Dr.

Babasaheb Ambedkar Technological University

Lonere - 402 103
(Diploma Wing)

Proposed Curriculum
For
III Year Diploma (Chemical Engineering)
Aligned with NEP
(W. E. F. 2024-25)
 INDEX
Sr Course Course Title Page No.
No. Code
Semester-V

01 DCH3101 Heat Transfer Operation

02 DCH3102 Environmental Pollution and Control
03 DCH3103 Chemical Engineering Drawing and
Calculations
04 DCH3104 Elective -I
05 DCH3105 Management Skills and TQM
06 DCH3106 Heat Transfer Operation Lab
07 DCH3107 Environmental Pollution and Control
Lab
08 DCH3108 Chemical Engineering Drawing and
Calculations Lab
09 DCH3109 Minor Project / Seminar
10 DCH3110 Industrial Training (After IV Sem
Evaluated in V Sem)
Sr Course Course Title Page No.
No. Code
Semester- VI
01 DCH3201 Chemical Reaction Engineering
02 DCH3202 Mass Transfer Operation
03 DCH3203 Elective -II
04 DCH3204 Elective -III
05 DCH3205 Entrepreneurship Development
06 DCH3206 Chemical Reaction Engineering Lab
07 DCH3207 Mass Transfer Operation lab
08 DCH3208 Major Project
 Dr. Babasaheb Ambedkar Technological University, Lonere
Proposed Learning and Assessment Scheme for Diploma Programs (W. E .F. 2024-25)
Diploma in chemical engineering
Semester –V
Sr. Course Title Course Course Total Learning Scheme Credits Assessment Scheme
No. Code Type IKS Actual Contact SL NL
Hrs Hrs./Week Hrs/ Hrs/
for Week Week
CL TL LL SL FA- SA- FA- PR/ Total
Sem
MSE ESE TW OR
1 Heat Transfer Operation DCH 3101 AEC 4 3 1 - 1 5 5 20 20 60 -- -- 100
2 Environmental Pollution and DCH 3102 DSC 3 3 - - 1 4 4 20 20 60 -- -- 100
Control
3 Chemical Engineering DCH 3103 AEC 3 3 - - 1 4 4 20 20 60 -- -- 100
Drawing and Calculations.
4 Elective -I DCH 3104 AEC 3 3 - - 3 3 20 20 60 -- --
100
-
5 Managerial skills and TQM DCH 3105 SEC 3 3 - - - 3 3 20 20 60 -- -- 100
6 Heat Transfer Operation Lab DCH 3106 AEC - - - 2 - 2 2 60 40 100
-- -- --
7 Environmental Pollution and DCH 3107 DSC - - 2 2 60 40
Control Lab 100
- - 2
-- -- --
8 Chemical Engineering DCH 3108 AEC 60 40
- - - 2 - 2 2 -- -- -- 100
Drawing and Calculations
Lab
9 Minor Project/Seminar DCH 3109 AEC 60 40
- - - 3 3 3 -- -- -- 100
Total 16 12 1 9 3 28 28 28 100 300 240 160 900
 ELECTIVE – I
Momentum Transfer
Membrane Technology
Biochemical Engineering

Abbreviations: CL-Classroom Learning, TL-Tutorial Learning, LL-Laboratory Learning, FA-Formative Assessment, SA-
Summative Assessment, PR/OR – Practical/Oral, MSE-Mid Sem Examination, TW-Term Work, IKS- Indian Knowledge
System, NL-National Learning
*SL-Subject wise Self learning includes online course, assignments/models, case study, industry exposure/internship,etc. (Self-
Learning hours shall not be reflected in Time Table)
Course Category: DSC – Discipline Specific Course; AEC – Ability Enhancement Course; SEC – Skill Enhancement Course; VEC – Value Education Courses, @
Internal Assessment, #-No Theory Examination.
 Dr. Babasaheb Ambedkar Technological University, Lonere
Proposed Learning and Assessment Scheme for Diploma Programs (W. E.F. 2024-25)
Diploma in chemical engineering
Semester –VI
Sr. Course Title Course Course Total Learning Scheme Credits Assessment Scheme
No. Code Type IKS Actual Contact SL NL
Hrs Hrs/Week Hrs/ Hrs/
for CL TL LL Week Week SL FA- SA- FA- PR/ Total
Sem
MSE ESE TW OR
1 Chemical Reaction DCH 3201 AEC 6 4 2 - 1 7 7 20 20 60 -- - 100
Engineering -

2 Mass Transfer Operation DCH 3202 DSC 4 3 1 - 1 5 5 20 20 60 -- - 100

-
3 Elective -II DCH 3203 AEC 3 3 - - - 3 3 20 20 60 -- - 100
-
4 Elective -III DCH 3204 DSC 3 3 - - - 3 3 20 20 60 -- - 100
-
5 Entrepreneurships DCH 3205 SEC 3 3 - - - 3 3 20 20 60 -- - 100
Development -

6 Chemical Reaction DCH 3206 DSC - - - 2 2 60 40 100

Engineering Lab 2 -- -- --

7 Mass Transfer Operation DCH 3207 60 40 100

DSC - - - 2 2 2 -- -- --
Lab
8 Major Project DCH 3208 60 40 100
AEC - - - 2 3 3 -- -- --

