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AREA 2500
Page 44 ~ J-826
9.0
FIRST AID
EYE: Immediate and continuous irrigation with flowing water for at least 30
minutes is imperative. Prompt medical consultation is essential.
SKIN: Wash off in flowing water or shower.
INGESTION: Do not induce vomiting. Give large amounts of water or milk if available
and transport to medical facility,
INHALATION: Remove to fresh air if effects occur. Consult a physician,
NOTE TO PHYSICIAN: May cause tissue destruction leading to stricture. If lavage
is performed, suggest endotracheal and/or esophageal
control. if burn is present, treat as any thermal bum, after
decontamination. No specific antidote. Supportive care,
‘Treatment based on judgment of the physician in response
to reaction of the patient.
imcr
AREA 2500
Page 45 — J-826
10.0 MATERIAL SAFETY DATA SHEETS
Attached are the material safety data sheets for the following items:
10.1 Dow Gas / Spec MDEA Sol4-826
AREA 2600
CONDENSATE STABILIZATION4-826
10
2.0
3.0
40
50
6.0
70
AREA 2600
CONDENSATE STABILIZATION
BLE OF CONTENTS
INTRODUCTION
PROCESS DESCRIPTION
2.1 Condensate Flash Drum
22 Condensate Preheat
23. Condensate Stabilizer
24 — Condensate Cooling and Storage
25 Residue Gas Compression
PREPARATION FOR INITIAL STARTUP
3.1 System Checkout
3.2 Purging the System
START-UP
41 Establish Circulation
42 Begin Recompression
NORMAL OPERATION
5.1 Key Operating Parameters
NORMAL SHUTDOWN
EMERGENCY/SAFETY SHUTDOWNJ-826
10
AREA 2600
CONDENSATE ST. ‘TION
INTRODUCTION
This manual covers the basic procedures for the commissioning, preparation, start-up,
normal operation, normal shutdown, and emergency shutdown of the Condensate
Stabilization Section, Area 2600. Since the Stabilization Section forms only a part of the
overall system, it is not possible for the basic procedures presented to cover all
operational contingencies. The information presented should be carefully reviewed by
‘operating personnel with respect to proper operator reactions to deviations and
difficulties, which will arise. All interconnections between Phase One and Phase Two,
reference the “Interconnections” sections at the beginning of this manual.AREA 2600
Page 2 - J-826
2.0 PROCESS DESCRIPTION
‘The process description can be better followed by referring to the P&l D's 826-D-6102-1
through 826-D-6102-7
‘The Condensate Stabilization section is designed to stabilize 31.14 m’thr (4700 BPD) of
condensate to a maximum Reid Vapor Pressure of 0.703 kg/cm’ (absolute).
24
Condensate Flash Drum
Condensate from V-2101 and V-2102 flows into one side of V-2601, the
Condensate Flash Drum. Liquid from V-2501, the amine unit inlet Separator also
is sent to this portion of the vessel. Another liquid feed stream is sent to the
other side of this flash drum from V-2103, the gas plant Cold Separator. An
overflow weir separates the two liquid sides of the vessel.
A splitrange pressure controller, PIC-26301, maintains the pressure in the flash
drum by controlling the flow of flashed vapor from V-2601 to V-2603, the
Interstage Scrubber (for K-2601) through PV-26301A, and to the flare via PV-
263018 if necessary. A high high pressure switch, PSHH-26302 is provided as a
safeguard. Upon activation, PSHH-26302 will cause a plant ESD to be
performed.
