SOIL INSTRUMENTS (M) SDN BHD

CALCULATION OF MEASUREMENT UNCERTAINTY Report No: MU/EOS/MTS/18/006

TEST NAME : Admixture for Concrete, Mortar and Grout

Date Updated 10/9/2018

Report Ref: SIM/MTS/PT/CS/0001/28d Updated by Nurul Azira

compressive Symbol Formula Value

strength 42.99
Test Parameters Symbol Trial 1 Trial 2 Trial 3 Test Data St.Dev σ σ = F*1000/(LW)
Load Applied (kN) F 935 994 992 974 33.50 CF dσ/dF = 1000/(LW) 0.044
Sensitivity
Length (mm) L 150 150 150 150.00 0.000 CL dσ/dL = -1000F/(L2W) -0.287
Coefficient
Width (mm) W 152 150 151 151.00 1.000 CW dσ/dW = -1000F/(LW2) -0.285
Compressive Strength(N/mm²) σ 43.0

Distribution Type of Sensitivity

Component of Uncertainty Source symbol Range/st.dev Divisor/Dist. Std. Uncty UiCi (UiCi)2 DoF νi (UiCi)4/νi %contribution
Type evaluation Coefficient

Applied Load (kN)-observation machine UA(F) normal A 33.50 1.732 19.3420 0.044 0.8539 0.7292 2 0.26588778912 95.49
Applied Load (kN) - calibration cal. Cert machine Ucal(F) normal B 3.9 2.0000 1.9500 0.0442 0.0861 0.0074 60 9.156181E-07 0.97
Applied Load(kN) - resolution cal. Cert machine Ures(F) rectangular B 0.1 1.7321 0.0577 0.0442 0.0025 0.0000 infinity 0 0.00
Length (mm) - repeatability vernier UA(L) normal A 0.000 1.7321 0.0000 -0.2866 0.0000 0.0000 2 0 -
Length(mm) - calibration vernier Ucal(L) normal B 0.01 2.0000 0.0050 -0.2866 -0.0014 0.0000 60 7.0263878E-14 0.00
Length(mm) - resolution vernier Ures(L) rectangular B 0.01 1.7321 0.0058 -0.2866 -0.0017 0.0000 infinity 0 0.00
Width (mm) - repeatability vernier UA(W) normal A 1.000 1.7321 0.5774 -0.2847 -0.1644 0.0270 2 0.00036491195 3.54
Width (mm)-calibration vernier Ucal(W) normal B' 0.01 2.0000 0.0050 -0.2847 -0.0014 0.0000 60 6.8420991E-14 0.00
Width(mm)-resolution vernier Ures(W) rectangular B 0.01 1.7321 0.0058 -0.2847 -0.0016 0.0000 infinity 0 0.00
Unit
Unit N/mm2 or MPa SUM 0.7637 (N/mm2)2
Note: 1N/mm² = 1MPa Combined Uncertainty 0.8739 N/mm2
Effective DoF. & K 2.19
Equipment ID No (Compressive Machine): SIM/HQ/E/0195 Uncertainty based on SAMM & ILAC , K= 2.01
k 2
Equipment ID No (Caliper): SIM/HQ/E/0288 Expanded Uncertainty (±) 1.7 N/mm2

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 SOIL INSTRUMENTS (M) SDN BHD
CALCULATION OF MEASUREMENT UNCERTAINTY Report No : MU/EOS/MTS/18/004b

Test name: Compressive and Flexural Strength of Prismatic Test Specimens from Cement Mortar Date Updated : 10/9/2018
Updated by : Nurul Azira

Report Ref: SIM/MTS/ILC/CFS/CM/0001/28d - 0003/28d

Max Load Compressive

Sample I.D Weight (kg) Depth Width (kN) Strength (MPa) Quantity Symbol Equation Value
ILC/C 0004-1-1 0.57 41 40 87.6 54.8 Compressive Strength σ σ=F/(DW) 53.1
ILC/C 0004-1-2 0.57 41 40 83.9 52.4
ILC/C 0004-2-1 0.57 40 40 86.8 54.3 Sensitivity Coeff. (Load) CF dσ/dF=1000/(DW) 0.625
ILC/C 0004-2-2 0.57 40 40 85.6 53.5
ILC/C 0004-3-1 0.57 41 40 84.9 53.1
ILC/C 0004-3-2 0.57 41 40 86.7 54.2
ILC/C 0005-1-1 0.58 40 40 87.5 54.7
ILC/C 0005-1-2 0.58 40 40 86.9 54.3
ILC/C 0005-2-1 0.59 40 40 81.8 51.1
ILC/C 0005-2-2 0.59 40 40 80.5 50.3
ILC/C 0005-3-1 0.59 40 40 81.4 50.9
ILC/C 0005-3-2 0.59 40 40 81.9 51.2
ILC/C 0006-1-1 0.57 41 40 87.6 54.8
ILC/C 0006-1-2 0.57 41 40 83.1 51.9
ILC/C 0006-2-1 0.57 41 40 86.6 54.1
ILC/C 0006-2-2 0.57 41 40 85.5 53.4
ILC/C 0006-3-1 0.58 40 40 85.6 53.5
ILC/C 0006-3-2 0.58 40 40 85.2 53.3
Average 86 53.1
Standard Deviation 2.3 1.4

