple leads) between these two parts. The small gap
created by a wire allows hot air to escape, which can damage or
melt nearby parts.
7890 Series GC IPB
Mainframe
Oven temperature troubleshooting
See the 7890 GC Troubleshooting manual for more detailed
procedures and details. The table below lists summary
information for reference.
WA R N I N G
The exhaust coming from the back of the GC is very hot. Keep
hands and face away from the exhaust vent.
Oven does not heat up
1 Press [Status] to check for errors to report to Agilent.
2 Power cycle the GC.
3 Check oven flapper operation.
a Increase oven temperature by at least 20 degrees.
b Verify that the oven flaps in the back of the GC are closed.
Listen to verify that the fan is operating.
If the fan is on but the flap is open, the flap motor or the
analog & power board is not functioning properly.
If the fan is off but the flap is closed, the fan motor or the
analog & power board is not functioning properly.
If the fan is off and the flap is open, the analog & power
board is probably bad.
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Mainframe
Oven not cooling or never cools
Check oven flapper operation.
1 Decrease oven temperature by at least 20 degrees.
2 Verify that the oven flaps in the back of the GC are open.
Listen to verify that the fan is operating.
If the fan is on but the flap is closed, the flap motor or the
analog & power board is not functioning properly.
If the fan is off but the flap is open, the fan motor or the
analog & power board is not functioning properly.
If the fan is off and the flap is closed, the analog & power
board is probably bad.
If using cryo cooling:
Check for sufficient cryo coolant.
Check if operating limits have been exceeded.
Bad cryo valve
Clogged cryo cooling nozzle
Cryo cooling tank does not have proper "dip tube." See the
GC, GC/MS, and ALS Site Preparation Guide.
Bad A&P board
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7890 Series GC IPB
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Testing resistance of the heater coil
If you believe that your heater coil is cracked or otherwise
damaged and has caused an open circuit, you can check it by
measuring its resistance.
WA R N I N G
Before proceeding, turn off the main power switch and unplug the
power cord.
CAUTION
Make sure you are properly grounded with an ESD strap before
continuing.
1 Turn the instrument power off.
2 Disconnect the oven heater leads (P3, P4) from the AC power
board.
3 Use an ohmmeter to measure resistance at the connectors.
Acceptable resistance ranges (in ohms) are given below.
Acceptable resistances range from the nominal value for a new,
cold heater to +5% from the nominal value.
NOTE
Resistance goes up approximately 3% after heating the coil.
Nominal cold heater
resistances, ohms
Standard oven
Fast-ramp oven
120 V
9.079.52
n/a
200 V
n/a
17.7818.7
220 V
n/a
21.5122.6
230 V
33.0634.71
23.5124.7
240 V
n/a
25.6026.9
n/a = not available
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Cryo valve installation/replacement
A cryogenic valve allows liquid nitrogen or CO2 to be dispersed
into the double-walled plenum of the GC oven where the fan
blows the vapors into the oven itself. Use the procedures that
follow to install a new cryogenic valve or to replace an existing
cryogenic valve or nozzle.
Installing a new cryo valve
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the left side cover on the instrument and remove the
plug for the cryo valve.
If a side mount carrier is installed on the left side of the
instrument, remove its left cover by removing the two bottom
screws, sliding the panel towards the back of the instrument
and lifting it off.
4 Remove the knockout on the left side of the instrument. Use
a screwdriver to pry it out.
5 Insert the cryogenic valve probe though the insulation into
the oven plenum.
6 Screw the valve to the side of the GC oven using the two Torx
T-20 screws provided.
7 If you are installing COC cryo blast for the front and/or rear
inlet(s), connect it at this time. See Cool On-Column Inlet
for details.
8 Plumb the valve to the liquid nitrogen or carbon dioxide
source.
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7890 Series GC IPB
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9 Plug the cryo valve's wiring harness into the five pin
connector to the left of the valve.
10 Route the cryo tubing through the cutout in the GC side
cover and reinstall the cover.
If a side mount carrier is installed, route the cryo tubing out
of the slot in the back of the carrier.
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Mainframe
Replacing an existing cryo valve
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the left side cover on the instrument.
If a side mount carrier is installed, remove its left cover by
removing the two bottom screws, sliding the panel towards
the back of the instrument and lifting it off.
4 Shut off the cryo fluid supply and crack the valve at the
supply to release any residual pressure.
5 Use a 9/16-inch wrench to disconnect the cryogenic fluid
supply tube at the cryo valve.
6 Disconnect the cryo valve's wiring harness from the
connector to the left of the valve.
7 Remove the two Torx T-20 screws holding the old cryo valve
and pull it straight out from the instrument.
8 To remove the valve from the bracket, disconnect any cryo
blast plumbing from the valve at the Swagelok tee. Remove
the two Torx T-20 screws on the bottom of the bracket.
9 To replace the cryogenic nozzle, proceed as follows:
a Use a 9/16-inch wrench to unscrew the old nozzle. Discard
the nozzle.
b Wrap the threads of the new nozzle with PTFE tape, being
careful not to cover the first two threads of the nozzle.
c Screw on the new nozzle and tighten firmly with a
9/16-inch wrench.
10 Insert the cryogenic valve probe though the insulation into
the oven plenum.
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7890 Series GC IPB
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11 Screw the valve assembly back on to the side of the GC oven
using the two Torx T-20 screws.
12 If you are installing COC cryo blast for the front and/or rear
inlet(s), connect it at this time. See Cool On-Column Inlet
for details.
13 Plumb the valve to the liquid nitrogen or carbon dioxide
source.
14 Plug the cryo valve's wiring harness into the connector to the
left of the valve.
15 Route the cryo tubing through the cutout in the GC's side
cover and reinstall the cover.
If a side mount carrier is installed, route the cryo tubing out
of the slot in the back of the carrier.
Removing the valve from the valve bracket (N2 valve shown)
Cryo blast attachments
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370
Mainframe
7890 Series GC IPB
Mainframe
Replacing the oven sensor
The oven temperature sensor can be replaced after removing
the oven shroud.
WA R N I N G
Before proceeding, turn off the oven and let it and any heated
zones cool. Turn off the main power switch and unplug the power
cord.
1 Remove the oven shroud as described in Replacing the oven
shroud assembly.
2 Loosen the two Torx T-20 screws securing the sensor
retainer to the back of the shroud.
3 Slide the old sensor out of the retainer. Thread a new sensor
through the opening in the rear of the oven.
4 Slide the new sensor under the retainer. One of the grill holes
on the front of the shroud is stamped. Make sure that the end
of the sensor is positioned behind the stamped hole before
tightening the retainer.
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Mainframe
Replacing the oven door sensor
The oven door sensor installs above the oven door button, and
connects to a cable that runs to the GC keyboard and display.
WA R N I N G
Before proceeding, turn off the oven and let it and any heated
zones cool. Turn off the main power switch and unplug the power
cord.
To remove the old sensor:
1 Prepare the GC. To replace the over door sensor, you will
need to tilt the GC slightly. You may need to vent and
disconnect any MS devices or otherwise move instruments
that block access or otherwise prevent you from lifting the
right side of the GC enough to reach underneath it.
2 Remove the display and keyboard assembly. See Replacing
the keypad assembly and display board. (As part of this
step, you will disconnect the door sensor cable from the
display.)
3 Pull the oven door sensor cable back through the electronics
carrier.
4 Remove the 1/4-inch socket head screw that secures the oven
door sensor to the GC.
5 Pull the oven door sensor cable through and remove the
sensor from the GC.
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7890 Series GC IPB
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To install the new sensor:
1 Feed the oven door sensor cable down through the hole
behind where the sensor mounts.
Feed cable back
into open area
behind the door
button plates.
2 With one hand, tilt the GC (raise the right side) enough to be
able to reach under it and grab the sensor cable. (Prop up if
needed.)
3 While holding the GC up, pull the cable down and through
the opening, then feed it back up and into the space behind
the oven door latch plate. Gently let the GC down.
Electronics carrier
Through hole
Reach through the
bottom of the GC
to help pull the
cable through the
opening as shown.
4 Use tweezers or similar to pull the cable up and then feed the
cable through the opening in the electronics carrier.
5 Install the oven door sensor using the 1/4-inch socket head
screw. Keep the sensor face square (flat) to the oven door.
7890 Series GC IPB
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Mainframe
The face of the sensor should be parallel to the outer edge of
the GC frame.
Sensor
1/4-in. SHCS
Cable routed to electronics carrier
6 With one hand, tilt the GC (raise the right side) and use your
other hand to set the cable wires in the retaining clip on the
GC frame. Make sure the cable wires route as shown in the
figures. Proper routing prevents the GC frame and oven door
button from clipping the cable.
Cable wires in
retaining clip
7 Reinstall the keyboard and display assembly. Check oven
door operation.
8 Turn on the GC and verify that the door sensor functions
properly.
9 Return the system to operating conditions.
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7890 Series GC IPB
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Replacing the oven shroud, oven fan, and oven fan motor
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 At the front of the GC, remove all obstructing items from
inside the oven (column(s), column hanger(s), inlet/detector
insulation cups, and so forth).
4 At the rear of the GC, disconnect the oven sensor cable at the
Analog and Power board and feed the cable back to the rear
7890 Series GC IPB
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Mainframe
of the GC. Also disconnect the two oven heater leads at the
AC board.
5 From the oven, remove the two lower screws securing the
oven shroud and loosen the upper two. These are special
stainless steel screws: the ones removed must not be
confused with any other screws.
6 Lift the shroud over the upper screws and work it out of the
oven.
NOTE
376
Connectors for the oven heater wires and for the oven sensor must be
carefully worked through the access hole at the rear of the oven. There is
also a 'plug' of insulation which may fall from the access hole during this
process: it must be replaced in reassembly from the rear of the GC.
7890 Series GC IPB
Mainframe
7 Inspect the oven heater and its supporting circular quartz
glass rod: they must be undamaged in any way.
NOTE
7890 Series GC IPB
Be very careful to not disturb the oven temperature sensor: it is fragile
and easily damaged. Also, its physical location is critical to proper oven
temperature control: do not alter its position in any way.
377
Mainframe
8 In replacement, insert oven heater leads first through the
access hole, followed by the oven sensor cable.
9 Before removing the oven fan, note its hub's physical location
on the fan motor shaft so as to return it to the same position
in reassembly.
10 Being careful to not deform its blades, remove the fan by
loosening the 5/32-inch Allen setscrew on its hub and then
pulling the fan from the motor shaft.
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7890 Series GC IPB
Mainframe
11 At the rear of the GC, disconnect the fan motor ground lead.
Then disconnect the cable to the Analog and Power board
and work the cable back to the rear of the GC.
WA R N I N G
The oven fan motor is heavy! Make sure you have a firm grip on
the motor before removing / replacing it. Always handle the
motor by the body. Do not carry the motor by the shaft.
12 Remove three 7-mm nuts with lockwashers and cone washers
to release the motor. Remove the top nut last to maintain
mechanical support for the motor. Manually support the
motor as the top nut is removed.
13 Reassembly is the reverse of these steps with the following
considerations:
Each motor mount must have both an inner and outer
cone washer
Orient the motor such that its power cable exits towards
the electronic side of the GC
Reinstall the top nut first to support weight of the motor
After motor reassembly into the GC, check that its shaft
extends perpendicularly from the back oven wall. If not
perpendicular, there may be mounting part(s) missing or
misplaced, and/or mounting nut(s) untightened.
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Mainframe
In fan replacement, make sure the fan's hub is returned to
its original location, or slightly rearward from being
exactly flush with the end of the motor shaft. Also make
sure the setscrew is tightened against the flat side of the
motor shaft.
For the oven heater/sensor shroud, if not already done,
inspect the oven heater and its supporting circular quartz
glass rod: they must be undamaged in any way
After the oven heater/sensor shroud is reinstalled,
remember to return the plug of insulation in the access
hole at the back of the oven.
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7890 Series GC IPB
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Replacing the oven flapper assembly
CAUTION
Components can be damaged by electrostatic discharge (ESD). Be
sure to wear a grounded ESD strap while performing this procedure.
1 Remove rear GC cover.
2 Remove left side GC cover.
3 Disconnect flapper motor cable and pull it back to the motor.
4 If present, remove the PTV N2 cryo feed line cover by
removing two screws. If necessary, also remove the bracket
behind the feed line cover.
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Mainframe
5 Loosen three captured T-20 screws to remove the flapper
assembly. To support the weight of the assembly, the
top-most screw should be removed last.
6 Pull the assembly straight out.
7 In replacing the assembly, steps are the reverse of removal
steps.
Install the top-most screw first to support the weight of the
assembly
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7890 Series GC IPB
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Replacing the flapper or flapper motor
This disassembly procedure enables you to replace either the
flapper or flapper motor.
1 Remove the flapper assembly. See Replacing the oven
flapper assembly.
2 Remove the T-20 set screw on the coupling between motor
and flapper shafts.
3 Remove three T-10 screws securing the motor to the frame.
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Mainframe
4 Slide the motor off the flapper shaft and replace it with a
new motor.
If you are replacing the flapper, slide the flapper out of the
duct assembly.
Be careful to not lose the bushing at the upper end of the
flapper shaft.
In reassembly, do the following:
Insure the upper part of the flapper shaft is inserted into its
bushing at the top of the duct before securing motor
mounting screws.
Line up the hole in the flapper shaft with the set screw on
the coupler mounted on the motor shaft.
Verify the flapper operation by:
Observing the flapper behavior at turn on. The flapper
self-adjusts by closing.
Set the oven temperature to 70C. The flapper should close.
Set the oven temperature to 45C. The flapper should go to
full open.
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7890 Series GC IPB
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Replacing Components Inside the Electronics Panel
Accessing the analog and power board
To access the analog and power board in the rear of the
electronics carrier, you must first remove:
The ALS controller board
The valve bracket
The logic board
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Mainframe
Replacing the ALS board
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the right side panel.
4 Remove 2 T-20 screws holding the assembly to the back of the
electronics carrier.
5 Slide out the ALS assembly.
6 Pinch and pull the 2-wire power connection at the bottom of
the assembly and set the assembly aside.
386
7890 Series GC IPB
Mainframe
7 Carefully pinch and disconnect the flex cable from J8 on the
Analog & Power board.
8 Pull the ALS module free from the back panel.
9 Connect the flex cable of the new ALS module to the Analog
& Power board.
10 Slide the ALS module hook into the 4th slot.
11 Connect the 2-wire power cable.
12 Secure the assembly with 2 screws.
13 Plug in the ALS modules and power on the GC.
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Mainframe
14 Press [Service Mode] and select Diagnostics, ALS Status. Verify
that the ALS controller model number and firmware revision
appear on the display.
15 Update the ALS controller board firmware if necessary.
For more information, see the Electronics carrier IPB.
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7890 Series GC IPB
Mainframe
Replacing the fuse on the ALS controller board
A small fuse on the ALS controller board protects it from
over-currents originating in the ALS components (Injector, for
example), or shorts in their cables. The fuse is associated with
the 42 VAC circuit. You can easily replace this fuse.
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Gather ESD protection, T-10 driver, and tweezer.
4 Remove the ALS controller board. See Replacing the ALS
board.
5 Unscrew the T-10 screw and remove the cover.
6 Using the tweezer, carefully replace the fuse.
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Mainframe
7 Reinstall the cover. Insure that the connectors are visible.
8 Reinstall the ALS controller board.
9 Before plugging in any ALS components (for example
injectors), power on the GC. Check Service Mode |
Diagnostics | ALS status to make sure the model number and
firmware revision of the board are displayed.
10 If appropriate, update the firmware to the ALS controller.
Troubleshooting
If the ALS Controller is not installed, check the cable
connections. Consider replacing the assembly.
If the firmware revision is blank, the ALS controller board
may not be programmed correctly.
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7890 Series GC IPB
Mainframe
Removing the valve bracket
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the GC right side cover.
4 Remove the ALS board. See Replacing the ALS board.
5 Remove all cables connected to the upper side of the valve
bracket (the illustration shows 2).
6 Loosen the screws at the top left and top right corners of the
bracket. Remove the bracket.
7 Disconnect the wiring harness from the Analog and Power
board at P22.
7890 Series GC IPB
391
Mainframe
Replacing the logic board
The logic board contains information specific to the GC and its
configuration, including methods, sequences, serial number,
date of manufacture, the Gateway, Subnet Mask, and IP address
of the LAN, logs, oven type, AUX heater configuration(s), and so
forth. These items must be reentered after the new logic board
is installed.
If the GC is functional, use the keypad to view and record the
following information:
Configuration-required
Gas types
Cryogenic cooling, if present
Heater assignments: valve box, MSD transfer line, others
Valve types
If the configuration includes non-Agilent components or
specials, you may need to re-enter custom heater or
pneumatic PIDs. View and record this information.
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the right side electronics panel cover.
392
7890 Series GC IPB
Mainframe
4 Disconnect the ribbon cable to the keyboard/display.
5 Disconnect the communications bus cable and cable to the
keypad and display. If present, also remove the external LAN
cable.
6 For the G3430-61010, G3430-60120, or G3430-60101 logic
and communication board, loosen the thumbscrew in the
bottom right corner of the board. If you have a G3430-60100
logic and communication board remove the two screws that
secure the logic board to the rear panel.
G3430-60101 (G3430-61010 and G3430-60120 are similar):
7890 Series GC IPB
393
Mainframe
G3430-60100:
7 Slide the logic board toward you while using a rocking
motion to unplug the board from its analog and power board
receptacle.
8 Once free of the analog and power board, slide the logic
board to the left and lift it out.
9 For 7890B, main board G3430-61010 does not use a battery
backup. Skip to the next step.
For 7890A, verify the battery backup is ON. With respect to
the new logic boards (G3430-60120 and G3430-60101), verify
battery backup switch is ON (change if needed). For the
G3430-60100 board, switch the two battery-connect switches
found next to the battery: BOTH switches must be in
positions away from the analog and power board (see above).
G3430-60101:
394
7890 Series GC IPB
Mainframe
G3430-60120 and G3430-60100:
NOTE
If switches are incorrectly-set (battery disconnected), critical internal GC
information will be lost any time AC power is not present.
10 Reinstallation is the reversal of removal steps.
11 Restore power to the GC.
12 The zero offsets for the flow and pressure sensors are stored
on the logic board rather than in the EPC modules. You must
now zero all sensors. Navigate to Service Mode | Diagnostics
| Electronics | Pneumatics to do this.
13 You must now restore information stored on the logic board
specific to the GC and its configuration.
14 Press Service mode. Scroll to Diagnostics and press [Enter].
15 Scroll to Instrument Status. Press [Enter].
16 Press [.][.][Mode/Type], select the country, and press [Enter].
17 Press [.][.] and enter the 8-digit serial number; press [Enter].
18 Scroll to Mfr date. Press [.][.] and enter 6 digits in ddmmyy
format. Press [Enter].
19 You have changed the configuration of the GC. See Changing
the GC configuration for important information regarding
GC methods.
Check GC configuration
Gas types
Cryogenic cooling
Heater assignments: valve box, MSD transfer line, others
Valve types
If the configuration includes non-Agilent components or
specials, you may need to re-enter custom heater or
pneumatic PIDs.
7890 Series GC IPB
395
Mainframe
Replacing the analog and power board
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the right side electronics panel cover.
If present, remove the ALS controller module. See Replacing
the ALS board.
4 Remove the logic board. See Replacing the logic board.
5 If present, disconnect valve box heater/sensor(s) from the
valve bracket and remove the bracket. See Removing the
valve bracket.
6 Disconnect cables at all board receptacles. G3430-60150
Analog and power board shown below (G3430-60151 is
similar).
396
7890 Series GC IPB
Mainframe
7 Remove 8 T-20 screws:
One is a long grounding screw found at the lower right
corner of the board
One screw is difficult to locate next to and above the
transformer receptacle near the right center of the board
In all cases, locate the specific screw first before you
attempt to remove it: a misplaced screwdriver may
damage nearby board components.
8 Slide the board slightly outward and to its left to release it
from the GC. G3430-60151 Analog and power board shown
below (G3430-60150 is similar).
7890 Series GC IPB
397
Mainframe
9 Installation of the new board is essentially the reverse of
removal steps with the following considerations:
Make sure the long grounding screw is returned to its
proper location
Be careful in returning all screws to their proper locations
in that you avoid accidental contact with / damage to
nearby board components
10 For the G3430-60150 Analog and power board there are three
LEDs at the upper left corner of the board: red, yellow, and
398
7890 Series GC IPB
Mainframe
green. The LEDs for the G3430-60151 Analog and power
board are located in the middle on the right next to the
REMOTE connector. When power is restored, yellow and green
LEDs should be lit (on) indicating, respectively, that
regulated and unregulated +5 VDC supplies are functional.
The red LED is lit only under FAULT conditions.
NOTE
7890 Series GC IPB
Note: The G3430-60151 analog and power board requires GC firmware
version A.01.09 or greater. If you have replaced a G3430-60150 board with
the newer G3430-60151 board, and the GC firmware is < version A.01.09,
the GC will boot into manufacturing test mode (MMON). To use the GC,
connect to it using Agilent Instrument Utility or Lab Advisor (see Using
Lab Advisor Tools: firmware update) and update the firmware.
399
Mainframe
Replacing Components Inside the Lower Rear Metal Cover
400
Item
Description
Qty
GC chassis
Pneumatics fan
Screw
Flapper assembly
Oven fan motor
Transformer
AC power board
7890 Series GC IPB
Mainframe
Replacing AC board fuse sets
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the lower rear metal cover from the GC.
4 Replace the necessary fuse set. Use of a fuse puller is
recommended for ease of removal.
NOTE
7890 Series GC IPB
The two sets of fuses on the AC board are each always replaced as a set.
401
Mainframe
Replacing the AC board
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the rear lower metal cover on the GC.
4 The AC board is located below the oven flapper assembly.
Disconnect cables (4), 2 wires to AC power receptacle, and 3
wires to the oven triac located below the board. The
configuration plug on the original board must be removed
and moved to the new replacement board.
5 At the front right corner of the board, disconnect the on/off
power switch's connecting push rod by pushing the rod
forwards towards the front of the GC until it releases from
the switch on the board.
6 Rotate the mounting thumbscrew counterclockwise until an
audible "click" sound is heard. Then slide the board slightly
towards the center of the GC and lift it off its standoffs.
402
7890 Series GC IPB
Mainframe
7 In reassembly, pay attention to the following:
Do not forget to reconnect the power switch push rod.
Make sure the new board is located on its standoffs. Then
slide it slightly away from the center of the GC such that the
mounting thumbscrew is properly positioned.
Engage the thumbscrew threads by pressing it downwards
gently while rotating clockwise.
7890 Series GC IPB
403
Mainframe
Replacing the oven triac
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
3 Remove the AC board. See Replacing the AC board.
404
7890 Series GC IPB
Mainframe
CAUTION
Carefully note BOTH physical orientation of the triac AND which of
its three leads connects to each of its terminals. A mistake here in
reassembly may destroy the new triac and/or result in a lack of
proper oven control.
4 Remove three wires from the triac.
5 Remove two 5.5-mm hex nuts with captured lockwashers
securing the triac.
6 Lift the triac straight up to remove it. Also, if necessary,
remove the thin piece of plastic film found under the triac.
7 In reinstallation, remember to first install the piece of plastic
film supplied with the new triac.
7890 Series GC IPB
405
Mainframe
Replacing the power transformer
1 Cool down the oven.
2 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
WA R N I N G
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
The transformer is very heavy! Make sure you have a firm grip on
the transformer before removing / replacing it.
3 Remove the lower rear metal cover on the GC.
406
7890 Series GC IPB
Mainframe
4 Disconnect the cable from the transformer to the AC board.
Also disconnect the ground wire to the GC frame. Finally,
disconnect the cable harness to the Analog and Power Board
and feed the harness and connector back to the rear of the
GC. Feed the two smaller cable connectors through first to
maximize room to pass through the largest of the three cable
connectors.
5 Note the orientation of the old transformer with respect to
the various cables, then remove the Allen bolt to release the
transformer. Carefully lift it from the GC.
6 In replacement, make sure the lower pad is in place, then
orient the new transformer onto the pad.
7 Replace the upper pad and associated hardware. In restoring
cables, feed the large cable and connector through to the
electronics side of the GC first.
7890 Series GC IPB
407
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
10 Valves
Valves 409
Valve Box 417
Actuators 423
Valve actuator drivers 431
Typical Valve Configurations 442
Troubleshooting 452
Agilent Technologies
408
Valves
10
Valves
Valves are used to modify the carrier gas flow during an
analysis. Among their uses are:
Highly reproducible injections, both liquid and gas
Changing the order of columns
Backflushing to eliminate high-boilers
Column selection
and many others. Some examples are included in this section.
In this GC, valves are rotated by air-driven actuators. This keeps
electrical activity away from where hot sample might leak. The
air is controlled by solenoid valves located behind the right side
cover.
7890 Series GC IPB
409
10 Valves
Introduction
This document does not provide instruction for first time
installation of any of the options discussed. The add-on sheets,
which accompany the various options, exist for just this
purpose, and should be referenced when performing a first time
installation.
The valves described in this manual are W-series minivalves,
manufactured by VALCO Instruments Co, Houston, Texas. The
valve body is made of Nitronic-60 nickel steel with 1/16-inch
fittings.
Proper instrument operation will prolong the life of the valve
system. Read all the accompanying information and avoid the
following operational abuses:
Exceeding the specified temperature and pressure ranges
Plugging a valve with column packing or sample
precipitation
Scoring valve surfaces with column packing or particulates
in liquid or gas sample
Contaminating the system with samples (non-eluting
materials) or poor quality support gases
Because valves operate best at a constant temperature, the GC
places valves in their own heated compartment.
WA R N I N G
410
To reduce the fire hazard when sampling flammable gases or
liquids under pressure, operators should routinely make
pressure-leak tests of the plumbing, fitting and valves. Both valve
positions should be checked. Depending on the nature and
pressure of the sample stream, periodic pressure leak test and
visual inspection should be made since wear or use could cause
leaks to develop. Leaks may occur inside the valve box and be
concealed from the operators view.
7890 Series GC IPB
Valves
10
Valco W-series minivalves
Valves consist of a driver, valve body, rotor, and preload
assembly.
Valve bodies
Body parts are made from Nitronics 60 nickel steel. If required,
the valve may also be produced from Hastelloy C. External
tubing (plumbing) is connected to the valve body ports by
ferrules and fittings provided with the instrument.
The left (CCW, counterclockwise) and right (CW, clockwise)
stops on general purpose valve bodies limit rotor rotation so the
correct flow path results when the index pin is close to or
against either stop of the index lip.
CAUTION
7890 Series GC IPB
Intermediate positions of the rotor may result in an interrupted flow
path which could cause damage to the valve or other components
in the chromatograph.
411
10 Valves
Valve rotors
Rotor type can be identified by color:
An off-white rotor is made of a PTFE composite and may be
used from room temperature to 200C.
A black rotor is made of polyimide and may be used from 100
to 350C.
CAUTION
The life of a valve is shortened if used outside its specified
temperature range. Do not mix rotor types in the same system.
The rotor seats on a highly polished conical surface. When
properly seated, the polished surface prevents leakage around
the rotor and between non-selected ports. The finish precludes
adsorption of most GC samples.
The rotor assembly is a one-piece part with an integral molded
and machined conical hub and the parts necessary for proper
seating. The sample contacts only the PTFE composite (low
temperature) or polyimide (high temperature) as well as the
stainless steel of the valve.
Grooves in the rotor surface form the paths between specific
ports. The index pin prevents rotation beyond either stop of the
index lip. Valve ports are connected by the grooves only when
the index pin is close to or against either stop. Intermediate
positions result in flow shutoff through the valve and possible
damage if left in this position.
Preload assembly (not shown)
This assembly consists of a body, a spring, and an adjusting nut.
It holds the rotor in the valve body.
412
7890 Series GC IPB
Valves
10
Valco W-series minivalve
Valve bodies
Body parts are made from Nitronics 60 nickel steel. If required,
the valve may also be produced from Hastelloy C. External
tubing (plumbing) is connected to the valve body ports by
ferrules and fittings provided with the instrument.
The left (CCW, counterclockwise) and right (CW, clockwise)
stops on general purpose valve bodies limit rotor rotation so the
correct flow path results when the index pin is close to or
against either stop of the index lip.
CAUTION
7890 Series GC IPB
Intermediate positions of the rotor may result in an interrupted flow
path which could cause damage to the valve or other components
in the chromatograph.
413
10 Valves
Valve rotors
Rotor type can be identified by color:
An off-white rotor is made of a PTFE composite and may be
used from room temperature to 200C.
A black rotor is made of polyimide and may be used from 100
to 350C.
CAUTION
The life of a valve is shortened if used outside its specified
temperature range Do not mix rotor types in the same system.
The rotor seats on a highly polished conical surface. When
properly seated, the polished surface prevents leakage around
the rotor and between non-selected ports. The finish precludes
adsorption of most GC samples.
The rotor assembly is a one-piece part with an integral molded
and machined conical hub and the parts necessary for proper
seating. The sample contacts only the PTFE composite (low
temperature) or polyimide (high temperature) as well as the
stainless steel of the valve.
Grooves in the rotor surface form the paths between specific
ports. The index pin prevents rotation beyond either stop of the
index lip. Valve ports are connected by the grooves only when
the index pin is close to or against either stop. Intermediate
positions result in flow shutoff through the valve and possible
damage if left in this position.
414
7890 Series GC IPB
Valves
10
General purpose valves
The 6- and 10-port general purpose valves are suitable for
column switching, isolation, backflushing, and other uses as
well as gas sampling.
Gas sample valves
The standard gas sample valves have 1/16-inch zero dead
volume fittings and an internal port diameter of 0.016-inch.
6-port valve (actuator side view) showing flow path grooves
Gas sample loops
A 0.25 mL sample loop is included with all gas sampling valve
systems. 10 mL and 5 mL loops occupy one valve position,
limiting the number of valves that can be housed in a valve
compartment.
Adjustable restrictor valves
Adjustable restrictors are used to balance flow resistance
between the two valve positions. They are available with
ambient to 225C (part no. 0101-0633) or ambient to 350C
(part no. 0101-0948) operating ranges.
7890 Series GC IPB
415
10 Valves
Liquid sample valves
Agilent Technologies offers 4-port LSVs with 0.2, 0.5, or 1 L
internal loops.
These valves are designed for liquefied gases under pressure
such as ethane, propane, butane, LNG, etc. They are not
intended for nonvolatile liquids (at room conditions) where a
concealed leak could allow an accumulation or pool of liquid to
form that may present a significant fire hazard.
All liquid sample valves have 1/16-inch fittings. The 0.5 L size
is available in low- (1000 psig limit) and high-pressure (5000
psig) versions; the other sizes are low-pressure (1000 psig) only.
An adjustable restrictor may be used on the sample outlet line
to maintain internal sample pressure to keep a compressed gas
liquefied.
Temperature ranges
CAUTION
1/16 inch PTFE rotor valves
0 to 200 C
Adjustable restrictor valves
Ambient to 225 C
The life of an LSV is shortened if used outside its specified pressure
and temperature ranges. Highly dangerous leaks can occur if the
valve box temperature ever exceeds the specified temperature
limits.
Adjustable restrictor valve
The adjustable restrictor supplied with a liquid sample valve is
designed for temperatures up to 225C; it is NOT compatible
with high-temperature valves.
416
7890 Series GC IPB
Valves
10
Valve Box
Installing the valve box
The valve box sits on top of the GC and contains the valves and
plumbing, heated zones and sensors, and the insulation.
1 Use a pair of diagonal cutters to remove the metal cutout on
the top of the GC.
WA R N I N G
Be careful of sharp edges!
Cut toward the outside edge of the tabs so that the valve box
will fit correctly.
2 Screw the aluminum standoffs into the valve box bottom
plate using one Torx T-20 screw for each standoff.
3 Screw the valve box bottom plate onto the top of the GC
using three Torx T-20 screws.
4 There are six holes in the plate for up to four valves. The
outside holes on each side of the plate are for valves and the
inside holes are for plumbing into the GC. Punch out the
pre-perforated insulation from the holes you plan to use.
5 Use two Torx T-20 screws to mount the heater block(s) on the
valve box bottom plate.
6 Install the heater/sensor into the heater block(s) and secure
the leads to the valve box bottom plate with the U-clamp and
two Torx T-10 screws.
NOTE
Make sure that the sensor is seated all the way in the heater block.
7 Insert the valve(s) into the appropriate hole(s) in the heater
block and secure each valve with two long Torx T-10 screws.
