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Amine System-Condensate Stabilization-Hot Oil System

5.- Amine System-Condensate Stabilization-Hot oil system
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0% found this document useful (0 votes)
336 views25 pages

Amine System-Condensate Stabilization-Hot Oil System

5.- Amine System-Condensate Stabilization-Hot oil system
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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AREA 2500 Page 44 ~ J-826 9.0 FIRST AID EYE: Immediate and continuous irrigation with flowing water for at least 30 minutes is imperative. Prompt medical consultation is essential. SKIN: Wash off in flowing water or shower. INGESTION: Do not induce vomiting. Give large amounts of water or milk if available and transport to medical facility, INHALATION: Remove to fresh air if effects occur. Consult a physician, NOTE TO PHYSICIAN: May cause tissue destruction leading to stricture. If lavage is performed, suggest endotracheal and/or esophageal control. if burn is present, treat as any thermal bum, after decontamination. No specific antidote. Supportive care, ‘Treatment based on judgment of the physician in response to reaction of the patient. im cr AREA 2500 Page 45 — J-826 10.0 MATERIAL SAFETY DATA SHEETS Attached are the material safety data sheets for the following items: 10.1 Dow Gas / Spec MDEA Sol 4-826 AREA 2600 CONDENSATE STABILIZATION 4-826 10 2.0 3.0 40 50 6.0 70 AREA 2600 CONDENSATE STABILIZATION BLE OF CONTENTS INTRODUCTION PROCESS DESCRIPTION 2.1 Condensate Flash Drum 22 Condensate Preheat 23. Condensate Stabilizer 24 — Condensate Cooling and Storage 25 Residue Gas Compression PREPARATION FOR INITIAL STARTUP 3.1 System Checkout 3.2 Purging the System START-UP 41 Establish Circulation 42 Begin Recompression NORMAL OPERATION 5.1 Key Operating Parameters NORMAL SHUTDOWN EMERGENCY/SAFETY SHUTDOWN J-826 10 AREA 2600 CONDENSATE ST. ‘TION INTRODUCTION This manual covers the basic procedures for the commissioning, preparation, start-up, normal operation, normal shutdown, and emergency shutdown of the Condensate Stabilization Section, Area 2600. Since the Stabilization Section forms only a part of the overall system, it is not possible for the basic procedures presented to cover all operational contingencies. The information presented should be carefully reviewed by ‘operating personnel with respect to proper operator reactions to deviations and difficulties, which will arise. All interconnections between Phase One and Phase Two, reference the “Interconnections” sections at the beginning of this manual. AREA 2600 Page 2 - J-826 2.0 PROCESS DESCRIPTION ‘The process description can be better followed by referring to the P&l D's 826-D-6102-1 through 826-D-6102-7 ‘The Condensate Stabilization section is designed to stabilize 31.14 m’thr (4700 BPD) of condensate to a maximum Reid Vapor Pressure of 0.703 kg/cm’ (absolute). 24 Condensate Flash Drum Condensate from V-2101 and V-2102 flows into one side of V-2601, the Condensate Flash Drum. Liquid from V-2501, the amine unit inlet Separator also is sent to this portion of the vessel. Another liquid feed stream is sent to the other side of this flash drum from V-2103, the gas plant Cold Separator. An overflow weir separates the two liquid sides of the vessel. A splitrange pressure controller, PIC-26301, maintains the pressure in the flash drum by controlling the flow of flashed vapor from V-2601 to V-2603, the Interstage Scrubber (for K-2601) through PV-26301A, and to the flare via PV- 263018 if necessary. A high high pressure switch, PSHH-26302 is provided as a safeguard. Upon activation, PSHH-26302 will cause a plant ESD to be performed. The side of V-2601 fed by the liquid from V-2103 contains a coalescer bed to help separate entrained glycol from the liquid hydrocarbon phase. The hydrocarbon phase level is controlled by a cascaded control loop where a level controller LIC-26102 resets the set point of a flow controller FIC-26403 which controls the flow of liquid to the top of T-2601, the Condensate Stabilizer