BITUMEN DERIVATIVES

PRODUCT CATALOGUE

For the Roads of

Today and Tomorrow

IndianOil Total Pvt. Ltd.

(Joint venture of IndianOil and TotalEnergies Marketing Services)
 About Us

Road construction sector in India is undergoing a ITPL is a 50:50 joint venture between Indian Oil
paradigm shift with a renewed focus on sustainable Corporation and TotalEnergies Marketing Services.
infrastructure development. Modern and emerging ITPL combines the Marketing and R&D strengths of
technologies are instrumental in changing the face of both IndianOil and TotalEnergies to manufacture and
Indian road construction. This will lead to the rise of market innovative bitumen formulations and
demand for improved material for road construction. superior quality products.
To meet the challenges of present and future in road With our culture of innovation, safety, and
construction, Indian Oil Corporation, joined hands sustainability, ITPL is poised to contribute significantly
with TotalEnergies, a broad energy company based at to the pavement sector in India.
France, to form IndianOil Total Pvt. Ltd. (ITPL).
 Our Promoters

Indian Oil Corporation TotalEnergies

Indian Oil Corporation (IOCL) is India’s highest-ranked TotalEnergies is a broad energy company that
energy PSU in fortune global 500 listing. IOCL is an produces and markets energies on a global scale, oils
integrated energy major with a presence in almost all and biofuels, natural gas and green gases,
the streams of oil, gas, petrochemicals, and renewables, and electricity.
alternative energy sources.
Active in more than 130 countries, TotalEnergies puts
IOCL is the largest producer and market leader in sustainable development in all its dimensions at the
viscosity grade Bitumens in India with a state-of-the- heart of its projects and operations to contribute to
art R&D center based in Faridabad. the well-being of people.
 A Comprehensive
Range of BITUMEN
POLYMER
MODIFIED BITUMEN
EMULSIONS
Bitumen Derivatives (PMB)

ITPL offers a comprehensive range of bitumen

derivative products for all the requirements of
road construction. Our products are manufactured
in strict accordance with the highest quality and
safety standards in adherence to our HSEQ policy. CRUMB RUBBER NATURAL RUBBER
MODIFIED BITUMEN MODIFIED BITUMEN
(CRMB) (NRMB)

Bitumen Product Range

EMULSION – RAPID SETTING MICRO SURFACING EMULSION

DURAPAVE EMULSIS RS1 DURAPAVE EMULSIS MiSu

POLYMER MODIFIED BITUMEN (PMB)

EMULSION – MEDIUM SETTING
Styrelf® PMB 40
DURAPAVE EMULSIS MS
Styrelf® PMB 70
Styrelf® PMB 40 Super
EMULSION – SLOW SETTING Styrelf® PMB 40 Hyma
DURAPAVE EMULSIS SS1 Styrelf® PMB 64-10 S/H/V/E
DURAPAVE EMULSIS CSS-1h (ASTM) Styrelf® PMB 70-10 S/H/V/E
DURAPAVE EMULSIS SS2
Styrelf® PMB 76-10 S/H/V/E
Styrelf® PMB 82-10 S/H/V/E
COLD MIX EMULSION Styrelf® PMB 76-22 S/H/V/E
DURAPAVE EMULSIS CM A technology of Total
DURAPAVE EMULSIS CM MS
DURAPAVE EMULSIS CM MS2 CRUMB RUBBER MODIFIED
DURAPAVE EMULSIS CM SS2 BITUMEN (CRMB)
CRFlex® 55 / CRFlex® 60

POLYMER MODIFIED EMULSION

NATURAL RUBBER MODIFIED
DURAPAVE EMULSIS RS PoMo BITUMEN (NRMB)
DURAPAVE EMULSIS SS PoMo NRFlex 40 / NRFlex 70
 Manufacturing Facilities

