Standard Unit Glass Equipment GOAL
Standard Unit Glass Equipment GOAL
STANDARD UNITS
INTRODUCTION
Standard Units/ Assemblies are multi-purpose units having flexibility of utility. These units have been standardized by incorporating
all basic & essential features such as heating, stirring, condensation, fractionation, cooling etc. for multi-purpose use. Therefore,
though termed “Standard Units” from constructional view point they actually serve as “Flexi Units” from utility point of view.
These units find use in educational institutions, R&D centers and industries. They can be conveniently and quickly modified according
to specific process needs due to modular construction. Borosilicate glass offers additional benefits of universal corrosion resistance,
visibility and cleanliness.
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STANDARD UNITS
1. Glass Reactor With Metal Jacket
2. Simple Distillation Unit
3. Reaction Unit
4. Fraction Distillation Unit
5. Reaction Distillation Unit
6. Liquid-Liquid Extraction Unit
7. Solid-Liquid Extraction Unit
8. Assembly over GLR
9. Gas Scrubber
10. Multi Purpose Unit
11. Mobile Mixing System
NEW 12. Essential Oil Distillation Unit
13 Agitated Glass Nutsche Filter, Peptide Synthesizer
Goel Scientific offers Glass Reactor with Metal Jacket for chemical &
pharmaceutical industries for process development. Glass reactor will have
metal jacket and metal insulation.
Key Features:
Ÿ Reactor lift for easy opening i.e optimised for easy vessel cleaning.
Ÿ Temperature monitoring and control.
Ÿ Gas purging available.
Ÿ Vacuum / exhaust piping arrangement.
Ÿ Additional feeders / receivers as per requirement.
Ÿ Solid feeding arrangement.
Ÿ Ready for Cryogenic reactions (-50°C).
Ÿ Mixed systems with pressure reactor and vacuum distillation.
VENT/VACUUM
VALVE
SS-PTFE LINED
STIRRER
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STANDARD UNITS
SIMPLE DISTILLATION UNIT
It consists of a vessel mounted in a heating bath and fitted with a condenser for
VAPOUR LINE
condensing the vapours. A receiver with drain valve can be added for receiving
the condensate.
The units are available in vessel sizes of 20, 50, 100, 200, 300 & 500 L and is LIQUID
suitable for operation under atmospheric pressure and full vacuum. INLET
REACTION UNIT
This unit is used for carrying out reactions under stirred condition and with
provision for simple reflux distillation. VENT / VACUUM
The reaction vessel is mounted in a heating bath and fitted with addition vessel,
motor-driven stirrer and provision for condensation with refluxing. The product
is sub-cooled and collected in a receiver.
The units are available in vessel sizes of 20, 50, 100, 200, 300 & 500 L and is
suitable for operation under atmospheric pressure and full vacuum. CONDENSER
ADDITION
VESSEL
REFLUX
Unit Reactor Bath Addition Vapour Condenser Cooler Receiver DIVIDER
BOTTOM OUTLET
DRAIN VALVE
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STANDARD UNITS
FRACTIONAL DISTILLATION UNIT
CONDENSER The top product is sub-cooled and collected in receivers. The bottom product is
finally drained from the reboiler through a drain valve.
The units are available in vessel sizes of 20, 50, 100, 200, 300 & 500 L and is
REFLUX suitable for operation under atmospheric pressure and full vacuum
DIVIDER
HEATING BATH
FINAL RECEIVER
This is a versatile unit and can be used as Reaction Distillation Unit, Fractional
VENT / VACUUM Distillation Unit or a combination of both. All features of Reaction Distillation
Unit and Fractional Distillation Unit are incorporated.
The units are available in vessel sizes of 20, 50, 100, 200, 300 & 500 L and is
suitable for operation under atmospheric pressure and full vacuum.