The side of V-2601 fed by the liquid from V-2103 contains a coalescer bed to
help separate entrained glycol from the liquid hydrocarbon phase. The
hydrocarbon phase level is controlled by a cascaded control loop where a level
controller LIC-26102 resets the set point of a flow controller FIC-26403 which
controls the flow of liquid to the top of T-2601, the Condensate Stabilizer via a
control valve, FV-26403. This loop provides a more stable flow of reflux to the
stabilizer than would straight level control, and therefore a more stable tower
operation. A low low level switch, LSLL-26105 has been provided as a
precaution, Upon activation, this switch will cause NV-26503 to close.(AREA covu
Page 3 — J-826
2.0 PROCESS DESCRIPTION - continued -
22
23
This side of the flash drum has a boot in which the aqueous glycol phase is
accumulated, The interface level in this boot is controlled by LIC-26103 and LV-
26103. A low low level switch, LSLL-26116 is provided as a precaution. Upon
activation, this switch causes NV-26506 to close; preventing hydrocarbon from
being sent to the Glyco! Unit.
‘The other side of the flash drum has only a hydrocarbon phase. Its level is
controlled by @ cascaded control loop where a level controller, LIC-26101, resets
the set point ofa flow controller, FIC-26402, which allows the liquid to flow as the
feed to T-2601, the Condensate Stabilizer, via a control valve, FV-26402. This
oop provides a more stable feed flow to the stabilizer than would straight level
Control, and therefore a more stable tower operation. A low low level switch,
LSLL-26104 is provided as a safeguard. Upon a
NV-26502 to close.
ion, this switch will cause
Condensate Preheat
The condensate leaving the flash drum via FV-26402 is heated by exchange with
stabilizer bottoms in €-2605 A/B, the Cold Condensate Preheater. Local
temperature indicators monitor the performance of this exchanger. Condensate
passes through the tubes of this exchanger and then on to E-2604, the
Condensate Preheater. Local temperature indicators monitor the performance of
this exchanger. The heated condensate then is fed to T-2601, the Condensate
Stabilizer. The stabilizer bottoms passes through the shell side of this exchanger
and then on to €-2605 A/B and on to AC-2608, the Condensate Cooler
Condensate Stabilizer
The Condensate Stabilizer, T-2601 is a fractionation column with a trayed section
below the feed and a packed section above the feed. The trayed section has 11
valve trays. Cold liquid from the flash drum via FV-26403 is fed at the top of thecr
2.0
AREA 2600
Page 4 ~ J-826
PROCESS DESCRIPTION ~ continued -
24
packed section to provide reflux for the Stabilizer. The high vapor pressure
components are fractionated out of the condensate and exit the top of T-2601 as
vapor. The top pressure of the tower during normal operation floats on the first
stage suction pressure of K-2601. If the Stabilizer off gas is to be flared,
pressure on the tower can be controlled by PIC-26303A and PV-26303A.
Overhead temperature of the Stabilizer is monitored by a DCS temperature
indicator, T-26202.
E-2601, the Condensate Stabilizer Reboiler, is a kettle reboiler that provides
vapor for the bottom fractionation section of the Stabilizer. Vapor is generated
from the condensate in the shell of the reboller by heat exchange with hot oil
flowing through the tubes of the reboiler, and returns to the column below the
bottom tray (11). The level in the surge section of the reboiler is controlled by
LIC-26106 and LV-26106 on the liquid outlet line from the reboiler. A low low
level switch, LSLL-26107 is provided as a safeguard. Upon activation this switch
will cause NV-26518 on the condensate line going to storage to close, thereby
preventing vapor from being introduced into the condensate storage tanks
Hot oil flow to the reboiler is controlled by a cascaded control loop with a
temperature controller TIC-26201, which resets the setpoint for a flow controller
FIC-26404, which controls the flow of hot oil through a control valve FV-26404 on
the hot oil supply line to E-2601. The temperature is measured in the trayed
section of T-2601.
Condensate Cooling and Storage
Stabilized condensate leaving the surge portion of E-2601 passes through the |
shell side of &-2604, the Condensate Preheater, and is cooled further by
exchanging heat with stabilizer feed in E-2605 AJB. It then is cooled to 49°C by
the Condensate Cooler, AC-2605, and air-cooled heat exchanger.