via a control valve, FV-26403. This loop provides a more stable flow of reflux to the stabilizer than would straight level control, and therefore a more stable tower operation. A low low level switch, LSLL-26105 has been provided as a precaution, Upon activation, this switch will cause NV-26503 to close. (AREA covu Page 3 — J-826 2.0 PROCESS DESCRIPTION - continued - 22 23 This side of the flash drum has a boot in which the aqueous glycol phase is accumulated, The interface level in this boot is controlled by LIC-26103 and LV- 26103. A low low level switch, LSLL-26116 is provided as a precaution. Upon activation, this switch causes NV-26506 to close; preventing hydrocarbon from being sent to the Glyco! Unit. ‘The other side of the flash drum has only a hydrocarbon phase. Its level is controlled by @ cascaded control loop where a level controller, LIC-26101, resets the set point ofa flow controller, FIC-26402, which allows the liquid to flow as the feed to T-2601, the Condensate Stabilizer, via a control valve, FV-26402. This oop provides a more stable feed flow to the stabilizer than would straight level Control, and therefore a more stable tower operation. A low low level switch, LSLL-26104 is provided as a safeguard. Upon a NV-26502 to close. ion, this switch will cause Condensate Preheat The condensate leaving the flash drum via FV-26402 is heated by exchange with stabilizer bottoms in €-2605 A/B, the Cold Condensate Preheater. Local temperature indicators monitor the performance of this exchanger. Condensate passes through the tubes of this exchanger and then on to E-2604, the Condensate Preheater. Local temperature indicators monitor the performance of this exchanger. The heated condensate then is fed to T-2601, the Condensate Stabilizer. The stabilizer bottoms passes through the shell side of this exchanger and then on to €-2605 A/B and on to AC-2608, the Condensate Cooler Condensate Stabilizer The Condensate Stabilizer, T-2601 is a fractionation column with a trayed section below the feed and a packed section above the feed. The trayed section has 11 valve trays. Cold liquid from the flash drum via FV-26403 is fed at the top of the cr 2.0 AREA 2600 Page 4 ~ J-826 PROCESS DESCRIPTION ~ continued - 24 packed section to provide reflux for the Stabilizer. The high vapor pressure components are fractionated out of the condensate and exit the top of T-2601 as vapor. The top pressure of the tower during normal operation floats on the first stage suction pressure of K-2601. If the Stabilizer off gas is to be flared, pressure on the tower can be controlled by PIC-26303A and PV-26303A. Overhead temperature of the Stabilizer is monitored by a DCS temperature indicator, T-26202. E-2601, the Condensate Stabilizer Reboiler, is a kettle reboiler that provides vapor for the bottom fractionation section of the Stabilizer. Vapor is generated from the condensate in the shell of the reboller by heat exchange with hot oil flowing through the tubes of the reboiler, and returns to the column below the bottom tray (11). The level in the surge section of the reboiler is controlled by LIC-26106 and LV-26106 on the liquid outlet line from the reboiler. A low low level switch, LSLL-26107 is provided as a safeguard. Upon activation this switch will cause NV-26518 on the condensate line going to storage to close, thereby preventing vapor from being introduced into the condensate storage tanks Hot oil flow to the reboiler is controlled by a cascaded control loop with a temperature controller TIC-26201, which resets the setpoint for a flow controller FIC-26404, which controls the flow of hot oil through a control valve FV-26404 on the hot oil supply line to E-2601. The temperature is measured in the trayed section of T-2601. Condensate Cooling and Storage Stabilized condensate leaving the surge portion of E-2601 passes through the | shell side of &-2604, the Condensate Preheater, and is cooled further by exchanging heat with stabilizer feed in E-2605 AJB. It then is cooled to 49°C by the Condensate Cooler, AC-2605, and air-cooled heat exchanger. (@ PRrROrAc 