A.

Standar NaOH

Berat Oksalat = 0,63 gram

Volume = 100mL (labu ukur)

Volume HCl dipipet sebanyak 5mL

NaOH K (mS/cm)
No Rata - rata
(mL) Data 1 Data 2
1 0 1.74 1.62 1.68
2 1 1.34 1.29 1.315
3 2 1.23 0.89 1.06
4 3 1.11 0.66 0.885
5 4 0.76 0.73 0.745
6 4.2 0.77 0.74 0.755
7 4.4 0.84 0.81 0.825
8 4.6 0.92 0.83 0.875
9 4.8 0.96 0.86 0.91
10 5 1 0.88 0.94
11 5.2 1.03 0.93 0.98
12 5.4 1.08 0.99 1.035
13 5.6 1.15 1.02 1.085
14 5.8 1.22 1.08 1.15
15 6 1.3 1.11 1.205
 B. Penentuan konsentrasi CH3COOH 0,1 N

Volume CH3COOH = 5mL ( di pipet )

NaOH K (mS/cm)
No Rata - rata
(mL) Data 1 Data 2
1 0 0.15 0.15 0.15
2 0.2 0.14 0.14 0.14
3 0.4 0.13 0.14 0.135
4 0.6 0.15 0.13 0.14
5 0.8 0.17 0.16 0.165
6 1 0.19 0.18 0.185
7 1.2 0.21 0.2 0.205
8 1.4 0.25 0.23 0.24
9 1.6 0.28 0.25 0.265
10 1.8 0.33 0.3 0.315
11 2 0.35 0.35 0.35
12 2.2 0.38 0.38 0.38
13 2.4 0.41 0.43 0.42
14 2.6 0.44 0.46 0.45
15 2.8 0.47 0.48 0.475
 C. Penentuan konsentrasi CH3COOH 1 N

Volume CH3COOH = 5mL (di pipet)

NaOH K (mS/cm) Rata -

No
(mL) Data 1 Data 2 rata
1 0 0.5 0.49 0.495
2 1 0.44 0.44 0.44
3 1.2 0.43 0.43 0.43
4 1.4 0.45 0.44 0.445
5 1.6 0.46 0.45 0.455
6 1.8 0.47 0.46 0.465
7 2 0.48 0.47 0.475
8 2.2 0.53 0.48 0.505
9 2.4 0.56 0.5 0.53
10 2.6 0.59 0.52 0.555
11 2.8 0.61 0.54 0.575
12 3 0.63 0.56 0.595
13 4 0.73 0.65 0.69
14 5 0.81 0.72 0.765
15 6 0.96 0.9 0.93
D. Penentuan Konsentrasi HCl 0.1 N

NaOH K (mS/cm) Rata -

No
(mL) Data 1 Data 2 rata
1 0 3.65 3.99 3.82
2 1 3.26 3.49 3.375
3 2 2.68 2.89 2.785
4 3 2.23 2.26 2.245
5 4 1.71 1.64 1.675
6 4.2 1.6 1.6 1.6
7 4.4 1.3 1.51 1.405
8 4.6 1.28 1.45 1.365
9 4.8 1.26 1.4 1.33
10 5 1.16 1.35 1.255
11 5.2 1.12 1.3 1.21
12 5.4 1.1 1.23 1.165
13 5.6 1.07 1.19 1.13
14 5.8 1.08 1.2 1.14
15 6 1.09 1.24 1.165
16 1.23 1.35 1.29
17 8 1.67 1.7 1.685
Standarisasi NaOH

Standarisasi NaOH 0.1 N

1.8
1.6
Konduktivitas (mS/cm)

1.4
1.2
1
0.8
0.6
0.4
0.2
0
0 1 2 3 4 5 6 7
NaOH (mL)

Penentuan Konsentrasi CH3COOH 0.1 N

Penentuan konsentrasi CH3COOH 0.1 N

0.5
0.45
Konduktivitas (mS/cm)

0.4
0.35
0.3
0.25
0.2
0.15
0.1
0.05
0
0 0.5 1 1.5 2 2.5 3
NaOH (mL)
Penentuan konsentrasi CH3COOH 1 N

Penentuan Konsentrasi CH3COOH 1 N

1
0.9
Konduktivitas (mS/cm)

0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
0 1 2 3 4 5 6 7
NaOH (mL)

Penentuan Knsentrasi HCl 0.1 N

Penentuan konsentrasi HCl 0.1 N

4.5
4
3.5
Konduktivitas (mL)

3
2.5
2
1.5
1
0.5
0
0 1 2 3 4 5 6 7 8 9
NaOH (mL)
Perhitungan

A. Standarisasi NaOH

Berat oksalat = 0.63 gram (Mr = 126 )

Volume = 5 mL

V.NaOH x N. NaOH = V.oksalat x N.oksalat

N. NaOH = 5 mL x 0.1 N

4.2 mL

N. NaOH = 0.1190 N

B. Penentuan konsentrasi CH3COOH 0.1 N

Volume = 5 mL

V. CH3COOH x N. CH3COOH = V. NaOH x N. NaOH

= 0.8 x 0.1190

N. CH3COOH = 0.0190 N

C. Penentuan konsentrasi CH3COOH 1 N

Volume = 5 mL

V. CH3COOH x N. CH3COOH = V. NaOH x N. NaOH

= 1.6 x 0.1190

= 0.0380 N
D. Penentuan konsentrasi HCl 0.1 N

Volume = 5mL

V. HCl x N. HCl = V. NaOH x N. NaOH

= 5.8 x 0.1190

= 0.1380 N