(@
PRrROrAc25
i
i
AREA 2600
Page 5 — J-826
2.0 PROCESS DESCRIPTION - continued -
The cooled and stabilized condensate now flows to TK-2601 A/B/C the
Condensate Storage Tanks. The tanks levels are DCS monitored by LI-26112
(TK-2601) and L1-26113 (TK-2601B), LI-26114 (TK-2601C). Temperature of the
condensate is DCS monitored by TI-26207 (TK-2601A), TI-26208 (TK-2601B),
TI-26209 (TK-2601C). Low Low Level Switches, LSLL-261 14 (TK-2601A), LSLL-
26115 (TK-260 B), LSLL-26118 (TK-2601C) have been provided as precautions.
Upon activation, these switches will cause the Condensate Booster Pumps, P-
601 AB, to shut off.
Residue Gas Compression
Gas leaving T-2601 flows to V-2602, the Inlet Scrubber for K-2601, the Residue
Gas Compressor. Entrained liquids are separated form the gas and are sent to
drain via a local level control loop. The scrubbed gas is then compressed by the
first stage of K-2601. It is then air cooled by AC-2602, the Interstage Gas
Cooler, and passes into V-2603, the Interstage Scrubber. Liquids condensed by
‘AC-2602 are separated from the gas and sent to T-2601 by a local level control
loop. The gas is then compressed by the second stage of K-2601 and is cooled
by AC-2603, the After Gas Cooler. The gas is then routed to either F-2101 or V-
2101NV-2102 (depending on which is in service) in the 2100 area.Page 6 - J-826
3.3.4
3.3.2
333
3.0 PREPARATION FOR INITIAL START-UP.
3.1 System Checkout
Following the completion of mechanical installation and electricallinstrument
interconnections to controls, the systems should be checked out and all
deficiencies corrected.
Inspect vessels internally as well as possible from manways and hand
holes. Remove any weld slag, dirt, debris, or any other foreign material
Check out all piping against the Petrofac PEID's and verify
3.3.2.1 All items are installed. All items and piping is of proper sizes and
pressure ratings.
3.3.2.2Control valves and check valves installed in the proper flow
direction
3.3.2.3 Relief valve nameplate settings are correct.
3.3.2.4 Free operation and travel of manual valves.
3.3.2.5 Removal of temporary braces and tie downs, if any.
Using compressed air, blow scale and dirt from piping as well as possible.
Pressure the system to 0.5 to 0.7 kg/cm*(g) (7-10 psig). Check all flanges
and connections for leaks with soap solution or other suitable means of
detection, Correct any leaks._
AREA 2600
Page 7 - J-826
3.3.4
3.3.5
3.36
334
3.32
3.0 PREPARATION FOR INITIAL START-UP — continued -
Install lubricants in pumps, compressors and motors as required. Verify
electric power supply to motors. Disconnect drivers and verify free
movement of pump and compressor shafts. “Bump “ motors to verify
correct rotation. Reinstall shaft couplings and verify correct alignment.
‘Check out instrumentation and controls
3.3.6.1 Verify proper installation and ranges for local pressure gauges
and temperature gauges.
3.35.2 Verify proper installation of orifice plates and thermocouples.
3.3.5.3 Verify installation and continuity of all interconnections between
the unit and control room.
3.3.5.4 Establish instrument air supply to all users.
3.3.5.5 Commission control loops and verify proper controller action,
calibrations, and control valve action/travel.
3.3.8.6Verity alarms and interlock actions, ESD system, ESD
instruments, and action of ESD valves and instrumentation.
Remove all unnecessary construction debris, scaffolding, and the like
from the unit area.
3.2 Purging the System
‘At this point, itis necessary to purge the air from the system. Before hydrocarbon
is introduced to the unit, it is important that oxygen be purged with an inert gas.
This protects against the formation of an explosive mixture.
‘A supply of inert gas for purging the unit must be available,
Make sure all hydrocarbon lines to the unit are blocked in.AREA 2600
Page 8 - J-826
3.23
3.24
3.25
3.0 PREPARATION FOR INITIAL START-UP - continued -
Introduce inert gas slowly to the equipment at convenient points.