To ensure an efficient and reliable supply of

Jodhpur, Rajasthan products to the customers, ITPL has set up
manufacturing facilities at strategic locations. At
present, ITPL has full-fledged state-of-the-art
manufacturing plants at Jodhpur in the state of
Haldia, West Bengal Rajasthan, Haldia in the state of West Bengal, and
Chennai in the state of Tamil Nadu.
Mumbai HO
In near future, ITPL will be investing in setting up
Chennai, Tamilnadu
state-of-the-art bitumen derivative plants in
Haldia, Mathura, Chennai, Barauni, Koyali & Vasco.
Research and Development

ITPL offers a detailed technical evaluation of a complete

range of products to the customers. ITPL’s state-of-the-
art labs are equipped with the latest equipment
for analysis of Performance Grade Binders
(PMB/CRMB) with DSR (Dynamic Shear
Rheometer) and short term and long-term aging
process through RTFO (Rolling Thin Film Oven) /
PAV (Pressure Aging Vessel).

Technical Assistance
The Technical Assistance to customers is a result of in depth experience and expertise of
IndianOil and TotalEnergies which includes:

• Training on storage, handling, and applications • Laboratory support for optimal mix design.
of the products. • Technical support on Hot Mix and Cold Mix
• Technical Assistance to define the best processes from production to applications.
conditions to obtain the required performance
of the products.
 3rd floor, Gala Impecca, Vijay Nagar Colony,
J. B. Nagar, Andheri Kurla Road, Andheri (E),
IndianOil Total Pvt. Ltd. Mumbai, Maharashtra, 400 059 India.
(Joint venture of IndianOil and TotalEnergies Marketing Services) Email: [email protected] Tel: +91 22 6907 7400.
 Emulsion – COLD MIX
CM & CM Ss2

ApplicationS:
Cold Mix technology is a highly engineered but simple & effective solution. It is used for paving
rural roads, farm link roads, and low volume roads.

Product Certifications:
Bureau of Indian Standards (BIS): CM/L- No-3015129

Available Grades:
1.DURAPAVE EMULSIS CM
2.DURAPAVE EMULSIS CM-SS2

specifications:
DURAPAVE EMULSIS CM, CM-SS2 meets the specifications as per IRC: SP: 100-2014

BENEFITS:
• Energy efficient and environment friendly and low temperature curing.
• Highly adhesive properties and water resistant and enhances easy drainage of water.
• Enhances structural strength of layers.
• Safe and non – hazardous due to elimination of heating and burning.
• Continuous construction in rainy season and extends construction period in a year.
• Inbuilt property of anti-stripping agent provides better mix quality and surface finish.
• Higher volume of construction & speedy completion of roads.

DURAPAVE EMULSIS Cold Mix is available in

Packing: • 200 Kg • MS Drum • RC Drum • New HDPE Drum

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Technical SpecificationS

Test EMULSIS CM EMULSIS CM-SS2

Characteristics UOM
Method
Min Max Min Max
Residue on 600 micron IS 8887-2018
% – 0.05 – 0.05
Sieve in % by Mass ANNEX-B
Viscosity at 25°C by
Saybolt Furol Viscometer IS 3117 Sec 33 40 30 150

Coagulation at low IS 8887-2018

– NIL NIL NIL NIL
Temp. ANNEX-C
Storage stability after IS 8887-2018
% – 2 – 2
24 Hrs. ANNEX-D

Particle Charge IS 8887-2018

– Positive Positive Positive Positive
ANNEX-E
Coating ability & water Resistance:
a) Coating, dry IS 8887-2018
– Good Good Good Good
aggregate ANNEX-F
b) Coating, after IS 8887-2018
– Fair Fair Fair Fair
spraying ANNEX-F
c) Coating, wet IS 8887-2018
– Fair Fair Fair Fair
aggregate ANNEX-F
d) Coating, after IS 8887-2018
– Fair Fair Fair Fair
spraying ANNEX-F
Miscibility with IS 8887-2018 No- No- No- No-
–
water ANNEX-H Coagulation Coagulation Coagulation Coagulation
Stability to mixing with IS 8887-2018
% – 2 – 2
cement (Coagulation) ANNEX-G
Test on Residue:
a) Residue by IS 8887-2018
% 60 – 60 –
Evaporation ANNEX-J
b) Penetration of
Residue at 25°C/ IS 1203-1978 – 60 120 60 120
100gm/ 5Sec
c) Ductility of Residue
IS 1208-1978 Cm 50 – 50 –
at 27°C
d) Solubility in
IS 1216-1978 % 98 – 98 –
Trichloroethylene
 Crumb Rubber Modified Bitumen
CRFlex® 55/60

ApplicationS:
CRFlex® 55/60 is specially formulated with unique technology that enables homogeneity,
stability and consistent properties of binder. To achieve this, special stabilizing additives are
used under special manufacturing process resulting in unique properties that are consistent
and as per the latest technical guidelines.