Uncertainty Calculation for: Compressive Strength

Component Symbol Unit Evaluation Dist. Range/st dev. Divisor/factor std. Ui Ci (UiCi)2 νi (CiUi)4/νi % contribution
Repeatability: Load (F) UA(F) kN A normal 2.3 4.24 0.55 0.625 0.1161 5 0.00269447297165 28.190
Calibration: Compression Machine Ucal(F) kN B normal 1.74 2 0.87 0.625 0.295664 60 0.00145695396423 71.807
Resolution: Machine Ures(F) kN B rectangular 0.01 1.73 0.01 0.625 0.000013 infinity 0 0.003
Unit
SUM 0.4117
UC 0.64 MPa
Eff Dof 40.84
SAMM req., k = 2
Equipment ID No (Compressive Machine): SIM/HQ/E/0326a k 2
UE (±) 1.3 MPa

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 SOIL INSTRUMENTS (M) SDN BHD Report No : MU/EOS/MTS/18/005
CALCULATION OF MEASUREMENT UNCERTAINTY
Date Updated : 10/9/2018
Test name: Determination of Cement Fineness By Air Permeability Updated by : Nurul Azira
(Blaine Method)

Report Ref: SIM/MTS/ILC/CF/BM/0001

Quantity Unit Trial 1 Trial 2 Trial 3 Average St. Dev

Mass of cell+filter paper+disk (m1) g 68.83 68.83 68.83 68.83
mass of sample+cell+filter paper+disk (m2) g 71.85 71.88 71.86 71.86
Mass of sample (m3) g 2.79 2.79 2.79 2.79
ρ of sample g/cm3 2.99 2.99 2.99 2.99
ρ0 of ref. cement g/cm3 3.15 3.15 3.15 3.15
t s 70 68 67 68.33 1.53
t0 s 93 93 93 93
Specific Surface S cm2/g 3490 3439 3414 3448

Quantity Symbol Equation Value

Specific Surface S (ρ0*√t*S0)/(ρ*√t0) 3447.72
Sens. Coeff t Ct 1/2*(ρ0*S0)/(ρ*√t*√t0) 25.23

Note: S0= 3818cm2/g

Uncertainty Calculation for: Specific Surface

Ci (UiCi)2 (CiUi)4/νi % cont.

Component Symbol Unit Evaluation Dist. Range/st dev. Divisor/factor std. Ui νi
Repeated Observation: Time UA(t) s A normal 1.53 1.732050807569 0.881917104 25.23 495.028910749 2 122526.811 75.67
Calibration: Stopwatch Ucal(t) s B normal 1 2 0.5 25.23 159.116435598 60 421.967335 24.32
Resolution: Stopwatch Ures(t) s B rectangular 0.01 1.732050807569 0.005773503 25.23 0.02121552475 infinity 0 0.00

Unit
SUM 654.1666
UC 25.5767 cm2/g
Eff DoF 3.48
Based on SAMM & ILAC, k = 2
Equipment ID No (Stopwatch): SIM/HQ/E/0361 k 2
UE (±) 51.2 cm2/g

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 SOIL INSTRUMENTS (M) SDN BHD Report No : MU/EOS/MTS/18/008
CALCULATION OF MEASUREMENT UNCERTAINTY
Date Updated : 10/9/2018
Test name: Determination of Residue by Oven Drying Updated by : Nurul Azira
(Liquid Admixture)

Report Ref: SIM/MTS/PT/ADM/ROD/0001-0003

Quantity Trial 1 Trial 2 Trial 3 Average St. Dev Quantity Symbol Equation Value
m2, mass of stoppered bottle with sand (g) 56.185 60.215 59.315 58.6 2.115 Residue by Oven Drying %m (m4-m2)/(m1-m2)*100 19.8
m1, mass of stoppered bottle with sand & sample (g) 60.365 64.245 62.74 62.5 1.956 Sens. Coeff m1 Cm1 100(m4-m2)/(m1-m2)2 -5.10
m3, mass of sample (m2-m1) (g) 4.18 4.03 3.425 3.9 Sens. Coeff. m2 Cm2 100(m4-m1)/(m1-m2)2 20.69
m4, mass of stoppered bottle with sand & dry residue (g) 57.005 60.995 60.015 59.3 2.07928673668 Sens. Coeff. m4 Cm4 100/(m1-m2) -25.78
m5 = m4 - m2 (g) 0.82 0.78 0.7 0.8
Residue by Oven Drying (m 5/m3)*100% 19.6 19.4 20.4 19.8 0.565