25 i i AREA 2600 Page 5 — J-826 2.0 PROCESS DESCRIPTION - continued - The cooled and stabilized condensate now flows to TK-2601 A/B/C the Condensate Storage Tanks. The tanks levels are DCS monitored by LI-26112 (TK-2601) and L1-26113 (TK-2601B), LI-26114 (TK-2601C). Temperature of the condensate is DCS monitored by TI-26207 (TK-2601A), TI-26208 (TK-2601B), TI-26209 (TK-2601C). Low Low Level Switches, LSLL-261 14 (TK-2601A), LSLL- 26115 (TK-260 B), LSLL-26118 (TK-2601C) have been provided as precautions. Upon activation, these switches will cause the Condensate Booster Pumps, P- 601 AB, to shut off. Residue Gas Compression Gas leaving T-2601 flows to V-2602, the Inlet Scrubber for K-2601, the Residue Gas Compressor. Entrained liquids are separated form the gas and are sent to drain via a local level control loop. The scrubbed gas is then compressed by the first stage of K-2601. It is then air cooled by AC-2602, the Interstage Gas Cooler, and passes into V-2603, the Interstage Scrubber. Liquids condensed by ‘AC-2602 are separated from the gas and sent to T-2601 by a local level control loop. The gas is then compressed by the second stage of K-2601 and is cooled by AC-2603, the After Gas Cooler. The gas is then routed to either F-2101 or V- 2101NV-2102 (depending on which is in service) in the 2100 area. Page 6 - J-826 3.3.4 3.3.2 333 3.0 PREPARATION FOR INITIAL START-UP. 3.1 System Checkout Following the completion of mechanical installation and electricallinstrument interconnections to controls, the systems should be checked out and all deficiencies corrected. Inspect vessels internally as well as possible from manways and hand holes. Remove any weld slag, dirt, debris, or any other foreign material Check out all piping against the Petrofac PEID's and verify 3.3.2.1 All items are installed. All items and piping is of proper sizes and pressure ratings. 3.3.2.2Control valves and check valves installed in the proper flow direction 3.3.2.3 Relief valve nameplate settings are correct. 3.3.2.4 Free operation and travel of manual valves. 3.3.2.5 Removal of temporary braces and tie downs, if any. Using compressed air, blow scale and dirt from piping as well as possible. Pressure the system to 0.5 to 0.7 kg/cm*(g) (7-10 psig). Check all flanges and connections for leaks with soap solution or other suitable means of detection, Correct any leaks. _ AREA 2600 Page 7 - J-826 3.3.4 3.3.5 3.36 334 3.32 3.0 PREPARATION FOR INITIAL START-UP — continued - Install lubricants in pumps, compressors and motors as required. Verify electric power supply to motors. Disconnect drivers and verify free movement of pump and compressor shafts. “Bump “ motors to verify correct rotation. Reinstall shaft couplings and verify correct alignment. ‘Check out instrumentation and controls 3.3.6.1 Verify proper installation and ranges for local pressure gauges and temperature gauges. 3.35.2 Verify proper installation of orifice plates and thermocouples. 3.3.5.3 Verify installation and continuity of all interconnections between the unit and control room. 3.3.5.4 Establish instrument air supply to all users. 3.3.5.5 Commission control loops and verify proper controller action, calibrations, and control valve action/travel. 3.3.8.6Verity alarms and interlock actions, ESD system, ESD instruments, and action of ESD valves and instrumentation. Remove all unnecessary construction debris, scaffolding, and the like from the unit area. 3.2 Purging the System ‘At this point, itis necessary to purge the air from the system. Before hydrocarbon is introduced to the unit, it is important that oxygen be purged with an inert gas. This protects against the formation of an explosive mixture. ‘A supply of inert gas for purging the unit must be available, Make sure all hydrocarbon lines to the unit are blocked in. AREA 2600 Page 8 - J-826 3.23 3.24 3.25 3.0 PREPARATION FOR INITIAL START-UP - continued - Introduce inert gas slowly to the equipment at convenient points. Pressure the unit up to about 1.25 kg/cm?