Product Certifications: Bureau of Indian Standards (BIS): CM/L-No-8400162409

specifications: The product meets the specifications as per IS 17079:2019.

Available Grades:
• CRFlex® 55 • CRFlex® 60

BENEFITS:
• Higher resistance to deformation at elevated pavement temperatures.
• Better adhesion between aggregate and binder.
• Higher fatigue life and delayed cracking and reflective cracking.
• Overall improved performance in extreme climatic conditions and under heavy
traffic conditions.
• Better water resistance.
• Resistance to creep and higher indirect tensile strength.
• Lower susceptibility to daily and seasonal temperature variations.

Packing: CRFLEX® 55/60 is available in Bulk

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Specifications in Accordance with IS 17079 : 2019

Property Requirement Requirement Method

CRFlex® 55 CRFlex® 60 Reference
Penetration at 25°C,
0.1mm, 100gm.5Sec 60 – 30 50 – 20 IS 1203-1978

Softening Point, (R & B), °C, Min 55 60 IS 1205-1978

Flash Point, COC, °C, Min. 220 220 IS 1209-1978

Elastic Recovery of half thread in Annexure-A
60 60
ductilometer 15°C, %, Min 17079:2019
Complex Modulus (G*/Sin δ) as Min.
64 70 15462:2019
1 kPa at 10 rad/s, at a temperature C
̊ .
Separation, difference in Softening point Annexure-B
4 4
(R & B), °C, Max 17079:2019
Viscosity at 150°C, Poises 4-8 6 - 12 1206 (Part 2)
Thin film oven test on residue
Loss in Mass, %, Max 1 1 IS 9382-1979

Increase in Softening point, °C, Max 5 5 IS 1205-1978

Reduction in penetration of residue,
35 35 IS 1203-1978
at 25 °C, %, Max
Elastic Recovery of half thread in Annexure-A
35 35
ductilometer 25 °C, %, Min 17079:2019
Complex Modulus (G*/Sin δ) as Min.
64 70 15462:2019
2.2 kPa at 10 rad/s, at a temperature °C

Procedure Recommended Temperature Range

Mixing / Coating with Aggregates 170 - 185 °C

Laying of Mix 150-170 °C

Beginning of Compaction Over 140 °C

End of Compaction 110-120 °C

 Emulsion – COLD MIX
CM MS & Ms2
ApplicationS:
Cold Mix technology is a highly engineered but simple & effective solution. It is used for paving
rural roads, farm link roads, and low volume roads.

Product Certifications: Bureau of Indian Standards (BIS): CM/L- No-3015129

Available Grades: 1) DURAPAVE EMULSIS CM-MS 2) DURAPAVE EMULSIS CM-MS2

Specifications:
DURAPAVE EMULSIS CM-MS & MS2 meets the specifications as per IRC: SP: 100-2014

BENEFITS:
• Energy efficient and environment friendly.
• Low temperature curing.
• Highly adhesive properties.
• Water resistant and enhances easy drainage of water.
• Enhances structural strength of layers.
• Safe and non – hazardous due to elimination of heating and burning.
• Continuous construction in rainy season.
• Extends construction period in a year.
• Inbuilt property of anti-stripping agent provides better mix quality.
• Higher volume of construction & speedy completion of roads.

