‘act ts mth a Sa a ta Ay Designation: 113-14 (Reapproved 2018) Standard Test Method for Reheat Change of Refractory Brick’ onl sa pre ae US Dae of fe Scape | This test method cover the determination ofthe pa nei near change of refractory brick. when heated under presribed cones. 1.2 The vals ltd inch pound vi att erga 2 anda. The als sve in paenteses ae raematcl ners to St nis that re provi for ison ly fae ot consid sandr sgn manis pes he wg Tet Mb inven and 13 This onda does nor parpor 1 adres all of the safety concern, If amy osoctaed ith es wae I 8 the respons of he wer of hs sendrd to etl appre rae safer hee and enviromental practces and deter ‘nine the aplicbiiy of elroy natn pir tows. 1 This international sno war developed aor dace with ternational vecognced principle standard {anton extalshed in the Decision Principles forthe Development of Ieretiona Stndais, Guides and Recon inendtions ve by the Word Tade Oration Tehntcal ‘Berrie o Trade (TBI) Commitee 2, Referenced Documents 21 ASMA Standards? C131 Tes Methods for Sve, Dimersonal Measuren=as, fed Bulk Density of Refractory Back and Insulating rec (C179 Tet Med for Ding an Ping Linear Change of Retraction Pati aod Ranming Mix Specinens (e's Meth! foe Retest Chae eating Peck ‘CaS Tet Method for Reheat Change of Facay Nezles a a "Fr in pe Ne 31 ad Mae 29% Ons SR pe i 0 te ams AST Cnc Sens eee Tea ol of TN and Sleeves (Widow 1997? EDMVEDIM Speciation for Temperture lecomatine oes (emf Tables for Stanrdied Themacoples 3 Sigicance and Use 5.1 Refacory rick and shapes of dieeat compositions iba onigne permanent liner changes alr beating ‘hating This et method provides a standard pocedae for Tring anus cies of tacos with appropiate heating 32 Liner rlet changes blind by his est method are ‘stable for as in esenrch and development ao ofen edo ‘xablsh wen seitetons between prodicers and £00 2.3 Cate sold be exected i seletng samples that are ‘epreseitive of he predt Seng esta ha he chee ‘elected arpropra othe produc 44 Apparatus 4.1 Kil of sch denon ta the specif heating schele snd smopere can be tani trout the heating 42 Linear Measuring Device, capable of being read t0 (002. (0.3m) over spa of 10 (254 mm). A ook rue, ts spied i Tat Mths C134, vermin caliper, oe tae device nay be use 43 Gus Sampling and Anais Eqvoment, cable of eterning the prea ee oxygen and oa comune In the atmonpereo the est chanbe. 5, Test Specimens 51 Ferenc et se thee rectangular specimens messing 9 by 4vsty Borin, 24 by 1189 to 76 mann ie rif sale shapes approaching ese dimensions a chosly {posse These maybe corel ick of he specied ‘Seto tes pcos cto of lee shapes. 452 Using ceramic pit rayon, abe each specimen, and rake aefercace mak a cach enon the center be fa oad it pn wi fi tcl i wend 2Gy c113 14 (2019) facet indent he exact poitlon whee the resumen is mal. Meas he length On each he the est specie {othe nesest O02 in (0.3 rn. 6, Procedure 64 Placing Specimens in Klr—Place the est spcinens i the ils tat each rests edgwis, that i, on 29 by 218 ‘in, (28 by 6 or 76m) face ad only ot couse hgh, Place each spcinen upon ie conesponging face of pp Tes of equlreactorness Place bcween the fest specimen andthe sopporing Wika lye of utube relcory mate tha non reac wer the tet condtons ad parsing a ASTM No. 16(-1:mm) seve (latent oa e-esh Tyler ‘Standard Sei) a retin om ao ASTM No. 40 (4254) sieve (quale toa 3s-nesh Tyler Stale Serie), Plce tach specimen so tht it no ls than 1, mm) rom ter et pecimens or fom te Tana wall, 62 Temperaure Mosrranent~Messre the tempers. within he io by meaas of a appro cal theo feuple Refer to Speciation E2WE2HOM, Tables | ond 2, forthe tokranes and upper enperaore init Tr se of ‘aris themacouples, At higher tempers, the therao Ceuple may te withaw and elated opto ton Pyomeer canbe used. Pace the hor jucton othe theo Soup oh the pyran so a 1 reper he empertine ofthe test specimens. Make enpertte readings neva fe preter than I5-min. Check the kiln prodclly by "eocoupes,promtrs, or pyomrle cont oes ht temperate ovr te er nt ier by more than 25° (ere. (63 Test Atosphere—At all tengeratues above 1470°F (800%) the farce smospere sal cota ain of (03% oxygen and 0% combustibles. Take. gtranalyse samples om he face ehanber proper. 