(g) (18 psig). Vent the inert gas from all available equipment and piping extremities, so that all of the equipment and piping are purged as well as possible. When venting the inert gas/air, vent down to about 0.1 kg/em“(g) (1-2 psig). Close all vents, and repeat inert gas pressurization/depressurization. Continue purging Until oxygen content is below 1%, as measure with portable analyzers. It will take approximately 4 to 6 purges to reduce the oxygen to less than 1% If desired, the unit can be separated into several sections, and each section purged individually Warning - Do not vent the purge gases to the flare, as this could produce an explosive or flammable mixture in the flare line. When purging is complete, maintain the system at pressure for a pre- determined amount of time for a leak test. If pressure decreases, look for ‘and correct any leaks. Note that ambient temperature fluctuations can also cause slight pressure fluctuations in the system. After leak testis complete, the equipment can be maintained at about 0.7, kg/em*(g) (10 psig). AREA 2600 Page 9 — J-826 4.0 START-UP 44 Establish Circulation ‘The Stabilization Unit will need to be commissioned concurrently with the Gas Plant since there are no temporary condensate storage facilities. 444 412 413 416 Ensure FIC-26402, FIC-26403, LIC-26103, and LIC-26106 are in manual and the corresponding control valves closed. Ensure all flare lines are open, and all required utilities are available. Ensure that hot oil is available to start the reboiler, E-2601 Ensure that the block valve to V-2602 is closed, and a block vaive at PV- 26301A and the bypass are closed Commission PIC-26301 and PIC-26303A and place set at their normal set points. automatic mode (Once condensate is introduced from V-2101 or V-2102, a liquid level in V- 2601 will be indicated by LIC-26101. After it reaches the normal liquid level, open FV-26402 25% and observe the effect on the level. Adjust valve position until level is fairly stable, and then place LIC-26101 in automatic. Similarly, when a liquid level is indicated by LIC-26102; open FV-26403 25%, observe, adjust until stable, and then place LIC-26102 in automatic. Start the fans to AC-2605, the Condensate Cooler, AREA 2600 Page 10 - J-826 4.0 START-UP — continued - 4.1.7, Soon after opening FV-26402 a liquid level in E-2601, the Condensate Stabilizer Reboiler, will be indicated by LIC-26106. Gradually start the flow of hot oil to E-2601 by opening FV-26404 15%. Commission LIC- 26106 and place in automatic mode. 4.1.8 Gradually adjust the flow of hot oil to the reboiler until the temperature indicated by TIC-26201 reaches 129°C; then place TIC-26201 in automatic set at 129°C. 4.1.9. Check DCS instruments and local instruments to insure unit is operating properly. Tune all control loops that need tuning. Take out any other bypasses, which might have been used for start-up so that all safeguarding instruments are functional 42 Begin Recompression Once the Condensate Stabilizer is operating at its normal operating temperature and pressure, the off gas from the tower can be recompressed and routed back to the gas plant by K-2601, the Residue Gas Compressor. 4.2.1 Slowly open the inlet block valve to V-2602. 4.2.2. Ensure that the block valve on the inlet of V-2603 is open. 4.2.3. Start K-2601 following the procedure given in the manufacturer's operation manual. ‘The unit should now be commissioned and operational. ® PRTROFAC AREA 2600 54 52 53 Page 11 — J-826 5.0 NORMAL OPERATION It is important to monitor the unit regularly to make sure that all the temperatures, pressures, flows, and levels are at their normal conditions. Prompt corrective action to ‘any abnormal condition will result in increased safety, less downtime, and more on-spec product, A listing of expected operating conditions at design capacity is included in Section 5.1 ‘Some of the major items to be monitored by the operators are: Stabilizer Pressure - The Stabilizer overhead pressure must remain constant for stable tower operation and compressor operation. Reboiler - The amount of reboiing in E-2601 is the key variable for the fractionation achieved in the Condensate Stabilizer, and