S P E C I F I C A T I O N S

Infrared Spectroscopy

Spectrum 3 FT-IR
Spectrometers

Spectrum 3 FT-IR with UATR

Introduction
The PerkinElmer Spectrum 3™ is the gold standard in FT-IR and FT-NIR spectrometers,
enabling laboratories to obtain the highest quality and most reproducible data with
exceptional ease. A broad range of “plug-and-go” sampling accessories and software
packages ensure the best solution for a range of applications. Whatever your specific
laboratory requirements, the Spectrum 3 delivers best-in-class accuracy, precision and
reliability ensuring the utmost confidence in your results.

PerkinElmer Spectrum 3 FT-IR spectrometers are built to the highest ISO-9001 manufacturing
standards. This document presents technical information and typical performance
specifications for the Spectrum 3 FT-IR instruments based on recent factory tests.
OPTICAL PERFORMANCE
Wavelength Range 8,300 – 350 cm-1 with 11000 – 375 cm-1 with For dedicated optimised NIR operation,
optimized, proprietary KBr proprietary extended range the Spectrum 3 FT-NIR and dual range
beamsplitter 7,800-225 cm-1 KBr beamspplitter and dual NIR/MIR are available. See seperate
with CsI beamsplitter option source option technical specification sheet for details
Spectral Resolution 0.4 cm-1 for the 3028 cm-1 band in Methane
Wavenumber Accuracy 0.02 cm-1 at 2,000 cm-1
Signal-to-Noise 10,000:1 peak-peak, 5 seconds 15000:1 peak-peak, 5 seconds
34,000:1 peak-peak, 1 minute 50,000:1 peak-peak, 1 minute
with high performance pack

Wavelength Repeatability
Mid-IR ±0.02 cm-1 at 1,600 cm-1 ±0.007 cm-1 achievable
Near-IR ±0.02 cm-1
at 7,200 cm-1
(±0.004 nm at 1,390 nm)
Time Resolved Spectroscopy Optional FastScan module Up to 100 scans/sec at 16 cm-1 resolution

OPTICAL SYSTEM
General Sealed and desiccated optical unit. Vibration isolated baseplate.
Interferometer Improved rotary Michelson interferometer for fast scanning, self-compensating for dynamic alignment changes
due to a tilt and shear, incorporating high reflectivity, first-surface aluminum-coated optics.
Optics Kinematically mounted, zero alignment optics.
Mirrors High reflectivity and a low-angle off axis design.
Detectors Capabilities for two permanently installed internal detectors, plus external detector via General Purpose
Optical Bench (GPOB). Single software click to switch active detectors. For internal detectors, choose from:
• High linearity Lithium tantalate
• Fast-recovery FR-DLaDTGS
• Mercury cadmium telluride (MCT)
Source Long-life source with proprietary hot-spot stabilization. User replaceable.
Beamsplitter • Standard optimised KBr
• Extended range KBr option
• Extended range CsI option
Desiccant Accepts disposable packs or rechargeable desiccant cartridges. Visible desiccant lifetime indicator.
External Beam Ports Optional external beam ports providing 2 additional output plus 1 additional input beam.
General Purpose Optical Bench (GPOB) Optional optical bench available for custom accessories and detectors.
Validation Software controlled validation wheel containing a polystyrene reference material, traceable to a NIST standard
for wavenumber accuracy and a Schott NG11 filter for ordinate repeatability.
Full Optical Upgradeability Single range Spectrum 3 systems can be upgraded to multi-range IR/NIR or IR/FIR optical benches.