Pressure the unit up to about 1.25 kg/cm?(g) (18 psig). Vent the inert gas
from all available equipment and piping extremities, so that all of the
equipment and piping are purged as well as possible. When venting the
inert gas/air, vent down to about 0.1 kg/em“(g) (1-2 psig). Close all vents,
and repeat inert gas pressurization/depressurization. Continue purging
Until oxygen content is below 1%, as measure with portable analyzers. It
will take approximately 4 to 6 purges to reduce the oxygen to less than
1%
If desired, the unit can be separated into several sections, and each
section purged individually
Warning - Do not vent the purge gases to the flare, as this could produce
an explosive or flammable mixture in the flare line.
When purging is complete, maintain the system at pressure for a pre-
determined amount of time for a leak test. If pressure decreases, look for
‘and correct any leaks. Note that ambient temperature fluctuations can
also cause slight pressure fluctuations in the system.
After leak testis complete, the equipment can be maintained at about 0.7,
kg/em*(g) (10 psig).AREA 2600
Page 9 — J-826
4.0 START-UP
44
Establish Circulation
‘The Stabilization Unit will need to be commissioned concurrently with the Gas
Plant since there are no temporary condensate storage facilities.
444
412
413
416
Ensure FIC-26402, FIC-26403, LIC-26103, and LIC-26106 are in manual
and the corresponding control valves closed.
Ensure all flare lines are open, and all required utilities are available.
Ensure that hot oil is available to start the reboiler, E-2601
Ensure that the block valve to V-2602 is closed, and a block vaive at PV-
26301A and the bypass are closed
Commission PIC-26301 and PIC-26303A and place
set at their normal set points.
automatic mode
(Once condensate is introduced from V-2101 or V-2102, a liquid level in V-
2601 will be indicated by LIC-26101. After it reaches the normal liquid
level, open FV-26402 25% and observe the effect on the level. Adjust
valve position until level is fairly stable, and then place LIC-26101 in
automatic. Similarly, when a liquid level is indicated by LIC-26102; open
FV-26403 25%, observe, adjust until stable, and then place LIC-26102 in
automatic.
Start the fans to AC-2605, the Condensate Cooler,AREA 2600
Page 10 - J-826
4.0 START-UP — continued -
4.1.7, Soon after opening FV-26402 a liquid level in E-2601, the Condensate
Stabilizer Reboiler, will be indicated by LIC-26106. Gradually start the
flow of hot oil to E-2601 by opening FV-26404 15%. Commission LIC-
26106 and place in automatic mode.
4.1.8 Gradually adjust the flow of hot oil to the reboiler until the temperature
indicated by TIC-26201 reaches 129°C; then place TIC-26201 in
automatic set at 129°C.
4.1.9. Check DCS instruments and local instruments to insure unit is operating
properly. Tune all control loops that need tuning. Take out any other
bypasses, which might have been used for start-up so that all
safeguarding instruments are functional
42 Begin Recompression
Once the Condensate Stabilizer is operating at its normal operating temperature
and pressure, the off gas from the tower can be recompressed and routed back
to the gas plant by K-2601, the Residue Gas Compressor.
4.2.1 Slowly open the inlet block valve to V-2602.
4.2.2. Ensure that the block valve on the inlet of V-2603 is open.
4.2.3. Start K-2601 following the procedure given in the manufacturer's
operation manual.
‘The unit should now be commissioned and operational.
®
PRTROFACAREA 2600
54
52
53
Page 11 — J-826
5.0 NORMAL OPERATION
It is important to monitor the unit regularly to make sure that all the temperatures,
pressures, flows, and levels are at their normal conditions. Prompt corrective action to
‘any abnormal condition will result in increased safety, less downtime, and more on-spec
product,
A listing of expected operating conditions at design capacity is included in Section 5.1
‘Some of the major items to be monitored by the operators are:
Stabilizer Pressure - The Stabilizer overhead pressure must remain constant for
stable tower operation and compressor operation.