Technical SpecificationS
Properties Specification- Typical test Result Typical test Result
EMULSIS MS & MS2 CM-MS CM-MS2
Viscosity at 50⁰C (Say bolt Viscometer) 50 - 300 54 - 55 54 - 55
Residue on 600 Micron IS Sieve, % max 0.05% 0.002 - 0.02 0.026 - 0.027
Storage Stability after 24 hrs, % Max 1.0% 0.3 - 0.5 0.3 - 0.5
Binder Residue by Evaporation Min 65% 65 - 66 65 - 66
Average Setting time, hrs – 1 4

Packing: DURAPAVE EMULSIS Cold Mix is available in • 200 Kg • MS Drum • RC Drum • New HDPE Drum

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Emulsion – Medium Setting
MS

ApplicationS:
DURAPAVE EMULSIS MS is ideally suited and designed for:
• Pothole filling/patch work • Premix carpet work
• Strong bonding with existing surface • High stability of patches.
The product meets the specifications as per IS 8887:2018.

Product Certifications: Bureau of Indian Standards (BIS): CM/L- No-3015129

BENEFITS:
• Coats and bond loose mineral particles on the surface of the base course in repair works.
• To seal surface pores and make the surface of the base course water-resistant.
• Instant setting and high compaction.

Technical SpecificationS
Test Unit of Specification
Characteristics
Method Measurement Min Max
Residue on 600 micron IS 8887-2018
% – 0.05
Sieve in % by Mass ANNEX-B
Viscosity at 50°C by Saybolt
IS 3117 Sec 50 300
Furol Viscometer
Coagulation of emulsion at IS 8887-2018
– NIL NIL
low temp. ANNEX-C

Storage stability after 24 Hrs. IS 8887-2018

% – 1
ANNEX-D

Particle Charge IS 8887-2018

– Positive Positive
ANNEX-E
IS 8887-2018 No- No-
Miscibility with water –
ANNEX-H Coagulation Coagulation
Test on Residue:-

a) Residue by Evaporation IS 8887-2018

% 65 –
ANNEX-J
b) Penetration of residue at
IS 1203-1978 – 60 150
25°C/ 100gm/ 5Sec
c) Ductility of residue at 27°C IS 1208-1978 Cm 50 –
d) Solubility in Trichloroethylene IS 1216-1978 % 98 –

Packing: DURAPAVE EMULSIS MS is available in • Bulk • 200 Kg • MS Drum • RC Drum • New HDPE Drum

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Emulsion – Rapid Setting
Rs1

ApplicationS:
DURAPAVE EMULSIS RS1 emulsion is manufactured in state of the art formulation process and
quality control. It is applied on aged and primed bituminous surfaces. The product meets the
specifications as per IS 8887:2018.

Product Certifications: Bureau of Indian Standards (BIS): CM/L- No-3015129

BENEFITS:
• Maintain good bond between the existing layer and new bituminous layer.
• Strong resistance to movement of structural layers.
• Forms strong water resistant layer to prevent any water table changes.
• Seal the pores and make the surface water resistant.
• Provides good adhesion between the layers on good spraying.

Technical SpecificationS
Test Unit of Specification
Characteristics
Method Measurement Min Max
Residue on 600 micron IS 8887-2018
% – 0.05
Sieve in % by Mass ANNEX-B
Viscosity at 50°C by Saybolt
IS 3117 Sec 20 100
Furol Viscometer
Coagulation of emulsion at IS 8887-2018
– NIL NIL
low Temp. ANNEX-C
Storage stability after 24 Hrs. IS 8887-2018
% – 2
ANNEX-D
Particle Charge IS 8887-2018
– Positive Positive
ANNEX-E
IS 8887-2018 No- No-
Miscibility with water –
ANNEX-H Coagulation Coagulation
Test on Residue:-
a) Residue by Evaporation IS 8887-2018
% 60 –
ANNEX-J
b) Penetration of Residue at
IS 1203-1978 – 80 –
150
25°C/ 100gm/ 5Sec
c) Ductility of Residue at 27°C IS 1208-1978 Cm 50
d) Solubility in Trichloroethylene IS 1216-1978 % 98 –

Packing: DURAPAVE EMULSIS RS1 is available in • Bulk • 200 Kg • MS Drum • RC Drum • New HDPE Drum

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Emulsion – Slow Setting
Ss1 (IS)
ApplicationS:
DURAPAVE EMULSIS SS1 is specially designed oil based bituminous emulsion with low viscosity
extended setting time and stability with cement. It is an ideal product for coating
WM M/WBM surfaces. The product meets the specifications as per IS 8887:2018.