Total 19 16 3 6 2 28 28 28 100 300 240 160 900

 Abbreviations: CL-Classroom Learning, TL-Tutorial Learning, LL-Laboratory Learning, FA-Formative Assessment, SA-
Summative Assessment, PR/OR – Practical/Oral, MSE-Mid Sem Examination, TW-Term Work, IKS- Indian Knowledge
System, NL-National Learning
*SL-Subject wise Self learning includes online course, assignments/models, case study, industry exposure/internship, etc. (Self-
Learning hours shall not be reflected in Time Table)
Course Category: DSC – Discipline Specific Course; AEC – Ability Enhancement Course; SEC – Skill Enhancement Course; VEC – Value Education Course.

ELECTIVE – II
Numerical Methods
Petroleum Technology
Polymer Technology
ELECTIVE – III
Chemical Plant Economy and Energy Management
Fuels and Combustion
Rheology of Complex fluids

7
 SEMESTER-V
Course Title Heat Transfer Course Code DCH 3101
Operation
Learning Scheme Assessment Scheme: Credits- 4
Classroom Learning 4 Hrs/Week Self-Learning (SL) 20 Marks
CL)
Tutorial Learning 0 Hrs/Week Formative Assessment (FA) 20 Marks
(TL)
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
The students should be able to understand different modes of heat flow, principles of heat transfer,
different heat transfer equipment’s, & their uses. They also understand the fundamental quantitative
methods of calculation with special relevance to chemical engineering & practical utility viz, the
application of the principles to the design of heating & cooling equipment.
Course Outcomes:
After completion of this course the students are expected to be able to demonstrate following
knowledge, skills and attitudes:
1. Determine the rate of heat transfer by conduction.
2. Apply the concept of convection to operate heat exchangers
3. Determine the rate of heat transfer by convection.
4. Determine the amount of heat transfer by radiation.
5. Choose proper heat transfer equipment for various applications
6. Calculate energy associated with evaporators
Unit Cont Hrs Marks
ents
SL FA SA
Unit-1 Conduction 6 3 3 7
1.1 Modes of heat transfer - definition with examples, Fourier’s
law-statement, mathematical expression, Thermal
conductivity - definition, relation with temperature
1.2 Description of steady state conduction, Unsteady state heat
conduction
1.3 Derivation of rate of heat flow by conduction through
rectangular block, composite wall, cylinder, sphere &
numerical
1.4 Study of variation of thermal conductivity with
temperature optimum thickness of insulation -concept &
definition
Unit-2 Convection-I 6 4 4 9
2.1 Natural & forced convection – definition &example,
Film coefficient – concept, definition and unit
2.2 Derivation of overall heat transfer coefficient from hot
fluid to cold fluid through metal wall. Effect of surface
coefficient on overall heat transfer coefficient
2.3 Dimensional analysis for heat transfer for understanding
8
 the use of Reynold’s number, prandtl number, Nusselt
number and Grashoff number in calculating film
coefficient
2.4 Calculating heat transfer coefficient in laminar &
turbulent flow. Convective heat transfer in laminar and
turbulent boundary layers
Unit-3 Convection-II 7 4 4 9
3.1 Co-current & counter current heat flow- concept, schematic
representation &comparison, Concept of Log Mean Temp.
Difference, derivation & numerical based on this
3.2 Boiling – definition of saturated pool boiling, boiling curve,
study of film boiling, nucleate boiling & transition boiling
3.3 Condensation – definition, Dropwise & film wise
condensation – definition & relative merits & demerits,
effect of vertical & horizontal heat transfer surface on heat
transfer coefficient
3.4 NTU – epsilon method for exchanger evaluation
Unit-4 Radiation 6 3 3 11
4.1 Radiation- Definition & examples, Definition of
absorptivity, reflectivity and transmissivity
4.2 Laws of radiation- statement & mathematical expression
of Plank’s Law, Wien’s displacement law, Stefan
Boltzman law, Definition, mathematical expression &
description of Kirchoff’s law
4.3 Mathematical expression for rate of radiation between
two surfaces, numerical based on that, Definition of
black body, Gray body
4.4 luminous and non-luminous gases, emissivity, Emissive
power, Combined heat transfer, i.e. conduction,
convection and radiation together.
Unit-5 Heat Transfer Equipment 6 3 3 12
5.1 Different heat transfer equipment in chemical industry-
names & uses
5.2 Diagram, construction, working of different types of-
Double pipe Heat Exchangers, Shell & Tube Heat
Exchanger, Single pass & multiple pass heat exchangers
5.3 Extended Surface heat exchanger, plate type heat exchanger
5.4 condensers & vaporizers
Unit-6 Evaporation 5 3 3 12
6.1 Definition of evaporation, comparison of Evaporation &
Drying
6.2 Statement & effects of properties that influences
evaporation, Definition & description of capacity &
economy of evaporator, methods to improve economy
6.3 Material & enthalpy balance for single effect evaporator,
9
 numerical based on this topic to calculate area of
evaporator
6.4 Detailed study of construction, working, diagram &
application of open pan evaporator, Horizontal tube
evaporator, Vertical tube evaporator, Long tube vertical
evaporator, forced circulation evaporator, vapour
Recompression
Total 36 20 20 60