CONDENSER
REFLUX DIVIDER Unit Reactor Bath Addition Vapour Condenser Cooler Receiver
REACTIONAL Cat.Ref Capacity KW Vessel Line HTA M2 HTA M2 Size
DIST.COLUMN
MOTOR FRU20 20 L 4.0 2L 80 DN 0.35 0.10 2L, 5L
FRU50 50 L 6.0 5L 100 DN 0.50 0.20 5L, 10L
ADDITION FRU100 100 L 9.0 10 L 150 DN 1.50 0.35 10L, 20L
VESSEL FRU200 200 L 12.0 20 L 150 DN 1.50 0.35 10L, 20L
PRODUCT COOLER
FRU300 300 L 18.0 20 L 225 DN 2.50 0.50 20L, 20L
VACUUM FRU500 500 L 24.0 50 L 300 DN 4.00 0.70 50L, 50L
FIRST RECEIVER
VESSEL
VENT/VACUUM
STIRRER VALVE
HEATING
BATH FINAL RECEIVER
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STANDARD UNITS
LIQUID-LIQUID EXTRACTION UNIT
Liquid extraction, sometimes called solvent extraction, is the separation of
constituents of a liquid solution by contact with another insoluble liquid. The
unit described here is for a semi-batch operation. VENT
The units are available in vessel sizes of 20, 50, 100, 200 & 300 L and is suitable
VAPOUR
for operation under atmospheric pressure.
PIPELINE
EXTRACTION
VESSEL
The solid to be extracted is put inside a glass fiber bag and placed in an extraction
vessel. Solvent from the reboiler is continuously evaporated, condensed and
OVER HEAD
circulated through a reflux divider by means of piping network and valves. When
CONDENSER
desired/ steady concentration of solute is achieved in the solution the operation
is discontinued. The solution is drained off and collected for further use.
REFLUX DIVIDER
After charging fresh solid in fiber bag and solvent in reboiler, the cycle can be
restarted again.
The units are available in vessel sizes of 20, 50, 100, 200 & 300 L and is suitable
for operation under atmospheric pressure.
EXTRACTION
VESSEL VAPOUR
PIPELINE
Unit Reactor Bath Vapour Extraction Condenser VALVE
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STANDARD UNITS
ASSEMBLIES OVER GLASS LINED REACTOR
Glass Lined Reactors are used instead of glass reactors specially when scale of
operation is large and relatively high pressure steam is to be used as heating
media. Quite often assemblies like Simple Distillation Unit, Reaction Distillation
Unit, Fractional Distillation Unit etc. are installed above glass lined reactors. The
basic features of these assemblies remain the same but glass shell and tube
heat exchanger is preferred due to large scale of operation. A typical fractional
distillation unit type assembly over GLR is shown in adjacent figure.
CONDENSER
Cat.Ref. Reactor Cap. Vapour column Condenser HTA M²
VAPOUR LINE GRU 250 250 L 80mmX1.5m 1.5X2
GRU 500 500 L 100mmX2m 1.5X2
VENT/VACUUM GRU 1000 1000 L 100mmX2m 2.5X2
GRU 2000 2000 L 150mmX3m 2.5X3
VALVE
GRU 3000 3000 L 150mmX2m 4.0X2
RECEIVER
DRAIN VALVE
REACTOR
GAS SCRUBBER
VENT
Goel offer Pilot Plant Gas Scrubber for various gases likes HCl, Cl2, SO2, Br2, HBr,
NOx etc or any other corrosive gases. These scrubbers use the media as water /
Aq. NaOH / any other suitable solvent which can neutralise the exhaust gases.
Our Pilot plant scrubber are ranging from 20L vessel capacity to 500L vessel
capacity and scrubber diameter from 80DN to 300DN.
CHW
PACKED RETURN We can also design and offer big size scrubber in Glass up to 800DN (i.e.
COLUMN
400/450/600/800DN). Our scrubber will be having inbuilt Cooler to remove the
heat of absorption. We also offer mini Blower of PP/FRP on request along with
CONDENSER the Pilot Plant Scrubber.
Pilot Plant Gas scrubber are mainly used in pharmaceutical, chemical, refinery &
other industries. Glass scrubber offer process visibility as well as excellent
CHW corrosion resistance. Being a Glass Scrubber pressure drop across the scrubber
SUPPLY will be minimized.
GAS
IN
CIRCULATION
PUMP
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STANDARD UNITS
MULTI PURPOSE UNIT
CONDENSER
JACKETED PIPE
VFD
MOTOR
JACKETED
VESSEL
RECEIVER
G Goel Offer multipurpose pilot plant for chemical and pharmaceutical industries for process
development, scale-up, process simulation and kilo-scale cGMP production in batch and semi-
batch operation. The pilot plant used for chemical processing includes solid charging, liquid
charging, reaction, heating / cooling, rectification, auto / manual reflux arrangement, layer
separation, product cooler, vacuum catch pot, vacuum header etc.