8 Plumb the valves in the appropriate configuration. A variety
of valve configurations are diagrammed in the Typical Valve
Configurations section in this chapter.
9 Orient all of the valves in the OFF (CCW) position.
7890 Series GC IPB
417
10 Valves
10 Place the valve box insulation in the valve box top. Make sure
the perforations in the insulation line up properly with the
valve box top.
11 Insert the insulation retainer plate in the bottom of the valve
box top and secure it to the threaded studs using the two
5.5-mm nuts.
Tighten the nuts until they are flush with the top of the stud.
Make sure the holes in the retainer plate line up with the
perforations in the insulation.
12 While wearing a pair of protective gloves and holding the
valve box top over a waste receptacle, punch or cut out the
insulation from the appropriate holes.
13 Use two Torx T-20 screws to secure the valve box top over the
installed valves, making sure the heater/sensor leads are
routed under the appropriate cutout(s).
Make sure the valve box top is oriented correctly with holes
punched out over the installed valves.
14 Install the actuators as described in the Actuators section
of this chapter.
Figure 7
418
Removing the sheet metal cutout. 6890 shown.
7890 Series GC IPB
Valves
7890 Series GC IPB
Figure 8
Attaching the standoffs to the bottom plate
Figure 9
Attaching the bottom plate to the GC
10
419
10 Valves
Figure 10 Attaching heater block to the bottom plate
Figure 11 Installing valves
420
7890 Series GC IPB
Valves
10
Figure 12 Valve in the OFF position (top view)
Figure 13 Installing the valve box top assembly
7890 Series GC IPB
421
10 Valves
Removing the valve box assembly
1 Place the main power switch in the off position.
WA R N I N G
Hazardous voltages are present in the instrument when the power
cord is connected. Avoid a potentially dangerous shock hazard by
disconnecting the power cord before working on the instrument.
2 Unplug the line power cord from its receptacle.
3 Allow some time for the oven and heated zones to cool.
4 When the oven has cooled, turn off all gas supplies.
5 Switch the solenoid valve off so the actuator is in its fully
extended position (piston rod extended).
6 If variable restrictors are present, remove their mounting
hardware in the following order: two Torx T-20 screws, hex
nut, and mounting bracket for each restrictor valve.
7 Remove the two Torx T-20 screws securing the valve box top
assembly to the standoffs. Lift the valve box top assembly
straight off the valve box. Be careful not to move the valve
rotor index pin from its "at rest" position.
NOTE
If valve/actuator alignment is to be made, see Valve actuator alignment
in this section.
8 To reassemble: Align the two mounting holes in the valve box
top assembly with the standoffs in the valve box. Lower the
box top assembly until it rests on the standoffs.
9 Secure the valve box top assembly with two Torx T-20
mounting screws. Tighten these screws firmly. Reinstall
hardware for variable restrictors if present.
10 Exercise the valve(s) on and off a few times to verify
operation.
422
7890 Series GC IPB
Valves
10
Actuators
Valve rotors are driven by air-operated actuators. The air is
controlled by solenoid valves inside the right side panel.
Installing the actuators
The actuators use pneumatic pressure (40 to 70 psi) to switch
the valves between their two positions.
1 After installing the valves and valve box as described in the
Valve Box section, you can install the valve actuators.
2 Set each actuator to the appropriate degree of rotation. Move
the grenade style pin to the hole on the actuator marked with
the correct degree of rotation, as shown below:
Four port valvesPlace the pin in the 90 hole
Six port valvesPlace the pin in the 60 hole
Ten port valvesSame as six port valves, but with the
tubular 36 actuator limiter on the pin.
3 Mount an actuator over each valve installed using two Torx
T-20 screws.
4 Engage the actuator drive shaft coupler with the valve.
a Loosen the hex nut on the actuator near the drive shaft.
b Slide the shaft down.
c Insert a flat bladed screw driver in the slot on the top of
the actuator and turn the shaft back and forth until you
feel the coupler engage the valve.
d Tighten the set screw.
5 Install the valve actuator drivers.
7890 Series GC IPB
423
10 Valves
Mounting the actuator on the valve box
Engaging the actuator drive shaft with the valve
424
7890 Series GC IPB
Valves
10
Setting the actuator's degree of rotation
7890 Series GC IPB
425
10 Valves
Installing the actuator on a heated valve box
WA R N I N G
The valve box is insulated with a fibrous material that can cause
irritation to the skin, eyes, and mucous membranes. Always wear
gloves when working with the insulation. If the insulation is
flaky/crumbly, wear protective eyewear and a respirator.
Before continuing, install the heated zone kit (if purchased) as
described in the instructions included with that accessory. Also
install any new rotary valves into the valve box. Leave the GC
covers off and the power cord disconnected.
1 Hold the upper valve box over a trash can, then remove the
pre-cut insulation from the appropriate hole in the upper
valve box. Remove any excess or loose pieces from around
the hole.
2 Verify that all valve rotors are in the full counterclockwise
position (valve Off).
3 Locate the two half-moon cutouts at the bottom back of the
upper valve box. Place the upper valve box on top of the
lower valve box assembly, routing the heater/sensor wires
through the cutouts. Secure with two T- 20 mounting screws.
4 Install the new valve actuator.
a Insert the actuator through the valve box cover.
b Push the coupling/shaft assembly downward with a
flathead screwdriver until the slot on the coupling
engages the rotor index pin.
426
7890 Series GC IPB
Valves
10
If the coupling and valve do not engage, check that both are
fully counterclockwise and try again. If necessary, turn the
shaft slightly to engage the coupling.
c Secure the actuator to the valve box with two T- 20 Torx
screws provided in the kit.
5 For each actuator that mates with a newly installed valve:
a Loosen the adjustment set screw.
b Using a flathead screwdriver, turn the rotor adjustment
shaft counterclockwise until it stops, then back it off a
small amount (< 1 mm) to set one end of the rotor's
motion.
7890 Series GC IPB
427
10 Valves
c Tighten the adjustment set screw.
428
7890 Series GC IPB
Valves
10
Installing the actuator on a side mount bracket
1 Install the side mount bracket on the left side of the GC using
four machine screws.
2 Attach the clamp ring to the back of the bracket with two
screws.
3 Align the actuator assembly with the upper or lower
standoffs. The cylinder must be down. Insert the actuator
drive though the hole in the bracket, and secure with two T20 Torx screws.
7890 Series GC IPB
429
10 Valves
Valve actuator alignment
1 Remove the valve box top assembly. See steps 1 through 3 of
Removing the valve box assembly for the procedure.
2 Loosen the actuator link arm lock screw at each actuator
with a 3 mm hex key wrench so that the coupling/shaft
assembly is free to rotate. Push the coupling shaft fully into
the actuator.
3 Turn the valve rotor index pin of each valve
counterclockwise until it is 0.010 inch (0.25 mm) from the
counterclockwise (left-hand) valve stop.
4 Reinstall the valve box top assembly.
5 Gently rotate and push the coupling/shaft assembly with a
blade-type screwdriver until the slot on the coupling fully
engages the valve rotor index pin. Repeat this procedure for
each valve installed.
CAUTION
Use care in performing the following operation so as not to
accidentally turn the valve rotor away from its preset (step 3)
position.
6 Make sure that all solenoid valves are turned "off" by the
appropriate valve controller. Turn on the air supply to the
solenoid valve(s). The piston rod of each actuator will move
all the way out to the extended (OFF) position. Very firmly
tighten the link arm lock screw for each actuator.
7 Install the hardware for any variable restrictors present.
430
7890 Series GC IPB
Valves
10
Valve actuator drivers
Solenoid differences
Beginning in April 2010, a new type of solenoid valve became
available to drive the GC valve actuators. The new solenoid
valve, made by Airtek, is not compatible with the original
solenoid valve. They function in the same way, but mount
differently and require different valve brackets.
Which solenoid valve is installed?
Any valve installed on a GC before April 2010 used the original
style solenoid. Upgrading to the new solenoid requires a
replacement of the entire driver stack assembly (valve bracket,
elbow, solenoids, and mounting hardware).
You can easily distinguish between the solenoid valve types, as
shown below. The new style solenoid valve has a silver metal
fitting instead of a red pressure vent button.
Replacing an original solenoid valve
If replacing an original style solenoid valve, first try to order the
original replacement part. If that part is not available, then you
will need to replace the entire solenoid stack assembly. See the
chapter on Valves in the IPB for assembled stack part
numbers.
7890 Series GC IPB
431
10 Valves
Installing a new valve stack assembly
If installing a new valve stack assembly, order the new style
parts.
Original style
Assemble the valve driver block
The valve driver block accommodates up to four valve drivers. A
valve driver must be installed for each valve/actuator installed.
1 Install two mounting posts on the intake/exhaust endplate
(two large threaded holes). Install an O-ring in the
supply/exhaust ports on the inside of the plate.
2 Slide a valve driver over the mounting posts in the
orientation shown. Install two O-rings in the valve driver
supply/exhaust ports as shown.
3 For each additional valve installed, install two more
mounting posts and a valve driver with O-rings in the same
manner as the first.
4 When all the drivers have been installed, screw on the other
end plate with the two hex screws as shown.
432
7890 Series GC IPB
Valves
10
Install the bracket and cabling (original style)
1 Install the valve actuators before installing the valve actuator
drivers.
2 Screw the valve driver bracket into the right side of the GC
using the two captive screws.
3 Plug the connectors on the valve driver cable harness up
through the slots on the valve driver bracket.
4 Plug the larger 2 2 heater sensor connectors (P1, P2) into
the outside slots and the smaller 1 2 valve driver
connectors (P3 to P6) into the four middle slots.
5 Plug in the heater/sensor lead(s) from the valve heater
blocks on top of the GC. Thread the heater/sensor lead(s) to
the right side of the instrument, through one of the keyhole
wiring slots and into the P1 or P2 connector on the actuator
bracket.
7890 Series GC IPB
433
10 Valves
Installing the valve driver block
1 Slide the valve driver block down into the driver bracket
until the drivers plug into the connectors.
NOTE
To remove drivers from the driver block, use a hex wrench to unscrew
the two hex screws on the left side of the block. Remove the driver,
collapse the block to the width of the remaining drivers and reinstall the
hex screws.
2 Plug the other end of the valve driver cable harness into the
P22 connector on the analog and power board.
3 Wrap the threaded ends of the 90 elbow fitting in PTFE pipe
tape. Screw the fitting into the air supply intake on the side
of the valve driver block facing the rear of the GC.
The supply intake is the outside threaded hole, the one
farthest from the analog and power board.
4 Run a length of 1/4-inch tubing out the hole on the rear of the
GC in the lower left corner (when facing the rear of the
instrument). Connect this tubing to your air supply.
5 Unscrew the screw plugs (if present) on the top of each
driver you are using. Replace the screw plugs with tubing
connectors.
6 Plumb the tubing from each installed actuator to the tubing
connectors on the corresponding driver. The tubing from the
side of the actuator goes to the connector farthest from the
board. Grip the tubing with a piece of sandpaper and push it
onto the tubing connector.
434
7890 Series GC IPB
Valves
7890 Series GC IPB
10
435
10 Valves
New style
Replacing a solenoid valve (new style)
To replace a new style solenoid valve:
1 Turn off the valve actuator air supply.
WA R N I N G
The detector, inlet, oven top, and valve box may be hot enough to
cause burns.
2 Remove the GC right side cover.
WA R N I N G
Hazardous voltages are present when the GC electronics are
exposed.
3 Press and hold the switch on the bottom of one of the
solenoid valves until no residual air pressure remains.
4 Turn off the GC and unplug the power cord. If installed,
allow the heated valve box to cool.
5 Disconnect the valve box heater wires to the A1 connector.
436
7890 Series GC IPB
Valves
10
6 Disconnect the tubing from the broken or damaged solenoid
valve.
7 Remove the two screws that hold the end plates and existing
valves together.
8 Use a 4-mm hex key to remove the screw that holds the
solenoid stack left end plate in place.
7890 Series GC IPB
437
10 Valves
9 Remove the broken or damaged solenoid valve wires from the
wire connector on the valve bracket.
10 Replace the solenoid valve(s).
11 Plug the new solenoid valve wires into the appropriate valve
bracket connectors. See the diagram below.
12 Reassemble the solenoid stack including the new solenoid
valve and left end plate. While holding the valves in one
hand, align them as best as possible, then slide a screw
through the left end plate and solenoids.
Use 25 mm screws for 1 solenoid
Use 50 mm screws for 2 solenoids
Use 70 mm screws for 3 solenoids
Use 85 mm screws for 4 solenoids
Repeat for the second screw. Both screws should extend a
little bit out of the last solenoid.
13 Line up the stack screws with the holes in the right end plate
and assemble. Before tightening, align the solenoid valves so
their tops are even.
14 Use the screw removed in step 8 to install the left end plate
to the valve bracket. Be careful not to trap any wires behind
the plate.
15 Reconnect the valve box heater wires to the A1 connector.
16 Connect the tubing from the actuator to the new solenoid
valve by pushing it into the press fitting.
The tubing from the side of the actuator connects to the
outside fitting on the solenoid (the fitting furthest from
the electronics board, labeled 2).
Trim the tubing as needed to keep installation neat.
438
7890 Series GC IPB
Valves
10
17 If installing new tubing, cut the tie-wrap around the tubing
leading from the actuator and route the tubing as shown
below.
7890 Series GC IPB
439
10 Valves
18 Turn on the valve actuator air.
WA R N I N G
Hazardous voltages are present when the GC electronics are
exposed.
19 Connect the GC power cord and turn on the GC.
20 Press the switch under each solenoid to activate it and
pressurize the system.
21 The solenoid valve replacement is complete. If no other
accessories or parts require installation, reinstall all GC
covers.
440
7890 Series GC IPB
Valves
10
Installing the valve driver (solenoid) bracket, cabling, and elbow
fitting (new style)
1 Install the valve actuators before installing the valve actuator
drivers (solenoids).
2 Screw the valve driver bracket into the right side of the GC
using the two captive screws.
3 Plug the valve driver bracket cable harness into P22 on the
GC board.
4 Plug the connectors on the valve driver cable harness up
through the slots on the valve driver bracket.
Plug the larger 2 2 heater sensor connectors A1 and A2 into
the outside slots and the smaller 1 2 valve driver
connectors V1 to V4 into the four middle slots.
5 Wrap the threaded ends of the 90 elbow fitting in PTFE pipe
tape. Screw the fitting into the air supply intake on the side
of the valve driver block facing the rear of the GC.
The supply intake is the outside threaded hole, the one
farthest from the analog and power board.
6 Run a length of 1/4-inch tubing out the hole on the rear of the
GC in the lower left corner (when facing the rear of the
instrument). Connect this tubing to your air supply.
7890 Series GC IPB
441
10 Valves
Typical Valve Configurations
442
7890 Series GC IPB
Valves
10
Option numbers
Numbers of the form n0n are for standard temperatures
(ambient to 200 C).
Numbers of the form n3n are for high temperatures (100 to
350 C).
Custom Plumbing (diagram required), Option 700 or 730
Custom Plumbing (Diagram Required), Option 700 or 730
Gas Sampling Option, Option 701 or 731
Gas Sampling Option, Option 701 or 731
7890 Series GC IPB
443
10 Valves
Column Isolation, Option 702 or 732
Column Isolation, Option 702 or 732
High temperature needle valve supplied with option 732
Two Stream Selection (Requires Gas Sampling), Option 703 or 733
Two Stream Selection (Requiers Gas Sampling), Option 703 or
753
444
7890 Series GC IPB
Valves
10
Backflush to Detector, Option 704 or 734
Backflush a Precolumn to Vent, Option 705 or 735
7890 Series GC IPB
445
10 Valves
Column Selection (Unused Column Isolated), Option 706 or 736
Sequence Reverse, Option 707 or 737
446
7890 Series GC IPB
Valves
10
Sequence Reverse with Backflush of Column 1, Option 708 or 738
Custom Plumbing (Diagram Required), Option 800 or 830
Custom Plumbing (Diagram Required)), Option 800 or 830
7890 Series GC IPB
447
10 Valves
Gas Sampling with Backflush of Precolumn to Vent, Option 801 or 831
Gas Sampling with Backflush of Precolumn to Vent, Option 801
or 831
Gas Sampling with Backflush to Detector, Option 802 or 832
Gas Sampling with Backflush to Detector, Option 802 or 832
448
7890 Series GC IPB
Valves
10
Gas Sampling of Alternate Streams, Option 803 or 833
Gas Sampling with Sequence Reverse, Option 804 or 834
7890 Series GC IPB
449
10 Valves
Gas Sampling with Sequence Reverse and Backflush of Column 1, Option
805 or 835
Gas Sampling with Sequence Reverse and Backflush of Column
1, Option 805 or 835
Column Selection with Backflush to Vent, Option 806 or 836
450
7890 Series GC IPB
Valves
10
Liquid Sampling, Options 850, 852, 854, and 856
7890 Series GC IPB
451
10 Valves
Troubleshooting
Most of the problems associated with sampling valves are
related to peak broadening in transfer lines and inlets, sample
adsorption by the valve or transfer lines, leaks, and
perturbations in the baseline.
Chromatographic symptoms
Troubleshooting valves and their related plumbing is primarily
a matter of systematic checking and verification of unimpaired
mechanical operation of any moving part. This requires an
understanding of how the valve functions internally and how
the plumbing is configured. A plumbing diagram is essential for
effective troubleshooting.
The following "symptom-cause" list gives the most commonly
encountered problems found with valves and their solution.
Symptom
Possible cause
Lost peaks (degradation) Valve or transfer lines
too hot
Reduce temperature 50
C, reevaluate
Transfer line activity
Use nickel or Hastelloy
tubing
Lost or tailing peaks
Valve or transfer line too
cold
Increase temperatures
50 C, reevaluate
Baseline perturbation
Slow valve rotation
Increase actuator
pressure
Rotor distorted
Replace rotor
Sample/column
pressure too different
Add back-pressure
regulator to sample drain
Peak tailing broad peaks Column overload
452
Solution
Use smaller sample loop
Increase split flow
Flow too slow
Increase column flow
Increase split flow
System voids
Check connections
Reduce volume of
connecting tubing
7890 Series GC IPB
Valves
10
Loss of sensitivity or excessive drift
Several possible causes exist for overall deterioration of the
chromatogram.
Contamination in the valve requires a thorough cleaning.
Internal leakage requires a complete disassembly and
inspection of the mating surfaces.
Poor temperature control may require a full check of
electronic and thermal components.
Lack of proper conditioning techniques, columns, etc.
Failure or deterioration of other components (columns,
detectors, etc.).
Loss of peaks in specific areas of the chromatogram
Entire sections of chromatographic data can be lost due to a
valve that does not rotate or one that rotates improperly. Other
than obvious component failures (solenoid, actuator, etc.),
improper adjustments and misalignments cause most problems.
Check that adequate air (about 482 kPa or 70 psi) is
supplied.
Check the valve. Is it rotating?
If the valve rotates, check for proper alignment of the
actuator, mechanical binding or slippage of connecting parts.
Check for blocked flow paths with valve in both positions.
Extraneous peaks
Air peaks are sometimes seen in a chromatogram when leakage
occurs because the valve rotor does not seal properly. These
leaks may not be detectable using the soap-bubble method.
If a leak is suspected but cannot be located with soap bubbles, a
pressure check will determine definitely if a leak exists.
Extraneous peaks can occur due to contamination or improper
conditioning of the valve. If leaks are not apparent, clean or
condition the valve.
Other causes, totally unrelated to the valve, may produce
similar symptoms. Impure carrier gas (i.e., containing water)
can cause extraneous peaks.
7890 Series GC IPB
453
10 Valves
Peak broadening and tailing
Voids in the flow system (valve and connecting tubing) cause
tailing and peak broadening. Use inlets and liners with small
internal diameters and connect the valve to the inlet or column
with short lengths of connecting tubing of narrow inner
diameter.
If early-eluting peaks are too broad, stationary phase or thermal
focusing effects should be used with packed-column ports or
increased split flows when capillary split inlets are used. Inlets
should be equipped with narrow inner diameter liners, and
narrow-bore connecting tubing should be used between the
valve and inlet.
Baseline shifts
Baseline perturbations are caused by changes in column flow as
the valve is rotated and as the sample loop equilibrates to
system pressure. Slow valve rotation momentarily stops carrier
gas flow and, when the valve stops rotating, a sudden increase
in flow occurs which slowly returns to the set point. Check
actuator pressure (usually 40 to 75 psi), valve rotor tension, and
valve temperature to ensure that the valve rotates as quickly as
possible. A restrictor or backpressure regulator can be added to
the sample vent line to maintain the sample loop at system
pressure. This will reduce the time it takes for the flow to
stabilize after the valve is switched.
Baseline upsets
Frequently, baseline upsets are seen on chromatograms when
valves are switched. These upsets are caused by pressure
changes within the system, injections of large volume samples,
or by changing the amount of restriction in the flow path. These
upsets will become more of a problem when high sensitivity is
required. Addition of a fixed restriction downstream from the
valve may help minimize the upset. Changes in column length
may also help reduce the upsets.
Fixed restrictors are used immediately before flame detectors
to prevent flameout and are used in some instances to prevent
pressure surges from damaging TCD filaments. An adjustable
restrictor (needle valve) can also be used where a matched
restriction is desired but not for preventing pressure or flow
surges.
Often confused with baseline upsets, an offset is a shift in the
baseline that does not return quickly to the original level.
454
7890 Series GC IPB
Valves
10
Baseline offsets may be caused by air leaks but more commonly
are due to a change in gas purity or flow rate in the detector.
Poor carrier gas or improperly conditioned filters and traps
should be suspected whenever offsets occur.
Variation in peak area and retention time
The amount of sample contained in the loop and, therefore, the
amount injected onto the column is affected by loop pressure
and temperature. Variations in pressure and temperature lead
to variability in peak areas. Flow restrictors or back-pressure
regulators help to maintain constant loop pressure, and valve
boxes help maintain temperature.
Leaks can occur in the valve itself or at any of the connecting
points with transfer lines. Leaks usually cause area
irreproducibility, retention times changes, and increases in the
area of air peaks (with thermal conductivity detectors). Leaks
in rotors can sometimes be fixed by tightening the nuts holding
the rotor in the valve body. Leaks in connections are usually
found with an electronic leak detector or with a liquid leak
detection fluid (e.g., Snoop).
Pressure check
Leak checking the plumbing involved in a valve system must be
done carefully and methodically. The pressure check method
below will indicate, but sometimes not isolate, a leak in the flow
path. Since this method does not necessarily isolate the leak,
other leak check methods may be needed to locate the leak
specifically.
NOTE
Each valve in a system has two flow paths, ON and OFF. A leak
sometimes occurs in only one of these two positions. Check both.
1 Disconnect the detector from the valve system.
2 Cap the valve system at its outlet and pressurize to 689 kPa
(100 psi). Allow 2 to 5 minutes for pressure to equilibrate. If
your instrument has flow control, it should read zero flow.
3 Turn off the gas supply at the source.
4 Generally, the pressure will drop quickly for approximately
30 to 60 seconds, then stabilize. After this initial pressure
drop, the gauge should not indicate more than a 7 to 14 kPa
(1 to 2 psi) drop during a 10 minute period.
7890 Series GC IPB
455
10 Valves
5 If no leak is indicated, actuate all valves and repeat steps 2 to
4.
6 If a leak does show up, try to pinpoint the source using a
soap bubble meter. Do not assume that the leak exists only at
the valve. Often plumbing connections such as unions or
bulkhead fittings are at fault. See Valve Box should it
become necessary to expose the valve system.
7 If the leak cannot be found easily, divide the system in half
and repeat the pressure check. Continue dividing in halves,
and pressure check until the leak is isolated.
456
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
11 Capillary flow technology (CFT)
devices
CFT overview 458
Ultimate union 460
Agilent Technologies
457
11 Capillary flow technology (CFT) devices
CFT overview
CFT devices consist of a plate and tubing. Ultimate unions are
often used with CFT devices and are described here.
A CFT plate consists of two thin metal plates that are bonded
together. Gas passages are left between the plates, and tubing
fittings are brazed to the surface. Finally, the gas passages are
deactivated. This results in a sturdy and inert unit with a very
low thermal mass.
Accessories contain the plate, plus installation/use instructions
and some related parts (ferrules, nuts, tubing, etc.) needed for
use.
The following accessories and plates are available at the time of
writing.
Description
Accessory
Plate only
Deans switch
G2855B
G2855-61500
Splitter, 2-way with
make-up gas
G3180B
G3180-61500
Splitter, 2-way without
make-up gas
G3181B
G3181-60500
Splitter, 3-way with
make-up gas
G3183B
G3183-60500
Quick Swap for MSD
G3185B
G3185-60065
Tubing connects plates with one another and with other parts
of the analytical path.
Description
Part Number
CPM-1/16-inch x 0.010 -inch id tube, 50cm
G1580-80060
CPM-1/16-inch x 0.20-inch id tube, 50cm
G1580-80062
Fused silica, deactivated, 0.20 mm x 5 m
160-2205-5
Fused silica, deactivated, 0.25 mm x 5 m
160-2255-5
Fused silica, deactivated, 0.18 mm x 10 m
160-2615-10
Fused silica, deactivated, 0.10 mm x 5 m
160-2635-5
Miscellaneous parts are used in making column connections.
458
7890 Series GC IPB
Capillary flow technology (CFT) devices
7890 Series GC IPB
Description
Part number
Oven bracket kit
G2855-60140
Reducing union, 1/8-inch to 1/16-inch
0100-0241
Restrictor, SS, 1/16-inch od x 0.01-inch id x 1 m
0100-2354
Union, SS, 1/16-inch
0100-0124
Screw, T-20, M4 x 8 mm
0515-2755
Column storage fitting
G2855-20590
Wire, SS, 0.015-inch x 40 mm
G2855-60593
Plug for CFT fittings or unions
G2855-60570
QuickSwap transfer line locking nut
G3185-20501
Deans switch supplies kit
G2855-60150
11
459
11 Capillary flow technology (CFT) devices
Ultimate union
This union combines a stainless steel body, inert metal ferrules,
and very low dead volume to provide durable connections of
capillary columns, retention gaps, pre-columns, and other
capillary devices.
Tools and kits
The kits do not contain ferrules. The appropriate size must be
ordered separately.
460
Part number
Description
G3182-61580
Union kit, deactivated
G3182-61581
Union kit, non-deactivated
G2855-20530
Internal nut
G2855-20555
Swaging nut
8710-0510
5/16 x 1/4 open end wrench (need 2)
5181-8836
Column cutter
7890 Series GC IPB
Capillary flow technology (CFT) devices
11
Metal ferrules and nuts
Identify the internal diameter of your column and select the
part number for the appropriate sized nut and ferrule. Each
packet contains an internal nut.
Part number
Description
5184-3569
Metal ferrules, 0.1- to 0.25-mm columns, pkg of 10
5184-3570
Metal ferrules, 0.32-mm columns, pkg of 10
5188-2789
Metal ferrules, 0.53-mm columns, pkg of 10
Assembling nut, ferrule and swaging nut
1 Thread the column end through the internal nut and the
ferrule leaving approximately 3 cm of column protruding
beyond the ferrule. Thread the swaging nut onto the internal
nut with the column protruding.
2 Tighten the two nuts together a little at a time, occasionally
checking to see if the ferrule is grabbing the column. When
the ferrule just starts to grab, notice the position of the nut
and then tighten the nuts by turning 60 degrees (one flat).
7890 Series GC IPB
461
11 Capillary flow technology (CFT) devices
3 Remove the swaging nut.
4 Rest the ceramic column cutter on the small end face of the
ferrule at a 45-degree angle.
462
7890 Series GC IPB
Capillary flow technology (CFT) devices
11
5 Scribe the column, then break off the end. It should break off
with approximately 0.3 mm of column extending beyond the
ferrule. It is important that you cut the column to a
maximum of 0.5 mm beyond the swaged ferrule end. The end
of the column need not be perfectly square, but should not
have cracks that extend under the ferrule.
7890 Series GC IPB
463
11 Capillary flow technology (CFT) devices
Connecting and disconnecting columns
Connecting columns
Connect columns to the union with internal nuts and
preswaged SilTite ferrules. Finger-tighten the nuts. Further
tighten with a wrench only 15 to 20 degrees.
Disconnecting columns
Loosen and remove the internal nut. If the column and ferrule
do not come free, insert a pointed object (pen, paper clip) into
the ferrule release hole and press firmly. You will hear a click as
the ferrule releases.
Mounting the union
The ultimate union is probably too heavy to be supported only
by the capillary columns. Use the oven wall clip to support the
weight of the union by attaching it to an opening in the oven
wall.
464
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
12 Electrical
Power options 466
Converting the power option 469
Remote start/stop connection 470
Remote control 471
Measuring inlet and detector heater and PRT resistance
Temperature sensor resistance 475
Oven heater coil resistance 476
Setting the instrument power configuration 477
Line voltage configuration plug 478
Ceramic and glass fuses 479
AC power board schematic 480
Oven shroud 481
Agilent Technologies
472
465
12 Electrical
Power options
There are 8 power option kits. These contain the configuration
plug, oven shroud, label, and power connector for each option. If
you are converting from one power option to another you can
order the kit or order the unique individual parts.
The power cord must be ordered separately. See Power cords.
Regular oven
There are 4 power options for the regular oven:
G1530-63800 Regular power kit 120V
G1530-63810 Regular power kit 220V
G1530-63820 Regular power kit 230V
G1530-63830 Regular power kit 240V
Kits
120VAC
G1530-63800
220VAC
G1530-63810
230VAC
G1530-63820
240VAC
G1530-63830
Configuration
plug
G1530-60690
G1530-60710
G1530-60720
G1530-60730
Oven shroud
G1530-61610
G1530-61230
G1530-61670
G1530-61240
Label
G1530-90928
G1530-90921
G1530-90922
G1530-90923
Power
receptacle
G1530-61550
G1530-61560
G1530-61560
G1530-61560
Clamp
1400-1663
Common to all regular power options:
0515-1084 Screw, M3x0.5x12mm T20, quantity 2 for power
input assembly
0515-2711 Screw, M4X0.7x12mm T20, coated, quantity 4 for
shroud
0535-0043 Nut with lock washer, M4X0.7x3.2mm 7mm for
grounding wire
05890-00460 Insulation plug for heater/sensor tube
G3430-00104 Heater Wire Insulation Sleeving
466
7890 Series GC IPB
Electrical
12
Fast oven
There are 4 power options for the fast oven:
G1530-63840 Fast power kit 200V (Japan)
G1530-63850 Fast power kit 208 or 220V
G1530-63860 Fast power kit 230V
G1530-63870 Fast power kit 240V
Kits
200VAC
208 220VAC 230VAC
240VAC
G1530-63840 G1530-63850 G1530-63860 G1530-63870
Configuration
plug
G1530-60700
G1530-60710
G1530-60720
G1530-60730
Oven shroud
G1530-61620
G1530-61630
G1530-61650
G1530-61640
Label
G1530-90924
G1530-90925
G1530-90926
G1530-90927
Common to all fast power options:
0515-1084 Screw, M3x0.5x12mm T20, quantity 2 for power
input assembly
0515-2711 Screw, M4X0.7x12mm T20, coated, quantity 4 for
shroud
G1530-61550 Power input assembly
1400-1663 Clamp, 1.25x1.0 inch
0535-0043 Nut with lock washer, M4X0.7x3.2mm 7mm for
grounding wire
05890-00460 Insulation plug for heater/sensor tube
G3430-00104 Heater Wire Insulation Sleeving
7890 Series GC IPB
467
12 Electrical
Table of GC voltage by country
468
Country
Kit
Voltage
Oven type
Australia, 10 amp
G1530-63830
240 V
Regular
Australia, South
Africa
G1530-63870
240 V
Fast
China
G1530-63810
220 V
Regular
China, Hong Kong
G1530-63850
220 V
Fast
Continental Europe,
dual phase
G1530-63860
230 V
Fast
Continental Europe,
single phase: Russia
G1530-63850
220 V
Fast
Denmark,
Switzerland, 10 amp
G1530-63820
230 V
Regular
India, Denmark,
Switzerland, 16 amp
G1530-63860
230 V
Fast
Israel
G1530-63850
220 V
Fast
Japan
G1530-63840
200 V
Fast
United Kingdom,
Ireland
G1530-63870
240 V
Fast
USA
G1530-63800
120 V
Regular
USA
G1530-63850
208 V
Fast
USA
G1530-63870
240 V
Fast
7890 Series GC IPB
Electrical
12
Converting the power option
This procedure outlines the steps you must complete to prepare
a GC for use in another country or to configure for a different
oven heating speed.