Product Certifications: Bureau of Indian Standards (BIS): CM/L- No-3015129

BENEFITS:
• High penetration of the existing base course.
• Sealing of loose mineral particles.
• To harden the base course.

Technical SpecificationS
Test Unit of Specification
Characteristics
Method Measurement Min Max
Residue on 600 micron IS 8887-2018
% – 0.05
Sieve in % by Mass ANNEX-B
Viscosity at 25°C by Saybolt
IS 3117 Sec 20 100
Furol Viscometer
Coagulation of emulsion at IS 8887-2018
– NIL NIL
low Temp. ANNEX-C

Storage stability after 24 Hrs. IS 8887-2018

% – 2
ANNEX-D

Miscibility with water IS 8887-2018

– Immiscible Immiscible
ANNEX-H
Distillation, By Volume at:
a) 190°C – % 20 55
b) 225°C – % 30 75
c) 260°C – % 40 90
d) 316°C – % 60 100
e) Residue at 360°C IS 1213-1978 % 50 –
Water Content,by Mass IS 1211-2018 % – 20
Test on Residue:
a) Solubility in Trichloroethylene IS 1216-1978 % 98 –

Packing: DURAPAVE EMULSIS SS1 is available in • Bulk • 185 Kg • MS Drum • RC Drum • New HDPE Drum

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Emulsion – Slow Setting
Ss2
ApplicationS:
DURAPAVE EMULSIS SS2 a specially designed tailor-made water based bituminous emulsion
with medium viscosity and extended setting time and stability with cement. The product meets
the specifications as per IS 8887:2018.

Product Certifications: Bureau of Indian Standards (BIS): CM/L- No-3015129

BENEFITS:
• Binds loose aggregates.
• Good penetration in to the base course.
• Makes the base course water resistant.

Technical SpecificationS
Test Unit of Specification
Characteristics
Method Measurement Min Max
Residue on 600 micron IS 8887-2018
Sieve in % by Mass % – 0.05
ANNEX-B
Viscosity at 25°C by Saybolt IS 3117 Sec 30 150
Furol Viscometer
Coagulation of emulsion at IS 8887-2018
low Temp. – NIL NIL
ANNEX-C
Storage stability after 24 Hrs. IS 8887-2018 % – 2
ANNEX-D
Particle Charge IS 8887-2018 – Positive Positive
ANNEX-E
IS 8887-2018 No- No-
Miscibility with water – coagulation coagulation
ANNEX-H
Test on Residue:
a) Residue by Evaporation IS 8887-2018 % 60 –
ANNEX-J
b) Penetration of Residue at
25°C/ 100gm/ 5Sec IS 1203-1978 – 60 120

c) Ductility of Residue at 27°C IS 1208-1978 Cm 50 –

d) Solubility in Trichloroethylene IS 1216-1978 % 98 –

Packing: DURAPAVE EMULSIS SS2 is available in • Bulk • 200 Kg • MS Drum • RC Drum • New HDPE Drum

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Emulsion – Slow Setting
CSS1 (h)

ApplicationS:
DURAPAVE EMULISIS CSS-1H is used as:
• Prime Coat • Fog seal/crack seal • Slurry seal
The product meets the specifications as per ASTM D2397-13.

Product Certifications: Bureau of Indian Standards (BIS): CM/L- No-3015129

BENEFITS:
• Excellent penetration into miniature pores of sub bases.
• Extended breaking easy spray.
• Penetrate the cracks & crevices and impart strength to the layers.
• Bonds well to cool, damp substrates/surfaces and Low temperature cure.
• Bind loose aggregates together strongly.
• Highly adhesive with multiple applications.