is generally controlled by the flow rate of hot oil through FV-26404, Operating parameters are affected by ambient conditions, condensate compositions, etc. A listing of key operating variables with normal values is given in Section 5.1, but these are not absolute, Also see the “Alarm and Trip List’, In ‘Appendix 1 sa werd e esned Locee-nd (6),u0/64] Loree ainssoid | __ ww 2ocaz-HHsa) loner uBIy UB v|_pue Lorez-old 10 uoNesedo Hey] (6),woEX0Z~| gor | -Old Lose-n| 7 nus o1giy 1ogrd osneo wa jonoimormory| | teas cnon | moscror | risgzr| 9 tose rr anys 01 FY Lord 2sne9 jn Jono} I Ho! | oso | aos ros | tise] erviose-i 0192-11 pue so1sz| "140 uoneiode yo0ud "fes8800u 2809 01 81S92-AN o5ne UM ona MOLNOI y|_jfoIUED eMUeU LO goLSz-ATeDRIA| _% OBS | _%605 | goL92-011 -opoGou L09e-3 co197-11 pue goisz| jor} a06y011) -o1140 uoyerade vaoup -Aress009u yoo8 wu) {2808 01 862-AN asneo WM onal NoLMoIy| _jroueD eMuew vo goLsz-nTeDRIa| swszosz | %605 | soLse-orn| seis O82" (083 W214 @ asne ion UE £O1Z-A Pooy Aijenjuans jym jana] YBIY y| ‘ZOL9z-11 Pue ZOLS2| ayesuapu09| -o1140 uoyesado spot e380 eo wna 280)9 01 €0G02-AN o6n29 NM or9] NO} MoI OaUED MOY eUEW UO COPOE-Ad e0eIal _Kosci01 | wos _|zoL9z-o11} _useld Looe-A queid se6 ou) 0} J9[u! 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The following steps are to be performed during a normal (scheduled) shutdown of the Gas Plant, but pertain only to the Condensate Stabilization section (Area 2600). 6.1 Shut off K-2601 according to manufacturer's instructions and close the inlet block valve to V-2602 and the black valve at PV-26301A, 6.2 Close a block valve at FV-26404, preventing flow of hot il 6.3 If the shutdown is for a short period, leave the control points for level controllers, flow controllers, pressure controller, etc., at their current settings to facilitate start up. 6.4 If equipment repairs are to be undertaken, isolation and cleaning of that piece of equipment will be required. When cleaning equipment, steps to prevent loss of condensate inventory should be taken first, and then preparation of the equipment to reduce any hazard to a minimum should follow. Follow operations standards for appropriate procedures for isolation, vessel entry, etc. 6.5 If the system is down for an extended period of time, the gas should be vented down to minimum pressure and displaced with inert gas. Permorac 7.0 AREA 2600 Page 15 ~ J-826 Refer to the CauselEffect Diagrams for details of the shutdown systems. Drawing 826-03-1-DL-850-1 A/B/C and Drawing 826-03-1-DL-850-2 AB TA a WN Esp ‘An ESD can be initiated by any of several instruments in the facility, as well as signals from outside of the unit from the master safety system. The ESD can also be activated my pressing the ESD button in the control room or one of the field locations should an emergency situation arise which necessitates such action Operating personnel should verify levels and pressure and confirm they are in a safe range. All ESD points have to be reset before starting plant Interconnections for the ESD system between Phase One and Phase Two are covered in the Cause and Effect Diagrams J-826 AREA 2700 ‘HOT OIL SYSTEM J-826 1.0 20 3.0 40 5.0 6.0 70 AREA 2700 HOT OIL SYSTEM TABLE OF CONTENTS INTRODUCTION PROCESS DESCRIPTION 2.1 Hot Oil Expansion Tank 2.2 Hot Oil Pumps 2.3 Hot Oil Filtration 24 Hot Oil Heater 2.5 Hot Oil Storage Tank PREPARATION FOR INITIAL START-UP 3.1 System Checkout 3.2 Heater Dry-out 3.3 Purging the System 3.4 System Fill START-UP 41 Establish Circulation 42 Start Hot Oil Heater NORMAL OPERATION 5.1 Key Operating Parameters NORMAL SHUTDOWN EMERGENCY / SAFETY SHUTDOWN 1.0 AREA 2700 HOT OIL SYSTEM INTRODUCTION ‘This manual covers the basic procedures for the commissioning, preparation, start-up, ormal operation, normal shutdown, and emergency shutdown of the Hot Oil System, ‘Area 2700. For interconnections between Phase One and Phase Two, reference the “Interconnections” sections at the beginning of this manual, AREA 2700 Page 2 - J-826 2.0 PROCESS DESCRIPTION The process description can be better followed by referring to the P&l