Reboiler - The amount of reboiing in E-2601 is the key variable for the
fractionation achieved in the Condensate Stabilizer, and is generally controlled
by the flow rate of hot oil through FV-26404,
Operating parameters are affected by ambient conditions, condensate
compositions, etc. A listing of key operating variables with normal values is given
in Section 5.1, but these are not absolute, Also see the “Alarm and Trip List’, In
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JAREA 2600
Page 14 — J-826
6.0 NORMAL SHUTDOWN
The Condensate Stabilizer cannot be shut down independently from the Gas Plant
(Area2100). The following steps are to be performed during a normal (scheduled)
shutdown of the Gas Plant, but pertain only to the Condensate Stabilization section
(Area 2600).
6.1 Shut off K-2601 according to manufacturer's instructions and close the inlet block
valve to V-2602 and the black valve at PV-26301A,
6.2 Close a block valve at FV-26404, preventing flow of hot il
6.3 If the shutdown is for a short period, leave the control points for level controllers,
flow controllers, pressure controller, etc., at their current settings to facilitate start
up.
6.4 If equipment repairs are to be undertaken, isolation and cleaning of that piece of
equipment will be required. When cleaning equipment, steps to prevent loss of
condensate inventory should be taken first, and then preparation of the
equipment to reduce any hazard to a minimum should follow. Follow operations
standards for appropriate procedures for isolation, vessel entry, etc.
6.5 If the system is down for an extended period of time, the gas should be vented
down to minimum pressure and displaced with inert gas.
Permorac7.0
AREA 2600
Page 15 ~ J-826
Refer to the CauselEffect Diagrams for details of the shutdown systems.
Drawing 826-03-1-DL-850-1 A/B/C and Drawing 826-03-1-DL-850-2 AB
TA
a WN
Esp
‘An ESD can be initiated by any of several instruments in the facility, as well as
signals from outside of the unit from the master safety system. The ESD can also
be activated my pressing the ESD button in the control room or one of the field
locations should an emergency situation arise which necessitates such action
Operating personnel should verify levels and pressure and confirm they are in a
safe range. All ESD points have to be reset before starting plant
Interconnections for the ESD system between Phase One and Phase Two are
covered in the Cause and Effect DiagramsJ-826
AREA 2700
‘HOT OIL SYSTEMJ-826
1.0
20
3.0
40
5.0
6.0
70
AREA 2700
HOT OIL SYSTEM
TABLE OF CONTENTS
INTRODUCTION
PROCESS DESCRIPTION
2.1 Hot Oil Expansion Tank
2.2 Hot Oil Pumps
2.3 Hot Oil Filtration
24 Hot Oil Heater
2.5 Hot Oil Storage Tank
PREPARATION FOR INITIAL START-UP
3.1 System Checkout
3.2 Heater Dry-out
3.3 Purging the System
3.4 System Fill
START-UP
41 Establish Circulation
42 Start Hot Oil Heater
NORMAL OPERATION
5.1 Key Operating Parameters
NORMAL SHUTDOWN
EMERGENCY / SAFETY SHUTDOWN1.0
AREA 2700
HOT OIL SYSTEM
INTRODUCTION
‘This manual covers the basic procedures for the commissioning, preparation, start-up,
ormal operation, normal shutdown, and emergency shutdown of the Hot Oil System,
‘Area 2700. For interconnections between Phase One and Phase Two, reference the
“Interconnections” sections at the beginning of this manual,AREA 2700
Page 2 - J-826
2.0 PROCESS DESCRIPTION
The process description can be better followed by referring to the P&l D's 826-D-7102-1
‘Through 826-D-7102-6
‘The Hot Oil System is designed to provide a heat source for the process requirements of
the Glycol Reboiler (Area 2300), Amine Stripper Reboiler (Area 2500), Condensate
Stabilizer Reboiler (Area 2600), Gas Chiller Reclaimer (Area 2100/2800) and Fuel Gas
Heaters (Area 2900)
24
22
2.3
Hot Oil Expansion Tank
‘The heating medium used in this system, Chemtherm 550, is collected in a
horizontal vessel V-2701, the Hot Oil Expansion Tank. The vessel is blanketed
with natural gas and held at a positive pressure by PCV-2701 and PCV-2702.