The basic requirements for use of the fast heating oven are:
The electric service must be capable of providing >= 200 V at
>=15 amperes.
In the United States, the electric service must be 208 V or
240 V.
Procedure
1 Select the appropriate power option kit. See Power options.
There are 8 power option kits. These contain the
configuration plug, oven shroud, label, and power connector
for each option. If you are converting from one power option
to another you can order the kit or order the unique
individual parts. Compare the parts listings for the present
and new power option to see what must be replaced.
2 Select the appropriate power cord. See Power cords.
3 Cool down the oven.
4 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
5 If necessary, replace the oven shroud. See Replacing the
oven shroud, oven fan, and oven fan motor.
6 Replace the oven configuration plug. See Line voltage
configuration plug.
7 If necessary, replace the power cord connector.
8 Attach the new label.
9 Power on the unit. Watch for any errors after self-test.
7890 Series GC IPB
469
12 Electrical
Remote start/stop connection
Prepare (low)Request to prepare for analysis. Receiver is any
module performing pre-analysis activities.
Start (low)Request to start run/timetable. Receiver is any
module performing runtime-controlled activities.
Ready (high)System is ready for next analysis. Receiver is any
sequence controller.
Stop (low)Request to reach system ready state as soon as
possible (for example, stop run, abort or finish, and stop
injection). Receiver is any module performing
runtime-controlled activities.
470
7890 Series GC IPB
Electrical
12
Remote control
Remote control allows easy connection between single
instruments or systems to ensure coordinated analysis with
simple coupling requirements.
Start RelayA 120 millisecond contact closure
Control of analysis is maintained by signal readiness READY for
next analysis, followed by START of run and optional STOP of
run triggered on the respective lines. In addition, PREPARE and
START REQUEST may be issued.
The signal levels are defined as standard TTL levels (0 V is logic
true, +5 V is logic false).
Input Load >= 2.2 kOhm against +5 V
Output type is open collector.
Remote control timing
7890 Series GC IPB
471
12 Electrical
Measuring inlet and detector heater and PRT resistance
If you suspect that an inlet or detector heater or PRT is
defective, you can check its resistance and compare against the
expected nominal values.
To check the resistance of an inlet or detector heater, or to
check the resistance of an inlet or detector PRT:
To measure the inlet or detector heater or PRT resistance:
1 Turn off the GC main power switch and disconnect its power
cord.
WA R N I N G
CAUTION
Hazardous voltages are present in the mainframe when the GC
power cord is connected. Avoid a potentially dangerous shock
hazard by disconnecting the power cord before removing any GC
panels.
Components can be damaged by static electricity: be sure to wear
an ESD strap grounded to the GC chassis while performing this
procedure.
2 Remove the GC panels required to access the zone's
heater/sensor connector to be tested.
For inlets, remove the inlet cover and GC left side panel
For detectors, remove the electronics cover and GC right
side panel
472
7890 Series GC IPB
Electrical
12
3 Remove the connector from the GC chassis.
4 Use an Ohmmeter to measure the resistance across the
connector pins of the heater/sensor cable.
For heated zones the PRT is connected to the white wires
on pins 2 and 3 of the connector.
With the heater/sensor connector removed from the GC,
there should be no connection to ground on any of the
four pins. A reading of ~0 indicates a possible shorted
sensor or heater.
5 Compare the results against the resistance values in the
tables below.
7890 Series GC IPB
473
12 Electrical
Sensor resistance
The approximate resistance of a temperature sensor is:
R = 100 + (.35 t)
where R is resistance in ohms and t is sensor temperature in C.
Table 29 Temperature Sensor Resistance by Heater Temperature
C
+0
+10
+20
+30
+40
+50
+60
+70
+80
+90
+100
100.00
103.90
107.79
111.67
115.54
119.40
123.24
127.07
130.89
134.70
138.50
100
138.50
142.28
146.06
149.82
153.57
157.32
161.04
164.76
168.47
172.16
175.84
200
175.84
179.51
183.17
186.82
190.46
194.08
197.70
201.30
204.88
208.46
212.03
300
212.03
215.58
219.13
222.66
226.18
229.69
233.19
236.67
240.15
243.61
247.06
400
247.06
250.50
253.34
257.34
260.75
264.14
267.52
270.89
274.25
277.60
280.93
Nominal inlet and detector heater/sensor resistances
474
Inlet or Detector
Heater type
Nominal heater
resistance
Sensor
type/comments
Split/splitless
70 W
23
100 PRT
Purged packed
70 W
23
100 PRT
Cool on-column
60 W
26-27
100 PRT
Multimode
150 W
~9
Type K
Thermocouple
Resistance, cold: ~
13
PTV
150 W
~9
Type K
Thermocouple
Resistance, cold: ~
13
Volatiles interface 60 W
26-27
100 PRT
FID
70 W
23
100 PRT
TCD
70 W
23
100 PRT
NPD
70 W
23
100 PRT
uECD
70 W
23
100 PRT
FPD
60 W (2 each)
26-27
100 PRT (2 each)
7890 Series GC IPB
Electrical
12
Temperature sensor resistance
The approximate resistance of a temperature sensor is:
R = 100 + (.35 x t)
where R is resistance in ohms and t is sensor temperature in C.
Table 30 Temperature Sensor Resistance by Heater Temperature
C
+0
+10
+20
+30
+40
+50
+60
+70
+80
+90
+100
100.00
103.90
107.79
111.67
115.54
119.40
123.24
127.07
130.89
134.70
138.50
100
138.50
142.28
146.06
149.82
153.57
157.32
161.04
164.76
168.47
172.16
175.84
200
175.84
179.51
183.17
186.82
190.46
194.08
197.70
201.30
204.88
208.46
212.03
300
212.03
215.58
219.13
222.66
226.18
229.69
233.19
236.67
240.15
243.61
247.06
400
247.06
250.50
253.34
257.34
260.75
264.14
267.52
270.89
274.25
277.60
280.93
7890 Series GC IPB
475
12 Electrical
Oven heater coil resistance
If you believe that your heater coil is cracked or otherwise
damaged and has caused an open circuit, you can check it by
measuring its resistance.
To measure the resistance:
1 Turn the instrument power off.
2 Disconnect the oven heater leads (P3, P4) from the AC power
board.
3 Use an ohmmeter to measure resistance at the connectors.
Acceptable resistance ranges (in ohms) are given below.
Acceptable resistances range from the nominal value for a new,
cold heater to +5% from the nominal value.
NOTE
Resistance goes up approximately +3% after heating the coil.
Table 31 Resistances of the Heater Coil
Nominal cold heater resistances, ohms
476
Standard oven (1600
VA)
Fast-ramp oven (2250
VA)
120 V
9.07 9.52
n/a
200 V
n/a
17.78 18.7
220 V
n/a
21.51 22.6
230 V
33.06 34.71
23.51 24.7
240 V
n/a
25.60 26.9
7890 Series GC IPB
Electrical
12
Setting the instrument power configuration
There are seven possible line voltage power configurations for
the GC.
To change the power configuration for the instrument, you must
install the appropriate types of the following components:
Line voltage configuration plug
Ceramic fuses on the AC power board
Oven shroud assembly
These three components are explained in the topics that follow.
Table 32 Voltage configuration information
Voltage (10%, +5%)
Frequency (Hz)
Maximum power
consumption (VA)
Power line
requirement
Oven type
120 V
48-66
2,250
20-amp dedicated
receptacle
Regular
200 V
48-66
2,950
15-amp dedicated
receptacle
Fast-heating
208 V
48-66
2,950
15-amp dedicated
receptacle
Fast-heating
220 V
48-66
2,950
15-amp dedicated
receptacle
Fast-heating
230 V
48-66
2,250
10-amp dedicated
receptacle
Regular
230 V
48-66
2,950
16-amp dedicated
receptacle
Fast-heating
240 V
48-66
2,950
13- or 16-amp
dedicated receptacle
Fast-heating
7890 Series GC IPB
477
12 Electrical
Line voltage configuration plug
There is a different line voltage configuration plug on the AC
power board for each power configuration. Each configuration
uses three or five jumper wires, each connecting to two
different pins on the plug. The 120 VAC configuration uses five
jumper wires and all other configurations use three jumper
wires.
Figure 14 Top view
Jumper locations for power configuration plug
Transformer
120 VAC
200 VAC
208/220 VAC
230 VAC
240 VAC
3 13
2 13
3 13
5 13
3 13
6 15
6 12
6 12
69
69
14
14
14
14
9 14
Oven fan
1 10
48
478
7890 Series GC IPB
Electrical
12
Ceramic and glass fuses
The two sets of fuses on the G3440A AC power board:
Two ceramic fuses to protect the board from the oven heating
circuit (F1, F2)
Two glass fuses to protect the board from the main supply
(F3, F4)
See the table below for the part numbers. When replacing both
the glass and ceramic fuse types, always replace them in pairs.
I.D.
Description
System
Part number
F1
Ceramic Type F 20A/250 V
Oven heater
2110-0098
F2
Ceramic Type F 20A/250 V
Oven heater
2110-0098
F3
Glass Type F 8A/250 V
Main supply
2110-0036
F4
Glass Type F 8A/250 V
Main supply
2110-0036
7890 Series GC IPB
479
12 Electrical
AC power board schematic
The AC power board supplies AC power to the oven heater and
to the main transformer.
480
7890 Series GC IPB
Electrical
12
Oven shroud
There are two different oven shrouds depending on the power
option used. The oven shroud contains the oven heater and
sensor as part of the assembly. If you need to replace the heater
or sensor, you should replace the entire shroud assembly. See
Replacing the oven shroud, oven fan, and oven fan motor for
more details.
Table 33 Part numbers for Oven Shrouds and Configuration Plugs
Voltage
Shroud part no.
Configuration plug part
no.
120 V
G1530-61610
G1530-60690
230 V
G1530-61670
G1530-60720
Regular oven shrouds
Fast ramping oven shrouds
7890 Series GC IPB
200 V
G1530-61620
G1530-60700
208 V
G1530-61630
G1530-60710
220 V
G1530-61630
G1530-60710
230 V
G1530-61650
G1530-60720
240 V
G1530-61640
G1530-60730
481
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
13 Firmware
Firmware overview 483
To Update GC Firmware 484
Firmware history 487
Confirm firmware update 495
Problems and solutions 496
Clearing battery-backed PF-RAM (7890A only)
Set the default method 500
Default method listing 501
497
Agilent Technologies
482
Firmware
13
Firmware overview
The firmware is the programming that controls the entire GC.
Periodic updates to correct errors and/or add features are
available from the Agilent Web site and may be downloaded to
the GC using the Agilent G4600AA Instrument Utilities
software that shipped with the 7890A GC.
To successfully update GC firmware, you can use any version of
the Instrument Utilities software. Do not use any other
firmware update utility. To access the firmware update utility
in Instrument Utilities, open the software and look for the
Firmware Update link. You do not need to be monitoring the
instrument.
About 160 7890A GCs were shipped to channel partners,
distributors, and regional sales offices with very early versions
of firmware. Contact the CAS factory problem manager (FPM)
for instructions on how to update these units.
The latest version of Instrument Utilities software includes the
ability to update the board serial number in the event that this
was not done at the GC after replacing the logic board. (It is still
best to update the serial number at the GC front panel after
changing the logic board.) This version can also successfully
update GCs without a manufacture date.
7890 Series GC IPB
483
13 Firmware
To Update GC Firmware
To update the GC firmware, use Agilent Instrument Utiltiies,
version B.01.06 or greater. When possible always use the latest
version of Instrument Utilities.
The software maintains configuration information (including
serial number) when updating a GC. However, any stored
methods are lost. Click Restore to restore the active method after
updating firmware.
NOTE
The Firmware Update utility requires full control of the instrument. Be
sure to disconnect any Agilent data systems before using the Firmware
Update utility.
1 Open Instrument Utilities.
NOTE
Once you connect to an instrument in the Firmware Update screen, no
other tasks can be performed on the instrument until you Disconnect.
2 Make sure the instrument/component is turned on and not in
use. Make sure any sampler or other device is also connected
and turned on.
3 Record any information about the device stored in the device
itself, for example, any local methods or service information
(Early Maintenance Feedback counters, runtime details, and
so forth).
4 Select Firmware Update from the explorer pane.
5 Select the desired instrument from the Instrument list and
click Connect.
If it is not available, click Add New Instrument to open
Configure Instruments. Add the new instrument, then return
to firmware update.
6 Highlight the row of the component you wish to update.
7 Select the desired firmware version from the Available
drop-down list. If the desired firmware version is not
available, add it as follows:
a Go to the Agilent web site at
http://www.chem.agilent.com/en-US/Support/Downloads
/firmware/Pages/default.aspx.
b Download the updated firmware for your instrument type.
484
7890 Series GC IPB
Firmware
13
c Unzip the firmware file(s).
d In the Firmware Update utility, click Add. Browse to and
select the files unzipped in the previous step. The new
firmware version will now appear in the Available
drop-down list.
8 Click Update.
9 When prompted, save the active method and configuration
data. You will restore the data from this file in a later step.
WA R N I N G
Do not turn off power to the device during firmware update.
10 When the process completes, the instrument reboots.
Reconnect to the instrument, then click Restore. Select the
previously-saved data file to restore the active method.
11 Click Disconnect to disconnect the firmware update utility
from the instrument.
7890 Series GC IPB
485
13 Firmware
Troubleshooting problems
If the Instrument Utilities fails to connect to the GC, reboot the
PC and try again.
If the firmware does not completely download to the GC, reboot
the GC and try again. (Note that firmware download takes time,
so be patient.)
If the firmware update fails, try again. Reboot the GC and PC if
needed.
486
7890 Series GC IPB
Firmware
13
Firmware history
NOTE
The firmware history here is up to date as of the release of this manual.
Check service notes and the firmware download site (Agilent internal:
http://cas.service.agilent.com/gc/Firmware/firmware_file_downloads.h
tm) for more recent firmware versions and information.
Serial number <= number in table - the unit could be updated to
the latest revision.
Serial number > number in the table - the unit should already
have this revision or greater.
Revision
CN serial number US serial number
break
break
Service note
A.01.10.2
TBD
TBD
G3440A-45
A.01.10.1
TBD
TBD
G3440A-41, -39
A.01.10
TBD
TBD
G3440A-37
A.01.09.2
TBD
TBD
G3440-31
A.01.09.1
CN10839078
TBD
G3440-30
A.01.09
CN10831XXX
US10831015
G3440A-27
A.01.08
TBD
TBD
G3440A-20
A.01.07
CN10751086
US10751031
G3440A-18
A.01.06
CN10738001
US10737020
A.01.05
CN10731026
US10731014
A.01.04
CN10722043
US10722003
G3440A-05
A.01.03
CN10717036
US10717009
G3440A-04
A.01.02.581
CN10716014
US10715013
G3440A-03
A.01.02
CN10708001
US10710002
G3440A-
B.01.01
Externally, firmware downloads are available from the Agilent
web site.
Internally, go to:
http://cas.service.agilent.com/gc/Firmware/firmware_file_dow
nloads.htm (link active as of October 2009)
7890 Series GC IPB
487
13 Firmware
7890 A.01.10.2
Described in Service note G3440A-45
Fixes: 7890 GC keypad now allows entry of serial numbers for
injectors and tray. In certain circumstances the oven will not
shut down if it cannot reach temperature for reasons such as an
oven flap failure - This has now been fixed. Lab advisor can now
connect to the GC whilst it is in MMON mode resolving
firmware download connection problems. 7890 GC can now
store barcode labels that contain more than 34 characters
Injector light" is inconsistent with 7890 "Tower LED".
The error pertaining to the oven shut down may case very hot
air to be continuously released through the oven vent. It is
advisable therefore that this firmware be installed on the GC at
next visit. After installation of this firmware it is not necessary
to requalify either GC nor the ALS. Firmware files can be
obtained externally at http://www.chem.agilent.com/
_layouts/agilent/downloadFirmware.aspx?whid=50307 or
internally at
http://cas.service.agilent.com/gc/Firmware/firmware_file_dow
nloads.htm
488
7890 Series GC IPB
Firmware
13
7890 A.01.10.1
Described in Service note G3440A-41, G3440-39
The 7890A GC firmware, A.01.10.1 has recently been released.
Included in this firmware are not only enhancement and bug
fixes but diagnostic "watchdogs" to help resolve and track
possible future problems. Recent instrument failures have
occured that could have been avoided or troubleshot more
efficiently with the latest firmware installed.
GC Front/Back detector hardware fault (Team Track 02500)
Spurious error message. Error introduced in A.01.10. Evident at
power on. NPD Analog signal always 0.0V (Team Track 02501).
Error introduced in A.01.10. Digital Signal works OK. At times,
GC keyboard, UI & LAN response is sluggish/stalled (Team
Track 02502) PTV cryogenic cooling operating as per A.01.07.
Cryo did not control inlet during run. (Team Track 00233) Fixes
for External ready for 7820A. Fix method file upload and
download of inlet temperature ramps. Fix power up procedure
to not energize the small zone contactor when there is a shorted
driver. Fix detector thermal shutoff status messages. Fix
download of column calibration. Clean up small zone readiness
calculation. Fix small zone shorted sensor detection. Add delay
to valve state upload during a run. PVCS2476 Fix PTV Cryo for
SOLVENT VENT Time. Fix method download during a run for
non programmed zones. New PCOC PID's and control. MMI
Temperature minimum for MMI multimode inlet set to -180
degC (Team Track 00234) LVI with a 500ul syringe set incorrect
draw speed. (Team Track 00056) Fix Solvent Vent pressure
calculation, use gage pressure. Give MMI inlets 10 ramps. 7693
ALS 7890 System Calibration should fail if G4514A internal
calibration not completed (Team Track 00049) Tray LED does
not flash when G4514A does not find a bottle during return all.
(Team Track 00029). GC display updates BCR firmware revision
correctly after a firmware update. Tray chiller info and text
modified chiller temperature upper limit is now 60C. Give
MMI inlets 10 ramps Fix error in FPD single heater
configuration. Tray Chiller configuration items added under
Tray Config Tray Chiller temperature added to GC readiness
Sampler devices reset after a firmware update/SN change
causes 7890 to reconfigure QQQ Fix collision cell fault
messages. Add QQQ to system readiness, Add QQQ shutdown
test. Add QQQ diagnostic panels. Add Argon control mode to
QQQ based on ECD Nitrogen and Argon frit calibrations. Add
'QQQ' Collision cell gas controller Fix cannot pick collision cell
from aux epc list
7890 Series GC IPB
489
13 Firmware
7890 A.01.10
Described in Service note G3440A-37
Enhancements: Support for the 7693A ALS and associated
modules. Support for the 7000A Triple Quad GCMS. Support for
the MMI. Fixes: Fix PTV Cryo for SOLVENT VENT Time. Fix
method download during a run for non programmed zones. New
PCOC PID's and control. Fix missing small zone fault messages
and events. Fix download of column calibration. Clean up small
zone readiness calculations. Fix small zone shorted sensor
detection. Add delay to valve state upload during a run. Fix
power up procedure to not energize the small zone contactor
when there is a shorted driver. Fix detector thermal shutoff
status messages. Fixed readiness for external devices Fix
method file upload and download of inlet temperature ramps.
7890 A.01.09.2
Described in service note G3440A-31
Customers have been experiencing problems with oscillating
temperatures with the PCOC inlets of the 7890. When the inlet
was set to 50-80 degC, the temperature was seen to fluctuated
+/- 5 degC causing a not ready status. In some cases the
temperature would stabilize but only after a considerable length
of time. Replacing the heater or even the whole weldment may
or may not fix the problem.
Solution : The heating control coefficients (PIDs) have been
modified in the firmware to better control and resolve these
fluctuating temperatures. The new firmware revision is
A.01.09.2 If you have have a customer with a PCOC inlet,
regardless of whether they are experiencing temperature
problems or not, it is advisable to update the firmware to
A.01.09.2
Additional Information
In addition to the PCOC resolution one further problem has
been fixed with this version. It has been noted that the DC210
led on the logic board intermittently flashes when the normal
state is solid on. The status of this led does not affect the
normal operation of the GC. To avoid all confusion firmware
has now forced this led to lit all of the time.
490
7890 Series GC IPB
Firmware
13
7890 A.01.09.1
Described in service note G3440A-30
A list of defects fixed are as follows: Fix cryo trap for JAS Fix
oven cryo shutdown. Fix download during run for oven thermal,
and pressure zones. Fix download during a run for column flow
programs. PCM AuxC reports as PCM AuxB Not Ready
(p_aux.c) Fix detector makeup mode for download. Fix status
message for bad serial #. Fix entering zero value for analog out.
Fix analog out for detector OFF.
7890 A.01.09
Described in service note G3440A-027
Changes applicable to Customers and Support Providers are as
follows.
Able to specify Cryo Type for User Aux Heaters
Fixed analog out noise problem.
Turn on PMT voltage when FPD flame is turned ON.
Turn off FID air and H2 on ignition fail and gas shutdown
Enable test signals for valve box heaters
Add current limit to NPD SetBead voltage. If current exceeds
100pA during bead turn on, detector will turn off.
Add ColComp setpoints to method.
Add zone_limit to AuxHeater config reporting
Add several aux temp models for ICPMS
Fix reporting of AuxDet Heater On/Off
Remove Cryo Focus Valve configuration.
Add Configure Collision Gas Control Module.
Fix status display to not allow flow on COC.
Add Column Compensation output in analog and digital
modes (via config detector).
Network settings (IP address, DHCP etc) can now be
modified from the keyboard
while in MMON mode.
ALS appeared to go off line after 3 weeks of continuous use.
Power reset resolved issue. Now fixed.
(ALS firmware A.01.01)
Gaps in Bar Code Reader can now be read. (ALS firmware
A.01.01)
7890 Series GC IPB
491
13 Firmware
7890 A.01.08
Described in service note G3440A-020
7890 A.01.07
Described in service note G3440A-018
7890A.01.04
Described in service note.G3440A-005.
The following defects or perceived defects were fixed:
Fixed PTV inlet configuration defect where Install Inlet
(Cryo) was not a selection in the configuration list after a
power cycle.
Fixed the PCM Autoflow zero feature. Symptom would
include PCM issues when in flow control mode. Measured
flow is greater than flow displayed on screen. To confirm
problem, navigate to Options, Calibration, PCM and scroll to
Flow zero. Press Off / No to reset to factory defaults after
updating firmware.
Fixed symptom where pneumatic shutdown of PCM cannot
be cleared without fixing the leak and power cycling the GC.
Symptom may appear as PCM does not accept On / Yes or
entering a new flow or pressure.
Fixed symptoms where text alignment is incorrect and the
cursor disappears when Options | Keyboard & Display |
Language is set to Chinese.
Fixed symptom where GC method is not downloaded from
control software.
Fixed the symptom where GC triggers a thermal shutdown
with the flaps wide open. Chromatographic results indicate
that the flaps were partially open for several runs.
Fixed the symptom where the PP inlet behaves as if there is
an oven track temperature mode.
Fixed the symptom where no exception or error message is
displayed when back detector heater, logic board, or EPC
module is "broken."
Fixed the symptom where your cannot program User Key 2
until after programming User Key 1. If you go through the
steps of programming User Key 2 before User Key 1, the key
will not work.
492
7890 Series GC IPB
Firmware
13
Default configuration for the Auxiliary 2 Heater changed to
MSD transfer line.
The following modifications were added to enable channel
partners to configure and control their applications:
Increased the maximum temperature of a small heated zone
from 400 to 450C. Using this maximum on our standard
inlet or detector may cause damage to the instrument.
Added a lock to the configuration settings so that someone
cannot modify the configuration without turning the lock off.
The lock is located under Options | Keyboard & display. At
power On the lock is set to On.
Added the capability to specify the wattage of the heater for
a small heated zone: inlet, detector or auxiliary heater.
Added the capability to configure 3 custom heaters with
specific PID coefficients and store those coefficients.
Added the capability for our channel partners to configure a
variety of heaters.
The Valve Box heater can be configured as an independent
isothermal heater.
Added the capability to configure an Auxiliary heated zone
to have a maximum temperature between 40 and 450 C.
Adds the capability to configure a 140 watt inlet or auxiliary
heater and program it to heat between 1 to 5 C/min.
Added the capability to configure the PTV without a heater.
7890 Series GC IPB
493
13 Firmware
7890A.01.03
Described in service note G3440A-004.
The modifications in this firmware revision include:
Adjusts control of oven flapper. Eliminates flapper not
closing completely.
Improves communication using DHCP with lower baud rate
hubs. Lower baud rate hubs include the generation of early
twisted-pair hubs. An example hub is the Hewlett-Packard
J3128A AdvanceStack Hub-8e 10 base-T hub with the speed
of 10 Mb/sec.
Fixes this symptom: Aux EPC channel 6 always reads 0
pressure in the software Edit Parameters screen.
7890A.01.02.581
Described in service note G3440A-003.
The modifications in this revision include:
Prevents interruption of firmware update process when
using the standard tool.
Fixes sequencing with multi-position and gas sampling
valves.
Fixes the displayed flow when column inlet is unspecified for
SSL and PTV inlets. The flow was displayed as zero, even
though the flow was accurate.
Prevents inappropriate thermal shutdown for inlet, detector,
and AUX heated zones when they are heating slowly.
Fixes pressure setpoint ranges for Pneumatic Control Module
(PCM).
Eliminates cycling or multiple GC reboots after a power
cycle.
494
7890 Series GC IPB
Firmware
13
Confirm firmware update
Confirm the firmware update by pressing [Status][Clear]. The
display should look like this.
Agilent 7890A GC
A.01.09
Power on successful
The firmware update will become part of the GC's Event Log.
When upgrading 7890A GC firmware from:
A.01.0x to A.01.07, or from
A.01.03, A.01.04, and A.01.05 to A.01.08/A.01.09
configuration information can be lost. See document
G3430-90035. The information is especially important if also
upgrading OLCDS or GC ChemStation or MSD Productivity
ChemStation.
Please check the following setpoints on the GC:
Inlet and detector gas types - Config | <Front or Back><Inlet
or Det>.
Heater configuration. For example, the MSD transfer line
may need reconfiguration.
LAN configuration information - Options | Communications.
Serial number and manufacturing date - Service Mode |
Diagnostics | Instrument Status.
CAUTION
7890 Series GC IPB
If the GC does not have a valid serial number, you may have issues
connecting with the ChemStation software. If the GC does not have
a valid manufacturing date, the configuration settings will not be
saved and will be lost if you power cycle the GC.
495
13 Firmware
Problems and solutions
If the update is interrupted or there is a defect in either of the
boards, the update may fail. Click on the link to see more
information about each of these symptoms.
GC firmware update unsuccessful and GC reboots into
MMON mode
ALS firmware update incomplete
Possible solutions to unusual behaviors
At installation and after a firmware update, we have had some
communication issues between the GC and the software. The
symptoms include unexpected changes to configuration or to
method setpoints. Here are some suggested actions for
eliminating these symptoms.
Load the default method. Press Method.
Replace the logic board.
a From the keyboard and display, check the configuration
and method in the hardware.
1 From the software, upload the GC method.
2 From the software, select Instrument | GC Configuration.
Review the GC configuration after clicking on Get GC
configuration.
3 From the software, select Instrument | Edit GC
parameters. Review your method setpoints.
Save the method under a new name.
496
7890 Series GC IPB
Firmware
13
Clearing battery-backed PF-RAM (7890A only)
After updating to a firmware revision before A.01.06, clearing
all or part of the PF-RAM memory has eliminated some
symptoms, such as, heater faults and corrupted OLCDS or
ChemStation methods.
Clearing some or all of the memory forces the GC to reload
defaults. See Default method listing for a listing of the values.
Partial clear
This procedure resets both configuration and current setpoints.
Here is a listing of what is reset to defaults.
Configuration items: Oven, Display, Inlets, Detectors, Aux
EPC modules, PCM EPC modules, Valves, Thermal Aux, and
Valve box.
Sequence items: All items stored under the sequence
including: Sample numbers, Overlap, Auto-injector, and
Method number.
Current setpoints (Workfiles): GC and ALS setpoints.
Instrument state flags: Run states, Blank run, Power fail,
Method directory dirty, Status table, Analog column
compensation values.
Procedure
1 Power OFF the GC.
2 Press and hold down [Clear].
3 Power ON the GC.
4 When the GC Status screen appears on the display, release
[Clear].
Total clear
This procedure clears all of the battery-backed PF-RAM. In
addition to what is reset by holding down the Clear key, these
items are reset to defaults:
ID items: Serial number, IP networking setpoints, Uptime
clock, Column names
Other: Service counters, Event log
7890 Series GC IPB
497
13 Firmware
Procedure
1 Power off the GC.
2 Remove the left-side panel to access the logic board. Find the
small DIP switch (G3430-60100) or DIP switches
(G3430-60120 and G3430-60101) between the battery and the
large connector.
3 For the G3430-60120 and G3430-60101 boards, move the
switch to OFF. For the G63430-60100 (shown below), move
both switches away from you toward the GC oven. This is the
Off position.
4 Wait 5 minutes to allow the battery-backed RAM to clear.
5 Reset the battery switches to On (G3430-60100 shown).
498
7890 Series GC IPB
Firmware
13
6 Power on the GC. The GC will post some messages about
loading default configuration and method files.
7 Re-enter any lost configuration information, such as, gas type
and method setpoints.
7890 Series GC IPB
499
13 Firmware
Set the default method
To set the default method conditions, do the following:
1 Press [Method].
2 Scroll to the last line of the table: Set default method and press
[Enter].
3 Press [On/Yes] to confirm the request.
500
7890 Series GC IPB
Firmware
13
Default method listing
This page lists the default configuration and method setpoints
for the GC.
Instrument
Post run hold time = 0
Auto Prep Run = Unknown
Keyboard lock = False
Type of connection = LAN
GCName = blank
GCNotes = blank
Table 34 Inlets
COC
PP
PTV
SSL
VI
True
True
True
True
True
COC oven track
False
False
False
Septum purge flow
Septum purge state
On
On
On
Septum purge switching
False
False
False
Purge switching time
Total flow
18
Total flow state
Off
Off
Off
Control mode
Pressure
Pressure
Pressure
Temperature state
Off
Off
Off
Initial hold time
Initial value
250
250
250
Post run value
250
250
Pressure state
Off
Off
Off
Initial hold time
Initial value
689475.7
689475.7
689475.7
Post run value
689475.7
689475.7
689475.7
Cryo
Off
Off
Off
Cryo temperature
25
25
25
Time out detection
Off
Off
Off
Time out time
30
30
30
Fault detection
Off
Off
Off
Quick cool
Off
Off
Off
Determine readiness
7890 Series GC IPB
501
13 Firmware
COC
PP
PTV
SSL
Gas saver time
Gas saver flow
20
20
20
Gas saver state
Off
Off
Off
Operation mode
Splitless
Solvent
vent
Split
Split ratio
100
100
Purge flow
15
15
15
Purge time
0.75
0.35
0.75
Pressure pulse
689475
689475
Pulse time
0.75
0.75
Vi Inject time
Vent flow
100
Vent pressure
344737
Vent time
0.25
VI
Columns 1 to 6
Ignore ready = True; except for Columns 3 through 6 = False
Mode = Constant pressure
Flow state = Unknown
Initial hold time = 0
Initial value = 1; except for Column 1 where Initial value = 0
Post run value = 1
Oven
Ignore ready = True
Cyro = Off
Use Temperature = 0
Time out detection = Off
Time out = 0
Fault detection = Off
Quick cool = Off
Equilibration time = 3
Temperature state = Off
Initial hold time = 0
Initial value = 50
502
7890 Series GC IPB
Firmware
13
Post run value = 50
Auxiliary Thermal Zones
Thermal Aux 1, Determine readiness = True
Thermal Aux 2, Determine readiness = True
Thermal Aux 3, Determine readiness = False
Table 35 Detectors
FID
FPD
NPD
TCD
ECD
Determine readiness
True
True
True
True
Temperature
250
200
250
250
Heater
Off
Off
Off
Off
Fuel flow
40
75
Fuel
Off
Off
Off
Off
Utility flow
450
100
60
10
Utility
Off
Off
Off
Off
Makeup flow
50
60
30
Makeup
Off
Off
Off
Off
Off
Constant total flow
False
False
False
False
False
Total flow
Electronics
On
On
On
Off
Flame
Off
Off
Off
Off
Off
State
Unknown
Unknown
Unknown
Unknown
Unknown
Off
Off
Off
Auxiliary flow and pressure control modules
For each of the 9 possible Aux EPC channels (AUX).
Determine readiness = False
For each of the PCM channels that function like a purged
packed inlet.