Technical SpecificationS
Specification
Test Unit of
Characteristics ASTM D2397-13
Method Measurement Min Max
Residue on 850 micron
ASTM D6933 % – 0.10
Sieve in % by Mass
Viscosity at 25°C by Saybolt
ASTM D244 Sec 20 100
Furol Viscometer
Storage stability after 24 hrs ASTM D6930 % – 1
Partical Charge ASTM D244 – Positive Positive
Stability to mixing with cement
ASTM D6935 % – 2
(% Coagulation)
Test on Residue:
a) Residue by Evaporation – % 57 –
b) Penetration of Residue at
– – 40 90
25°C/ 100gm/ 5Sec
c) Ductility of Residue at 27°C ASTM D244 Cm 40 –
d) Solubility in Trichloroethylene – % 97.5 –

Packing: DURAPAVE EMULSIS CSS-1H is available in • Bulk • 200 Kg • MS Drum • RC Drum • New HDPE Drum

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Polymer Modified Bitumen
PMB
A technology of TotalEnergies

ApplicationS:
STYRELF® PMB comprises a range of elastomerically modified bitumen PMB (E) SBS base block
copolymer. It is developed to provide high performance over a range of different applications
and different conditions. STYRELF® PMB meets specifications of IRC SP53:2010 having
advanced properties of softening point & elastic recovery. The product is fortified with
TotalEnergies patented cross linking agent. The produced PMB is homogenous and superior
quality PMB, which enhances life of the pavement.

Product Certifications: Bureau of Indian Standards (BIS): CM/L-No-3269160

Available Grades:
• STYRELF® PMB 40
• STYRELF® PMB 70
• STYRELF® PMB 40 Super

BENEFITS:
• Resistance at higher temperatures surface against rutting and ambient temperatures
against fatigue.
• Higher resistance at low temperatures against thermal cracking because of viscoelastic
nature.
• Better stripping resistance and ITSR (Indirect Tensile Strength Ratios).
• Better resistance against aging and oxidation.
• Proven record of longer life of pavement.
• Saves natural resources and reduced pollution levels by deferring the frequency of overlays
and period maintenance.
• Suitable as per Indian geography of moderate to extreme temperatures with lower
susceptibility to temperature variation.
• For national/ state highway/ city roads/ fly overs/ round about etc. with overall improved
mix performance.

Packing: STYRELF® PMB is available in Bulk.

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Technical SpecificationS
Property STYRELF STYRELF STYRELF
Test Method PMB - 40 PMB -70 PMB-40 Super
Penetration at 25°C, 0.1mm,
100gm.5Sec IS 1203-1978 30-50 50-80 30-50

Softening Point, (R & B), °C, Min IS 1205-1978 60* 55 70

FRAASS breaking point, °C, Max IS 9381-1979 -12 -16 -12

Flash Point, COC, °C, Min IS 1209-1978 220 220 220

IRC: SP:
Elastic Recovery of half thread in
ductilometer 15°C, %, Min 53-2010 60 60 70
ANNEX-2
Complex Modulus (G*/Sin δ) as IRC: SP:
Min. 1.0 kPa at 10 rad/s, at a 53-2010 76 70 76
temperature °C. ANNEX-1
IRC SP
Separation, difference in Softening
point (R & B), °C, Max 53-2010 3 3 3
ANNEX -3
Viscosity at 150°C, Poises 1206 Part 1 5-9 3-6 5-9

Thin film oven tests on residue

Loss in Mass, %, Max IS 9382-1979 1.0 1.0 1.0

Increase in Softening point,
IS 1205-1978 5 6 5
°C, Max
Reduction in penetration of
IS 1203-1978 35 35 35
residue, at 25 °C, %, Max
Elastic Recovery of half thread in IRC: SP:
ductilometer 25 °C, %, Min 53-2010 50 50 50
OR ANNEX-4

Complex Modulus (G*/Sin δ) as IRC: SP:

Min. 2.2 kPa at 10 rad/s, at a 53-2010 76 70 76
temperature °C ANNEX-1

Procedure Recommended Temperature Range

Mixing / Coating with Aggregates 170 - 185 °C

Laying of Mix 150-170 °C

Beginning of Compaction Over 140 °C

End of Compaction 110-120 °C

 Polymer Modified Bitumen
PMB 40 HYMA
A technology of TotalEnergies

ApplicationS:
STYRELF® PMB 40 (HYMA) is specially formulated with advanced polymers and special cross
linking agent. It is manufactured in state of the art facility with high shear process. It gives
uniform mixing & dispersion of polymer for superior adhesion between aggregate & binder
ensuring, longer life, flexural strength, reduced oxidation & overall stability of the pavement.