G The multipurpose pilot plant designed in such a way that we can modify the same easily as
per process requirement.
Available with
G Jacketed full glass reactor/ Cylindrical full glass reactor with Oil heating cooling bath / Spherical
full glass reactor with Oil heating cooling bath
G Multipurpose glass distillation overhead
G Stainless steel / MS epoxy coated / MS painted frame supporting
G Flame proof / Non flame proof / cGMP / non GMP models available
G Excellent corrosion resistant.
G Temp. Controller.
G Gas purging, solid charging / multi liquid addition.
G Vacuum / exhaust piping
G Additional feeders / receivers
G Solid feeding
STANDARD UNITS
MOBILE'MIXING SYSTEM
Cylindrical Miixng Reactor
Glass Reactors are ideally used for wide applications in laboratory, pilot plant &
MOTOR for small-scale production. They reduce the need for investment in permanent
installations & also reduce the pressure & temperature losses resulting from
pipeline installation.
These reactors are available with spherical shape & in cylindrical shape. These
PTFE BELLOW reactors are also available in cylindrical jacketed form.
STIRRER
CLOSURE
VESSEL
HOLDER
BOTTOM
OUTLET VALVE
BOTTOM OUTLET
VALVE
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STANDARD UNITS
ESSENTIAL OIL DISTILLERS
An essential oil is a concentrated hydrophobic liquid containing volatile (easily evaporated at normal temperatures) chemical compounds from plants. Essential
oils are also known as volatile oils, ethereal oils, aetherolea, or simply as the oil of the plant from which they were extracted.
Essential oils are generally extracted by distillation, often by using steam. We provide two modes through which one can produce essential oils viz. Steam
Distillation Unit & Vacuum Distillation Unit.
Steam distillation as a whole is a separation process which consists of distilling water together with other volatile and non-volatile components. The water is
heated up in the spherical vessel separately and the steam from the boiling water goes into the reactor where it reacts with the masses of trees and plants and
further carries the vapor of the volatiles to a condenser, where both are cooled and return to the liquid or solid state; while the non-volatile residues remain
behind in the reactor.
Vacuum
Vent
NEW
Addition
Vessel
Heat Exchanger
Vapour Line
Steam Inlet
Charging
Charging
Vacuum
Reactor Thermowell Thermowell Vent
Vessel
Receiver
Vessel
Vessel Holder
STANDARD UNITS
AGITATED GLASS NUTSCHE FILTER/
PEPTIDE SYNTHESIZER
Agitated Glass Nutsche Filter is a closed vessel designed to separate solid and
liquid by filtration under vacuum. The closed system ensures odourless
contamination free and non-polluting working conditions maintaining product
purity and hygiene. Agitated Nutsche Filters are extensively used in Herbal
products, Chemical product development, kilo lab operation,pharmaceutical
manufacturing, agro chemical and the food industry.
GENERAL DESCRIPTION
A typical unit consists of a dish shape vessel vessel with a perforated plate. The
entire vessel can be kept at the desired temperature by using a mixer / agitator
and jacket.It's completely leak-proof for vacuum or pressure service. The base
plate is having arrangement of bolting bar to hold the filter cloth. Suitable nozzles
can be provided including Manhole and Side discharge nozzle. PTFE Lined
Stirrersare used for Agitator shaft and solid PTFE blades are used to take high
torque generation during solid discharge and re-slurring operation.Drive
assembly consist of Motor with VFD, Mechanical Seal is provided for vacuum
application. Borosilicate Glass Vessel with different nozzles, Manual/Hydraulic
system is provided for movement of agitator as well as bottom plate. PTFE Filter
Support Plate.
Goel offer Glass ANF from 2 L to 300 L for Kilo Lab Operations with and without
jacket , with and without stirrer.
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STANDARD UNITS
HCL ADIABATIC ABSORPTION
Vent
HCl absorption columns are used for absorption of Hydrochloric gas, which statutorily
are not permitted to vent in to the atmosphere, and to produce the HCl acid. The
column is constructed with a series of packed sections, a gas introduction point below
that, a condenser on the top, and a cooler at the bottom. Make water is sprayed from
the top and acid is collected from the bottom. Packed Column
HCl absorption column are available in 80DN to 300DN diameter (for the gas rate
10Kgs/hr to 300Kg/hr approx..)