64 Test Temperature Schedule—Operate the in 10 2 19 conor to the appropriate heting sabe forthe cass of retary bung teed shown in Table I, Adj he ing ‘ring theo pid otha te ener wil vege the ‘pected temperature win $F (3 °C). Air conpleten af the sting schedule, cool the specimens inte hosed Ki to blow C0“ (425 C) before removing 68 Measuring Fir SpecinensRemesare the expec mens at roo emperatire in scence wih 2 fe ebbing the ends with an brie block to remove all Bt, 7. Caleaaton and Report 711 Calculate the pecenag war change based upon the ‘ign length ofeach speinen. Repost the average o the ‘he iovidlvalue the ees change in he et {Provision and Blas 81 Ineraborstory Tet Date—Aa intecabosory sound sobia test was conducted between eight brs a hee ‘ieee tenga, 81.1 In he ineraoratry sta, four types of rick were Vested. thee samples each, til of seven se ak each Ia 112 eating scodles, bik yes teste, avers ofall cmos, ad ecistaon ae gen in Tile 2. 82 Preiior—For the conpaneis of vacation sven in ‘ile 2 est result composed of thee samples should be cosired spiny eifrent ta conhdence lve of 95 5, Itt repeatabity or epoduity encod th prison dts sven in Tale 2. 3 Blar—Nojutialenatement on bis is posible sine tte ue physical proper of rfateres cant be et lhe by at acceptable reerence mtr 9. Keywords 9. beating schedule; reactor bik; eet chang; em erate easement est tongs ne fo Rabat ot Vros Types of tates es) een ean oe RT 7 Se aera reas rae as a em oe ; 38 am com ant ooo anh outs Soe owt i Bag Mere eee Seiy Mece mee SS eis Seis foe 2 os = Sram Seen, 7 - nee aSip or13—14 2019) ‘DOLE: Pee ty fori pais Seg mal us i‘prin std dl enh ira eed i on ni add hi i fe Designation: C133 -97 (Reapproved 2021) Standard Test Methods for Cold Crushing Strength and Modulus of Rupture of Refractories’ asad rent ‘Ths mda bn gd a bai fe Una of fe Seape 1.1 These text methods cover the detent of the cold cating sergth sa the cul of rope (MOR) of eed ro velracoy shapes ofall pes 12 The est meth pea inthe Following sections 13 The voles stein inch pod unis ae be regard ss sandr The ves ven n pense mathematical “omverson o Stuns ist ae provided for information oly td ae ot consbeed andar 1A Ths standart does not purport to aes al of the safety concern, if any. asoctoed wih suse 18 the esponiity ofthe nse of has sandr 0 etablh appro rote ay, health, and environment practices an der nine te applicability of eulrorylnrions pri 0 we. "15 This international stndand war developed accor nce wit inernatonalty recognized pricpler on ond lsaton established the Deesion on Prive forthe Development of nema Stondars, Guides and Recon imendetions tee bythe World Trode Organon Teco Ionirs to Dade (T8T} Commitee, 2. Referenced Documents ‘21 ASP Sands? (C2 Practice for Pepring Retracory Concrete Specimens ‘by Casting (CHOSE Practice for Pring and Drying Relatocy Pasie and Rang Mix Specimens A Datos for Ponce Weiieaon of Testing Machines geome Con tin mp C8“ H ce Ca Se eon Al ak of 3 Sigileance and Use 31. Te cold sengh of refactory rari sa nda on of it wit fre reactor earstrucion- (5 nt {tees of performance a levaed teperaes) 212 These et methods ae for determining the 1000 em erature sural strength i ve polt bending od mods fraps) ar compressive suength cold casing eng) OF Brak or al ior produ 33 Consieabl cafe must be used o compare the resus of diferent determinations of the cold crsagseagih o& ‘ous of ptr. The specimen ie and hap, he ar of the specimen faces (hath afore, Saved, Frond, the ‘intone nes daring testing the kui geome Sd thet of load aplstion may ll sigiiealy et the ‘uel reas bind Corpo of the resus bawees Aree detceinations sold notte mae om or ae of ‘hose prnmetr fer between tho vo detentions $34 The eltv rato ofthe hye ran sito the smallest secinen dimension may sgnealy fect te numerical fens For esample, elle it apeciensconuning ge linc ay pent ie ree than he ck om ch fey were cut Under ag cicustancer shoal 6 by by 1 (I32 by 25 by 25mm) specimens be prepared and tested fr rine conining gris with + masz gain dimension ‘ceding 0.25 in (64m). 