Determine readiness = True
Mode = Forward pressure control
Total flow = 0
Pressure = 689475.7
7890 Series GC IPB
503
13 Firmware
Pressure State = Off
Initial hold time = 0
Initial value = 689475.7
Post run value = 689475.7
For each of the PCM channels that function like an Aux EPC
channel.
Determine readiness = False
Pressure state = Off
Initial hold time = 0
Initial value = 689475.7
Post run value = 689475.7
Valves
For GC x GC Valve.
GCxGC Valve sample time = 250
Modulation time = 60000
Valve idle state = Off
Delay time = 60000
For each of the 8 possible valves.
Valve initial state = Off
For Cyro-focusing valve.
Pre-run time = 1
Hold time =1
504
7890 Series GC IPB
Firmware
13
Table 36 Automatic liquid sampler
Fan
Pre-wash A Reps
Volume
Draw speed
Dispense speed
Viscosity delay
Pre-wash B Reps
Volume
Draw speed
Dispense speed
Viscosity delay
Sample wash Reps
Volume
Draw speed
Dispense speed
Viscosity delay
Depth offset
Sample pumps Reps
Draw speed
Dispense speed
Viscosity delay
Depth offset
Sample volume
Draw speed
Viscosity delay
Depth offset
Injection dispense speed
Pre-injection dwell time
Post-injection dwell time
Large volume reps
Large volume delay
Post-wash A Reps
Volume
Draw speed
Dispense speed
Viscosity delay
Post-wash B Reps
Volume
Draw speed
Dispense speed
Viscosity delay
7890 Series GC IPB
Front injector
On
0
80
200
10
0
0
80
200
10
0
0
80
200
10
0
0
6
200
10
0
0
10
200
0
0
10
0
0
1
0
0
80
200
10
0
0
80
200
10
0
Back injector
On
0
80
200
10
0
0
80
200
10
0
0
80
200
10
0
0
6
200
10
0
0
10
200
0
0
10
0
0
1
0
0
80
200
10
0
0
80
200
10
0
505
13 Firmware
Tray
Temperature = 0
Barcode reader = false
Mixing intensity = Unknown
Time = 0
First sample preference = 2
Enable ALS tray = False
Overlapped injection mode = No overlap
Overlapped injection delay = 0
Service counters
Twenty (20) counter IDs set to a default number.
Enabled = False.
Signals
Each of the 4 digital signals are set to
Test Plot at 50 Hertz
Signal is saved = False.
506
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
14 Firmware Instructions for Channel
Partner Devices
Firmware overview for channel partners 508
Tuning a small heated zone 509
Thermal Aux Configuration 510
Valve Box Configuration 521
Inlet configuration 525
Cryo focus valve configuration 540
Cryo trap configuration 541
Detector configuration 543
Agilent Technologies
507
14 Firmware Instructions for Channel Partner Devices
Firmware overview for channel partners
This section contains instructions for installing and configuring
channel partner inlets, detectors, thermal aux zones, and cryo
focus valves, on an Agilent 7890 Series GC. Each section
includes information on:
How to wire your hardware
How to configure the GC to recognize your hardware
How to access the method parameter screen for your
hardware
For configuration of standard Agilent devices for the GC, see
the Accessory Installation sheets and the Agilent 7890A GC
Advanced User Guide or 7890B Operation Manual.
508
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Tuning a small heated zone
1 Disable the I and D terms. The D term is set to zero to disable
it, but the I term has an inverse effect, i.e. the larger the I
term the smaller its effect, so set the I term to its maximum
value.
2 Increase the P term as needed to achieve oscillation, then
decrease it until the oscillation is barely maintained. Note
the value of the P term, which we call Ku, and the period of
the oscillation in seconds, which we call Pu.
3 Use these values in one of the standard PID tuning methods,
such as Ziegler-Nichols, to calculate the PID terms.
For example: using Ziegler-Nichols tuning the PID values would
be:
P = Ku / 1.7
I = Pu / 2
D = Pu / 8
Ziegler-Nichols is probably a good tuning to use for any zone
that needs to be temperature programmed. It has a small
amount of overshoot but it settles fairly quickly. For zones that
don't need to be temperature programmed there are other
tunings that have less overshoot but are slower to settle, such as
Tyreus-Luyben tuning. The PID values using Tyreus-Luyben
tuning are:
P = Ku / 2.2
I = Pu * 2.2
D = Pu / 6.3
Reference: http://www.chem.mtu.edu/~tbco/cm416/zn.html
7890 Series GC IPB
509
14 Firmware Instructions for Channel Partner Devices
Thermal Aux Configuration
There are several control models to select for the standard
Agilent thermal aux zones. These include the AED transfer line,
the MSD transfer line, and the Nickel catalyst. This section only
covers the custom configuration of a thermal zone that is
available by selecting User configurable heater as the auxiliary
heater type during configuration. See the Agilent 7890A GC
Advanced User Guide or 7890B Operation Manual for
configuration of standard thermal aux zones.
Up to 3 thermal auxiliary zones can be configured. All 6 of the
GC's small heated zones are available for use. If cooling and
heating are required in the thermal zone's control, a cryo valve
is selected during configuration of a thermal zone.
Heater and cryo connection locations
Each heater connector has a 40 to 180 watt heater power supply
and a temperature sensor for the control loop. Labels on the
wiring harness near the connector identify the connection. The
labels match the GC display except for the FI or BI wiring
harness labels displayed as FINLET and BINLET.
510
Connector label / GC display
identifier
Connector location on GC
A1
Right side electrical compartment
position A1 (far left) on valve bracket
electrical harness
A2
Right side electrical compartment
position A2 (far right) on valve bracket
electrical harness
FI/FINLET
Left top side of GC frame adjacent to
front inlet
BI/BINLET
Left top side of GC frame adjacent to
back inlet
F-DET
Right side electrical compartment at
top position adjacent to front detector
B-DET
Right side electrical compartment at
top position adjacent to back detector
FV
Left top side of GC frame adjacent to
front inlet
BV
Left top side of GC frame adjacent to
back inlet
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Connections assigned to a thermal zone
Each Aux thermal zone can support one of two fixed heating
connections containing a heater and temperature sensor. When
one of the two allowed heater connections is configured to an
Aux Zone the other connection is not available for thermal zone
assignment. Additionally each thermal zone can support a cryo
valve.
Thermal Zone
Thermal Aux 1
Thermal Aux 2
Thermal Aux 3
Heater
Connection
Aux1 or
BI/BINLET
Aux2 or B-DET
FI/FINLET or
F-DET
Cryo Valve
Connection
BV
BV
FV
The User Configurable Heater allows heated zones ranging
from 40 watts to 180 watts.
7890 Series GC IPB
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14 Firmware Instructions for Channel Partner Devices
Auxiliary Type Selection
After assigning a heater or heater and cryo valve to an Aux
thermal zone and rebooting the GC, you configure the type of
device requiring thermal control. This is done by selecting the
Auxiliary type: field from the configuration menu and pressing
the [Mode/type] key. Several Agilent standard devices are listed
along with a selection for a User configurable heater.
When configuring a device for thermal control that is not listed
you can select the User configurable heater and create a
custom thermal control model. All but the User configurable
heater control model have a fixed maximum device setpoint of
400 deg C. The only auxiliary type to support a cryo valve is
User configurable heater.
Auxiliary type
Use
AED transfer line
For the AED transfer line
MSD transfer line
For the Agilent GC/MSD transfer line
Nickel Catalyst
For the Agilent nickel catalyst
Unknown
User configurable heater
512
For creation of a custom thermal
device
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
User Configurable Heater
The control algorithm used to maintain a stable temperature
setpoint requires several constants in order to model the
thermal response of a physical device. These constants can be
modified to model a custom control device when the Auxiliary
type: is set to User configurable heater.
Custom heater parameters
The PID and Mass fields These fields allow entry of custom
constants for the Proportional, Integral, Derivative, and Mass
associated with a thermal device's control algorithm.
The Power field This field allows for entry of the maximum
power that the heater requires. This value must be within 10%
of the actual maximum or an error is generated.
The Maximum Programming Rate field Enter the maximum rate
that the temperature of the device can change from one
temperature to another in a fixed period of time. If this field is
left at the default value of zero, the device cannot be
temperature controlled.
The Maxmimum Setpoint field Enter the maximum setpoint
allowed for the custom thermal device. The GC will not allow
the user to enter a value higher than this number.
Sensor Pressing [Mode/Type] on this field brings up the
sensor type for selection. Select from RTD and TC.
The zone control model Pressing [Mode/Type] on this field
brings up the available zone control models summarized in the
table.
7890 Series GC IPB
Control Model
Use
SS
Isothermal zone with cryo
PTV
High power requirement with cryo and
the ability to program temperature
ramps during a run
COC
Low power requirement with cryo and
the ability to program temperature
ramps during a run
513
14 Firmware Instructions for Channel Partner Devices
Programmable temperature zones
The PTV and COC zone control models for the User
configurable heater Auxiliary type and the Unknown Auxiliary
type, allow a temperature program to be entered for the device
similar to that available on an Agilent standard PTV and COC
inlet.
514
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Cryo control model
This field is only displayed if a cryo valve is configured in the
hardware.
Pressing [Mode/Type] on this field brings up the available cryo
control models summarized in the table.
7890 Series GC IPB
Cryo control model
Use
PTV
A control model that is similar to the
Agilent PTV inlet.
CryoTrap
A control model that lowers a device's
temperature anywhere during a run
and then increase the device's
temperature at a later time during the
run.
515
14 Firmware Instructions for Channel Partner Devices
Configuring the thermal Aux zone (Firmware A.01.07)
1 With the GC disconnected from its power source, install the
device containing the heater and temperature sensor and
optionally install a cryo valve.
2 Plug the heater and sensor cable from this device into one of
the six small heated zone connections.
3 Optionally plug the cryo valve 24-volt power supply into the
FV or BV connector.
4 With all covers installed, attach the power supply to the GC
and power the GC on.
5 Unlock the GC configuration. Press the [Options] key, select
Keyboard & Display and press the [Enter] key. Scroll down
to Hard Configuration Lock and press the [off] button.
6 From the section above titled "Connections assigned to a
thermal zone" determine the Aux Zone (1, 2 or 3) that you are
using based on the heater connection.
7 On the GC keypad press [Config] [Aux Temp #] press the
number of the thermal zone 1, 2, or 3.
8 With Unconfigured: selected press the [Mode/Type] key on
the GC keypad and if necessary scroll to see all selections.
You must only make a selection that contains the GC
identifier for the heater zone that your device is attached to.
If a cryo valve is attached to the FV or BV connector, the GC
also displays a selection for your heater zone and a cryo
valve configuration. Press [Enter] to complete your selection.
9 When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
10 On the GC keypad, press [Config] [Aux Temp #] press the
number of the thermal zone 1, 2, or 3. The display now shows
your configured devices.
11 Scroll to Auxiliary type: and press the [Mode/Type] key on
this field to bring up the available Auxiliary types. Select
User Configurable Heater to create a custom thermal device
and press [Enter].
12 If a cryo valve is included in this Aux Temperature zone,
scroll to Cryo type: press the [Mode/Type] key and select the
coolant supplied to the cryo valve. Next scroll to Cryo
516
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
control model: and press the [Mode/Type] key and select a
suitable model from the list.
When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps.
On the GC keypad, press [Config] [Aux Temp #] press the
number of the thermal zone 1, 2, or 3. The display now shows
your configured devices.
13 Next scroll to and enter the initial values for Proportional
gain, Integral time, Derivative time and Mass. These values
are usually later modified based on empirical results until
stable thermal performance is achieved.
14 Scroll to Power (watts) and enter the maximum power used
to heat the device.
15 Scroll to Maximum programming rate and enter a rate of
temperature rise per minute that your device is capable of
achieving.
16 Scroll to Maximum setpoint and enter a value that is within
the safe operating temperature of the device.
17 Scroll to the Sensor: field and make sure the sensor type
agrees with your hardware. To change the sensor type, press
the [Mode/Type] key and select the RTD or TC
(thermocouple with conversion board) type.
When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps.
On the GC keypad, press [Config] [Aux Temp #] press the
number of the thermal zone 1, 2, or 3. The display now shows
your configured devices.
18 Scroll to Zone control model: and press the [Mode/Type]
key on this field to bring up the available zone control
models. Select a suitable control model and press [Enter].
When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps.
7890 Series GC IPB
517
14 Firmware Instructions for Channel Partner Devices
On the GC keypad, press [Config] [Aux Temp #] press the
number of the thermal zone 1, 2, or 3. The display now shows
your configured devices.
19 Power cycle the GC to lock this configuration.
20 On the GC keypad press [Aux Temp #]. If other Thermal Aux
zones exist, press the keypad number (1, 2, or 3) for this
zone. This display the Thermal Zone's parameter list for
entering operating values for a method.
518
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Configuring the thermal Aux zone (Firmware A.01.08 and A.01.09)
1 With the GC disconnected from its power source, install the
device containing the heater and temperature sensor and
optionally install a cryo valve.
2 Plug the heater and sensor cable from this device into one of
the six small heated zone connections.
3 Optionally plug the cryo valve 24 volt power supply into the
FV or BV connector.
4 With all covers installed, attach the power supply to the GC
and power the GC on.
5 Unlock the GC configuration. Press the [Options] key, select
Keyboard & Display and press the [Enter] key. Scroll down to
Hard Configuration Lock and press the [off] button.
6 From the section above titled "Connections assigned to a
thermal zone" determine the Aux Zone (1, 2 or 3) that you are
using based on the heater connection.
7 On the GC keypad press [Config] [Aux Temp #] press the
number of the thermal zone 1, 2, or 3.
8 With Unconfigured: selected press the [Mode/Type] key on
the GC keypad and if necessary scroll to see all selections.
You must only make a selection that contains the GC
identifier for the heater zone that your device is attached to.
If a cryo valve is attached to the FV or BV connector, the GC
also displays a selection for your heater zone and a cryo
valve configuration. Press [Enter] to complete your selection.
9 When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
10 On the GC keypad, press [Config] [Aux Temp #] press the
number of the thermal zone 1, 2, or 3. The display now shows
your configured devices.
11 Scroll to Auxiliary type: and press the [Mode/Type] key on
this field to bring up the available Auxiliary types. Select
User Configurable Heater to create a custom thermal device
and press [Enter].
12 If a cryo valve is included in this Aux Temperature zone,
scroll to Cryo type: press the [Mode\Type] key and select the
coolant supplied to the cryo valve. Next scroll to Cryo control
7890 Series GC IPB
519
14 Firmware Instructions for Channel Partner Devices
model: and press the [Mode/Type] key and select a suitable
model from the list.
13 To display all the configuration parameters select View
Custom Heater Conf and press [On/Yes].
14 Next scroll to and enter the initial values for Proportional
gain, Integral time, Derivative time and Mass. These values
are usually later modified based on empirical results until
stable thermal performance is achieved.
15 Scroll to Zone control model: and press the [Mode/Type] key
on this field to bring up the available zone control models.
Select a suitable control model and press [Enter].
16 Scroll to the Sensor: field and make sure the sensor type
agrees with your hardware. To change the sensor type, press
the [Mode\Type] key and select the RTD or TC
(thermocouple with conversion board) type.
17 Scroll to Power (watts) and enter the maximum power used
to heat the device.
18 Scroll to Maximum setpoint and enter a value that is within
the safe operating temperature of the device.
19 Scroll to Maximum programming rate and enter a rate of
temperature rise per minute that your device is capable of
achieving.
20 Power cycle the GC to lock this configuration.
21 On the GC keypad press [Aux Temp #]. If other Thermal Aux
zones exist, press the keypad number (1, 2, or 3) for this
zone. This display the Thermal Zone's parameter list for
entering operating values for a method.
520
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Valve Box Configuration
The GC allows for a valve box hardware configuration consisting
of one or two heaters in the valve box. An Agilent standard
configuration uses one or two 70 watt heaters in the valve box.
If you set the Custom Heater Conf. Parameter to [Off/ No] the
PID, Mass, and Power fields use values optimized for these 70
watt heaters and any custom setting is ignored.
You may also design a custom heated valve box with a need for
different heater parameters. To do this, set the Custom Heater
Conf. Parameter to [On /Yes] and enter custom values for the
PID, Mass, and Power fields.
7890 Series GC IPB
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14 Firmware Instructions for Channel Partner Devices
Heater connection locations
Each heater connector has a 40 to 180 watt heater power supply
and a temperature sensor for the control loop. Labels on the
wiring harness near the connector identify the connection.
522
Connector label / GC display
identifier
Connector location on GC
A1
Right side electrical compartment
position A1 (far left) on valve bracket
electrical harness
A2
Right side electrical compartment
position A2 (far right) on valve bracket
electrical harness
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Custom heater parameters
Custom Heater Conf.
Set the value to [On/Yes] to enable your custom heater
parameters entered below. Setting the value to [Off/No] defaults
to the Agilent standard valve box values for these numbers.
View Custom Heater Conf.
Set the value to [On/yes] to display the custom heater field
values of PID, Mass, and Power.
The PID and Mass fields
These fields allow entry of custom constants for the
Proportional, Integral, Derivative, and Mass associated with a
thermal device's control algorithm.
The Power field
This field allows for entry of the maximum power that the
heater requires. This value must be within 10% of the actual
maximum or an error is generated.
7890 Series GC IPB
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14 Firmware Instructions for Channel Partner Devices
Configuring the Valve Box Zone
1 With the GC disconnected from its power source, install the
custom heater(s) and temperature sensor(s). You can install
up to 2 heaters and temperatures for this zone.
2 Plug the heater and sensor cable(s) from the heater(s) into
the A1 and/or A2 small heated zone connection.
3 With all covers installed, attach the power supply to the GC
and power the GC on.
4 Unlock the GC configuration. Press the [Options] key, select
Keyboard & Display and press the [Enter] key. Scroll down
to Hard Configuration Lock and press the [off] button.
5 On the GC keypad press [Config] [Aux Temp #] and select
Valve Box.
6 With Unconfigured: selected press the [Mode/Type] key on
the GC keypad and select one of the following: Install Heater
A1; Install Heater A2; Install 2 htr A1 & A2.. Press [Enter] to
complete your selection.
7 When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
8 On the GC keypad, press [Config] [Aux Temp #] and select
valve box. The display now shows your configured heater(s).
9 To allow use of the custom heater parameters, scroll to
Custom Heater Conf. And press the [On/Yes] key.
10 To display all the configuration parameters select View
Custom Heater Conf and press [On/Yes].
11 Next scroll to and enter the initial values for Proportional
gain, Integral time, Derivative time, and Mass. These values
are usually later modified based on empirical results until
stable thermal performance is achieved.
12 Scroll to Power (watts) and enter the maximum power used
to heat the device.
13 Power cycle the GC to lock this configuration.
14 On the GC keypad press [Aux Temp #] and select Valve Box.
This displays the Valve box heating setpoint value for a
method.
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7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Inlet configuration
A custom inlet can be configured using a channel partner PTV
with or without a heater or cryo valve. Additionally a channel
partner PCM configuration allows an Agilent PCM flow control
to be used in a heated inlet control loop.
This section does not cover the configuration of the standard
Agilent inlet EPC modules. See the Agilent 7890A GC Advanced
User Guide or 7890B Operation Manual for the configuration
of Agilent standard inlets.
7890 Series GC IPB
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14 Firmware Instructions for Channel Partner Devices
Hardware configuration
Use this table to determine the allowable hardware
configurations, where the hardware electrical connection must
be made, and the configuration to select for this hardware as
displayed by the GC. All hardware must be installed before
attempting to configure the inlet.
GC configuration
display selections
Hardware
Configuration
EPC wiring
connection
Heater wiring
connection
Cryo valve connection
Install Front Inlet
PTV + HTR
EPC1
FI
None
Install Front Inlet
(CRYO)
PTV+HTR+CRYO
EPC1
FI
FV
Install Front Inlet (NO
HTR)
PTV
EPC1
None
None
Install Front Inlet
PCM + HTR
EPC1
FI
None
Install Front Inlet
(CRYO)
PCM+HTR+CRYO
EPC1
FI
FV
Install Back Inlet
PTV + HTR
EPC2
BI
None
Install Back Inlet
(CRYO)
PTV+HTR+CRYO
EPC2
BI
BV
Install Back Inlet (NO
HTR)
PTV
EPC2
None
None
Install Back Inlet
PCM + HTR
EPC2
BI
None
Install Back Inlet
(CRYO)
PCM+HTR+CRYO
EPC2
BI
BV
Front inlet PTV
Front inlet PCM
Back inlet PTV
Back inlet PCM
526
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
EPC module installation
A PCM or PTV EPC installed in the standard EPC module
location for a front or back inlet can be custom configured as a
channel partner (CP) inlet by the GC. This requires removal of
the top EPC module cover.
7890 Series GC IPB
EPC wiring harness label
Location
EPC1
Left front EPC module slot
EPC2
Left back EPC module slot
527
14 Firmware Instructions for Channel Partner Devices
Heater and Cryo installation
Optionally install and attach your inlet device's heater and inlet
controlled cryo valve to the GC's wiring harness. This requires
the removal of the left side GC cover.
528
Wiring harness label
Location
FI
Left top side of GC frame adjacent to
front inlet
FV
Left top side of GC frame adjacent to
front inlet
BI
Left top side of GC frame adjacent to
back inlet
BV
Left top side of GC frame adjacent to
back inlet
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
The Inlet configuration display
Gas type
Pressing the [Mode/Type] key on this field brings up the choices
for carrier gases connected to an inlet. Select the carrier gas
going to this inlet and press the [Enter] key.
Cryo Parameters
These parameters are displayed when a cryo valve is included in
the hardware configuration.
Cryo type
Pressing the [Mode/Type] key on this field brings up the choices
for cryo gas connected to the inlet's cryo valve. Select the cryo
gas connected to the inlet's cryo valve and press the [Enter] key.
Changing this type requires rebooting the GC. This field
displays when a cryo valve is configured to the inlet.
Cryo
Use the [On/Yes] key to enable cryo cooling on this inlet. The
[Off/No] key disables cryo cooling. This field displays when a
cryo valve is configured to the inlet.
Use Cryo temperature
Enter a maximum temperature for cryo cooling activation. This
field displays when a cryo valve is configured to the inlet and
the cooling type is not air.
Cryo timeout
Enter a time in minutes for the cryo valve to close if no run has
started before this time elapses. This field displays when a cryo
valve is configured to the inlet and the cooling type is not air.
Cryo fault
The GC can shut down temperature control of the inlet if
setpoint is not reached in 16 minutes. Use the [On/Yes] key to
enable temperature shutdown on this inlet. The [Off/No] key
disables temperature shutdown. This field displays when a cryo
valve is configured to the inlet.
7890 Series GC IPB
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14 Firmware Instructions for Channel Partner Devices
Custom heater parameters
The control algorithm used to maintain a stable temperature
setpoint requires several constants in order to model the
thermal response of a physical device. To access these
constants, from the inlet's configuration display select View
Custom Heater Conf and press [On/yes].
The PID and Mass fields These fields allow entry of custom
constants for the Proportional, Integral, Derivative, and Mass
associated with a thermal device's control algorithm.
The Power field This field allows for entry of the maximum
power that the heater requires. This value must be within 10%
of the actual maximum or an error is generated.
The Maximum Setpoint field Enter the maximum setpoint
allowed for the custom thermal device. The GC will not allow
the user to enter a value higher than this number.
Sensor Pressing the [Mode/Type] key on this field brings up
the sensor type for selection. Select from RTD and TC.
The Maximum Programming Rate field Enter the maximum rate
that the temperature of the device can change from one
temperature to another in a fixed period of time. If this field is
left at the default value of zero, the device cannot be
temperature controlled. An inlet with a zone control model of
PTV or COC requires a non-zero valve to allow temperature
programming.
The zone control model Pressing the [Mode/Type] key on this
field brings up the available zone control models summarized in
the table below.
Control Model
Use
SS
Isothermal zone with cryo
PTV
High power requirement with cryo and the ability to program temperature ramps during a run
COC
Low power requirement with cryo and the ability to program temperature ramps during a run
Programmable temperature inlets
The PTV and COC zone control models allow a temperature
program to be entered for the device similar to that available on
an Agilent standard PTV and COC inlet. The SS zone control
530
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
model is for isothermal control and therefore can't be
programmed.
Configured hardware
The last few lines of the inlet's configuration screen lists the
hardware controlled by the inlet. One line shows the EPC
modules slot location and type. Another line indicates the
heater used and its wattage, and the final line the cryo valve
use.
7890 Series GC IPB
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14 Firmware Instructions for Channel Partner Devices
Configuring a custom inlet (Firmware A.01.05)
1 With the GC disconnected from its power source, install a
PCM or PTV EPC module in the front or back inlet EPC
module location. Plug the EPC module into the correct
wiring harness connector. See EPC module location above.
2 Optionally install the inlet device containing the heater and
temperature sensor.
3 Plug the heater and sensor cable from this device into one of
the inlet's heated zone connections. See the "Heater and Cryo
Installation" section above for the wiring harness connector
to use.
4 Optionally install a cryo valve and plug it into the 24 volt
power supply into the FV or BV connector.
5 With all covers installed, attach the power supply to the GC
and power the GC on.
6 Unlock the GC configuration. Press the [Options] key, select
Keyboard & Display and press the [Enter] key. Scroll down
to Hard Configuration Lock and press the [off] button.
7 On the GC keypad press [Config] [Front Inlet] for the
configuration of a front inlet device or [Config] [Back Inlet]
for the configuration of a back inlet device.
8 With Unconfigured: selected press the [Mode/Type] key on
the GC keypad and if necessary scroll to see all selections.
See the table in the Hardware Configuration section for the
correct display line to select. Press [Enter] to complete your
selection.
9 When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
10 Select the configuration display for this inlet. The display
now shows your configured hardware devices.
11 Scroll to Gas type: and press the [Mode/Type] key on this
field to bring up the available carrier gas types. Select the gas
type attached to the inlet and press [Enter].
12 If a cryo valve is included in this inlet, scroll to Cryo type:
press the [Mode\Type] key and select the coolant supplied to
the cryo valve. Set the Cryo, Cryo timeout, and Cryo fault
parameters as required. See above.
532
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
13 To display all the configuration parameters select View
Custom Heater Conf and press [On/Yes]. This displays all
the heater parameters that can be set.
14 Scroll to Zone control model: and press the [Mode/Type]
key on this field to bring up the available zone control
models. Select a suitable control model and press [Enter].
15 Next scroll to and enter the initial values for Proportional
gain, Integral time, Derivative time and Mass. These values
are usually later modified based on empirical results until
stable thermal performance is achieved.
16 Scroll to the Sensor: field and make sure the sensor type
agrees with your hardware. To change the sensor type, press
the [Mode\Type] key and select the RTD or TC
(thermocouple with conversion board) type.
17 Scroll to Power (watts) and enter the power used to heat the
device.
18 Scroll to Maximum setpoint and enter a value that is within
the safe operating temperature of the device.
19 Scroll to Maximum programming rate and enter a rate of
temperature rise per minute that your device is capable of
achieving. This setting is not used with the SS zone control
model which does not allow temperature programming.
20 Power cycle the GC to lock this configuration.
21 On the GC keypad press [Front Inlet] or [Back Inlet] to
display the inlet's parameter list for entering operating
values for a method.
7890 Series GC IPB
533
14 Firmware Instructions for Channel Partner Devices
Configuring a custom inlet (Firmware A.01.07)
1 With the GC disconnected from its power source, install a
PCM or PTV EPC module in the front or back inlet EPC
module location. Plug the EPC module into the correct
wiring harness connector. See EPC module location above.
2 Optionally install the inlet device containing the heater and
temperature sensor.
3 Plug the heater and sensor cable from this device into one of
the inlet's heated zone connections. See the "Heater and Cryo
Installation" section above for the wiring harness connector
to use.
4 Optionally install a cryo valve and plug it into the 24 volt
power supply into the FV or BV connector.
5 With all covers installed, attach the power supply to the GC
and power the GC on.
6 Unlock the GC configuration. Press the [Options] key, select
Keyboard & Display and press the [Enter] key. Scroll down
to Hard Configuration Lock and press the [off] button.
7 On the GC keypad press [Config] [Front Inlet] for the
configuration of a front inlet device or [Config] [Back Inlet]
for the configuration of a back inlet device.
8 With Unconfigured: selected press the [Mode/Type] key on
the GC keypad and if necessary scroll to see all selections.
See the table in the Hardware Configuration section for the
correct display line to select. Press [Enter] to complete your
selection.
9 When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
10 Select the configuration display for this inlet. The display
now shows your configured hardware devices.
11 Scroll to Gas type: and press the [Mode/Type] key on this
field to bring up the available carrier gas types. Select the gas
type attached to the inlet and press [Enter].
12 If a cryo valve is included in this inlet, scroll to Cryo type:
press the [Mode\Type] key and select the coolant supplied to
the cryo valve.
534
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
Select the configuration display for this inlet.
13 Set the Cryo, Cryo timeout, and Cryo fault parameters as
required. See above.
14 Scroll to Zone control model: and press the [Mode/Type]
key on this field to bring up the available zone control
models. Select a suitable control model and press [Enter].
When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
Select the configuration display for this inlet.
15 To display all the configuration parameters select View
Custom Heater Conf and press [On/Yes]. This displays all
the heater parameters that can be set.
16 Next scroll to and enter the initial values for Proportional
gain, Integral time, Derivative time and Mass. These values
are usually later modified based on empirical results until
stable thermal performance is achieved.
17 Scroll to Power (watts) and enter the power used to heat the
device.
18 Scroll to Maximum setpoint and enter a value that is within
the safe operating temperature of the device.
19 Scroll to Maximum programming rate and enter a rate of
temperature rise per minute that your device is capable of
achieving. This setting is not used with the SS zone control
model which does not allow temperature programming.
20 Scroll to the Sensor: field and make sure the sensor type
agrees with your hardware. To change the sensor type, press
the [Mode\Type] key and select the RTD or TC
(thermocouple with conversion board) type.
21 Power cycle the GC to lock this configuration.
7890 Series GC IPB
535
14 Firmware Instructions for Channel Partner Devices
22 On the GC keypad press [Front Inlet] or [Back Inlet] to
display the inlet's parameter list for entering operating
values for a method.
536
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Configuration procedure
1 With the GC disconnected from its power source, install the
device containing the cryo focus valve.
2 Plug the 24 volt actuator cable from this device into the FV or
BV connection.
3 With all covers installed, attach the power supply to the GC
and power the GC on.
4 Unlock the GC configuration.
5 Press the [Config] key and select cryo focus valve from the
list by scrolling to this entry and pressing [enter].
6 For Firmware A.01.05: Select the Cryo Focus valve attached
to FV or BV.
For Firmware A.01.07 through A.01.09: With
Unconfigured: selected, press [Mode/Type] and select the
Cryo Focus valve attached to FV or BV.
7 After rebooting the GC, selecting the configuration for this
cryo valve will show the valve properly associated to the FV
or BV connector.
8 To display the method parameters for the cryofocus valve
press the [Valve #] key. If other valves exist, scroll down to
set the Cryo focus equib time and Cryofocus delay time.
7890 Series GC IPB
537
14 Firmware Instructions for Channel Partner Devices
Configuring a custom inlet (Firmware A.01.08 and A.01.09)
1 With the GC disconnected from its power source, install a
PCM or PTV EPC module in the front or back inlet EPC
module location. Plug the EPC module into the correct
wiring harness connector. See EPC module location above.
2 Optionally install the inlet device containing the heater and
temperature sensor.
3 Plug the heater and sensor cable from this device into one of
the inlet's heated zone connections. See the "Heater and Cryo
Installation" section above for the wiring harness connector
to use.
4 Optionally install a cryo valve and plug it into the 24 volt
power supply into the FV or BV connector.
5 With all covers installed, attach the power supply to the GC
and power the GC on.
6 Unlock the GC configuration. Press the [Options] key, select
Keyboard & Display and press the [Enter] key. Scroll down to
Hard Configuration Lock and press the [off] button.
7 On the GC keypad press [Config] [Front Inlet] for the
configuration of a front inlet device or [Config] [Back Inlet]
for the configuration of a back inlet device.
8 With Unconfigured: selected press the [Mode/Type] key on
the GC keypad and if necessary scroll to see all selections.
See the table in the Hardware Configuration section for the
correct display line to select. Press [Enter] to complete your
selection.
9 When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
10 Select the configuration display for this inlet. The display
now shows your configured hardware devices.
11 Scroll to Gas type: and press the [Mode/Type] key on this
field to bring up the available carrier gas types. Select the gas
type attached to the inlet and press [Enter].