Uncertainty Calculation for: Residue by Oven Drying

Component Symbol Unit Evaluation Dist. Range/st dev. Divisor/factor std. Ui Ci (UiCi)2 νi (CiUi)4/νi % contribution
Repeated Observation: (%m) UA(%m) % A normal 0.565 1.732 0.3262 1.00 0.10642 2 0.00566278507 99.39
Calibration: Weighing Balance(m 1) Ucal(m1) g B normal 0.001 2 0.0005 -5.10 0.00001 60 7.0306265E-13 0.01
Resolution: weighing balance (m 1) Ures(m1) g B rectangular 0.001 1.732 0.0006 -5.10 0.00001 infinity 0 0.01
Calibration: Weighing Balance (m 2) Ucal(m2) g B normal 0.001 2 0.0005 20.69 0.00011 60 1.9078313E-10 0.10
Resolution: weighing balance (m 2) Ures(m2) g B rectangular 0.001 1.732 0.0006 20.69 0.00014 infinity 0 0.13
Calibration: Weighing Balance (m 4) Ucal(m4) g B normal 0.001 2 0.0005 -25.78 0.00017 60 4.604137E-10 0.16
Resolution: weighing balance (m 4) Ures(m4) g B rectangular 0.001 1.732 0.001 -25.78 0.00022 infinity 0 0.21
Unit
SUM 0.1071 (N/mm2)2
UC 0.3272 N/mm2
Based on SAMM, k = 2
Eff DoF 2.02
Equipment ID No (weighing balance): SIM/HQ/E/0262 k 2
UE (±) 0.7 %

Prepared By: Checked By:

 SOIL INSTRUMENTS (M) SDN BHD
CALCULATION OF MEASUREMENT UNCERTAINTY Report No : MU/EOS/MTS/18/004a

Test name: Compressive and Flexural Strength of Prismatic Test Specimens from Cement Mortar Date Updated : 10/9/2018
Updated by : Nurul Azira

Report Ref: SIM/MTS/ILC/CFS/CM/0001/2d - 0003/2d

Max Load Compressive

Sample I.D Weight (kg) Depth Width (kN) Strength (MPa) Quantity Symbol Equation Value
ILC/C 0001-1-1 0.58 41 40 61.5 38.4 Compressive Strength σ σ=F/(DW) 36.1
ILC/C 0001-1-2 0.58 41 40 63.2 39.5
ILC/C 0001-2-1 0.58 41 40 64.4 40.3 Sensitivity Coeff. (Load) CF dσ/dF=1000/(DW) 0.625
ILC/C 0001-2-2 0.58 41 40 60.1 37.6
ILC/C 0001-3-1 0.57 41 40 63.0 39.4
ILC/C 0001-3-2 0.57 41 40 64.1 40.1
ILC/C 0002-1-1 0.57 41 40 56.1 35.1
ILC/C 0002-1-2 0.57 41 40 54.4 34.0
ILC/C 0002-2-1 0.57 41 40 53.3 33.3
ILC/C 0002-2-2 0.57 41 40 46.1 28.8
ILC/C 0002-3-1 0.57 41 40 53.5 33.4
ILC/C 0002-3-2 0.57 41 40 53.7 33.6
ILC/C 0003-1-1 0.57 41 40 57.5 35.9
ILC/C 0003-1-2 0.57 41 40 59.3 37.1
ILC/C 0003-2-1 0.58 41 40 62.6 39.1
ILC/C 0003-2-2 0.58 41 40 53.7 33.6
ILC/C 0003-3-1 0.57 41 40 57.5 35.9
ILC/C 0003-3-2 0.57 41 40 56.9 35.6
Average 61 36.1
Standard Deviation 4.9 3.1

Uncertainty Calculation for: Compressive Strength

Component Symbol Unit Evaluation Dist. Range/st dev. Divisor/factor std. Ui Ci (UiCi)2 νi (CiUi)4/νi % contribution
Repeatability: Load (F) UA(F) kN A normal 4.9 4.24 1.16 0.625 0.5213 5 0.05435886847348 63.810
Calibration: Compression Machine Ucal(F) kN B normal 1.74 2 0.87 0.625 0.295664 60 0.00145695396423 36.188
Resolution: Machine Ures(F) kN B rectangular 0.01 1.73 0.01 0.625 0.000013 infinity 0 0.002
Unit
SUM 0.8170
UC 0.90 MPa
Eff Dof 11.96
SAMM req., k = 2
Equipment ID No (Compressive Machine): SIM/HQ/E/0326a k 2
UE (±) 1.8 MPa

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