DATA SYSTEM AND ELECTRONICS

Signal Sampling Over-sampling delta-sigma converter.
Communication TCP/IP interface allows direct connection with LAN.
Instruments can be configured with their own IP address allowing control via the internet.
Calibration Transfer Optional Absolute Virtual Instrument (AVI) – actively standardizes instrument response to further improve
repeatability and protect data integrity.
Atmospheric Compensation Minimizes effect of atmospheric water and CO2 on the sample spectra without the need for reference or
calibration spectra. Operates at various instrument setttings without having to recalibrate the correction.
Accessory Recognition Spectrum 3 accessories and ATR top plates are automatically detected as soon as they are locked into the
sampling area. Instrument parameters are optimized for the installed accessory. Serial numbers for accessories
and top plates are stored with all data.
Error Trapping All sample spectra are checked for common spectroscopic and sampling problems. Key instrument components
are continuously monitored.
Productivity • Spectrum 3 Smart Panel allows at-bench view of diagnostics and instrument control in addition to standard PC or panel PC control.
• Look-ahead function automatically detects when a sample is placed into the sample compartment.
Data is collected while the operator is entering sample information.
• On-instrument remote user interface and software Sample Table allows remote, continuous sampling at
the instrument eliminating analysis steps and speeding operation.
 BENCH DETAILS
Size 520 mm x 600 mm x 300 mm (W x D x H).
Weight 34 kg

SOFTWARE
General A single software platform incorporates all of the functions required for infrared analyses; instrument control,
data manipulation and analysis, and flexible report utilities. A suite of optional software packages provide
advanced capabilities or functions designed for specific application areas.
Sample Table Increases productivity by enabling multiple samples to be defined in batches. Integrates with Smart Panel
allowing remote continuous operation.
User Interface Password-protected user login function. Access to methods and routines, menu, toolbar and toolbox functions
can be controlled by a supervisor.
Reports Quick print facility for graphs, spectra and results windows. User defined templates can be created to enable
custom printed and electronic reports.
Processing 1st-4th derivative with a variable filter, smooth (Savitsky-Golay, moving average and triangular), difference,
normalization, A, %T, %R, KM, LOG (1/R), ordinate modes, cm-1, nm and micron abscissa modes, +,-,*,/,
difference, baseline correction, smooth, deconvolution, normalize, interpolate, blank, Kramers-Kronig, advanced
ATR correction, peak table, peak height and peak area.
Materials Testing Patented COMPARE™ spectral comparison algorithm and Euclidean searching. Spectral searching against
commercially available or customer-developed libraries. Multi-component search option for up to 10 components.
Advanced ATR preprocessing options to allow improved searching of ATR spectra against transmission libraries.
Quantitative Analysis Single frequency, method development software. Includes Beer’s Law, PLS and PCR quantitative prediction.
Adulterant Screening Unique chemometrics-based approach to estimation of adulterants in spectra. Simple method development
requires just typical pure spectra and spectra of potential adulterants.
Validation Instrument performance and user configurable system suitability routines available as standard. Instrument
Scheduler facility allows auto-programming of instrument validation testing.
Macros Macro Editor and Equations Editor provide the ability to setup sequences of data collection and custom spectral
processing. These procedures can then be stored and repeated using a single mouse click. Simple user-interface
development designed for Touchscreen PC interaction - Spectrum Touch software option.
User Training Use, common maintenance and software operation. Context-sensitive help provides assistance throughout
the software.
Further Optional packages
21 CFR Part 11 Enhanced Security™ (ES) software meets the technical requirements for the FDA’s 21 CFR Part 11.
Cloud Connectivity PerkinElmer NetPlus for IR option allows operators within organisations to collaborate by securely sharing
IR data, methods and more via the cloud.
Sample Analysis Workflows AssureID™ software designed for FT-IR and FT-NIR materials testing and product verification.
Supports Mid-IR and NIR products testing through a customizable wizard-style interface.
Simple turnkey Compare, SIMCA, quantitative analyses with user defined instructions and
reports can be readily configured. OLE-DB compliant data storage with ES and non-ES versions available.
Quantitative Analysis Optional method development software for PLS and PCR quantitative method development.
Validation CD Data validation CD contains test algorithm descriptions, test data and results for data transform algorithms.
Comprehensive UOQ/IQ/OQ documentation and services available.

PerkinElmer, Inc.
940 Winter Street
Waltham, MA 02451 USA
P: (800) 762-4000 or
(+1) 203-925-4602
www.perkinelmer.com

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