Product Certifications:
Bureau of Indian Standards (BIS): CM/L-No-3269160

Specifications:
STYRELF® PMB 40 (HYMA) meets the specifications as per AASHTO M332: 2014

BENEFITS:
• Highly modified binders can give dramatic improvement in pavement resistance to rutting
and fatigue damage.
• In severe distress situations, highly modified binders are likely to double pavement life.
• Ideal for extreme temperatures & loading areas such as airport runway applications,
critical areas, flyovers, junctions and roundabouts.
• Higher resistance at low temperatures (<-28°C) and higher temperatures surface (80°C)
against thermal cracking & rutting because of extreme viscoelastic nature.
• Helps reduce crust thicknesses up to 20 %, ideal for perpetual pavements

Packing:
STYRELF® PMB 40 HYMA is available in Bulk.

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Specifications in Accordance with AASHTO M332: 2014

Property Test Method Specification

Grade AASHTO M 332:2014 PG76E-28

Viscosity@135°C, Max, Pa.s ASTM D4402 3

Polymer Content, Min, % Mass Supplier Certificate 7.5

SBS Polymer Content (FTIR, Min, % Mass ASTM E168, E1252 7.5
Separation Test: Absolute difference between
G* @ 76°C and 10 rad/s of Top and Bottom ASTM D7173 10
Specimens, Max %
Solubility, Min, % ASTM D2042 99

Flash Point, Min °C ASTM D92 230

Softening Point (R & B) °C Min IS 1205 90

Elastic Recovery of Half Thread in
ductilometer at 15°C %, Min IRC SP 53:2010 90

Rolling Thin Film Oven (RTFO) Residue

Mass Change, Max, % ASTM D2872 1

MSCR Jnr3.2 @ 76°C, Max, kPa-1 ASTM D7405 0.1

MSCR, Recovery R3.2@ 76°C, Min, % ASTM D7405 90

Pressurized Aging Vessel (PAV) Residue
PAV Aging Temperature °C ASTM D6521 100
Dynamic Shear, G*Xsin delta @ 25°C and
ASTMD7175 5000
10rad/s, Max, kPa
Bending Beam, S @ -18°C and 60°C,
Max, Mpa ASTM D6648 300

Bending Beam, m-value @ -18°C and

60°C, Min , Mpa ASTM D6648 0.3

Procedure Recommended Temperature Range

Mixing / Coating with Aggregates 170 - 185 °C

Laying of Mix 150-170 °C

Beginning of Compaction Over 140 °C

End of Compaction 110-120 °C

 Polymer Modified Bitumen
PMB PG GRADING
A technology of TotalEnergies

ApplicationS:
The STYRELF® PMB group of binders comprising a range of elastomerically modified bitumen
PMB SBS base block copolymer. It is developed to provide high performance over a range of
different applications and different conditions. The product is fortified with TotalEnergies
patented cross linking agent. The produced PMB is homogenous and superior quality PMB,
which enhances life of the pavement.

Product Certifications: Bureau of Indian Standards (BIS): CM/L-No-3269160

Available Grades:
• STYRELF® PMB 64-10 S/H/V/E
• STYRELF® PMB 70-10 S/H/V/E
• STYRELF® PMB 76-10 S/H/V/E
• STYRELF® PMB 82-10 S/H/V/E
• STYRELF® PMB 76-22 S/H/V/E

Benefits:
• Resistance at higher temperatures surface against rutting and ambient temperatures
against fatigue.
• Higher resistance at low temperatures (-10°C) against thermal cracking because of
viscoelastic nature.
• Better stripping resistance and ITSR (Indirect Tensile Strength Ratios).
• Better resistance against aging and oxidation compared to normal VG grades.
• Proven record of longer life of pavement.
• Saves natural resources and reduced pollution levels by deferring the frequency of overlays
and period maintenance.
• Suitable as per Indian geography of moderate to extreme temperatures with lower
susceptibility to temperature variation.
• Recommended for national/ state highways/ city roads/ fly overs/ round about etc. with
overall improved mix performance.
• PMB grades available from selection criteria of standard (S) to extremely heavy (E) traffic
condition as per IS 15462:2019.