45 Thistest method is sell fo esearch and developmen ogineeng application and design, manifctring press onion for developing pursing specications. (COLD CRUSHING STRENGTH Apparats 41 Teng Machine—Any for of senda wechaicl or hyeanie compression testing machine conforming 40 the ‘urements of Practices Et ay be ed om fa gh i uh nag i mir tis pt rt tae pe he@y c129-27 ort) Spherical Bearing Block—The plane suis of the spherical bearing lok (= Fig 1) hal ave a a hich ‘ul oor gener tan th crs econ of he et spain. 5. Tes Specimens 1 Brick ad Shapes (bth deny greter than 10 to? (1.60 glen) test specimens sal be 2. (Slam) bes elinder, i (Sm in amet by 2 nS) high. The belt should be pr! ot erga ection of ‘nly one speinen shal be cut fom sige shape and at ‘nny of the eign! races as posible shal be peeved. Ie Prepaig specimens from inept age ric sap, Iny method involving the ae of abrasives, sich 8 9 igh: Speed abasion whos, car dil of rubing bo tht ill race a specimen wit approsimaely pane and parle fides without weakening the Seucture of the peinen may be ted 52 alate Brick or Shapes typo tk density of 100 (oo (1:0 gh?) or greater than 45% ttl pore oF ‘oth The et specimens shall be 195 by 45 by 05 oe 3 (City 114 by 6tor 76mm, each ake oma der bik. Tus perninible tw prepare these pein fom he als resulta tam he todas of rope let ee Sections 9 — TA). The selected compression Te section sl be free of mick, chipped suices, an eho obvious detect, The tt terface shal be appoxinaely parle puns. 5.3 Custable Refuctorie—The ts specimens shal be 2 by 2 by ia (SI by 31 by Slam) bes or eying 7 i (tm) in dimer by 2 ia (Slum) ie prepared by ‘asing or guoing. Is peonasible a prpae one pecnen From each by 2 by 2 230 by 5 by Stem) bar ter the ‘moduls of rp test (86 Sections 9 ~ 18). The selected ompesion Test secon shall be fee of cracks, chipped Surfaces, and otberavous delet. The loaded surfaces sal Te approsimaey pall planes. Alsager mat be ed 220 t0230°F (105 to 110°C) for IB h (veri). Upoe removal fhe oven allow te spl fo oo aaa a Fatt rettg ge tothe ouch. Complete esting win 2 of removal foe the dying oven (See PraccesCM6? an C1084) 6 Procedure 6. At let fve specimens Gen an equivalent number of refetry shapes compo samp Nowe 2for eae weak pci aac o 62 Brick and Shapes—Plce a close er wall boa (or example, Mason?) 0.25 in. (64 mm) in thickness and texendiag O i. (12.7 mn) or more beyond the ees of the Trad Toes ofthe specimen Apply the loud paral! he Aires in which te bck was eriginalypresed 63 Regul and High Sength Castles Place acellose Ser wal bord 025 in. (8mm) in thks ad extending 1 a (12:7 mm) or mare beyond the edges he outed ces ofthe specimen. Aply the Toad the 2 by Zin (31 By Stem) or Zin (lenin) diameter face ae pependcia "he depth ofthe specinen 1s origialy este guaned 64 Inslting Brcko Shapes—Apply telat ey 1 the 4¥5 by bin, (114 by Tl4mm) surace of the tet specie 45 Insulating Cantal (pial bu dens of 100 199? (1.60 glen? or greater than 15% oa pros. oF bot — ‘ply the loa det the 2 by 2m 31 by Sm se and pespeadcla othe depth of te specinen as eriily str Eunos. 