12 If a cryo valve is included in this inlet, scroll to Cryo type:
press the [Mode\Type] key and select the coolant supplied to
the cryo valve. Set the Cryo, Cryo timeout, and Cryo fault
parameters as required. See above.
538
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
13 To display all the configuration parameters select View
Custom Heater Conf and press [On/Yes]. This displays all the
heater parameters that can be set.
14 Scroll to Zone control model: and press the [Mode/Type] key
on this field to bring up the available zone control models.
Select a suitable control model and press [Enter].
15 Next scroll to and enter the initial values for Proportional
gain, Integral time, Derivative time and Mass. These values
are usually later modified based on empirical results until
stable thermal performance is achieved.
16 Scroll to the Sensor: field and make sure the sensor type
agrees with your hardware. To change the sensor type, press
the [Mode\Type] key and select the RTD or TC
(thermocouple with conversion board) type.
17 Scroll to Power (watts) and enter the power used to heat the
device.
18 Scroll to Maximum setpoint and enter a value that is within
the safe operating temperature of the device.
19 Scroll to Maximum programming rate and enter a rate of
temperature rise per minute that your device is capable of
achieving. This setting is not used with the SS zone control
model which does not allow temperature programming.
20 Power cycle the GC to lock this configuration.
21 On the GC keypad press [Front Inlet] or [Back Inlet] to
display the inlet's parameter list for entering operating
values for a method.
7890 Series GC IPB
539
14 Firmware Instructions for Channel Partner Devices
Cryo focus valve configuration
Use the cryo focus valve when temperature control is not
required and the run must start out with a relatively low
temperature in a device which must be held for a fixed period of
time after the run begins. This valve is programmed to remain
open for a minimum time period prior to the run (equib time)
and a fixed period of time after the run begins (delay time).
Operation
The cryo focus valve control energizes the cryo valve actuator
for a minimum programmable time before a run begins and a
fixed amount of time after the run begins. These two time
setpoints are entered by the user pressing the [Valve] key and
then selecting the cryo focus valve from the valve list.
To start a run using manual injection, the user presses the [prep
run] key to actuate the valve. The run cannot start until the
equib time programmed elapses. The valve remains continually
energized from the time [prep run] is pressed until the delay
time programmed after the start run completes. The run starts
when the user presses the [Start] key. Using an automatic liquid
sampler or injection valve automates this process and it is only
necessary for the user to press the [Start] key.
Assigned connections
The cryo focus valve actuator is connected to the FV or BV 24
volt socket adjacent to the front and back inlet connections.
540
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Cryo trap configuration
This procedure applies to GCs with firmware version A.01.09.
Firmware A.01.09 or greater is required.
This procedure assumes that the cryo trap is installed such that:
the heater connects to the back inlet BI connector.
the valve actuator connects to back inlet BV connector.
To configure the cryo trap:
1 Press [Config], select Aux Temp # > Thermal Aux 1, press [Enter].
2 Press [Mode/Type], select Install BINLET with BV Cryo, press
[Enter].
3 Soft-reboot the GC. Press [Options], select Communications >
Enter > Reboot GC > [On/Yes] > [On/Yes].
4 Press [Config], select Aux Temp # > Thermal Aux 1 > [Enter].
Select Auxiliary Type: Unknown, press [Mode/Type], select User
Configurable Heater, press [Enter].
5 Soft-reboot the GC. Press [Options], select Communications >
Enter > Reboot GC > [On/Yes] > [On/Yes].
6 Press [Config], select Aux Temp # > Thermal Aux 1 > Cryo Type
(Valve BV): N2.
If Cryo Type (Valve BV) does not equal N2, then select Cryo Type
(Valve BV), press [Mode/Type], select N2 Cryo, press [Enter] then
[Clear].
7 Configure Aux 1 by scrolling to each entry listed below and
making the appropriate changes. After each step, press
[Clear] to ignore the reboot request. You will reboot later.
a Proportional Gain: 5.30, press [Enter] then [Clear].
b Integral Time: 10, press [Enter] then [Clear].
c Derivative Time: 1.00, press [Enter] then [Clear].
d Mass (Watt-sec/deg): 18, press [Enter] then [Clear].
e Power (Watts):
To find the watts to set here, scroll down approximately 6
positions to Back Inlet Status (BINLET). As an example, it
may read: BINLET (OK): 125 Watts. Use this reading (in this
example 125 Watts) as the parameter for Power (Watts).
Enter 125, press [Enter] then [Clear].
7890 Series GC IPB
541
14 Firmware Instructions for Channel Partner Devices
Cryo Control Mode > [Mode/Type]:
Cryo Control Type: PTV (ignore the first line, should already
be PTV)
Cryo Control Type: Cryo Trap, press [Enter] then [Clear].
g Zone Control Mode > [Mode/Type] > PTV, press [Enter]
then [Clear].
h Sensor > [Mode/Type] > Thermocouple, press [Enter] then
[Clear].
Maximum Setpoint: 400, press [Enter] then [Clear].
Maximum Programming Rate: 720, press [Enter] then
[Clear].
8 Soft-reboot the GC. Press [Options], select Communications >
Enter > Reboot GC > [On/Yes] > [On/Yes].
542
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Detector configuration
Use the following 3 tables to determine the component wiring
connections for the hardware configuration you are designing.
See the Agilent Advanced User guide for configuring Agilent
standard detector types.
7890 Series GC IPB
543
14 Firmware Instructions for Channel Partner Devices
FID Signal 1 Detector Hardware Connections
The following table lists the hardware connections for an
Agilent standard FID. Additionally listed is the hardware
connections required for a channel partner primary FID signal
board with or without a secondary FID or AIB signal board.
GC configuration
display selection
EPC wire harness
connection
Heater wire harness
connection
Signal 1 Detector
Board wire harness
connection
Signal 2 Detector
Board wire harness
connection
FID
EPC3
F-DET
F-DET
None
FID + AIB
None
None
F-DET
AUX DET1
CPDET FID, No htr, No
EPC
None
None
F-DET
None
CPDET FID & Htr, No
EPC
None
F-DET
F-DET
None
CPDET FID & EPC, No
Htr
EPC3
None
F-DET
None
CPDET FID & EPC &
Htr
EPC3
F-DET
F-DET
None
CPDET FID & AIB &
Htr, No EPC
None
F-DET
F-DET
AUX DET1
CPDET FID & AIB &
EPC, No htr
EPC3
None
F-DET
AUX DET1
CPDET FID & AIB &
Htr & EPC
EPC3
F-DET
F-DET
AUX DET1
CPDET FID & FID &
Htr, No EPC
None
F-DET
F-DET
AUX DET1
CPDET FID & FID &
EPC, No htr
EPC3
None
F-DET
AUX DET1
CPDET FID & FID & Htr
& EPC
EPC3
F-DET
F-DET
AUX DET1
FID
EPC4
B-DET
B-DET
None
FID + AIB
None
None
B-DET
AUX DET2
CPDET FID, No htr, No
EPC
None
None
B-DET
None
Front detector
Back detector
544
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
GC configuration
display selection
EPC wire harness
connection
Heater wire harness
connection
Signal 1 Detector
Board wire harness
connection
Signal 2 Detector
Board wire harness
connection
CPDET FID & Htr, No
EPC
None
B-DET
B-DET
None
CPDET FID & EPC, No
Htr
EPC4
None
B-DET
None
CPDET FID & EPC &
Htr
EPC4
B-DET
B-DET
None
CPDET FID & AIB &
Htr, No EPC
None
B-DET
B-DET
AUX DET2
CPDET FID & AIB &
EPC, No htr
EPC4
None
B-DET
AUX DET2
CPDET FID & AIB &
Htr & EPC
EPC4
B-DET
B-DET
AUX DET2
CPDET FID & FID &
Htr, No EPC
None
B-DET
B-DET
AUX DET2
CPDET FID & FID &
EPC, No htr
EPC4
None
B-DET
AUX DET2
CPDET FID & FID & Htr
& EPC
EPC4
B-DET
B-DET
AUX DET2
14
In the above table, FID indicates a detector signal board with
igniter control support. CPDET FID indicates a channel partner
FID detector signal board without support for an igniter.
7890 Series GC IPB
545
14 Firmware Instructions for Channel Partner Devices
AIB Signal 1 Detector Hardware Connections
The following table lists the hardware connections required for
a channel partner primary AIB signal board with or without a
secondary FID or AIB signal board. The first two entries under
Front Detector and Back Detector entries are for the standard
legacy Agilent AIB installations.
GC configuration
display selection
EPC wire harness
connection
Heater wire harness
connection
Signal 1 Detector
Board wire harness
connection
Signal 2 Detector
Board wire harness
connection
Install AIB with No
Heater
None
None
F-DET
None
Install AIB with
Heater
None
F-DET
F-DET
None
CPDET AIB, No htr, No None
EPC
None
F-DET
None
CPDET AIB & Htr, No
EPC
None
F-DET
F-DET
None
CPDET AIB & EPC, No
Htr
EPC3
None
F-DET
None
CPDET AIB & EPC &
Htr
EPC3
F-DET
F-DET
None
CPDET AIB & AIB &
Htr, No EPC
None
F-DET
F-DET
AUX DET1
CPDET AIB & AIB &
EPC, No htr
EPC3
None
F-DET
AUX DET1
CPDET AIB & AIB &
Htr & EPC
EPC3
F-DET
F-DET
AUX DET1
CPDET AIB & FID &
Htr, No EPC
None
F-DET
F-DET
AUX DET1
CPDET AIB & FID &
EPC, No htr
EPC3
None
F-DET
AUX DET1
CPDET AIB & FID &
Htr & EPC
EPC3
F-DET
F-DET
AUX DET1
Front detector
546
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
GC configuration
display selection
EPC wire harness
connection
Heater wire harness
connection
Signal 1 Detector
Board wire harness
connection
Signal 2 Detector
Board wire harness
connection
Install AIB with No
Heater
None
None
B-DET
None
Install AIB with
Heater
None
B-DET
B-DET
None
CPDET AIB, No htr, No None
EPC
None
B-DET
None
CPDET AIB & Htr, No
EPC
None
B-DET
B-DET
None
CPDET AIB & EPC, No
Htr
EPC4
None
B-DET
None
CPDET AIB & EPC &
Htr
EPC4
B-DET
B-DET
None
CPDET AIB & AIB &
Htr, No EPC
None
B-DET
B-DET
AUX DET2
CPDET AIB & AIB &
EPC, No htr
EPC4
None
B-DET
AUX DET2
CPDET AIB & AIB &
Htr & EPC
EPC4
B-DET
B-DET
AUX DET2
CPDET AIB & FID &
Htr, No EPC
None
B-DET
B-DET
AUX DET2
CPDET AIB & FID &
EPC, No htr
EPC4
None
B-DET
AUX DET2
CPDET AIB & FID &
Htr & EPC
EPC4
B-DET
B-DET
AUX DET2
14
Back detector
7890 Series GC IPB
547
14 Firmware Instructions for Channel Partner Devices
Aux Detector Hardware Connections
EPC wire
GC
configuration harness
connection
display
selection
Heater wire
harness
connection
Signal 1
Detector
Board wire
harness
connection
Signal 2
Detector
Board wire
harness
connection
Aux Detector
1
TCD
EPC5
A1 or A2 or
BI/BINLET
AUX DET1
None
AIB
None
None
AUX DET1
None
None
None
AUX DET2
None
Aux Detector
2
AIB
The Aux Detector 1 TCD installation requires an extension
cable to reach the EPC module and detector board located in a
side mounted enclosure. The heater and sensor for the Aux TCD
also requires an extension cable.
EPC module installation
Optionally install and attach your detector device's EPC module
to the GC's wiring harness.
548
EPC wiring harness label
Use
EPC3
Front detector EPC module
EPC4
Back detector EPC module
EPC5
3rd detector TCD EPC module
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
Detector Board Installation
Wiring harness label
Use
F-DET
Front detector board
B-DET
Back detector board
AUX DET1
3rd detector TCD board or AIB
AUX DET2
Aux detector board AIB
Heater installation
Optionally install and attach your detector device's heater to the
GC's wiring harness.
7890 Series GC IPB
Wiring harness label
Use
F-DET
Front detector heater
B-DET
Back detector heater
A1
3rd detector heater
A2
3rd detector heater
549
14 Firmware Instructions for Channel Partner Devices
Configuring a custom detector
1 With the GC disconnected from its power source, remove the
electronics side panel and install the detector boards in the
detector slots. See the section on configuration and plug the
correct communications cable into the board.
2 Install the detector optionally containing a heater and
temperature sensor. Plug the heater and sensor cable from
this device into one of the six small heated zone connections.
See the "Heater Installation" section above for the wiring
harness connector to use.
3 Optionally install an FID EPC module in the front, back, or
aux detector EPC module location. Plug the EPC module into
the correct wiring harness connector. See EPC module
location above.
4 With all covers installed, attach the power supply to the GC
and power the GC on.
5 Unlock the GC configuration. Press the [Options] key, select
Keyboard & Display and press the [Enter] key. Scroll down
to Hard Configuration Lock and press the [off] button.
6 On the GC keypad press [Config] [Front Det] for the
configuration of a front detector device or [Config] [Back
Det] for the configuration of a back detector device or
[Config] [Aux Det #] for the configuration of a Aux detector
device.
7 With Unconfigured: selected press the [Mode/Type] key on
the GC keypad and if necessary scroll to see all selections.
Select your hardware configuration from the list and press
[Enter] to complete your selection.
8 When the GC prompts to power cycle the GC, reboot the GC
by pressing the [Options] key and select Communications.
From this option scroll down and select the reboot option
and press [Enter] on the GC keypad. This soft reboot keeps
the GC configuration unlocked for subsequent steps. Power
cycling the GC forces you to unlock the GC configuration on
power-up.
9 Select the configuration display for this detector. The display
now shows your configured devices.
10 For an FID installation, scroll to Gas type: and press the
[Mode/Type] key on this field to bring up the available
makeup gas types. Select the gas type and press [Enter].
11 Power cycle the GC to lock this configuration.
550
7890 Series GC IPB
Firmware Instructions for Channel Partner Devices
14
12 On the GC keypad press [Front Det] or [Back Det] or [Aux
Det #] to display the detector's parameter list for entering
operating values for a method.
7890 Series GC IPB
551
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
15 Service Mode Diagnostics
Service mode overview 553
Detector diagnostics 554
Signal board diagnostics 555
Multiplexed ADC 556
Pneumatics 557
Power diagnostics 558
Agilent Technologies
552
Service Mode Diagnostics
15
Service mode overview
Service mode generates a series of tables that include
information that can help with diagnosing problems. For
example, the detector signal board diagnostic includes
information to verify a short in an FID ignitor. It also contains a
measurement of the Noise in the signal output.
To access the service mode diagnostics:
1 Press [Service Mode].
2 Scroll to Diagnostics and press [Enter].
The list of diagnostics that are available vary with your
configuration. Here is an example of a 7890A GC with 2 inlets, 2
detectors, an AUX module, and a PCM module.
DIAGNOSTICS
Instrument status
Front inlet
Back inlet
Front detector
Back detector
Auxiliary pressure (1,2,3)
Pcm B
Thermal PID control
Electronics
7890 Series GC IPB
553
15 Service Mode Diagnostics
Detector diagnostics
For example, the detector signal board diagnostic includes
information to verify a short in an FID ignitor. It also contains a
measurement of the Noise in the signal output.
To access the detector diagnostics:
1 Press [Service Mode].
2 Scroll to Diagnostics and press [Enter].
3 Scroll to <Front, Back, or AUX detector> and press [Enter].
The list of diagnostics that are available vary with your
configuration. Here is an example of an FID detector.
FRONT FID DIAGNOSTICS
Detector Signal
Pneumatics module
Hydrogen gas
Air gas
Makeup gas
554
7890 Series GC IPB
Service Mode Diagnostics
15
Signal board diagnostics
Service mode is a series of tables that include information that
can help with diagnosing problems. For example, the detector
signal board diagnostic includes information to verify a short in
an FID ignitor. It also contains a measurement of the Noise in
the signal output.
To access the detector signal board diagnostics:
1 Press [Service Mode].
2 Scroll to Diagnostics and press [Enter].
3 Scroll to <Front, Back, or AUX detector> and press [Enter].
4 Scroll to Detector Signal and press [Enter].
The list of diagnostics that are available vary with your detector.
Here is an example of an FID detector.
FRONT SIGNAL (FID)
Signal Value
Noise
High Voltage
Ignitor:
ADC Offset:
Input disable
Ignitor voltage
Mode:
7890 Series GC IPB
0.00V
60.1mV
0.0
0
12.9V
0.0A
Ref: 2.48V
Off
Off
Normal
555
15 Service Mode Diagnostics
Multiplexed ADC
This information is based on Service Mode | Diagnostics |
Electronics | Multiplexed ADC.
MULTIPLEXED ADC
Definition
Reading noise
Reading value
Offset
Gain counts/volt
Gain counts/ohm
Reference
Temperature
Reading value
Reading value
Reading value
Reading value
Reading value
Reading value
Oven rtd
159.8
1801821
54907
4173672
14607
95.446
1801887
-95
-180
198
64
-45
There is a multiplexed analog-to-digital circuit (ADC) for each of
the following resistance temperature detectors (rtd):
Oven rtd reading
Front detector rtd reading
Back detector rtd reading
Front inlet rtd reading
Back inlet rtd reading
Auxiliary 1 rtd reading
Auxiliary 2 rtd reading
Line Sense reading
Temperature ref reading
Atmospheric pressure reading
Minus 24V power supply rdg
Logic current reading
24 volt poser supply reading
Valve current reading
To view the diagnostics for a particular reading,
1 With the cursor on the Definition line, press [Mode/Type].
2 Scroll to the reading that you want and press [Enter].
556
7890 Series GC IPB
Service Mode Diagnostics
15
Pneumatics
This information is based on Service Mode | Diagnostics |
Electronics | Pneumatics.
PNEUMATICS
Atmospheric
pressure
24 Volt valve drive
Zero all pressure
sensors
14.715
26.71
To zero all of the pressure sensors, do the following.
1 Set all flows and pressures to zero.
2 Disconnect the supply gases.
3 Wait 30 minutes.
4 Press [Enter] and confirm.
7890 Series GC IPB
557
15 Service Mode Diagnostics
Power diagnostics
This information is based on Service Mode > Diagnostics >
Electronics > Power Info.
POWER DIAGNOSTICS
Front inlet
Front detector
Auxiliary 1
Back inlet
Back detector
Auxiliary 3
Logic current
Valve current
24 Volts
-24 Volts
Zone supply
558
166.5 watts
70.1 watts
0.9 watts
73.9 watts
63.6 watts
65.4 watts
1.370 amps
0.326 amps
26.66 volts
-27.03 volts
42.92 volts
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
16 Accessories and options
For convenience, the table below lists the accessories and
options for the 7890 Series GCs. Please refer to ELSA for the
latest and most accurate selections.
Table 37 7890 Series GC accessories and options
Accessory
Option
Description
Notes
G3451A
102
Packed inlet with EPC, septum
purge. 0100 psi operation.
Configured for 0.53-mm columns.
Incompatible with MSD software
G1701CA or later. Includes liners
and adapters/connectors for
0.53-mm, 1/8-inch, and 1/4-inch
columns.
G3452A
112
0100 psi Split/splitless with EPC.
G3460A
113
0150 psi Split/splitless with EPC.
Select for use with 0.100 id
columns. Not optimal for 0.530 id
columns.
G3454A
122
On-column capillary inlet with EPC.
0100 psi temperature-programmed,
on-column capillary inlet system
with EPC.
Order a cryo accessory kit for use
with subambient oven temperatures
or for faster cycle time to near
ambient. Order 19245-60590 for
manual injection with a fused silica
needle.
G3510A
7890A only Multimode inlet with
liquid CO2 cooling
Only one type of cryogenic source
(LN2 or LC02) is allowed per
instrument regardless of number of
cryogenic accessories.Not
compatible with PTV (or 2nd MMI
on 7890A). Incompatible with 2nd
FPD, #651, #887 or #221.
G3511A
7890A only Multimode inlet with
LN2 or air cooling.
Inlets
Agilent Technologies
559
16 Accessories and options
Table 37 7890 Series GC accessories and options
Accessory
Option
Description
Notes
G3510B
7890B only Multimode inlet with
liquid CO2 cooling
Only one type of cryogenic source
(LN2 or LC02) is allowed per
instrument regardless of number of
cryogenic accessories.Not
compatible with PTV (or 2nd MMI
on 7890A). Incompatible with 2nd
FPD, #651, #887 or #221.
G3511B
7890B only Multimode inlet with
LN2 or air cooling.
G3500A
130
Cap PTV Inlet, with EPC,
Septumless, LC02 0100 psi,
septumless head, LC02 cryo.
Temperature range 60 C to 450 C
with 3 ramps and 3 operating
modes. Split, Splitless, solvent
venting. Only one PTV inlet allowed
per GC. If using oven cooling, it
must also be LCO2 cooled. CTC and
septumless PTV requires a 23"
syringe (not included).
G3501A
131
Capillary PTV Inlet with EPC,
Septum Head, LC02 0100 psi,
w/septum head, LC02 cryo.
Temperature range 60 to 450 C
with 3 ramps and 3 operating
modes. Split, Splitless, solvent
venting.
Only one PTV inlet allowed per GC.
If using oven cooling, it must also be
LCO2 cooled.
G3502A
132
Capillary PTV Inlet with EPC,
Septumless, LN2 0100 psi,
septumless head, LN2 cryo.
Temperature range 160 C to 450 C
with 3 ramps and 3 operating
modes. Split, Splitless, solvent
venting.Only one PTV inlet allowed
per GC. If using oven cooling, it
must also be LN2 cooled. CTC and
septumless PTV requires a 23"
syringe (not included).
G3503A
133
Capillary PTV Inlet with EPC,
Septum head, LN2 0100 psi,
septum head, LN2 cryo.
Temperature range 160 C to 450 C
with 3 ramps and 3 operating
modes. Split, Splitless, solvent
venting.Only one PTV inlet allowed
per GC. If using oven cooling, it
must also be LN2 cooled.
G3504A
142
Volatiles interface with EPC. 0100
psi. Split, splitless, or direct
injection. Deactivated.
Calibrated for use with H2 or He
carrier gas only.
Solvent Vapor Exit Accessory for
use on Cool on column inlet
Includes retention gap, pre-column,
analytical column, valve and 50 uL
autosampler syringe.
G2399A
560
7890 Series GC IPB
Accessories and options
16
Table 37 7890 Series GC accessories and options
Accessory
Option
Description
Notes
G3461A
210
FID with EPC. Flame ionization
detector with EPC for packed and
capillary columns.
Includes adapters and connectors
for capillary, 1/8-inch and 1/4-inch
columns.
G3462A
211
FID with EPC, optimized for capillary
columns only.
Includes digital control of all
detector gases. Includes connectors
for capillary columns.
G3432A
220
TCD with EPC. Thermal conductivity
detector with EPC.
Includes adapters/connectors for
capillary, 1/8-inch and 1/4-inch
columns.
G3437A
221
TCD with EPC mounted on left side
of GC.
Includes adapters/connectors for
capillary, 1/8-inch and 1/4-inch
columns.Incompatible with MSD or
CTC
G3437B
221
7890B Only. Side-mounted TCD with Includes adapters/connectors for
EPC mounted on left side of GC.
capillary, 1/8-inch and 1/4-inch
columns. Incompatible with MSD.
G2397AD
231
Micro Electron Capture Detector
with EPC
Includes adapters/connectors for
1/4-in. and capillary columns.
Micro Electron Capture Detector
with EPC for Japan.
Includes adapters/connectors for
1/4-in. and capillary columns.
Detectors
G2398AD
G3435A
240
Single flame photometric detector
(FPD) with EPC.
For use with packed and capillary
columns (1/4-in. glass columns
require adapter p/n G1532-20710,
not included). Requires two heated
zones.
G3435B
240
FPD Plus with EPC. Single flame
photometric detector with EPC.
7890A+ and 7890B only. For use
with packed and capillary columns
(1/4-in. glass columns require
adapter p/n G1532-20710, not
included). Requires:
Two heated zones.
G3444A PCB enhancement kit.
A.01.05 OLCDS, B.07.00
MassHunter or higher.
7890 Series GC IPB
561
16 Accessories and options
Table 37 7890 Series GC accessories and options
Accessory
Option
Description
Notes
G3436A
241
Dual flame photometric detector
(FPD) with EPC with make-up gas.
For use with packed and capillary
columns. For use with packed and
capillary columns (1/4" glass
columns require adapter p/n
G1532-20710, not included). Not
Compatible with any heated valve
options. Requires two heated zones
and two detector circuit board slots.
Not compatible with rear ALS.
G3436B
241
Dual flame photometric detector
(FPD) with EPC with make-up gas.
7890A+ and 7890B only. Not
compatible with any heated valve
box options. For use with packed
and capillary columns (1/4-in. glass
columns require adapter p/n
G1532-20710, not included).
Requires:
Two heated zones. and two
detector board slots.
G3444A PCB enhancement kit.
A.01.05 OLCDS, B.07.00
MassHunter or higher.
G3495A
250
NPD (white ceramic bead) for
packed and capillary columns.
G3496A
251
NPD (white ceramic bead) optimized Includes connectors for capillary
for capillary columns only.
columns.
G3463A
252
NPD (Blos bead) for packed and
capillary columns.
For use with packed and capillary
columns. Includes adapters and
connectors for capillary and
1/4-inch columns.
G3464A
253
NPD (Blos bead) optimized for
capillary columns only (not for use
with packed columns).
Includes connectors for capillary
columns.
G3490A
201
MSD interface.
For use with Agilent 5975 Series
MSD or Agilent 7000A Triple Quad
GC/MS or 7200 Q-TOF GC/MS).
Uses one heated zone.
G3456A
206
Analog input board. Single-channel
analog input board to accommodate
an external detector.
Mounts in detector board position.
Cable included.
19232C
925
TCD to FID Series Adapter
Requires FID for packed columns
(#210 or G3461A).
562
For use with packed and capillary
columns. Includes adapters and
connectors for capillary and
1/4-inch columns.
7890 Series GC IPB
Accessories and options
16
Table 37 7890 Series GC accessories and options
Accessory
Option
Description
Notes
G3470A
301
Aux EPC.
Provides three channels of auxiliary
0100 psi electronic pneumatics
control.
G3471A
309
Pneumatics Control Module.
Provides two channels of EPC. One
channel is either flow or pressure,
the second is pressure only.
Occupies one of two aux slots
and/or one of two inlet slots.
Maximum of three.
G3469A
205
EPC headspace interface.
Required for the EPC-ready Agilent
7694 headspace sampler (G1289B).
Optional for the G1290B and
G1888A headspace sampler.
G2855B
888
Capillary Flow Technologies Dean
Switch Requires two detectors, two
columns and either PCM (preferred)
or aux EPC.
Enables "heartcutting". Switch
includes high temperature ferrules
and calculation SW CD.
G3180B
889
Capillary Flow Technologies Splitter
with Makeup Gas
Requires either aux epc or PCM.
Typical application is to split column
effluent to two detectors. Includes
hw and Calculator SW. Requires MS
Excel.
G3183B
890
Capillary Flow Technologies 3 way
splitter with Makeup Gas.
Typical application is to split column
effluent to three detectors. Includes
hw and Calculator SW.Requires
either aux epc or PCM. Requires MS
Excel.
G3181B
Capillary Flow Technologies Splitter,
unpurged
Enables leak free splitting of column
effluent to two detectors. Does not
include installation.
G3184B
CFT Unpurged Tee for MSD Transfer
Line.
Pneumatics
CFTs
G3486A
G3487A
7890 Series GC IPB
887
CFT Flow Modulator Accessory
requires 7890A GC w/SSL inlet, FID
, PCM, ALS injector, G2070BA SW
(Ver B.03.02).
2D Data analysis SW is neither
provided nor supported by Agilent.
Also requires G3487A Checkout Kit.
CFT Flow Modulator Checkout Kit,
Includes various parts for checkout.
Required use with 7890A CFT Flow
Modulator ( G3440A#887 or
G3486A).
563
16 Accessories and options
Table 37 7890 Series GC accessories and options
Accessory
Option
Description
Notes
G1472A
Purged Ultimate Union kit for
GC/MS system with mounting and
instructions. Installation and
Familiarization are included.
Optional installation service is not
required.
G3182-61580
CPM Union kit
High temperature, inert, leak free
column connector with oven
mounting bracket
G1580-61060
CPM-1/16" Tube Assembly Kit
This kit provides leak-free, inert
connection from GC valve to CPM
system
Cryo
G3465A
311
Cryogenic oven and inlet cooling w/
C02
Provides cooling for oven and up to
two cool-on-column inlets if
installed. Not compatible with GC
QQQ (7000 MS).
G3467A
311
Cryogenic oven cooling w/C02
Provides cooling for oven only. If
PTV inlet is present, it must also be
LCO2 cooled. Not compatible with
GC QQQ (7000 MS).
G3468A
312
Cryogenic oven and inlet cooling w/
LN2
Provides cooling for oven and up to
two cool-on-column inlets if
installed. Not compatible with GC
QQQ (7000 MS).
G3466A
312
Cryogenic oven cooling w/ LN2
Provides cooling for oven only. If
PTV inlet is present, it must also be
LN2 cooled. Not compatible with GC
QQQ (7000 MS).
G3478A
307
Adds a nickel catalyst (methanizer)
Requires availability of rear injection
port position. If two injection ports
are required, contact your sales
assist engineer for alternatives.
Compatible with PCM in rear
position. Not compatible with
capillary-only FID.
G1530-80650
306
Exhaust deflector
Miscellaneous
G3485A
564
Manual Pneumatics Carrier
7890A and 7890A+Only Fits on left
side of 7890A for housing unheated
valves. Incompatible with MSD.
7890 Series GC IPB
Accessories and options
16
Table 37 7890 Series GC accessories and options
Accessory
Option
Description
Notes
G3485B
Manual Pneumatics Carrier
7890B Only Fits on left side of
7890A for housing unheated valves.
Incompatible with MSD.
G2887BA
Simulated Distillation software for
ChemStation (included with #651).
Requires ChemStation. See G3506A
below.
7890B Only
G6586AA
Agilent LTM Control Software.
Provides software control for up to
four LTM modules on one Agilent
7890/6890 GC.
7890B Only
G2646-60500
Oven Insert Accessory for fast oven
temperature ramping. Cuts the oven
volume in half.
Only compatible when using rear
inlet/detector. If using MSD, inlet
and MSD must be in rear position.
G3444A
7890A Logic Board Enhancements
Kits.
7890A Only Makes 7890A ready for
FPD+, Integrated Intelligence
features, serial port enhancements.
Requries software upgrades for
A.01.05 OLCDS and MassHunter
B.07.00 or higher.
G3494A
Bar Code Reader with USB
Connection for 7890B
7890A requires:
G3444A enhancement kit
A.01.05 OpenLAB or later, or
B07.00 MassHunter or later
G3494B
Bar Code Reader with Serial
Connection for 7890B
7890A requires:
G3444A enhancement kit
Valves
G1580A
751
Heated, automated valve box for one
valve
G1581A
752
Heated, automated valve box for
two valves
G3480-67585
860
Kit to interface an upstream gas or
liquid sampling valve to a capillary
or Multi-Mode inlet for sample
splitting and introduction into a
capillary or megabore column.
G2739A
Liquid sampling valve plumbing kit
G2740A
Gas valve plumbing kit
G2741A
Adds an adjustable restrictor to
control gas flows.
7890 Series GC IPB
Max temp of 225 C.
565
16 Accessories and options
Table 37 7890 Series GC accessories and options
Accessory
Option
Description
G2742A
874
Kit to interface a capillary inlet or
multimode inlet to a valve located
downstream
G2743A
7890A actuator kit. Adds automation
to a 7890 valve. It consists of an
actuator and solenoid valve.
G2743B
7890 Actuator Kit. Adds automation
to 7890 valve system for 7890 with
S/N = CN10201096 or later, or for
7890 S/N = US10281001 or later.
G2744A
Adds a heated zone to a 7890 valve
box
Notes
G2748A
861
Hardware kit to mount an unheated
gas sampling or liquid sampling
valve on the left side of the oven.
Incompatible with MSD. Requires
side carrier.
G3478A
307
Adds a nickel catalyst (methanizer)
to a 7890 Gas Chromatograph
Requires availability of rear injection
port position. If two injection ports
are required, contact your sales
assist engineer for alternatives.
Compatible with PCM in rear
position.
High Pressure Injection Device
Accessory. Requires SSL inlet and
one flow source from Aux EPC or
PCM module. User must provide
appropriate hardware to interface
sample to HPID.