Packing: STYRELF® PMB is available in Bulk.

Our Promoters: For Technical Queries, please contact:

Dr. Pankaj Kumar Jain, Vice President - Marketing and Technical
Mob: +91 8451804665 / Email: [email protected]
Anil Thondepu, Manager - Product Marketing
Mob: +91 8976773284 / Email: [email protected]
 Table 1 Requirements of Polymer Modified Bitumen (PMB) IS 15462:2019
(Clause 6.5 and 9.5.3)
Grades and Requirements Method of Test, Ref to
Characteristics
PMB PMB PMB PMB PMB IS/ASTM
64-10 70-10 76-10 82-10 76-22 Annex
(A) Tests to be Carried out on Original Binder
Softening Point (R & B), °C, Min. 60 65 70 80 75 – IS 1205
Elastic recovery of half thread in
70 70 70 85 80 Annex A –
ductilometer at 15 °C, Min.
Flash Point, COC, °C, Min. 230 230 230 230 230 – IS 1209
Viscosity at 150 °C, Pa.s, Max 1.2 1.2 1.2 1.6 1.5 – ASTM D 4402
Complex modulus (G*) divided by Sin
delta (G*Sin δ) as Min 1.0kPa,25mm
64 70 76 82 76 Annex B –
Plate,1mm Gap, at 10 rad/s, at a
temperature, °C, Min.
Phase Angle (δ), Degree Max. 75 75 75 75 75 Annex B –
Separation, difference in softening point
3 3 3 3 3 Annex C –
(R & B), °C, Max
FRAASS breaking point, °C, Max. -10 -10 -10 -10 -22 – IS 9381
B)Tests to be carried out on Rolling Thin Film Oven (RTFO) residue²
Loss in mass, %, Max. 1.0 1.0 1.0 1.0 1.0 – IS 9382
Complex modulus (G*) divided by
Sin delta (G*Sin δ) as Min 2.2kPa,
64 70 76 82 76 Annex B –
25mm Plate,1mm Gap, at
10 rad/s, at a temperature, °C
MSCR TEST
a) Standard Traffic (S)
Jnr 3.2 Max 4.5 kPa-1,
64 70 76 82 76 Annex D –
Jnrdiff Max75 percent
Test Temperature, °C
b) Heavy Traffic (H)
Jnr 3.2 Max 2 kPa-1,
64 70 76 82 76 Annex D –
Jnrdiff Max75 percent
Test Temperature, °C
c) Very Heavy Traffic (V)
Jnr 3.2 Max 1 kPa-1,
64 70 76 82 76 Annex D –
Jnrdiff Max75 percent
Test Temperature, °C
d) Extremely Heavy Traffic (E)
Jnr 3.2 Max 0.5 kPa-1,
64 70 76 82 76 Annex D –
Jnrdiff Max75 percent
Test Temperature, °C
C)Tests to be carried out on Pressure Vessel (PAV) residue³
Complex modulus (G*) multiplied by Sin
delta (G*sin δ) as Max 6000 kPa, 8mm
31 34 37 40 31 Annex C –
Plate, 2mm Gap, at 10 rad/s, at a
temperature

1) FRAASS Breaking Point only to be evaluated in case the project site has subzero temp conditions.
2) Method for Preparation of Rolling Thin Film Oven (RTFO) Residue is given in Annex E.
3) Method for Preparation of Pressure Aging Vessel (PAV) Residue is given in Annex F.

Procedure Recommended Temperature Range

Mixing / Coating with Aggregates 170 - 185 °C

Laying of Mix 150-170 °C

Beginning of Compaction Over 140 °C

End of Compaction 110-120 °C