This vessel provides surge volume for the hot oil system, and is not level
controlled. The vessel is protected from overpressure by a relief valve PSV-2703
which discharges to the flare header.
Hot Oil Circulation Pumps
Circulation of the Chemtherm 550 heating medium through the Hot Oil System is
achieved by the operation of the Hot Oil Circulation Pumps, P-2701 B/C
Minimum flow protection for these pumps is provided by a recycle line to V-2701
controlled by FIC-27403 and FV-27403,
Hot
iltration
A slipstream of the hot oil is taken from the discharge of P-2701 A/B/C and
routed through F-2701, the Hot Oil Filter. Degradation products and other
impurities are filtered out of the hot oil by this device. A differential pressure
indicator, PDI-27301 provides DCS monitoring of the pressure drop through this,
filter.24
25
Page 3-J-826
2.0 PROCESS DESCRIPTION - continued -
Hot Ol H
The Chemtherm 550 heating medium is heated to its hot supply temperature by
the Hot Oil Heaters, H-2701 A/B, H-2701 AVB are two pass, gas-fired vertical
cylindrical heater. Flow through each pass is flow controlled by a throttling valve,
FV-27401/2 or FV-27405I6 on the inlet piping to each pass. DCS flow indication
and control for each pass are provided by FIC-27401, FIC-27402, FIC-27405 and
FIC-27406
The outlet temperature of the hot oil is controlled by TIC-27205, which resets
FIC-27404, which controls the flow of fuel gas to the H-2701A burners through
FV-27404, TIC-27209, FIC-27407 and FV-27407 for H-2701B are the same as
for H-2701A. A portion of the hot oil flows to the Condensate Stabilizer Reboiler,
which requires @ hotter oil temperature than the other hot oil users. The lower
temperature of the rest of the oil is controlled by TIC-27207, which controls the
flow of cold oil bypassing H-2701 A/B and mixing with the rest of the hot oil
leaving H-2701A,B.
Hot Oil Storage Tank
‘An atmospheric storage tank TK-2701, the Hot Oil Storage Tank, is provided to
store additional hot oil inventory. Local level and temperature indication are
provided for this tank.AREA 2700
Page 4 — J-826
3.0 PREPARATION FOR INITIAL START-UP
34
‘System Checkout
Following the completion of mechanical installation and electrical/instrument
interconnections to controls, the systems should be checked out and all
deficiencies corrected,
344
Inspect vessels internally as well as possible from manways and hand
holes. Remove any weld slag, dirt, debris, or any other foreign material
Check out all piping against the Petrofac P&ID's and verity
3.1.2.1 All tems are installed. All items and piping is of proper sizes and
pressure ratings.
3.1.2.2Control valves and check valves installed in the proper flow
direction,
3.1.2.3 Relief valve nameplate settings are correct
3.1.2.4 Free operation and travel of manual valves.
3.1.2.5 Removal of temporary braces and tie downs, if any.
Verify all fiter media is on hand. Remove filter media for all filters. These
will be reinstalled after cleaning.
Using compressed air, blow scale and dirt from piping as well as possible.
Pressure the system to 0.5 to 0.7 kg/cm*(g) (7-10 psig). Check all flanges
and connections for leaks with soap solution or other suitable means of
detection. Correct any leaks.
Install lubricants in pumps and motors as required. Verify electric power
supply to motors. Disconnect drivers and verify free movement of pump
shafts. “Bump " motors to verify correct rotation. Reinstall shaft couplings
‘and verify correct alignment.