Only one can be installed, front
position only.
G3505A
G4338A
872
0.53 mm Column to Valve Interface
Requires mounting plate
05890-80660. Each plate can hold 5
interface adaptors.
G4339A
873
0.32 mm Column to Valve Interface
Requires mounting plate
05890-80660. Each plate can hold 5
interface adaptors.
566
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
17 Printed circuit boards
Summary of PCB Part Numbers 568
AC power board 569
Analog and power board 570
Logic and communications board (7890A) 572
Logic and communications board (7890B) 573
FID signal board 574
TCD signal board 575
uECD signal board 576
FPD signal board 577
NPD signal board 578
FID electrometer board 579
uECD electrometer board 580
NPD electrometer board 581
Analog input board 582
This section describes the following circuit boards and their
connections.
Some connectors are marked MTC, which stands for
Manufacturing Test Connector. There may or may not be a
connector loaded on the board. MTCs are used at the factory to
connect to test equipment so that the board can be exercised
without the need for a GC. These connectors are not used when
the board is installed in an instrument.
Agilent Technologies
567
17 Printed circuit boards
Summary of PCB Part Numbers
568
Description
Part number
AC power board
G3430-60050
Analog and power board
G3430-60151 (replaces G3430-60150)
Logic and communications board
G3430-60120 (replaces G3430-60101
and G3430-60100)
Keyboard/display connection board
G3430-60003
FID signal board
G3431-60020
TCD signal board
G3432-60010
uECD signal board
G3433-61020 (replaces G3433-60020)
FPD signal board
G3435-60010
NPD signal board
G3434-60021 (replaces G3434-60020)
FID electrometer board
G3431-60010
uECD electrometer board
G3433-60010
NPD electrometer board
G3434-60010
Analog input board
G3456-60010 (obsolete) shown,
G3433-61020 has similar connectors)
7890 Series GC IPB
Printed circuit boards
17
AC power board
Part number G3430-60050
7890 Series GC IPB
Connector
Function
See also
J1
Supplies power to transformer
primary windings.
Main transformer
P1 and P2
Supply line power to the AC board.
AC power board
schematic
P3 and P4
Supply power to the oven heater.
P5, P6 and P7
These three connectors take
jumpers to the oven triac. Each
jumper connects to the nearest
connector on the triac, which must
be properly oriented.
Replacing the oven
triac
P8
This takes the power configuration
plug, which must have the correct
jumpers for the voltage supplied.
Line voltage
configuration plug
P9
Oven control from logic board.
P10
MTC
569
17 Printed circuit boards
Analog and power board
Part number G3430-60150 (shown). Connectors for the
G3430-60151 are in the same location.
570
7890 Series GC IPB
Printed circuit boards
7890 Series GC IPB
17
Connector
Function
See also
J1
SIG 1. Analog output for signal 1.
Analog signal outputs
J2
SIG 2. Analog output for signal 2.
Analog signal outputs
J3
REMOTE. Synchronize start/stop
functions for up to 10 devices.
Remote Start/Stop
J4
EVENT. Control external devices,
either active (24 VDC) or passive
)contact closures).
External event
J5
96-pin data connection to analog
and power board.
J6
BCD. Accept BCD-coded input from
selection valves and other devices.
J7
Receive power from transformer
secondary.
Main transformer
J8
Ribbon cable to automatic liquid
sampler board.
RS-232 cable, ALS
controller
P1
Supply power to the Communication
harness.
Communication
harness
P2
Supply power to the oven fan.
P18
Connects to the Motor Harness and
AC Control cable.
Motor Harness & AC
Control Assembly
P21
Connects to Inlet/Detector harness.
Inlet/Detector harness
P22
Connects to the Auxiliary
Zone/Valve Box Harness.
Auxiliary zone/Valve box
harness
571
17 Printed circuit boards
Logic and communications board (7890A)
Part number G3430-60100 shown. Connectors for the
G3430-60120 and G3430-60101 boards are in the same
locations.
572
Connector
Function
See also
J1
External LAN port.
J3
MTC
P1
96-pin buss to analog and power
board.
P3+
MTC
P5
MTC
P7
Connects to Comm Buss on
Communications Harness.
Communication
harness
P8
44-pin ribbon cable to keyboard
and display.
Keyboard/Display
harness,Keyboard
interconnect board
7890 Series GC IPB
Printed circuit boards
17
Logic and communications board (7890B)
Part number G3430-61010 shown.
NEED GRAPHIC FOR 7890B
Connector
Function
J1
External LAN port.
J3
MTC
P1
96-pin buss to analog and power board.
P2
96-pin buss to analog and power board.
P3+
MTC
P4
96-pin buss to analog and power board.
See also
P6
7890 Series GC IPB
P7
Connects to Comm Buss on
Communications Harness.
Communication
harness
P8
44-pin ribbon cable to keyboard and
display.
Keyboard/Display
harness,Keyboard
interconnect board
573
17 Printed circuit boards
FID signal board
Part number G3431-60020
574
Connector
Function
J1
MTC
P1
Communications buss.
P2
Ignitor.
P3
MTC
P4
Signal from electrometer.
P5
MTC
See also
Communication
harness
7890 Series GC IPB
Printed circuit boards
17
TCD signal board
Part number G3432-60015
7890 Series GC IPB
Connector
Function
J2
Filament (upper 2) and PRT (lower 2)
connections.
P1
Communications buss.
P2
MTC
P3
Switching valve.
See also
Communication
harness
Replacing the
TCD switching
valve
575
17 Printed circuit boards
uECD signal board
Part number G3433-60020 shown below. (Replaced by
G3433-61020.)
576
Connector
Function
See also
P1
Communications buss.
Communication
harness
P2
Signal from electrometer.
P3
MTC
7890 Series GC IPB
Printed circuit boards
17
FPD signal board
Part number G3435-60010
7890 Series GC IPB
Connector
Function
See also
P1
Communications buss.
Communication
harness
P2
MTC
P3
High voltage to photomultiplier.
P4
Signal from electrometer.
P5
Ignitor.
P^
MTC
P7
MTC
577
17 Printed circuit boards
NPD signal board
Part number G3434-60021 (replaces G3434-60020)
578
Connector
Function
See also
P1
Communications buss.
Communication
harness
P2
Bead power.
NPD power cable
P3
MTC
P4
Signal from electrometer.
7890 Series GC IPB
Printed circuit boards
17
FID electrometer board
Part number G3431-60010
7890 Series GC IPB
Connector
Function
J1
Input from detector.
P1
Output to signal board.
579
17 Printed circuit boards
uECD electrometer board
Part number G3433-60010
580
Connector
Function
J1
Output to signal board.
J2
Input from detector.
7890 Series GC IPB
Printed circuit boards
17
NPD electrometer board
Part number G3434-60010
7890 Series GC IPB
Connector
Function
J1
Input from detector.
P1
Output to signal board.
581
17 Printed circuit boards
Analog input board
Part number G3456-60010
582
Connector
Function
See also
J1
External input cable.
Analog signal
outputs
P1
Communications buss.
Communication
harness
P3
MTC
P5
MTC
7890 Series GC IPB
Agilent 7890 Series Gas Chromatograph
7890 Series GC Service Manual
18 Illustrated Parts Breakdown
Inlets 584
Detectors 627
EPC Module Parts 669
Nickel Catalyst Accessory 674
Oven 676
Valves 685
Electronics and Fans 700
Covers 720
Tools 729
This section consists of parts lists and exploded views of the
instrument modules. It is a major reference for part
identification and part numbers.
For consumables and other customer-orderable parts, see the
latest Agilent Parts Finder software version and IPB models for
the 7890 Series GC.
In any table listing parts, a part with ID NS means the part is
not shown in the accompanying graphics.
Quantities listed are the quantities required in the assembly, not
necessarily the quantity to order (the quantity to order is not
the same as the quantity used when the parts are sold in
packages of more than one).
Agilent Technologies
583
18 Illustrated Parts Breakdown
Inlets
This section contains illustrated parts breakdowns for GC inlets
and related components.
Split/Splitless Inlet (SSL)
Multimode Inlet (MMI)
Purged Packed Inlet (PP)
Cool on-column inlet (COC)
Programmed Temperature Vaporization Inlet (PTV)
Volatiles Interface (VI)
584
7890 Series GC IPB
Illustrated Parts Breakdown
18
Split/Splitless Inlet (SSL)
Top level subassemblies for SSL inlet accessories:
G3452A 100 psi split/splitless with EPC, Kit
G3460A 150 psi split/splitless inlet with EPC, Kit
G3453B Inert flow path, 0100 psi
Description
Part number
SSL Inlet Accessory 0-100 PSIG without ship kit (includes
inlet weldment, EPC module, and split vent filter assy)
G3452-60500
SSL Inlet Accessory 0-150 PSIG without ship kit (includes
inlet weldment, EPC module, and split vent filter assy)
G3452-60509
SSL Weldment Assembly without EPC module (includes
inlet weldment and split vent filter assembly)
G3452-60512
SSL inlet body with heater/sensor and insulation
(includes inlet weldment only)
G3452-67000
SSL EPC module, 100 PSI
G3452-60552
SSL EPC module, 150 PSI
G3452-60510
EPC module
G3452-60512
G3452-67000
G3452-60500
SVLJ
RU
G3452-60509
SVLJ
6SOLWYHQWOWHUDVVHPEO\
7890 Series GC IPB
6SOLWVSOLWOHVVLQOHW
ZHOGPHQWDVVHPEO\
585
18 Illustrated Parts Breakdown
Split/Splitless Inlet, Top
Item
Description
Part number
Qty
Cap, Merlin Microseal, low pressure
Cap, Merlin Microseal, general purpose
Merlin Microseal
Top insert assembly, standard
Insert weldment, inert, 7890
Top SSL insert weldment assembly,
headspace
Top insert, AC gang fitting weldment
Top insert assembly, valve
Septum nut, standard
Septum, standard
See Parts Finder
See Parts Finder
See Parts Finder
G3452-60730
G3452-60586
G3452-60100
1
1
2
3
NS
NS
NS
NS
4
5
6
586
O-ring, 12/pk
(2 required for EPC module seal, 2
required for valve seal)
G3430-60011
G3480-67585
18740-60835
See Parts Finder
5180-4181
1
1
4
Screw, captive, M3
G1946-20168
Item
Description
Part number
Qty
Tubing assembly
G3430-60011
Split ring
0510-1306
Turn-top
G3430-40035
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
587
18 Illustrated Parts Breakdown
SSL Split Vent Trap
Item
Description
Part number
Qty
Vent line tube assembly
G3430-60526
Screw, captive, M4 x 20 mm, T-20
1390-1024
Trap shell, back assembly (does not
include item 9 or 10)
G3452-60506
Trap nut
G1544-20650
NS
Split vent trap
See Parts Finder
Threaded trap shell, front
G1544-20675
Proportional valve, split vent
G3430-60527
Screw, M3 x 16 mm T-10 to attach valve
0515-1141
NS
O-ring, 12/pk
(2 required for EPC module seal, 2
required for valve seal)
5180-4181
1/8-inch copper tubing with length, 50 ft.
Trim to 325 mm or 12.8 in.
5180-4196
Screw, M4 12 mm, T-20
0515-2496
10
Trap retainer (key)
G3452-00005
2
3
9
10
6
7
8
588
7890 Series GC IPB
Illustrated Parts Breakdown
18
Split Splitless Inlet Body
7890 Series GC IPB
Item
Description
Part number
Qty
Screw, M4 x 12 mm, Torx T-20 (captive)
C-clip
1390-1023
0510-1799
3
3
Inlet weldment
G3452-80570
Cap Inlet Shell Weldment Assembly, Inert
G3452-60570
Top insulation
G1544-00010
Heater/Sensor assembly
G1530-67950
Screw, M4 x 10 mm
0515-4788
Washer, 12/pk
5061-5869
Heater block
G3452-20500
Insulation block
G3452-00002
Insulation bottom
G3432-00003
10
SSL insulation cover
G3431-00005
11
Retaining nut for heater block
G1544-20590
12
Gold seal kit, includes washer
5188-5367
Gold seal, Ultra Inert, with washer
5190-6144
Gold plated seal with cross, split only
5182-9652
13
Reducing nut
18740-20800
14
Ferrule
See Parts Finder
15
Column nut
See Parts Finder
589
18 Illustrated Parts Breakdown
2
3
4
5
6
10
11
12
13
14
15
590
7890 Series GC IPB
Illustrated Parts Breakdown
18
Split Splitless Inlet Warmer
7890 Series GC IPB
Item
Description
Part number
Qty
SSL insulation kit, 3 pieces
5188-5241
Bottom insulation cover
19243-00070
Screw, M4 x 12 mm, Torx T-20,
chrome-plated
0515-2711
591
18 Illustrated Parts Breakdown
Multimode Inlet (MMI)
Top level subassemblies for the 7890B:
G3510B Multimode inlet, liquid carbon dioxide (CO2), kit
G3511B Multimode inlet, liquid nitrogen (N2), kit
Top level subassemblies for the 7890A:
G3510A Multimode inlet, liquid carbon dioxide (CO2), kit
G3511A Multimode inlet, liquid nitrogen (N2), kit
See the figures below.
Item
Description
Part number
7890A and 7890B
1
Inlet chassis
G3430-40011
MMI EPC module
G3510-60500
7890A Only
3
Multimode inlet, liquid carbon dioxide (CO2), kit
G3510-64000
Multimode inlet, liquid nitrogen (N2), kit
G3511-64000
7890B only
592
MMI LCO2 Module 7890B (includes EPC module,
inlet body, cables, cryo components, and
thermocouple PCA)
G3510-65200
MMI LN2 Module 7890B (includes EPC module,
inlet body, cables, cryo components, and
thermocouple PCA)
G3510-65300
7890 Series GC IPB
Illustrated Parts Breakdown
18
EPC module
2
Inlet body
Split vent valve
2
Inlet body
EPC module
Cryo valve, bracket, and insulation
7890 Series GC IPB
Split vent valve
Thermocouple
board and cryo
valve cable
593
18 Illustrated Parts Breakdown
EPC module
Cryo valve, bracket, and dual CO2
supply weldment
5
Inlet body
Split vent valve
Thermocouple board and
cryo valve cable
Split vent valve
Inlet body
EPC module
6
Cryo valve, bracket, and insulation
Thermocouple board and
cryo valve cable
594
7890 Series GC IPB
Illustrated Parts Breakdown
18
Multimode Inlet Body
Item
Description
Part number
Qty
NS
MMI EPC manifold
G3510-60500
MMI Full Weldment* (includes cryo
jacket)
G3510-64100
MMI cryo jackets
MMI LN2 jacket, 7890A only
G3510-81310
MMI LN2 jacket, 7890B only
G3510-81011
MMI CO2 jacket, 7890A and 7890B
G3510-81210
Column nut adapter
G3510-20018
Foil (LN2 only)
MMI Insulation (LN2 or LCO2)
19243-00069
MMI Metal Insulation Cup (LN2)
G3510-00001
MMI Metal Insulation Cup (LCO2)
G3510-00002
Tube, precise, 0.010-in. id x 1/16-in. od x
15 cm long
G2855-20700
NS
MMI CO2 kit, 7890A only
G3510-67520
NS
MMI LN2 kit, 7890A only
G3510-67530
NS
Brazed shell
G3510-81000
* UltraClean part
See the Agilent Parts Finder software and the Agilent chemical
analysis consumables and accessories catalog for Merlin
assemblies.
7890 Series GC IPB
595
18 Illustrated Parts Breakdown
596
7890 Series GC IPB
Illustrated Parts Breakdown
18
MMI Top Insert Assembly
Item
Description
Part number
Qty
Cap, Merlin Microseal, low pressure
Cap, Merlin Microseal, general purpose
Merlin Microseal
Top insert assembly, standard
Top SSL insert weldment assembly,
headspace
Top insert, AC gang fitting weldment
Top insert assembly, valve
Septum nut, standard
Septum, standard
See Parts Finder
See Parts Finder
See Parts Finder
G3452-60730
G3452-60100
1
1
2
3
NS
NS
NS
4
5
6
G3430-60011
G3480-67585
18740-60835
See Parts Finder
5180-4181
1
1
4
Screw, captive, M3
G1946-20168
Item
Description
Part number
Qty
Tubing assembly (top insert AC gang
fitting weldment)
Retainer ring
Turn-top (helix plate with molded handle)
G3430-60011
0510-1306
G3430-40035
1
1
2
3
7890 Series GC IPB
O-ring, 12/pk
(2 required for EPC module seal, 2
required for valve seal)
597
18 Illustrated Parts Breakdown
598
7890 Series GC IPB
Illustrated Parts Breakdown
18
MMI Split Vent Trap
Item
Description
Part number
Qty
Vent line tube assembly
G3430-60526
Screw, captive, M4 x 20 mm, T-20
1390-1024
Trap shell, back assembly (does not
include item 9 or 10)
G3452-60506
Trap nut
G1544-20650
NS
Split vent trap
See Parts Finder
Threaded trap shell, front
G1544-20675
Proportional valve, split vent
G3430-60527
Screw, M3 x 16 mm T-10 to attach valve
0515-1141
NS
O-ring, 12/pk
(2 required for EPC module seal, 2
required for valve seal)
5180-4181
1/8-inch copper tubing with length, 50 ft.
Trim to 325 mm or 12.8 in.
5180-4196
Screw, M4 12 mm, T-20
0515-2496
10
Trap retainer (key)
G3452-00005
2
3
9
10
6
7
8
7890 Series GC IPB
599
18 Illustrated Parts Breakdown
7890A MMI Temperature controller
Item
Description
Part number
Qty
Wiring harness cable
G3510-60110
Thermocouple board
G3430-60095
Screw, M4 x 6 mm, T-20 (attach board to
bracket)
0515-2832
Screw, M4 x 12 mm, T-20 (attach bracket
to carrier)
0515-2496
Bracket, PTV thermocouple board and
LCO2 valve (single CO2 bracket)
G3430-00058
Kit, containing thermocouple board and
wiring harness cable
G3510-67000
Figure 15 7890A Thermocouple board, bracket, and cables
600
7890 Series GC IPB
Illustrated Parts Breakdown
18
7890B MMI Temperature controller
Item
Description
Part number
Qty
Thermocouple board
G3430-60095
Bracket, cryo
Figure 16
Bracket, PTV thermocouple board, LCO2
cryo
G3430-00092
Bracket, PTV thermocouple board, LN2
cryo (Single CO2 bracket)
G3430-00058
Screw, M4 x 12 mm, T-20 (attach board to
bracket)
0515-2496
Screw, M4 x 12 mm, T-20 (attach bracket
to GC carrier)
1390-1023
Wiring harness cable
G3510-60110
Kit, containing thermocouple board and
wiring harness cable
G3510-67000
7890B Thermocouple board, bracket, and cable
7890 Series GC IPB
601
18 Illustrated Parts Breakdown
7890A MMI Cryo assemblies
602
Item
Description
Part number
Qty
NS
7890 MMI LCO2 kit (includes CO2 cryo
valve assembly, cryo bracket, insulation
cup)
G3510-67520
NS
7890 MMI LN2 kit (includes insulation
cover, cryo bracket, insulation cup, and
LN2 cryo valve assemblies)
G3510-67530
CO2 brazement (valve to IP tube)
G2617-80510
NS
Cap, protective without flange
1401-0044
NS
1/8-inch male connector without O-ring
G1543-80025
NS
Gland seal CO2
G1565-20590
NS
PTFE seal
G1565-20840
LN2 Noise reduction Restrictor
G3510-27000
7890 Series GC IPB
Illustrated Parts Breakdown
18
7890B MMI Cryo assemblies
Item
7890 Series GC IPB
Description
Part number
MMI LCO2 Module (includes MMI Full
Weldment - CO2, EPC module, grommet,
TC board, and cable)
G3510-65200
MMI Full Weldment - CO2 (includes CO2
cryo assembly, MMI body and split vent
valve, insulation and insulation cup)
G3510-60520
MMI LN2 Module 7890B (includes EPC
module, grommet, cryo valve bracket, TC
board, cable, and MMI Full Weldment LN2
assembly)
G3510-67300
MMI Full Weldment LN2 7890B (includes
LN2 cryo assembly, MMI body and split
vent valve, insulation and insulation cup)
G3510-60535
Qty
603
18 Illustrated Parts Breakdown
Purged Packed Inlet (PP)
Top level subassemblies for Purged Packed inlet accessories:
G3451A Purged-packed with EPC, Kit
604
Description
Part number
Purged-packed Inlet Accessory without ship kit
G3451-65520
Purged packed inlet weldment assembly without EPC
module
G3451-80506
Purged packed inlet EPC module
G3451-60551
7890 Series GC IPB
Illustrated Parts Breakdown
18
Purged Packed Inlet Upper Body
7890 Series GC IPB
Item
Description
Part number
Qty
Screw, Torx T-20, M4 x 12 mm
1390-1023
Top cover plate
G1543-00085
Top insulation
G1543-00100
Nut, Merlin Microseal
See Parts Finder
Septum, Merlin Microseal
See Parts Finder
Top insert weldment
19243-80570
Viton O-ring (12/pk)
5080-8898
Screw, Torx T-10, M3 x 16 mm
G1946-20168
Inlet weldment
G3451-80501
10
Thermal block
G1543-20765
11
Bottom nut
G1543-20580
12
Septum nut
18740-60835
13
Septum, 11 mm, low bleed (50/pk)
See Parts Finder
14
Heater/Sensor assembly
G1543-61540
NS
Top gasket insulation
G1543-00155
605
18 Illustrated Parts Breakdown
606
7890 Series GC IPB
Illustrated Parts Breakdown
18
Purged Packed Inlet Lower Parts
7890 Series GC IPB
Item
Description
Part number
Qty
15
PP insulation
G3432-00004
16
PP bottom insulation
G3432-00003
17
PP insulation cup
G3431-00005
18
C-clip
0510-1799
19
Glass liner (25/pk)
See Parts Finder
20
Vespel ferrule (10/pk)
5080-8774
21
Tubing nut (1/4-inch brass), 10/pk
5180-4105
22
Column adapter
See Parts Finder
23
Bottom plate for oven
G1543-00060
24
Screw, T-20, M4 x 12mm
0515-2711
25
Adapter insulation, 1/pk
19234-60715
26
Insulating cup
19234-60700
27
Ferrules
See Parts Finder
28
Column nut (capillary, universal, 2/pk)
See Parts Finder
607
18 Illustrated Parts Breakdown
608
7890 Series GC IPB
Illustrated Parts Breakdown
18
Cool on-column inlet (COC)
Top level subassemblies for Cool on-column inlet accessories:
G3454A Cool on-column inlet with EPC, Kit
For cryoblast parts for G3467A and G3468A see CO2
cryogenic cooling on page 682 or Liquid nitrogen (LN2)
cryogenic cooling on page 684.
19245-60590 for manual injection with a fused silica needle
7890 Series GC IPB
Description
Part number
Cool On-column Inlet Accessory without ship kit
G3454-60501
Cool On-column Inlet weldment assembly without EPC
module
G3454-60502
Cool On-column Inlet EPC module
G3454-60554
609
18 Illustrated Parts Breakdown
Cool on-column inlet body
610
Item
Description
Part number
Qty
Septum nut base assembly, for
.250/.320-mm columns
19245-80521
Septum nut base, for .530 mm columns
G1545-80520
Manual cooling tower assembly
(optional), for .200 mm columns
19320-80625
Duckbill for use with cooling tower, 10/pk 19245-40050
Screw, M4 12 mm long
0515-2711
Heatsink fin
G1545-00010
Heater/Sensor assembly
G1545-60520
Screw, M3 x 16 mm, T-10
1390-1022
10
Septa
See Parts Finder
11
Insert spring
19245-60760
12
Inserts (identify by number of rings on
insert)
See Parts Finder
13
Screw, M4 12 mm, T-20
0515-2496
14
Inlet weldment
G3454-80500
15
Inlet weldment insulation
G1545-20630
16
Cavity sleeve
19245-00060
17
Ferrules (identify by internal diameter)
See Parts Finder
18
Column nut
See Parts Finder
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
611
18 Illustrated Parts Breakdown
Programmed Temperature Vaporization Inlet (PTV)
Top level subassemblies for PTV inlet accessories:
G3500A Septumless head PTV, LCO2 Accessory with EPC,
Kit
G3501A Septum head PTV, LCO2 Accessory with EPC, Kit
G3502A Septumless head PTV, LN2 Accessory with EPC, Kit,
for 7890A only
G3502B Septumless head PTV, LN2 Accessory with EPC, Kit,
for 7890B only
G3503A Septum head PTV, LN2 Accessory with EPC, Kit, for
7890A only
G3503B Septum head PTV, LN2 Accessory with EPC, Kit, for
7890B only
Description
Part number
Septumless head PTV inlet, LCO2 accessory without ship
kit
G3500-65500
Septum head PTV inlet, LCO2 accessory without ship kit
G3501-65500
Septumless head PTV inlet, LN2 accessory without ship kit G3502-65500
Septum head PTV inlet, LN2 accessory without ship kit
G3503-60500
PTV EPC assembly, 100 PSI
G3500-60500
PTV Inlet chassis
G3430-40011
Septumless head
612
7890 Series GC IPB
Illustrated Parts Breakdown
18
Septum head
7890 Series GC IPB
613
18 Illustrated Parts Breakdown
PTV Inlet Body
Item
Description
Part number
Qty
Septumless head assembly
G2617-60507
Septumless head weldment
G3500-80000
Septum nut (see also Parts Finder.)
18740-60835
Septum head (see also Parts Finder.)
G3500-80001
PTV inlet assembly
G2617-60506
Cooling jacket
PTV, CO2 cooling jacket
G2617-60508
PTV N2 cooling jacket
G2619-60501
NS
PTV inlet assembly with cooling jacket
PTV inlet with CO2 cooling jacket
G2617-60518
PTV inlet with LN2 cooling jacket
G2617-60517
Silver seal (5/pk)
5182-9763
Graphpak inlet adapter (includes silver
seal and ferrule)
See Parts Finder
Ferrules for graphpak inlet
See Parts Finder
10
Split nut for inlet adapters
5062-3525
11
PTV liner
See Parts Finder
12
PTV insulation block
G2617-20510
NS
PTV cryo insulator
G2617-60510
NS
PTV ferrule assembly tool
G2617-80540
* See the Parts Finder and the Agilent chemical analysis consumables and
accessories catalog for Merlin assemblies and other consumables, such as the
Graphpak adapter and ferrules.
614
7890 Series GC IPB
Illustrated Parts Breakdown
18
1
2
6
7
8
9
10
11
12
7890 Series GC IPB
615
18 Illustrated Parts Breakdown
PTV Septumless head
Description
Part number
Qty
Septumless head
G2617-60507
PTFE ferrule (needle seal)
5182-9748
Service kit for SLH (Septumless head
repair kit: includes Kalrez seal, spring, and
Viton seal)
5182-9747
(3)
Kalrez seal (normally order item 2 instead) 5182-9759
(4)
Pressure spring (normally order item 2
instead)
5182-9758
(5)
Viton seal (normally order item 2 instead)
5182-9775
Valve body
5182-9757
Sealing element
5182-9760
Ferrule, 1/16-inch PTFE, for septumless
head carrier gas tube
0100-1375
PTV column adapter tube (includes
1/6-inch nut)
G2617-80550
10
PTV septumless head weldment (includes
jumper tube to septum purge channel)
G3500-80000
1
8
9
2
10
(3)
6
7
(4)
(5)
616
7890 Series GC IPB
Illustrated Parts Breakdown
18
PTV Split vent
7890 Series GC IPB
Description
Part number
Qty
NS
Replacement filter kit
G1544-80530
Proportional valve, split vent
G3430-60527
Screw, M3 x 16 mm, T-10
0515-1141
NS
O-ring, 12/pk (2 for EPC module seal, 2 for
valve seal)
5180-4181
Flow block, split vent trap
G3452-60506
Trap nut
G1544-20650
PTV front trap tubing assembly
G2617-80520
Screw, M4 x 12 mm, T-20
0515-2496
Nut, 1/16-inch SS
0100-0053
Ferrule, 1/16-inch SS
0100-1490
NS
Split vent trap
See Parts Finder
NS
Screw, M4 12 mm, T-20 (for trap
retainer)
0515-2496
NS
Trap retainer
G3452-00005
617
18 Illustrated Parts Breakdown
PTV Temperature controller
Item
Description
Part number
Qty
Cable, thermocouple
G2617-60505
Thermocouple interface board
G2617-60010
Screw, M4 x 12 mm long, T-20 (attach
board to bracket)*
0515-2496
Screw, M4 x 12 mm long, T-20 (attach
bracket to carrier)
0515-2496
Bracket, PTV thermocouple board and
LCO2 valve
G3430-00058
*. Some 7890A assemblies use Screw, M4 x 6 mm long, T-20 (attach board to bracket), p/n
0515-2832.
618
7890 Series GC IPB
Illustrated Parts Breakdown
18
PTV CO2 cryo assembly
Item
Description
Part number
Qty
7890 PTV LCO2 Cyro Assembly
(recommended repair level)
G3500-60515
Screw, #8-32 x .375 inch long (to attach
valve to bracket)
2510-0102
Bracket, PTV thermocouple board and
LCO2 valve
G3430-00058
Valve, PTV LCO2 cryo (included in
G3500-60515)
Cap, protective without flange
1401-0044
PTV CO2 brazement (valve to IP tube)
G2617-80510
NS
1/8-inch male connector without O-ring
G1543-80025
NS
Gland seal CO2
G1565-20590
NS
PTFE seal
G1565-20840
4
1
2
3
7890 Series GC IPB
619
18 Illustrated Parts Breakdown
PTV LN2 cryo assembly, 7890A
Item
Description
Part number
Qty
PTV LN2 nut plate
G2619-00040
PTV LN2 supply tube (included in 8)
G2619-20520
Screw, M4 x 12 mm, T-20 (attach nut plate)
0515-2496
PTV LN2 insulation cover
G2619-00030
Screw, M4 x 12 mm, T-20 (attach cover)
1390-1024
PTV LN2 cell inlet tube, for front inlet
PTV LN2 cell inlet tube, for back inlet
G2619-20510
G3500-20006
Screw, 8-32 x .312-inch, pan head, pozi (included
in 8)
2510-0043
7890 PTV LN2 Cryo Assembly (recommended
valve repair level). Includes cryo valve, mounting
bracket, PTV jumper cable, LN2 supply tube, and
mounting screws.
G3502-60510
PTV inlet tube insulation (included in 8)
G2619-00010
10
Mounting bracket, LN2 cryo valve (included in 8)
G3502-00001
11
Screw, M4 x 12 mm long, T-20
0515-2496
NS
PTV jumper cable (included in 8)
G2619-60502
NS
Connector, male (included in 8)
0100-0208
6
7
8
1
9
10
2
3
4
11
620
7890 Series GC IPB
Illustrated Parts Breakdown
18
PTV LN2 cryo assembly, 7890B
7890 Series GC IPB
Item
Description
Part number
Qty
PTV LN2 supply tube assembly, back
G3510-60008
PTV supply tube insulation
G3510-00021
PTV LN2 cell inlet tube, for front inlet
PTV LN2 cell inlet tube, for back inlet
G3502-20001
G3502-20002
Screw, 8-32 x .312-inch pan head, pozi (included
in 5)
2510-0043
7890 PTV LN2 Cryo Assembly
(Recommended valve repair level. Includes: cryo
valve mounted on cryo bracket, with LN2 supply
tubes and connector between the LN2 supply
tube and the cryo valve.)
G3502-60515
Mounting bracket, LN2 cryo valve (included in 5)
G3430-00021
PTV jumper cable (included in 5)
G2619-60502
Connector, male, 1/4-in. brass
0100-0208
Screw, M4 x 12 mm, T-20
0515-2496
621
18 Illustrated Parts Breakdown
5
1
6
2
622
7890 Series GC IPB
Illustrated Parts Breakdown
18
Volatiles Interface (VI)
Top level subassemblies for VI inlet accessories:
G3504A 100 psi Volatiles Interface with EPC, Kit
7890 Series GC IPB
Description
Part no.
