Faculty of Engineering
Petroleum Engineering Department
Oil properties Laboratory, 2nd stage
Experiment No. (6)
Flash and Fire Points by Pensky-Martens Closed
Cup Tester
Prepared by: Brosk Frya Ali
17/11/2013
11/25/2013
Aim of the experiment
• Classify the petroleum according to its flash point.
• Indicate how light or heavy the petroleum is.
• Find the best conditions for transporting & storing
petroleum products, to avoid any damages by the
temperature rise.
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INTRODUCTION
This flash point and fire point test method is a dynamic method
and depends on definite rates of temperature increases to control
the precision of the test method. Its primary use is for viscous
materials having flash point of 79°C (175°F) and above.
It is also used to determine fire point, which is a temperature
above the flash point, at which the test specimen will support
combustion for a minimum of 5 sec.
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Flash point
It is the lowest temperature at which sufficient vapor is
produced above the liquid to form a mixture with air that a
natural ignition can occur if a spark is present.
The flash point of a liquid hydrocarbon or an oil fraction
indicates its fire and explosion potential.
Liquids with a flash point less than 60.5 0C or 37.8 0C
depending on standard been applied are considered flammable,
while liquids with a flash point above those temperatures are
considered combustible.
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Fire point
It is the lowest temperature at which sufficient vapor is
produced above the liquid to form a mixture with air that a
flam can occur for (5) seconds if a spark is present.
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ASTM’s Flash Point Standards
The first ASTM standard for flash point was published in 1918
(1) as D 56, Test Method for Flash Point by Tag Closed Cup
Tester. Just three years later, two more flash point test methods
were published: D 92, Test Method for Flash Point by Cleveland
Open Cup Tester, and D 93, Test Method for Flash Point by
Pensky-Martens Closed Cup Tester. All three of these standards
are still in frequent use, with D 93 as the most prevalent, and the
one most often cited in regulations and specifications.
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Figure 1: General appearance.
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Apparatus
1- Cup of sample.
2- Thermometer.
3- Covering.
a- Constant cover. b- moving cover. c- exposing flame
system. d- permanent flame. e- movable means.
4- Heating.
a- air bath. b- upper plate.
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Discussion Section
1. Discuss the reasons of any error happened during the Exp.
And how can be corrected?
2. What is the advantage of flash & fire points?
3. Why the cup must be cleaned & dried before starting the
exp.?
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