645 Use he bering block on op of the est specimen, ant polon io tha the ene ofthe spe iin alignment ith {he vertkal als of the specinen Ge Tig). Keep the ‘spherical bearing block thoroughly labeled o ensue se ‘ie aden wich may be made By and unde ssl ina tad for each specimen, 67 Fordese relates with sain sng eure ese thn about 3 inp ext, odin Yo one hal of the anicipaed flue lool may be accomplished. st a5y aovenien rie excoting the speci rte, Sibu ‘Sch specimen shall be cried wih compressive oa ‘plied atthe andres specie in Table The aes shall fa vay by more thas 10 ofthe specie rate forthe ype Dt reractory Being ts {8 When sing & mechanical testing machine, Kos the blanco bat 3 const fete poston 69 Specnens re loads specified, tale. Fale is deed a the collapse of he specimen (ue supp he Fea) the redocton ofthe species gh 0 905 of ‘vigial value. The masini epi Toad ecoAly 198-87 (2021 [HOLE Sard an a eis gt Ct a cou mmpommy woo nat st) a CRETE ay Fee e ee, ane z ea a fase 3 See eaemtiea com neeetireee ‘Fates we pon er ag a oie 7, Caleuation| 7L Cala the cold rushing stent using sere s w ol erashing eng fin (MP, teal mania fond inetd bythe testing machine, Ine) and erage of tbe seas of he lop and bottom of the Specimey perpen tothe ite of apticion a th Tea, in? Co 8 Report 1 Report te followin: EL Designation of the materials tested (thas, manufacture, band, desertion, ot umber, te, 1.2 Specien configuration, inclding sz, shape, ee ign inthe ign rick or shape, he crater of the Ces (chaise ded, as pese, ase) an the specimen ‘wintaton dng tng 12 Preetmen, if any, gen tothe tet pices (fr example, cringing coking. te) ‘te unter or speimens tn sample 5.13 Inividal specimen dlmensons, the maximum ap pli Tota the cult ald easing seth for ech fpecimon (se 7-1: TL. Mean cold crushing suenth snd sandr devison foresch sample MODULUS OF RUPTURE, 9. Apparatus 81 Testing Mackine—Any fon of sadard mechasics or Iyaulie compresion testing michine conforming 10 the ‘ogurements f Prasces Et ay be wed ss mb ta rp en 92 Bearing Sufces. that shall havea rats of curvature of ‘in, (16 mm) or be linia ieee 6 ia (3D mm) in ieee Fa by yn. (152 by 25 by 25-n) specimens, ‘heel of crv shal be Yin. (8 at) o easel sbeces in (10a) in diameter Al such bering saraces ‘Sal be sag a feng at es ul he wih of the test specimen. The sapporing members forthe lower ‘ring sce shal be const 0 provide a means Fee heaigomea ofthe bering secs wide under surface of the test specimen Becuse the est brick may have a Tonia (wis. Apparatus o he design shown in Fis. 2 is reconmende, alhough ober types maybe used, provided {hey eoaforn to these reuitenen’. Asati ateatve signs shown ia 3. 1 Test Specimens 10. Brick and Shaper Cu density prea han 100 nt? (1.5 afer? )To prefered le specimens shal be sanded 9 by 4vhby 294 orn CB hy 114 by OF or Tom) bricks, oF specimens of equvalet size ground or et fom rectory ‘Shapes Inthe ete of pei shape, oly one specie shall ‘osible shal be preserved. Where ck sae ae nosso ‘rimpacale,eatve specimen sizes of 9 by 2 by 2a {@28 by 5 by 3 ma) ory I by Tn (152by 25 by25 mum) ny be prepared In preparing specimeas from ineguar or Tage shes any meth invaving the use of eases, such fet highspeed sion whee oe ribbing bl, that ill ‘rode » specimen with approximately ple and pre ‘Ses without weakening the mate may be ed 102 tuslarng Brick or Shapes (pica! lk dost of 100 UG (1.60 ghey or etl poraiy rete than 45%, o ‘oth Te tes specie shal be whol brick messing 9 Oy {isby 218 3228 by TI by 6 we A mo peinGp cr29~07 02s) whe md ons ets “rms tra Tomtom Nos: dines ping a 2 a ac: Sere elo ome pan G2 Recommended Deng of Bering Cyne for Modus of Future Test Beret a. 3 Aarau Sein of Baring Cyndere or ol ot "spt oe 103 Conable Refacories~The tet specimens sal be 9 ty 2 by 2226 by 31 by S-m) brs pepe by eslag ‘spectively, sbll be apyeoinately parallel planes.” Samples must be ied t 220 © 230° (1080 110°C) foe 188 (overigh- Upon removal om the oven, allow te sample © onary el conf the ouch, Compe esi win 2 hot removal fom the dying oven. (See Practices C852 and cunsa LL At eas fv specimens fro an equivalent number of rentry shapes compos samp Nom SFr eae weak spies ening wanes 2 stmon opie pte pee 12 Place tet pecinen ate the beating elders with span as