VI Inlet Accessory 0-100 PSIG without ship kit
G3504-65500
VI Weldment Assembly without EPC module
G3504-60506
VI EPC module, 100 PSI
G3504-60501
623
18 Illustrated Parts Breakdown
Volatiles Interface (VI)
624
Item
Description
Part number
Qty
VI top cover
G2319-00020
Top insulation
G2319-20580
Screw, M4 x 12 mm
1390-1023
Clamping plate
G2319-20540
Volatiles interface
G2319-60505
VI heater/sensor assembly
G2319-60503
Heater block assembly
G2319-60507
VI insulation, heater block
G2319-20530
Pneumatic fitting assembly
G3504-60500
10
Nut, 1/16-inch
19258-20830
11
SilTite Metal Ferrules, 1/16-in. x 0.5 mm
ID (10/pk)
5184-3570
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
625
18 Illustrated Parts Breakdown
Volatiles Interface Trap
626
Item
Description
Part number
Qty
T08PC Valve Chemraz 0.01
G3430-60527
Screw, M3 x 16 mm, T-10, to attach valve
0515-1141
NS
O-ring, 12/pk for valve seal
5180-4181
Flow block, split vent trap
G3452-60506
NS
Screw, M4 12 mm, T-20
0515-2496
NS
Trap retainer
G3452-00005
Trap nut
G1544-20650
VI front trap assembly
G2319-80530
NS
Split Vent Trap
See Parts Finder
Screw, captive, M4 x 20 mm, T-20
1390-1024
Nut, 1/16-inch
19258-20830
SilTite Metal Ferrules, 1/16" x 0.5mm ID
(10/pk)
5184-3570
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
627
18 Illustrated Parts Breakdown
Detectors
This section contains an illustrated parts breakdown for each of
the following 7890 GC detectors and related components.
Flame Ionization Detector (FID)
Flame Photometric Detector (FPD)
FPD+ (High Temperature FPD)
Microcell Electron Capture Detector (uECD)
Nitrogen Phosphorus Detector (NPD)
Thermal Conductivity Detector (TCD)
628
7890 Series GC IPB
Illustrated Parts Breakdown
18
Flame Ionization Detector (FID)
Top level subassemblies for FID detector accessories:
G3461A FID with EPC, Kit adaptable to either packed or
capillary columns.
G3462A Capillary FID with EPC
7890 Series GC IPB
Description
Part number
FID Detector Module, adaptable without ship kit
G3431-60506
FID Detector Module, capillary without ship kit
G3431-60500
FID Packed Weldment Assembly with pallet, electrometer,
and base
G3431-80508
FID Capillary Weldment Assembly with pallet,
electrometer, and base
G3431-80506
FID EPC Module
G3431-60531
FID Signal Board
G3431-60020
629
18 Illustrated Parts Breakdown
FID detector
630
Item
Description
Part number
Qty
Screw, M4 25 mm, Torx T-20
0515-2712
FID interconnect cover
G1531-00220
PTFE chimney (optional)
19231-21050
Collector assembly
For individual collector parts see Parts
Finder.
G1531-60690
Screw, M4 10 mm, Torx T-20
0515-2495
Interconnect J-clamp
19231-00040
Mounting pallet, FID
G1531-40020
FID Base Assembly
Cylindrical EMI suppressor, ferrite
9170-1730
10
Spring, electrometer interconnect
1460-2142
11
FID interconnect assembly
G1531-60715
12
FID electrometer
G3431-60015
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
631
18 Illustrated Parts Breakdown
FID Base Assembly
Item
Description
Part number
Qty
Base spanner nut
19231-20990
Thermal strap
G1531-00105
Screw, captive, M3, T-10
G1946-20168
O-ring, size 2-006, fluorocarbon, 12/pk
5180-4181
Jets
See Parts Finder
Adaptable FID, base weldment with jet
G3431-80509
Capillary column FID, base weldment with
jet
G3431-80507
Screw, M4 25 mm, Torx T-20
0515-2712
FID block insulation
G1531-60700
Adaptable FID column adapters:
FID/NPD capillary column
19244-80610
FID/NPD 1/8-inch packed column
19231-80520
FID/NPD 1/4-inch packed column
19231-80530
Nut warmer insulation and cup assembly.
19234-60700
10
Heater/sensor assembly
G1530-67950
NS
Insulation, nutwarmer (1/pk)
19234-60715
G3431-80509 includes jet 19244-80560, capillary adaptable,
61.5 mm
G3431-80507 includes jet G1531-80560, capillary optimized,
43 mm, .29 mm id
632
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
633
18 Illustrated Parts Breakdown
PM kits for the FID
See Parts Finder and the Agilent catalog for consumables and
supplies for consumable parts, or visit the Agilent Web site for
the latest information (www.agilent.com/chem/supplies).
FID PM kits
634
Description
Part no.
Maintenance kit, FID rebuilding
G1531-67001
Maintenance kit, FID cleaning
G1531-67000
7890 Series GC IPB
Illustrated Parts Breakdown
18
Flame Photometric Detector (FPD)
Top level subassemblies for FPD detector accessories:
G3435A Single FPD with EPC, Kit
G3436A Dual FPD with EPC, Kit
Description
Part number
FPD Detector Module, Single, without ship kit
G3435-60500
FPD Detector Module, Dual, without ship kit
G3436-60500
FPD Body Assembly (without EPC, signal board, or PMT)
G3435-60575
Dual FPD Body Assembly (without EPC, signal board, or
PMT)
G3435-60585
FPD EPC module
G3435-60535
FPD Signal board (1 for single FPD, 2 for dual FPD)
G3435-60010
Single FPD
EPC module
7890 Series GC IPB
635
18 Illustrated Parts Breakdown
636
7890 Series GC IPB
Illustrated Parts Breakdown
18
FPD inert transfer line parts
7890 Series GC IPB
Item
Description
Part number
Qty.
O-ring, FPD jet seal, white
0905-1608
Screw, M3 x 12 mm, T-10
0515-1084
Retaining clip
19256-00340
Inert transfer line
G3435-60555
Heater/Sensor assembly
G1535-60620
Capillary adapter seat
19256-21140
Capillary adapter nut
19256-21150
1/8-inch ferrule (10/pk)
0100-1332
1/8-inch nut (10/pk)
5180-4103
10
1/4-inch packed adapter
G1532-20710
637
18 Illustrated Parts Breakdown
638
7890 Series GC IPB
Illustrated Parts Breakdown
18
FPD ignitor and heat shield assembly
7890 Series GC IPB
Item
Description
Part number
FPD tube assembly:
Aluminum
Stainless Steel
19256-60700
19256-20705
Vespel ferrule, 1/4-inch id, 20/pk
5080-8774
Front ferrule, 1/4-inch id, brass, 10/pk
5180-4111
Back ferrule, 1/4-inch id, brass, 10/pk
5180-4117
Emissions block assembly
FPD, single
FPD, dual (not shown)
Ignitor replacement kit
A. O-ring
B. Spacer
C. Glow plug
19256-60800
13
Screw, M3 x 66 mm, T-10
0515-0680
12
Collet, ignitor
19256-20690
Ignitor cable assembly
G3435-60600
Heat shield gasket, white
19256-80045
First heat shield window
19256-80030
Heat shield disk
19256-20580
Stainless steel coupling
19256-20550
10
Lock washer (4 required)
2190-0584
11
Screw, M3 12, T-10 (4 required)
0515-1084
19256-80560
19256-80600
Qty.
1
639
18 Illustrated Parts Breakdown
640
7890 Series GC IPB
Illustrated Parts Breakdown
18
PMT and bracket assemblies
Single FPD
7890 Series GC IPB
Item
Description
Part number
Qty.
Chimney back cover
G1535-80520
Heater/Sensor assembly
G1535-60610
Transfer line support bracket, single
19256-00320
Bracket/Support
G1535-00010
Emissions block assembly, single
19256-60650
Filters:
Sulfur
Phosphorus
1000-1437
19256-80010
Filter spacer (used only with sulfur filter)
19256-20910
Sping, PMT
1460-1160
PMT housing assembly
19256-60510
641
18 Illustrated Parts Breakdown
5
6
2
7
8
9
642
7890 Series GC IPB
Illustrated Parts Breakdown
18
Dual FPD
7890 Series GC IPB
Item
Description
Part number
Qty.
11
Dual cover assembly
G1535-80530
12
Emissions block assembly, dual
19256-60690
13
Dual FPD chimney back
19256-00330
14
Dual main bracket
G1535-00040
15
Dual FPD chimney front
G1535-00030
643
18 Illustrated Parts Breakdown
FPD lens assembly
644
Item
Description
Part number
Qty.
Clamp
19256-00090
Screw, M3 25 (4 required)
0515-0683
Silicone O-ring, 0.926-inch id (orange)
0905-1099
Convex lens
1000-1438
Lens housing
19256-20900
Flange ring
19256-00200
O-ring 12/pk, Fluoroelastomer, 1.239-in.
ID
5061-5890
7890 Series GC IPB
Illustrated Parts Breakdown
18
FPD Covers
Item
Description
Part number
Single FPD top cover
G3435-80500
Dual FPD top cover
G3435-80501
Electronics top cover, with ground strap
Ground strap
G3435-60503
19256-60730
Auxiliary heater and valve control assembly
Aux zone/valve box harness
7890 Series GC IPB
G1530-60660
645
18 Illustrated Parts Breakdown
646
7890 Series GC IPB
Illustrated Parts Breakdown
18
FPD+ (High Temperature FPD)
Top level subassemblies for FPD+ detector accessories:
G3435B Single FPD+ with EPC, Kit
G3436B Dual FPD+ with EPC, Kit
Description
Part number
FPD High Temp, Single
G3435-60300
FPD High Temp, Dual
G3436-60300
FPD+ EPC module
G3435-60335
FPD Signal board (1 for single FPD, 2 for dual FPD)
G3435-60010
FPD+, Single
EPC module
Figure 17
FPD+, Single
7890 Series GC IPB
647
18 Illustrated Parts Breakdown
FPD+, Dual
EPC module
Figure 18
FPD+, Dual
FPD+ signal board
648
7890 Series GC IPB
Illustrated Parts Breakdown
18
FPD+ Assemblies
Table 38 Coupling, ignitor, and exit tube
ID
Description
Part number
Qty
O-Ring, 2-010, Fluorocarbon, brown (exit
tube)
0905-1014
Exit tube assembly, FPD+
G3435-60330
Screw, M3 X 6 mm long, pan head
0515-0680
FPD Ignitor cable assembly
G3435-60600
Collet, glow plug
19256-20690
Ignitor, cleaned w/copper gasket (for
FPD+, discard copper gasket)
19256-60750
Heat shield gasket, perfuoroelastomer
19256-80045
Window, first
19256-80030
Shield, heat
19256-20580
10
Lens housing coupling
G3435-20345
11
Screw, machine, M3 X 12 mm long, pan
head
0515-1084
12
Washer, lock, HLCL 3.0 3.1 MM-ID
6.2 MM-OD
2190-0584
NS
Washer-Flat metallic 3.2 mm-ID 9 mm-OD
1mm
3050-2326
NS
Spacer-Round 3.2 mm-ID 6 mm-OD
6mm-LG Br Z
0380-4876
7
1
2
8
9
10
3
4
11
5
12
7890 Series GC IPB
649
18 Illustrated Parts Breakdown
Table 39 Lens housing
ID
Description
Part number
Qty
BK7 Convex glass lens, 31.2mm f.l.
1000-1438
O-Ring 2-021 Silicone Rust Color
0905-0955
Clamp
19256-00090
Lens housing
G3435-20391
RING, FLANGE
19256-00200
SCREW, 3.0 25 PN TX
0515-0683
O-Ring, Size 2-123, Silicone, Rust Color
0905-1159
1
2
4
5
6
Table 40 Brazements and heaters
650
ID
Description
Part number
Qty
WS2 Coated M3x12 Screw
G3435-20357
Retaining Clip, FPD Heater-Sensor
19256-00340
FPD UP HEAT/SENS ASSY
G1535-60610
FPD Cell Brazement - Inert
G3435-60558
FPD Emission Block Heater Assembly
G3435-60610
7890 Series GC IPB
Illustrated Parts Breakdown
18
1
2
3
Table 41 Brackets, insulation, PMT, and filters
7890 Series GC IPB
ID
Description
Part number
Qty
Front detector cover assembly
G3435-81330
Chimney insulation
G3435-00340
Nut, hex, with lockwasher, M4
0535-0043
Chimney Insulation, Middle
G3435-00342
Screw, machine, M4 x 10-mm long
0515-2495
FPD Chimney back
19256-00320
WHC-375 Wire Clip
1400-3196
Filters
FPD Sulphur filter 394nm
1000-1437
Filter, P 5890 FPD
19256-80010
FPD Filter spacer (for sulfur filter only)
19256-20910
10
Spring, compression
1460-1160
11
PMT Assembly (single FPD+ and dual
FPD+ right side)
G3435-60360
12
FPD Main bracket
G3435-00370
651
18 Illustrated Parts Breakdown
1
5
8
9
2
10
11
4
5
12
6
7
5
Table 42 Covers (external)
ID
652
Description
Part number
Qty
M3 X 8mm Captive WS2 coated screw
G3430-20028
Single FPD+ top cover
G3435-81350
Ground strap
19256-60730
Electronics top cover, with ground strap
G3435-60503
7890 Series GC IPB
Illustrated Parts Breakdown
18
4
3
See Table 43 below for additional parts used only on the dual
FPD+.
Table 43 Dual FPD+ parts
7890 Series GC IPB
ID
Description
Part number
Qty
Dual FPD cover assembly
G3435-81360
FPD Cell brazement, dual - inert
G3435-60559
Dual wavelength main bracket
G3435-00375
PMT Assembly (Dual FPD+ only, left PMT,
short)
G3435-60370
DW FPD Chimney front
G1535-00030
PMT Assembly (right PMT, long)
G3435-60360
WHC-375 Wire Clip
1400-3196
Screw, machine, M4 x 10-mm long
0515-2495
653
18 Illustrated Parts Breakdown
7
8
7
8
5
654
7890 Series GC IPB
Illustrated Parts Breakdown
18
Microcell Electron Capture Detector (uECD)
Top level subassemblies for ECD detector accessories:
G2397AD ECD with EPC Accessory
G2398AD ECD with EPC Accessory for Japan
Description
Part number
ECD EPC module
G3433-60533
ECD Signal board
G3433-61020*
* Replaces ECD Signal board G3433-60020.
7890 Series GC IPB
655
18 Illustrated Parts Breakdown
Microcell Electron Capture Detector (uECD) parts
Item
Description
Part number
Qty
1
2
3
uECD top cover
uECD signal wire assembly
Anode/Ferrule/Nut assembly (specific
license required)
uECD thermal cover
Thermal cover clip
uECD top insulation
Screw, M4 10 mm, Torx T-20
Clamp, interconnect
Captive screw, detector pallet, M4 20
mm
FID pallet
Tubing, Tygon, 30 inch
Screw, M4 45 mm, Torx T-20
Screw, M4 12 mm, Torx T-20
ECD Insulation cup kit
Screw, M4 x 40mm T-20
G2397-00011
19233-60635
1
1
1
G1533-00030
19233-00095
G1533-00020
0515-2495
19231-00040
1390-1024
1
1
1
1
1
4
G1531-40020
0890-0934
0515-2484
0515-2496
G3433-00004
0515-4793
1
1
2
uECD make-up gas adapter weldment
assembly, includes:
Fused silica indented mixing liner
End cap
G3433-63000
G2397-20540
19233-20755
4
5
6
7
8
9
10
13
14
15
16
17
18
19
20
21
22
NS
23
24
25
26
27
28
29
30
656
Ferrules, capillary columns
Capillary column nut
Replacement ECD Cell (general license)
Replacement ECD Cell (JP Labelled)
Replacement ECD Cell (JP General)
uECD interconnect assembly
Screw, M4 10 mm, Torx T-20 to attach
electrometer
uECD electrometer without interconnect
Upper heated block
Heater/Sensor assembly
Lower heated block
uECD mounting plate
See Parts Finder
See Parts Finder
G2397-60610
G2397-60615
G2398-60615
G1533-60510
0515-2495
G3433-60010
G1533-20525
G1533-60625
19233-20515
G3433-60501
Nut warmer insulation and cup assembly.
Includes:
Nutwarmer insulation
Nutwarmer cup assembly
19234-60720
Ferrule, 1/4 in. Vespel (10/pkg)
1/4 in. nut, brass (10/pkg)
5080-8774
5180-4105
1
1
1
1
2
1
1
1
1
1
1
19234-60715
19234-60700
1
1
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
657
18 Illustrated Parts Breakdown
uECD Side Mount (3rd Detector) Parts
This section lists parts specific to the ECD mounted in the side
carrier as a third detector. For other service parts, see
Microcell Electron Capture Detector (uECD) parts.
G2397AD Micro ECD wit EPC
G2398AD Micro ECD with EPC (Japan only)
G3485B Manual Pneumatics Carrier for 7890B
G3440-68011 Mounting bracket kit
658
Item
Description
Part number
Qty
Third Detector Heated Zone Cable
G3432-60506
Third Detector EPC Communication Cable
G3432-60505
1/8-inch Bulkhead union, 316 SST
0100-0133
aT-Manifold Assy
G1176-60569
Screw, machine, M4 x 12 mm long
0515-2496
Screw, machine, M4 x 25 mm long
0515-2712
Bulkhead fitting retainer, 316 SST
0100-0137
Nutwarmer cup assembly
19234-60700
Label, ECD Caution
19233-90730
NS
Nut Warmer Insulation
19234-60715
7890 Series GC IPB
Illustrated Parts Breakdown
18
1
2
6
4
5
7890 Series GC IPB
659
18 Illustrated Parts Breakdown
Nitrogen Phosphorus Detector (NPD)
Top level subassemblies for NPD detector accessories:
G3495A NPD (white ceramic bead) for packed and capillary
columns
G3496A NPD (white ceramic bead) optimized for capillary
columns only
G3463A NPD (Blos bead) for packed and capillary columns
G3464A NPD (Blos bead) optimized for capillary columns
only
660
Description
Part number
NPD Detector Module, adaptable, without ship kit,
includes bead G1534-60670 (white)
G3434-60506
NPD Detector Module, capillary, without ship kit
G3434-60501
NPD Adaptable Weldment Assembly with pallet,
electrometer, and base
G3434-80508
NPD Capillary Weldment Assembly with pallet,
electrometer, and base
G3434-80507
NPD EPC Module
G3434-60502
NPD Signal Board
G3434-60021
7890 Series GC IPB
Illustrated Parts Breakdown
18
Nitrogen Phosphorus Detector (NPD) parts
Item
Description
Part number
Qty
1
2
3
4
5
6
7
8
9
Screw, M4 10 mm, Torx T-20
Hinged cover assembly
Screw, M3 8 mm, Torx T-10
NPD bead assembly
Screw, M4, Torx T-20, 10 mm long
Power cable assembly
Lid weldment
Collector funnel, standard
0515-2495
G1534-80521
0515-0655
See Parts Finder
0515-2495
G3434-60600
G1534-80510
G1534-20530
5182-9722
1
1
3
1
3
1
1
1
Screw, M4 10 mm long
J-clamp
Screw, M4 10 mm long
NPD interconnect assembly
Spring, interconnect
NPD electrometer
Pallet captive screws, M4 x 20 mm long
O-ring, size 2-006, fluorocarbon, 12/pk
Screw, captive, M3, T-10
Mounting pallet
Jets
0515-2495
1400-0015
0515-2495
G1534-60610
1460-2142
G3434-60010
1390-1024
5180-4181
G1946-20168
G1531-40020
See Parts Finder
Base weldment with jet
- Capillary column NPD
- Packed column NPD
1
1
2
1
1
1
4
3
1
1
1
1
G3434-80505
G3434-80506
21
NS
22
Lid stop/standoff
Insulation cap
G1534-20590
G1531-00130
NPD Insulation cup kit.
Includes:
G3434-00004
G3434-00001
G3434-00002
23
24
25
Heater/sensor assembly
Column adapters for packed NPD
G1530-67950
See Parts Finder
Cup insulation kit. Includes:
Insulation
Nutwarmer cup assembly
19234-60720
19234-60715
19234-60700
Flow measurement adapter
G1534-60640
10
11
12
13
NS
14
15
16
17
18
19
20
NS
7890 Series GC IPB
NPD ceramic replacement kit
Includes top and bottom C-rings and
upper and lower insulators.
3
1
1
661
18 Illustrated Parts Breakdown
662
7890 Series GC IPB
Illustrated Parts Breakdown
18
Thermal Conductivity Detector (TCD)
Top level subassemblies for TCD detector accessories:
G3432A TCD Accessory with EPC, Kit
G3437A TCD mounted on left-hand side of GC, Kit, for 7890A
GC
G3437B TCD with EPC mounted on left side of 7890B GC
19232C TCD to FID adapter kit
Description
Part no.
TCD Detector Module without ship kit (includes TCD cell,
heater and sensors, EPC module without switching valve,
signal board PCA, insulation cup assembly, and mounting
pallet)
G3432-60500
TCD base assembly, tested (includes filament block
assembly, delta PRT, heater/sensor, TCD switching valve,
detector baseline noise results)
G3432-60220
Acid tested TCD (includes filament block assembly and TCD
switching valve). Use only for specific applications, such as
fatty acid analysis.
G3432-60509
TCD EPC Module (without switching valve)
G3432-60532
TCD Signal Board
G3432-60015 *
*. Replaces G3432-60010, see service note G3440A-40.
Selecting a replacement TCD cell assembly
When replacing a TCD cell, normally order the TCD base
assembly (G3432-60220). This is the standard replacement part
for most users.
Customers performing analyses of certain acidic compounds,
for example, fatty acid analysis, may need the Acid Tested TCD
(G3432-60509). The Acid Tested TCD costs about twice as much
as a standard cell, and should only be ordered for the specific
applications that require it.
7890 Series GC IPB
663
18 Illustrated Parts Breakdown
Figure 19
TCD major component identification (top-mounted TCD, G3437B, shown)
Figure 20 G3432-60220, TCD base assembly
664
7890 Series GC IPB
Illustrated Parts Breakdown
18
Figure 21 G3432-60500, Acid tested TCD
7890 Series GC IPB
665
18 Illustrated Parts Breakdown
Thermal Conductivity Detector (TCD) parts
666
Item
Description
Part number
Qty
Screw, M4 12 mm, T-20
0515-2496
Thermal cover and insulation assembly
G1532-00027
O-ring, 12/pk (2 for EPC module seal, 4 for
valve seals)
5180-4181
Screw, captive, M3, T-10
G1946-20168
Screw, M4 10 mm, Torx T-20
0515-2711
TCD mounting pallet (top mount)
G3432-00002
TCD Insulation Cup Kit
G3432-00004
Screw, M4 x 40 mm, T-20
0515-4793
TCD seal insulation
G1532-00080
10
Column adapters, ferrules, and nut
See Parts Finder
11
TCD cell assembly
See Thermal
Conductivity
Detector (TCD)
on page 662.
12
PRT Sensor, TCD (Delta PRT)
G1532-60660
13
Heater/Sensor assembly
G1530-67950
14
Cylindrical EMI suppressor, ferrite
9170-1730
15
Screw, M4 12 mm, T-20 (attach detector
to oven top)
0515-2496
NS
TCD vent restrictor kit (See Table 44 and
service note G1530-25.)
G1532-60700
7890 Series GC IPB
Illustrated Parts Breakdown
18
1
2
4
5
11
12
13
14
15
7
8
9
10
7890 Series GC IPB
667
18 Illustrated Parts Breakdown
Reference gas switching valve
module.
668
This valve is located on the EPC
Item
Description
Part number
Qty.
Clamp, switching valve
G3432-20523
Valve, TCD Switching
G1532-60620
Screw, M3 x 12 mm T-10
0515-1084
Cable, switching valve
G1532-60550
7890 Series GC IPB
Illustrated Parts Breakdown
18
TCD vent restrictor kit Use this kit to eliminate baseline signal
spikes due to changes in laboratory air pressure due to doors
closing and similar events.
Table 44 TCD outlet restrictor kit G1532-60700 parts
7890 Series GC IPB
Item
Description
Part number
Qty.
Swagelok reducer
0100-0121
Restrictor
19232-60555
1/8-inch Graphite/Vespel ferrule (10/pk)
0100-1107
669
18 Illustrated Parts Breakdown
EPC Module Parts
Lookup table 669
Inlet modules 670
Detector modules 671
PCM modules 672
Aux EPCs 673
This section provides a quick reference to the EPC-related part
numbers.
Each proportional valve requires 2 O-rings (5180-4181, 12/pk).
The valve part numbers are for kits, which contain the valve,
screws, and a package of O-rings.
Lookup table
Each proportional valve has a part number on the valve. This
table lists the reorder part number for each proportional valve.
670
Part number on valve
Reorder
G3431-60508
G3430-67013
G3431-60509
G3430-67014
G3430-60527
G3430-67015
G3430-60528
G3430-67016
7890 Series GC IPB
Illustrated Parts Breakdown
18
Inlet modules
EPC modules
Description
Part number
O-rings
Slot
COC
G3454-60554
1 or 2
MMI
G3452-60552
1 or 2
PP
G3451-60551
1 or 2
PTV
G3500-60500
1 or 2
S/SL 100 PSI
G3452-60552
1 or 2
S/SL 150 PSI
G3452-60510
1 or 2
VI
G3504-60501
1 or 2
Split vent
Proportional valves
7890 Series GC IPB
Description
Carrier
Septum purge
COC
G3430-67013
G3430-67014
MMI
G3430-67013
G3430-67014
PP
G3430-67013
G3430-67014
PTV
G3430-67013
G3430-67014
G3430-67015
S/SL 100 PSI
G3430-67013
G3430-67014
G3430-67015
S/SL 150 PSI
G3430-67013
G3430-67014
G3430-67015
VI
G3430-67013
G3430-67014
G3430-67015
G3430-67015
671
18 Illustrated Parts Breakdown
Detector modules
EPC modules
Description
Part number
O-rings
Slot
uECD
G3433-60533
3 or 4
FID
G3431-60531
3 or 4
FPD
G3435-60535
3 or 4
FPD+
G3435-60335
3 or 4
NPD
G3434-60502
3 or 4
TCD
G3432-60532
3 or 4 or AUX Det
2
Proportional valves
Description
Air
uECD
Hydrogen
Reference
G3430-67013
FID
G3430-67013
G3430-67014
G3430-67014
FPD
G3430-67013
G3430-67013
G3430-67013
FPD+
G3430-67013
G3430-67013
G3430-67013
NPD
G3430-67013
G3430-67014
G3430-67014
TCD
672
Makeup
G3430-67013
G3430-67013
7890 Series GC IPB
Illustrated Parts Breakdown
18
PCM modules
EPC module
Description
Part number
O-rings
Slot
PCM
G3476-60501
1, 2, 5, or 6
Proportional valves
7890 Series GC IPB
Description
Carrier
AUX
PCM
G3430-67013
G3430-67016
673
18 Illustrated Parts Breakdown
Aux EPCs
EPC module
Description
Part number
Slot
AUX
G3470-60501
5 or 6 or AUX
Tubing weldment
Description
Part number
Pneumatic tubing with block connector and captive screw
G3430-60550
Figure 22 Tubing weldment
Proportional valves
674
Description
Channel
Channel
Channel
AUX
G3430-67013
G3430-67013
G3430-67013
7890 Series GC IPB
Illustrated Parts Breakdown
18
Nickel Catalyst Accessory
Top level subassemblies for FID detector accessories:
G3478A Nickel Catalyst Kit
G3440-60510 Nickel Catalyst Kit without ship kit
Item
7890 Series GC IPB
Description
Part number
Qty
Nickel catalyst assembly (items 2 through
8)
G3440-63002
Nickel catalyst hydrogen mix weldment
G3440-81000
NS
Screw,
Screw, M4 x 12 mm, captive
0515-2711
Top cover plate
G1543-00085
Heater/sensor assembly
G1580-61160
Top insulation
G1543-00100
Nut, hex, with lockwasher
0535-0043
Heater block
18900-20835
Screw, socket M4 20 mm
0515-0038
PP base insulation
G1543-00030
10
PP bottom insulation
G1543-00070
11
Adapter insulation
19234-60715
12
Insulating cup
19234-60700
675
18 Illustrated Parts Breakdown
676
7890 Series GC IPB
Illustrated Parts Breakdown
18
Oven
This section contains illustrated parts breakdowns for the
following 7890A GC components:
Oven assembly
Oven flapper assembly
CO2 cryogenic cooling
Liquid nitrogen (LN2) cryogenic cooling
7890 Series GC IPB
677
18 Illustrated Parts Breakdown
Oven assembly
678
Item
Description
Part number
Qty
Door hinge rod
G3430-20518
Oven door (non-removable)
G3430-60502
Oven heater shroud assemblies:
120V USA power
G1530-61610
200V Japan power
G1530-61620
220V Single phase power, Europe, and
208V USA power, single phase
G1530-61630
220V Single phase power, Hong Kong
G1530-61630
220V Single phase power, China
G1530-61630
220V China power, slow ramp
G1530-61230
220V Israel power
G1530-61630
230V Single phase power, Switzerland,
10 amp
G1530-61670
230V Denmark power, 10 amp
G1530-61670
230V Denmark/Switzerland power, 16
amp
G1530-61650
230V Continental Europe power
G1530-61650
240V Australia power
G1530-61640
240V South Africa/India power
G1530-61640
240V Great Britain/Ireland power
G1530-61640
240V USA power
G1530-61640
240V Australia power, slow ramp
G1530-61640
Screw, M4, Torx T-20, chrome plated
0515-2711
On/Off switch rod
G3430-40023
Hex nut, M4 x .7 3.2 mm
0535-0043
Motor, oven fan
G3430-60504
Washer
2190-0712
Door sensor assembly
G1530-80670
10
Oven door button
G3430-80513
11
Column clip kit (includes 4 spring clips
and screws)
G1530-61580
12
Oven sensor assembly
G1530-61030
13
Column hanger
1460-1914
14
Fan blade, stainless steel, and set screw
05890-80270
7890 Series GC IPB
Illustrated Parts Breakdown
18
6
1
7
2
8
3
4
9
5
10
13
3
14
11
4
12
7890 Series GC IPB
679
18 Illustrated Parts Breakdown
Removable oven door kit parts
680
Item
Description
Part number
Qty
NS
Removable oven door kit (includes screw,
door pin, hook plate, base plate, door, and
support spacer)
G3430-68640
Rod
G3430-20643
Screw: Mach M4 x 0.7, 20 mm, LG T-20
Pan HD SST
0515-0686
Lower Oven Flange Support Spacer
G3430-20645
Hook Plate
G3430-00647
Base Plate
G3430-00646
NS
Door, removable
G3430-60640
7890 Series GC IPB
Illustrated Parts Breakdown
18
Oven flapper assembly
7890 Series GC IPB
Item
Description
Part number
Qty
NS
Oven exhaust duct and flapper assembly
(includes 3 captured screws 1390-1023)
G3430-60008
Dual duct assembly
G3430-81001
Screw, Torx T-10, M3 12 mm (to attach
duct to oven)
1390-1023
Screw, Torx T-20, M4 x 12 mm (to attach
motor to shaft)
0515-2496
Screw, Torx T-10, M3 8 mm (to attach
motor to duct)
0515-0655
Flapper bushing
G1530-20550
Flapper shaft assembly
G3430--81002
Stepper motor assembly
G1530-60945
681
18 Illustrated Parts Breakdown
682
7890 Series GC IPB
Illustrated Parts Breakdown
18
CO2 cryogenic cooling
7890 Series GC IPB
Item
Description
Part number
Qty
Tee, brass, 1/8-inch
0100-0090
CO2 blast brazement (Cryoblast)
G1565-80550
Cryo bracket
G1565-00010
CO2cryo valve assembly (recommended
level for valve)
G1565-65510
1/8-inch male connector without O-ring
G1543-80025
CO2 inlet tube
G1565-20600
CO2 cryo inline filter
3150-0602
Cryoblast restrictor weldment
G1565-80590
CO2 weldment (oven cryo)
G1565-80505
10
Clamp screw
G1565-20560
11
Gland seal, CO2
G1565-20590
12
Screw, 8-32, .312-inch
2510-0043
NS
Screw Torx T-20, M4 12 mm
0515-2496
NS
PTFE seal
G1565-20840
683
18 Illustrated Parts Breakdown
684
7890 Series GC IPB
Illustrated Parts Breakdown
18
Liquid nitrogen (LN2) cryogenic cooling
7890 Series GC IPB
Item
Description
Part number
Qty
N2 blast brazement
G1566-80535
Tee, 1/8-inch brass union, 2/pk
5180-4160
Connector, male, 1/4-inch
0100-0208
Screw, 8-32, .312-inch
2510-0043
Cryo bracket
G1565-00010
N2 restrictor tube
G1566-20575
N2 cryo valve
G3430-60018
Liquid N2 nozzle
19310-20500
NS
Screw Torx T-20, M4 12 mm
0515-2496
NS
Pipe thread sealant tape, 1/4-inch wide
0460-1266
NS
N2 cryo valve/dual blast assembly
G1566-65508
NS
N2 cryogenic kit
G1566-65517
685
18 Illustrated Parts Breakdown
Valves
Top level subassemblies for Valve accessories:
G1580A Valve box for one valve
G1581A Valve box for two valves
This section contains illustrated parts breakdowns for the
following 7890 Series GC valves and related components. In
general, the valve parts are the same for both 7890 Series and
6890 Series GCs. The solenoid valve stacks have changed,
however. Be sure to order the correct version of parts or
upgrade the GC to the newer version if needed.