D's 826-D-7102-1 ‘Through 826-D-7102-6 ‘The Hot Oil System is designed to provide a heat source for the process requirements of the Glycol Reboiler (Area 2300), Amine Stripper Reboiler (Area 2500), Condensate Stabilizer Reboiler (Area 2600), Gas Chiller Reclaimer (Area 2100/2800) and Fuel Gas Heaters (Area 2900) 24 22 2.3 Hot Oil Expansion Tank ‘The heating medium used in this system, Chemtherm 550, is collected in a horizontal vessel V-2701, the Hot Oil Expansion Tank. The vessel is blanketed with natural gas and held at a positive pressure by PCV-2701 and PCV-2702. This vessel provides surge volume for the hot oil system, and is not level controlled. The vessel is protected from overpressure by a relief valve PSV-2703 which discharges to the flare header. Hot Oil Circulation Pumps Circulation of the Chemtherm 550 heating medium through the Hot Oil System is achieved by the operation of the Hot Oil Circulation Pumps, P-2701 B/C Minimum flow protection for these pumps is provided by a recycle line to V-2701 controlled by FIC-27403 and FV-27403, Hot iltration A slipstream of the hot oil is taken from the discharge of P-2701 A/B/C and routed through F-2701, the Hot Oil Filter. Degradation products and other impurities are filtered out of the hot oil by this device. A differential pressure indicator, PDI-27301 provides DCS monitoring of the pressure drop through this, filter. 24 25 Page 3-J-826 2.0 PROCESS DESCRIPTION - continued - Hot Ol H The Chemtherm 550 heating medium is heated to its hot supply temperature by the Hot Oil Heaters, H-2701 A/B, H-2701 AVB are two pass, gas-fired vertical cylindrical heater. Flow through each pass is flow controlled by a throttling valve, FV-27401/2 or FV-27405I6 on the inlet piping to each pass. DCS flow indication and control for each pass are provided by FIC-27401, FIC-27402, FIC-27405 and FIC-27406 The outlet temperature of the hot oil is controlled by TIC-27205, which resets FIC-27404, which controls the flow of fuel gas to the H-2701A burners through FV-27404, TIC-27209, FIC-27407 and FV-27407 for H-2701B are the same as for H-2701A. A portion of the hot oil flows to the Condensate Stabilizer Reboiler, which requires @ hotter oil temperature than the other hot oil users. The lower temperature of the rest of the oil is controlled by TIC-27207, which controls the flow of cold oil bypassing H-2701 A/B and mixing with the rest of the hot oil leaving H-2701A,B. Hot Oil Storage Tank ‘An atmospheric storage tank TK-2701, the Hot Oil Storage Tank, is provided to store additional hot oil inventory. Local level and temperature indication are provided for this tank. AREA 2700 Page 4 — J-826 3.0 PREPARATION FOR INITIAL START-UP 34 ‘System Checkout Following the completion of mechanical installation and electrical/instrument interconnections to controls, the systems should be checked out and all deficiencies corrected, 344 Inspect vessels internally as well as possible from manways and hand holes. Remove any weld slag, dirt, debris, or any other foreign material Check out all piping against the Petrofac P&ID's and verity 3.1.2.1 All tems are installed. All items and piping is of proper sizes and pressure ratings. 3.1.2.2Control valves and check valves installed in the proper flow direction, 3.1.2.3 Relief valve nameplate settings are correct 3.1.2.4 Free operation and travel of manual valves. 3.1.2.5 Removal of temporary braces and tie downs, if any. Verify all fiter media is on hand. Remove filter media for all filters. These will be reinstalled after cleaning. Using compressed air, blow scale and dirt from piping as well as possible. Pressure the system to 0.5 to 0.7 kg/cm*(g) (7-10 psig). Check all flanges and connections for leaks with soap solution or other suitable means of detection. Correct any leaks. Install lubricants in pumps and motors as required. Verify electric power supply to motors. Disconnect drivers and verify free movement of pump shafts. “Bump " motors to verify correct rotation. Reinstall shaft couplings ‘and verify correct alignment.

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