specifed ia Table 2 and with he load apled at Inkspan. Whenever posible, use rig, banded Surface oa bik spe as the son fice, that he ace in cont with th two boom bering cylinders. For estable Piece the depth dimension of he specimen as ogally est fr gio sce ats, he op surface te casing oe ned supe becomes uae ofthe propel crewed est Specimen 13 Bach specimen sul be broken st mdapan in enue it's ang appt aecoding othe stand odin ates [vee fn Table 2 For highstrength mati eqing longer than about 3a wo perform aes nia ding to one hal of the antepaed faitre fed maybe accomplished at ay comenem ne resting te peed ae, See, 5 Te sal ot vary mor thn ae ate fo the typeof relatory Being est. The mas ‘mum applied lols ecorde 114 When using echanial testing icine, keep the alan bem neously oning posion 12, Caleuation 121 Cakulitethe mods of repre wing By 2 Mon 39Ua66 aGly ors - 97 (2021) {ABLE 2 Sundar Lown te fr Modus of tre a Src Si Om nfo See AN, ae cee) faba (iaterapre ihamegmcamties Voxasxae” “agag) re a ‘oot fe ‘tieipesccrmmmeteones eR weery) Clam e. aah 8a aise ae ‘ee te Ta pay or BOGS panies (taxon ca a Ban 13) (one te eos Cananse) “ASKS! ° oe ‘ow Se ‘enc eaehicy int m 2 9 & ‘Tiegeens pea ta eer aro ran ay ods of ptr, n> (MP ‘tue apd trp, a (N), pu betes supp 8), tea o wi specimen, In Gr) and dep oF specie in (mm). Hat AB Report 12.1 Rept he flowing: GLLT Designation of ihe materials tested (that is, smanuictue, ba, deseripion, lt sumber. et) T.L2 Specimen eonguration, inci ie oeaton in the orignal bik o shape he charter of the aes (Ht, ‘grid, pres, cnt), the specimen eetation rig esting, Stee pan 1313 Preteament, if ay given t the tet ples (for example curing ring, coking.) TBLLA Number of specimens na sample 13113 Individual specimen dimersons, the maximus a i ld the lection othe rete plane and the eae ‘nodal of rote foreach speinea sce 12-1, 15.16 Mean medals of rope an stad vation for cach simple 14. Interlaboraory Tet Data—Aa nedaboenory study ws completed ainong eight borates i 1995. Fou ler types of efactries were est for cold erasing sength ‘nd cold nals frre by each boron. Te our yes ft retacovies were a dense frre insulting eerie. “ease cable, snd an insolating ease The denon of the Sretrcks were 9 by 45 by 25 i and the mesons of the cables were 9 by 2 by 2 in Befoe eng, blk density fn sone velocity were measured en al refeeory Bis 10 nore tniformiy- Refcory ticks were then candomly {Steed for dition f the pricing laboratories 14.2 Prciin—Tble 3 and Tle 4 conan the precision snes for the sol crashing stengh nd cold moles of ‘tue ress, respectively. 14.2.1 Repatabilin.—The maximum pense diference ue 0 tnt enor between we tat rls obi by ene ‘petro the seman he sae est equine is ‘ven by the repeat teval andthe relave repeat billy eral (The 9 sera ate ven it Tales 3 ta 4 "Two text wee that do not dir by more da he ‘epetbiity itera wil be eoasidered be from te same ppulatlon conversely Wo tress hat do ier by more than the repeabiiy inerval wll be considered © be rom sierent populations. 142.2 Roprodibiy—The maxim pernisible ier cnc ef fet er berween wo ro resus ine By ‘persons in ifernt aberais om the same materi tsing tHesame es ogipment sien byte epi teal “TABLE Pein Stat fr Cad rushing Strengthdil 133 - 97 (2021) (% and the clave eprodacbilty interval R. The 95 5 Feproduiiy eva ae given in Tables 3 an. Two est rele tht do not ifr by more tan the repre ieeral wl be considered fo be fom he same poplin: Enver, wo fest rss tht do ifr by more tn the ‘eproduiiy inerva wil be conidred ob fom diet populations 143 BiarNo jatifable tment canbe made co the bias of the test meted for messing the modules of rune af ine Se, ecg Marc fefetres sae the vale ofthe mda frp ci be led ony interns of «et eho, 18, Keywords 15.1 crushing suenghs modulus of rp refactore:enctor bk oon temperate ‘nna so esa eee sas ba ne eh a) oy a ak gna thao nay aoa meas Dig coma ny tage ere a eatin