Valve box assembly
Valve driver assembly
Valve actuator assembly (1 of 2)
Valve actuator assembly (2 of 2)
Valco W-Series minivalve (See Parts Finder.)
Miscellaneous Valve Parts
686
7890 Series GC IPB
Illustrated Parts Breakdown
18
Valve box assembly
7890 Series GC IPB
Item
Description
Part number
Qty
Screw, M4 12 mm, Torx T-20,
chromeplated
0515-2711
Valve box cover
G1580-00030
Valve box insulation, top
G1580-00050
Insulation retainer plate
G1580-00040
Hex nut, insulation plate
Screw, M3 30 mm, Torx T-10,
chromeplated
0515-2525
Heater block
G1580-20520
1 or
2
Standoff, valve box
G1580-20500
Valve box bottom plate
G1580-00010
10
Screw, M3 8 mm, Torx T-10,
chromeplated
0515-2726
11
Heater/Sensor harness cable clamp
1400-0015
12
Heater/Sensor assembly
G1580-61140
NS
Cable-tie strap
1400-0249
NS
Aluminum tube (split/splitless inlet only)
18900-20320
NS
In-line filter (sample in line)
0101-0532
687
18 Illustrated Parts Breakdown
688
7890 Series GC IPB
Illustrated Parts Breakdown
18
Valve driver assembly
For 7890A: If your GC has serial number CN10201096 or
greater, or serial number US10281011 or greater, use the
new-style valve driver assembly parts.
If your GC has a serial number less than listed above, use the
old-style valve driver assembly parts (if available).
For 7890B: All 7890B GCs use the new style valve driver
assembly parts.
7890 Series GC IPB
689
18 Illustrated Parts Breakdown
Valve driver assembly (original style)
690
Item
Description
Part number
Qty
Valve driver bracket
G1580-00070
Captured screw, M4 12 mm, Torx T-20
1390-1023
Valve driver wiring harness
G1530-60660
PTFE tubing, 5 m, 1.5 id, 3 mm od
5062-2483
Adapter fitting
5185-8386
Standoff (included with valves)
4-way Solenoid valves
O-ring (with valves and end plate kit)
Solenoid valve end plate kit
05890-61097
10
Screw, socket head, M5 x 16 mm long
0515-1214
11
Elbow fitting, 1/4-inch, male
0100-1632
12
Exhaust tubing, 1/4-inch od, 120 inch
0890-1489
NS
Heater cable assembly
G1530-60790
8
G1580-61095
4
10
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
691
18 Illustrated Parts Breakdown
Valve driver assembly (new style)
Item
Description
Part number
Qty
Valve driver bracket
G1580-00071
Captured screw, M4 12 mm, Torx T-20
Valve driver wiring harness
G1530-60660
PTFE tubing, 5 m, 1.5 mm id, 3 mm od
5062-2483
Exhaust tubing, 1/4-inch od, 120 inch
0890-1489
NS
Heater cable assembly
G1530-60790
Adapter fitting
5185-8386
Airtec Solenoid Valve w screws
G1580-68000
NS
Screws for One Valve Stack (M4 x 30)
5185-8381
Screws for Two Valve Stack (M4 x 50)
5185-8382
Screws for Three Valve Stack (M4 x 70)
5185-8383
10
Screws for Four Valve Stack (M4 x 85)
5185-8384
NS
One Valve Stack*
G1580-65111
NS
Two Valve Stack*
G1580-65112
NS
Three Valve Stack*
G1580-65113
11
Four Valve Stack*
G1580-65114
12
PT 1/8-inch male elbow fitting for tube
1/4-inch
5185-8385
13
Solenoid Valve End Plate Kit
G1580-61097
Includes bracket, solenoid(s), fittings, end plates, and
harness cable.
692
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
693
18 Illustrated Parts Breakdown
694
7890 Series GC IPB
Illustrated Parts Breakdown
18
Valve actuator assembly (1 of 2)
7890 Series GC IPB
Item
Description
Part number
Qty
Valve actuator assembly
19325-60660
Modified screw
19325-80030
Quick-release pin
Hose fitting
0100-1707
PTFE tubing 5m, 1.5mm ID, 3mm OD
5062-2483
36 Actuator limiter
18900-21000
End cap
Elbow fitting
Coupler/Shaft assembly
NS
Hex key, 3 mm
1
0100-2264
1
1
8710-0911
695
18 Illustrated Parts Breakdown
696
7890 Series GC IPB
Illustrated Parts Breakdown
18
Valve actuator assembly (2 of 2)
7890 Series GC IPB
Item
Description
Part number
Qty
Cylinder end cap
O-ring, 1.176-inch id
0905-1405
O-ring, 1.046-inch id
0905-0463
Piston
19325-20640
Actuator cylinder
Hose fitting
0100-1707
PTFE tubing 5m, 1.5mm ID, 3mm OD
5062-2483
Piston rod
Dowel pin
1480-0017
10
Link
19325-80010
11
Screw, socket head, M4 x 8 mm
12
Elbow fitting
3
0100-1707
697
18 Illustrated Parts Breakdown
698
7890 Series GC IPB
Illustrated Parts Breakdown
18
Miscellaneous Valve Parts
The table below lists several valve accessory kits and parts that
are useful when installing valves, valve boxes, and related parts.
Description
Comment
Part number
G1580A
Heated valve box for one valve
G1580A
G1581A
Heated valve box for two valves.
G1581A
Nut plate assembly
05890-80660
Capillary (SSL or MMI) inlet to
upstream sampling valve kit
Kit to interface an upstream gas or liquid sampling valve to a
capillary or Multi-Mode inlet for sample splitting and
introduction into a capillary or megabore column.
G3480-67585
G2739A Liquid valve plumbing kit
This kit contains the hardware needed to install a liquid
sample valve into a GC. It does not contain the valve or any
automation.
G2739A
G2740A Gas valve plumbing kit
This kit contains the hardware needed to install any 6 port or
10 port valve into a GC and build any of the standard
configurations. It does not contain the valve, automation,
loops or needle valves.
G2740A
G2741A Needle valve kit
Adds an adjustable restrictor to control gas flows. Max temp
of 225 C.This kit is needed when the customer requires to
have a column isolation configuration built into a GC.
G2741A
G2742A Downstream capillary port Kit to interface a split/splitless inlet or multi-mode inlet to a
to valve kit
valve located downstream.
G2742A
G2743B 7890 Actuator kit
G2743B
7890 Actuator Kit. Adds automation to 7890A/B valve system
7890Awith S/N = CN10201096 or later and 7890A S/N =
US10281001 or later
7890B (all S/Ns)
G2744A Heated zone kit
This kit is needed when adding a third heated valve to a GC
that already has two heated valves installed. The heated zone
will allow a 4th valve to be added if required.
G2744A
G2748A
Hardware kit to mount an unheated gas sampling or liquid
sampling valve on the left side of the oven. Requires side
carrier accessory (7890A: G3485A or 7890B: G3485B).
Incompatible with MSD.
G2748A
G3478A Nickel Catalyst
Adds a nickel catalyst (methanizer) to a 7890 Gas
Chromatograph. Requires back inlet position. Compatible with
PCM in rear position.
G3478A
G3505A high pressure injection
device accessory
Requires an SSL inlet and one flow source from an Aux EPC or
PCM module. User must provide appropriate hardware to
interface sample to HPID. One only. Front inlet only.
G3505A
7890 Series GC IPB
699
18 Illustrated Parts Breakdown
Description
Comment
Part number
G4338A Inert 0.530 mm id capillary
column to valve interface kit
Requires mounting plate 05890-80660. Each plate can hold 5
interface adaptors.
G4338A
G4339A Inert 0.320 mm id capillary
column to valve interface kit
Requires mounting plate 05890-80660. Each plate can hold 5
interface adaptors.
G4339A
G2855-60200 Swaging wrench
Swaging Nut or Swaging Wrench is required to swage SilTite
ferrule to column.
G2855-60200
G2855-20555 Swaging nut
Swaging Nut or Swaging Wrench is required to swage SilTite
ferrule to column.
G2855-20555
700
7890 Series GC IPB
Illustrated Parts Breakdown
18
Electronics and Fans
This section contains illustrated parts breakdowns for the
following 7890 GC electrical components.
Electronics carrier (logic, A&P, and LAN boards)
Keyboard Assemblies
AC circuit board components
AC power
Power cords
Main transformer
Analog input board (G1556A accessory)
Chassis fans
7890 Series GC IPB
701
18 Illustrated Parts Breakdown
Electronics carrier
The table below lists the 7890 Series GC electronics carrier
parts. To identify the parts, see Figure 23 for 7890B and
Figure 24 for 7890A.
702
Item
Description
Part number
Qty
NS
Fuse, ALS controller PCA, 7A 125V (ALS
control PCA)
2110-0961
Analog & Power board
see Table 45
Logic board
see Table 46
Harness, 4-wire communication buss
(LVDS communications harness)
G3430-60513
Harness, keyboard and display
G3430-60514
Backplane for Analog and power board
G3430-00114
Backplane for Detector signal boards
G3430-00085
Grounding screw, M4 25 mm, T-20 (for
#1)
0515-2712
Screw, M4 x 6 mm
0515-2832
10
Screw, self-tapping
0515-4897
10
Nut, hex, with lock washer M4 x 3.2 mm
thick
0535-0043
11
Grounding screw, M4 x 12 mm, T-20 (for
#6)
0515-2496
12
ALS Controller Assembly
G3430-60529
13
Cable, RS-232,7683 ALS controller
G2612-60510
14
Backplane right logic board
G3430-00114
15
Screw, T-20, M4 12 mm (attach ALS
board to carrier)
0515-2496
7890 Series GC IPB
Illustrated Parts Breakdown
18
The tables below list the logic and A&P board changes for the
7890 series GCs. Entries in italics are obsolete.
Table 45 Analog & Power board changes
Part number
Model
G3430-60150
(Obsolete)
7890A
G3430-60151
(Obsolete)
7890A
G3430-61050
7890B, 7890A
Min. firmware
Service Note
Features
Original board. Power supply LEDs
inside GC. LVDS FETs not overcurrent
protected.
A.01.09
G3440A-025A
Power supply LEDs viewable on the
back of the GC. LVDS FETs overcurrent
protected.
Modifications to improve the power line
hold up time. If the lights blink in the lab
(due to a few missed line cycles), the
new board will continue to supply
power to the system whereas the older
board would have caused the GC to
reboot.
Table 46 Logic board changes
Part number
Model
G3430-60100
(Obsolete)
7890A
G3430-60101
7890A
G3430-61020
7890A
A.01.11
G3430-61110
7890B, 7890A+
B.02.00
7890 Series GC IPB
Min. firmware
Service Note
Features
Original board. LAN LEDs inside GC.
Two battery switches.
G3440A-025A
LAN LEDs on back of GC. One battery
switch. Used by OEMs that require old
firmware.
G3440A-058A
LAN LEDs on back of GC. One battery
switch.
Real Time Clock module can be
replaced. Extra LVDS channels.
703
18 Illustrated Parts Breakdown
1
11
6
12
5
8
3
13
9
4
7
2
10
15
14
10
Figure 23
704
7890B Electronics carrier parts
7890 Series GC IPB
Illustrated Parts Breakdown
Figure 24
18
7890A Electronics carrier parts
7890 Series GC IPB
705
18 Illustrated Parts Breakdown
Keyboard Assemblies
7890A Keyboard and Display (original style)
Item
Description
Part number
Qty
Keyboard/display assembly with display
and harness
G3430-60555
Replacement keyboard assembly without
display
G3430-67500
Display
G3430-80003
Self-tapping screws
0624-1076
Keyboard/display harness
G3430-60514
Bracket
G3430-00098
Interconnect board
G3430-60003
Screw, M4 x 12 mm, T-20
1390-1023
NS
Screw, self-tapping, 1/4-inch (connect left 0515-4897
and bottom sides of assembly to
electronics carrier)
NS
Screw, M4 x 12 mm, T-20 (connects top
right corner of assembly to electronics
carrier)
0515-2496
Much of the keyboard/display is concealed by its plastic shell, so
that a conventional exploded view is not very helpful. Use the
schematic diagram below to identify parts.
706
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
707
18 Illustrated Parts Breakdown
7890A Keyboard and Display (new style)
Item
Description
Part number
Qty
Keyboard/display assembly with display
and harness (includes G3430-67500,
G3430-60554, and G3430-80003
assemblies)
G3430-60555
Replacement keypad assembly without
display, without keys
G3430-61080
NS
Replacement key and bezel assembly (no
cable harness, no board, no display)
G3430-67500
Display
G3430-80003
Self-tapping screws
0624-1076
Keyboard/display harness
G3430-60554*
Door sensor interconnect cable
G3430-60561
Grounding nut, for display harness
0535-0043
Keypad support spacer
G3430-60022
Keypad support screw
G3430-20034
NS
Screw, self-tapping, 1/4-inch (connect left 0515-4897
and bottom sides of assembly to
electronics carrier)
NS
Screw, M4 x 12 mm, T-20 (connects top
right corner of assembly to electronics
carrier)
0515-2496
*. Use for G3430-67500 and G3430-61080 keyboard assemblies.
708
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
709
18 Illustrated Parts Breakdown
7890B Keyboard and Display
Item
Description
Part number
Qty
Keyboard Assembly 7890B
G3440-60555
Display
G3430-80003
Screw, M4 x 12 mm, T-20 (connects top
right corner of assembly to electronics
carrier)
0515-2496
Screw, self-tapping, 1/4-inch (connect left 0515-4897
and bottom sides of assembly to
electronics carrier)
Keyboard/display harness
G3430-60554*
Replacement key and bezel assembly (no
cable harness, no board, no display)
G3430-67500
Self-tapping screws
0624-1076
Replacement keypad assembly without
display, without keys
G3430-61080
Keypad support spacer
G3430-60022
Keypad support screw
G3430-20034
10
Door sensor interconnect cable
G3430-60561
NS
Grounding nut, for display harness
0535-0043
*. Use for G3430-67500 and G3430-61080 keyboard assemblies.
710
7890 Series GC IPB
Illustrated Parts Breakdown
18
1
3
2
4
2
6
8
9
7890 Series GC IPB
10
711
18 Illustrated Parts Breakdown
AC circuit board components
712
Item
Description
Part number
Qty
Triac jumper (part of 5)
Screw, M4 x 20 mm long
Washer
AC configuration plug
3
1390-1024
USA and Canada 120V
G1530-60690
Japan 200V
G1530-60700
Continental Europe, 220V single phase
power
G1530-60710
Hong Kong, 220V, single phase
G1530-60710
China 220V
G1530-60710
China 220V, 10 amp slow ramp
G1530-60710
Israel 220V
G1530-60710
Switzerland/Denmark, 230V, 16A
G1530-60720
Switzerland power cable, 230V, 10A
G1530-60720
Denmark, 230V, 10A
G1530-60720
Continental Europe, 230V
G1530-60720
Australia, 240V
G1530-60730
South Africa/India, 240V
G1530-60730
United Kingdom/Ireland, 240V
G1530-60730
USA and Canada, 240V
G1530-60730
Australia 240V, slow ramp
G1530-60730
AC board (without triac kit)
G3430-60050
Ceramic fuse, type x, 20A/250V
2110-0098
Glass fuse, type F, 8A/250V
2110-0036
Triac kit, includes triac (item 9) and
thermal link pad (item 10)
G1530-61340
Triac
Order item 8
10
Pad (under triac)
1205-0934
11
Hex nut
0535-0031
7890 Series GC IPB
Illustrated Parts Breakdown
18
2
3
4
5
6
9
10
7890 Series GC IPB
11
713
18 Illustrated Parts Breakdown
AC power
Item
Description
Part number
Qty
EPC pneumatics carrier assembly with fan G3430-80503
NS
Screw, T-20, M4 12 mm (attach carrier
to oven)
0515-2496
Fan, pneumatics carrier
G3430-60006
NS
Screw, M4 X 30 mm, T-20
0515-0669
Washer, steel to attach motor
2190-0712
Nut with lock washer, M4 to attach motor 0535-0043
Oven flapper assembly
G3430-60008
Motor, oven fan, DC
G3430-60504
Nut with lock washer, M4 X 3.2 mm for
grounding straps (7 mm nut driver)
0535-0043
Transformer kit with large washers
G3430-60975
AC power board
G3430-60050
NS
Screw, M4, T-20
1390-1024
AC power inlet assembly (includes power
receptacle)
Regular oven
120 VAC (requires a C19 power cord)
G1530-61550
220, 230, 240 VAC (requires a C13 power
cord)
G1530-61560
Fast oven
All (200/208/220/230/240 VAC) (requires G1530-61550
a C19 power cord)
714
7890 Series GC IPB
Illustrated Parts Breakdown
7890 Series GC IPB
18
715
18 Illustrated Parts Breakdown
Power cords
The 7890 Series GC uses detachable power cords.
Countries
VAC
Description
Part number
C13, 10 amp
8120-1369
10 amp
8120-1378
Europe
C13, 10 amp
8120-1689
US / Canada / Taiwan /
Thailand
C13, 13 amp
8120-1992
Switzerland
C13, 10 amp
8120-2104
Denmark, Greenland
C13, 10 amp
8120-3997
India / South Africa
C13, 10 amp
8120-4211
Japan
10 amp
8120-4753
Israel
C13, 10 amp
8120-5182
Taiwan / South America
C19, 20A
8120-6360
Australia, New Zealand
Americas
120
Argentina
US
C19, 20 amp
8120-6894
Japan
C19, 20 amp
8120-6903
Chile
C13, 10 amp
8120-6978
Australia
C19, 16 amp
8120-8619
Great Britain /Hong Kong
/ Singapore/ Myanmar
C19, 13 amp
8120-8620
Europe
C19, 16 amp
8120-8621
Switzerland, Denmark
C19, 16 amp
8120-8622
Great Britain / Hong
Kong / Singapore /
Myanmar
C13, 10 amp
8120-8705
China
C19, 15 amp, Fast
8121-0070
C19, 15 amp
8121-0075
Israel
C19, 16 amp
8121-0161
Argentina
C19, 20 amp
8121-0675
India / South Africa
C19, 15 Amp
8121-0710
China
C13, 10 amp
8121-0723
Korea
C19, 16 amp
8121-1222
Korea
C13, 10 amp
8121-1226
15 A, 1.8M, C19
8121-1301
US
Thailand
716
8120-6869
120, 208, 240
240
220
7890 Series GC IPB
Illustrated Parts Breakdown
18
Main transformer
Part number G3430-60975
7890 Series GC IPB
717
18 Illustrated Parts Breakdown
Note: Some transformers will have solid color wires as given;
others may have black wires with color markers.
718
Connector (pin)
Wire color
Primary (1)
NC
Primary (2)
Orange
Primary (3)
Yellow
Primary (4)
Black
Primary (5)
NC
Primary (6)
Green
Primary (7)
Blue
Primary (8)
White
Primary (9)
Red
Secondary 1 (1)
Violet
Secondary 1 (2)
NC
Secondary 1 (3)
Orange
Secondary 1 (4)
NC
Secondary 1 (5)
Gray
Secondary 1 (6)
NC
Secondary 1 (7)
Red
Secondary 1 (8)
White
Secondary 1 (9)
Red
Secondary 1 (10)
Yellow
Secondary 1 (11)
Blue
Secondary 1 (12)
Yellow
Secondary 2 (1)
Red
Secondary 2 (2)
Red
7890 Series GC IPB
Illustrated Parts Breakdown
18
Analog input board (G1556A accessory)
7890 Series GC IPB
tem
Description
Part number
Qty
Analog input board
G3456-60010
General purpose analog output cable
assembly
G1530-60560
719
18 Illustrated Parts Breakdown
Chassis fans
720
Item
Description
Part number
Qty
Inlet fan assembly
G3430-60590
Pneumatics area fan
G3430-60006
7890 Series GC IPB
Illustrated Parts Breakdown
18
Covers
Plastic covers 721
Back covers 723
Auto-injector mounting and parking posts
7890A Side Carrier 726
7890B Side Carrier 727
Mainframe 728
7890 Series GC IPB
724
721
18 Illustrated Parts Breakdown
Plastic covers
NOTE
722
7890A GC shown. Plastic covers listed are the same for 7890A and 7890B
unless otherwise noted.
Item
Description
Part number
Qty
Pneumatics cover
G3430-60546
Detector cover
G3430-40007
NS
Detector cover for HS
G3430-60017
NS
Removable detector top cover for CTC
G3440-60013
Inlet cover (7 screws to attach to inlet
carrier)
G3430-60540
Cover, left side with plugs
G3430-60541
Rotating insert
G3430-40024
1 1/2-inch hole plug
5040-4643
1-inch hole plug
5040-4642
Bezel, oven, black plastic, with 2 retained
screws
G3430-60545
Electronics top cover (1 screw to attach)
G3430-60543
10
Cover, right side (1 screw to attach)
G3430-60542
NS
Screw, Captive M4 12 mm, T-20
1390-1023
NS
Screw, M4 12 mm, T-20
0515-2496
NS
Screw, M4, T-20
1390-1024
NS
Detector top cover repair kit
G3430-67648
7890 Series GC IPB
Illustrated Parts Breakdown
18
3
4
5
6
7
10
7890 Series GC IPB
723
18 Illustrated Parts Breakdown
Back covers
Covers
724
Item
Description
Part number
Qty
Cover, back upper
G3440-01090
Oven exhaust deflector (optional)
G1530-80650
Cover, back lower
G3430-00023
Screw, M4 12 mm, T-20
0515-2496
Lock washer, No. 8, 0.168 in.
7890 Series GC IPB
Illustrated Parts Breakdown
18
Auto-injector mounting and parking posts
7683B ALS
7890 Series GC IPB
Item
Description
Part number
Qty
Injector mounting post
G2613-20500
Parking post, dual purpose
05890-61525
725
18 Illustrated Parts Breakdown
7893A ALS, 7650 ALS
Item
Description
Part number
Qty
Injector mounting post
G4513-20561
Parking post, dual purpose
05890-61525
ALS Post Repair Kit
If the threaded portion of the ALS post is broken off in the inlet
chassis, order ALS Post repair Kit G3440-67001. The kit
contains:
Table 47 ALS Post Repair Kit contents
Description
Part number
Qty
Unique 7683 ALS mounting post
G2613-20505
Unique 7693 ALS mounting post
G4513-20574
Unique injection port cover
G3430-60022
The ALS posts in this kit are not compatible with the standard
injection port cover. The unique injection port cover in this kit
requires the unique ALS mounting posts.
726
7890 Series GC IPB
Illustrated Parts Breakdown
18
7890A Side Carrier
Description
Part number
Qty
Screw, M4 25 mm, Torx T-20
0515-2712
Pneumatic carrier assembly
G1530-60950
Screw, M4 12 mm, Torx T-20
0515-2496
Flow side cover
G1530-01240
Screw, M4 10 mm, Torx T-20, flathead
0515-2725
7890 Series GC IPB
727
18 Illustrated Parts Breakdown
7890B Side Carrier
Description
Part number
1/8-inch Bulkhead union, 316 SST
0100-0133
aT-Manifold assembly
G1176-60569
Screw, machine, M4 x 12 mm long
0515-2496
Screw, machine, M4 x 25 mm long
0515-2712
Bulkhead fitting retainer, 316 SST
0100-0137
3rd Detector box cover assembly
G3432-60001
Screw, machine, M4 x 10 mm long
0515-1269
NS
Blank label plate
G1530-91705
Qty
6
4
2
3
3
7
3
728
7890 Series GC IPB
Illustrated Parts Breakdown
18
Mainframe
Description
Part number
Qty
Inlet chassis, for SSL, PP, COC, and VI
inlets
G1530-40020
PTV Inlet chassis, required for MMI and
PTV. (Accepts all inlet types.)
G3430-40011
Standard inlet chassis
MMI and PTV inlet chassis
7890 Series GC IPB
729
18 Illustrated Parts Breakdown
Tools
This section contains parts not applicable to other sections.
Shipping Crates
Description
Part number
Where used
MS shipping crate
G2589-63001
for 5973 MSD
MS shipping crate
G3170-80000
for 5975 MSD
MS shipping crate
G3870-80100
for 5977 MSD
GC shipping container, 7890
G3430-98000
for 7890 series GC
7683 A/B Tray package
G2614-60500
for 7683A/B Tray, G2614A
7683 A/B Injector package
G2913-60480
for 7683B injector
Note: MS shipping crates include the wooden pallet, cardboard
carton, polyethylene bag, and protective foam. They do not
include transfer line packing, straps, or packing for a rough
pump.
730
7890 Series GC IPB
Illustrated Parts Breakdown
18
Hand tools
We assume you have a well-equipped toolbox, but some of the
special tools listed here will be helpful.
Table 48 7890 Series GC tool bag, 5182-3456
7890 Series GC IPB
Description
Part no.
Wrench, 1/4-inch to 5/16-inch
8710-0510
Wrench, open-end, 7/16-inch and 9/16-inch
8710-0803
Wrench, open-end, 1/2-inch and 7/16-inch
8710-0806
Wrench, open-end, 7/16-inch and 3/8-inch
8710-0972
Driver, nut, 7-mm
8710-1217
Cutter, tube
8710-1709
Screwdriver, Torx T-20
8710-1615
Screwdriver, Torx T-10
8710-1623
Tool bag
9222-3253
Tool, ferrule, .25.32 mm, 2 x 3 x 3/4-inch
RFT-2500
Tool, ferrule, .53 mm
RFT-5300
Lens, magnifying
G2855-40001
Septum tool, knurled handle
450-1000
731
18 Illustrated Parts Breakdown
Drivers
T-20 Torx Driver 5182-3465
T-20 Torx Key (for close-quarters work) 8710-1807
T-10 Torx Driver 5182-3466
732
7890 Series GC IPB
Illustrated Parts Breakdown
18
T-10 Torx Key (for close-quarters work) 8710-2140
#1 Pozidriv screwdriver 8710-0899
#2 Pozidriv screwdriver 8710-0900
Flat-blade screwdriver 8730-0008
1/4-inch Nut Driver 8710-1561 (FID Jets)
7-mm Nut Driver 8710-1217
Wrenches
Wrench, 1/4-inch to 5/16-inch 8710-0510
Wrench, open-end, 7/16-inch and 9/16-inch 8710-0803
Wrench, open-end, 1/2-inch and 7/16-inch 8710-0806
Wrench, open-end, 7/16-inch and 3/8-inch 8710-0972
Wrench, adjustable, 12-inch 8710-1712
Wrench, open-end, 3/16-inch x 1/4-inch 8710-2618
Wrench, open-end, 9/16-inch x 5/8-inch 8720-0010
Wrench, 7-mm x 8-mm 1340407010
Wrench, 6-mm x 7-mm 1340407011
Wrench, 8-mm x 10-mm 1340407012
Wrench, 6-mm x 6-mm 8710-2156
Wrench, 5-mm x 5-mm 8710-2157
Cutters/Crimpers/Strippers
Diagonal Cutters
Crimper/Wire Strippers
Tubing Cutters
Restek #20193 http://www.restekcorp.com
Agilent 8710-1709
Agilent precision tubing cutter for 1/16-in. SS tubing
5190-1442
Alternate for Europe:
HICHROM Ltd - Part No: HI-196
Description: Tubing Cutters - Price: 17.00
1 The Markham Centre Station Road Theale, Berkshire
RG7 4PE, UK Telephone: +44 (0) 118 930 3660
mailto:
[email protected]7890 Series GC IPB
733
18 Illustrated Parts Breakdown
Pliers
Channel lock pliers
Slip-joint pliers
Needle nose pliers
Agilent needle nose pliers 8710-0004
Agilent Truarc pliers 8710-0018
734
7890 Series GC IPB
Illustrated Parts Breakdown
18
Specialized tools for GC support
FID Flow Tool 19301-60660
FID Cleaning Kit 9301-0985, (.010-inch Guitar String)
Injection Port Cleaning Kit 480-0003
12 Piece File Kit RSF-1200
7890 Series GC IPB
735
18 Illustrated Parts Breakdown
(Ferrule Removal tool, not shown 440-1000)
Fiberglass Tape 0460-0186
PTFE Tape 0460-0016
White Gloves 8650-0030
NPT Adapter 0100-0118
5/16-inch by #20 Thread Chaser (Die), to clean 1/8-inch
Swagelok threads Other Supplier
On/Off Valve, 1/8-inch Ball Valve 0100-2144
Exacto Knife
Metric (8710-0641) and English Allen Wrench Hex Keys
Pin Vise and small drill bit
Tweezers 8710-0007
Micro Probes (Sharp Object) RMP-5005 Qty 5
Inspection Mirror 707-0027
1.25-inch socket and ratchet for removing FID brass
retaining nut
Column cutter wafer, 4/pk 5181-8836
6890 inlet wrench 19251-00100
7890 inlet wrench (for SSL and MMI) G3452-20512
736
7890 Series GC IPB
Illustrated Parts Breakdown
18
Electronic tools for GC support
Digital Multimeter (Agilent U1231A True RMS shown)
Power Outlet Test Tool (Radio Shack/Sears/Electrical
Supply)
Static Strap 9300-0969 (small) or 9300-0970 (large), 5 ft
cord/clip 9300-0980
Wrist strap, disposable, 4-LG 1-W 9300-1408
Various jumpers and clip leads electronic supply
ESD mat 9300-1484
Useful Cables not shown:
Crossover LAN Cable 5183-4649
9 Pin RS-232 Null Modem Cable G1530-60600
USB/RS-232 adapter cable 8121-1013
Sensor pin extractor 8710-1542
7890 Series GC IPB
737
18 Illustrated Parts Breakdown
738
7890 Series GC IPB
Illustrated Parts Breakdown
18
Pneumatic tools for GC support
7890 Series GC IPB
739
18 Illustrated Parts Breakdown
Electronic Leak Detector
G3388B (or G3388A)
5182-9646, 120 VAC
5182-9648, 220 VAC (Agilent)
Rotameter, Porter Model 65
Tube 1: 10-70 cc/min He, Tube 2: 85850 cc/min Air
http://www.porterinstrument.com/indust_21.php
Electronic Flow Meter
Preferred flow meter: Precision gas flow meter, flow range
5500 mL/min 5067-0223
ADM 1000 220-1170
ADM 2000 220-1171-U (Mass Flow Version)
Electronic "Mass" Flow Meter Flow Tracker
Model 1000 Flow Only 5183-4779
Model 2000 with Leak Detector 5183-4780
Universal Power Adapter 5183-4781
White Silicone Tubing:
4 meters 701-0016
7 cm 220-1179
PTFE tubing, 1/8-inch, 1 m long G1290-80050
740
7890 Series GC IPB
Illustrated Parts Breakdown
18
For Checking Inlet Pressure
Quality Analog Pressure Gauge (0-100 or 0-60 PSIG) adapted
with a Headspace Probe (301-013-HSP) need NPT adapter
0100-0118 and TCD Ferrules Set 5180-4103, 5182-9673,
5182-3477
Digital Pressure Gauge (0-100 PSIG) Omega Model
HHP-201 Adapted with 1/8-inch NPT adapter 0100-0111, SS
Capillary 5021-1831, Reducing Ferrule 0100-1342 and 530
uM Column Ferrule 5080-8773
NPD Flow adapter - G1534-60640
G1530-20610 - FID/NPD Jet Plug
"No-Hole" Column Ferrules 5181-7458
7890 Series GC IPB
741
18 Illustrated Parts Breakdown
FID Flow adapter - 19301-60660
5060-9055 uECD/TCD Detector Plug
Plastic 1/8-inch Swagelok Cap P/N 0100-2414 Qty 3
Replacement Septum Purge Fitting for EPC Module P/N
G2630-61720 (Not included in kit)
742
7890 Series GC IPB
Illustrated Parts Breakdown
18
Blanking plug, finger tight, 5020-8294. (Can be used with any
ferrule to duplicate using a no-hole ferrule.)
7890 Series GC IPB
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18 Illustrated Parts Breakdown
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7890 Series GC IPB