Sr. Suggested tasks for Self-Learning

No
1 Prepare a model of any type of heat exchanger
2 Conduct/participate in MCQ/Quiz.
3 Give seminar on relevant topic
4 Prepare a model of any one type of evaporator
Sr.
Reference Books
No
Title Author Publication
1
Unit operation of chemical Engineering, 4th W. L. McCabe J. C. Smith McGraw Hill
edition and P. Harriot 1985
2
Process Heat Transfer D. Q. Kern McGraw Hill,
1950
3 J. M. Coulson and J. F.
Chemical Engineering”, Vol. 1 ELBS Pergamon press,
Richardson 1970
4 P. K. Nag McGraw Hill
Heat & Mass Transfer, 3rd edition

Sr. Suggested Learning Websites/Portals/App

No
1 https://www.classcentral.com/course/swayam-heat-transfer-10061
2 https://youtu.be/ljmWQIkm61U?si=gVIFommZibuddLXT
3 http://ocw.mit.edu

10
 SEMESTER-V
Course Title ENVIRONMENTAL Course Code DCH 3102
POLLUTION CONTROL
Learning Scheme Assessment Scheme: Credits-4
Classroom Learning (CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) - Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1-Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives: Understand the effect of pollution due to various factors such as air, water, soil, and noise
on ecosystem.
Course Outcomes:
Students will be able to:
CO1: Relate the concept of major conflicts of development and environment
CO2: Learn the sources of air pollution and its control.
CO3: Comprehend the term water pollution with its classification and impacts.
CO4: Understand regulatory aspects of pollution control.
CO5: Analyse the hazardous waste with its management Course Outcomes (CO):

Unit Contents Hrs Marks

SL FA SA
Unit-1 Impact of man on the environment 7 3 6 6
Pollution of Air, Water, Soil- Impact of coal mining, Fossil fuel
related pollutants in the environment, Carbon emission and Global
warming, Reduction in carbon emission, Impact of Urban areas,
Environmental impacts of Hydroelectric and nuclear energy,
chemical pollution, solid waste, Marine pollution, ozone depletion.
Unit 2 Air Pollution and its control 7 4 5 5
Definition and scales of concentration, Classification and
Properties of air pollutants, Emission sources- Classification, other
methods of air pollution sources, Emission sources in India, Effect
of air pollution- Human Health, Air pollution effect on vegetation,
Materials, Damage to health, Vegetation and Materials in India.
Air pollution control methods
Control methods, Particular Emission control, Control of Gaseous
Emission

11
Unit 3 Sources and Classification of Water Pollutants 6 4 9 9
Water resources, Utilization of water, Types of water pollutants and
their Effects
Wastewater Sampling and Analysis
Sampling, Methods of Analysis, Determination of organic matter,
Determination of Inorganic Substance ,Physical Characteristics,
Water quality standards.
Unit 4 Wastewater Treatment 6 3 - 14
Basic process of Water Treatment, Primary Treatment, Secondary
treatment- Decomposition of organic waste, Aerobic Biological
treatment, Activated sludge process, Trickling Filters, Sludge
Treatment and disposal , Advanced Wastewater Treatment-
Removal of Suspended and Dissolved Solids, Nitrogen and
Phosphorus Removal, Chemical Oxidation
Unit 5 Solid Waste Management 6 3 - 12
Sources and Classification , Public Health Aspects, Methods of
collection , Disposal Methods – Open Dumping, Sanitary landfill ,
Incineration ,Composting, Potential Methods of Disposal –
Utilization , Recovery and Recycling.
Unit 6 Hazardous waste Management 5 3 - 14
Definition and Sources, Hazardous Wastes classification,
Hazardous waste Management strategy, Treatment Methods-
Physical , chemical and biological treatment, Disposal Methods-
landfill system, landfill closure, Underground Disposal.
TOTAL 36 20 20 60

Sr. No Reference Books

1 Environmental pollution C.S.RAO Mc Graw Hills, 1993,
control engineering fourth edition
Fundamentals of Krishnan Khannan, S. Chand Company Ltd.,1994.
2 Environmental Pollution,
Waste water engineering, Met Calf and Eddy, Tata Mc Graw Hill
3

12
 SEMESTER- V
Course Title PROCESS Course DCH3103
ENGINEERING Code
DRAWING
Learning Scheme Assessment Scheme: Credits- 4
Classroom Learning CL) 3Hrs/Week MSE 40 Marks
Tutorial Learning (TL) -Hrs/Week ESE 70Marks
Self-Learning (SL) 1 Hrs/Week Total 100Marks
Course Objectives:
1. Summarize the concepts of unit operations and unit processes in chemical engineering.
2. Impart knowledge on the concepts of design of major equipment
3. student should be able to visualize views of assembled parts and be acquainted with selection and
operation of different equipment’s.

Unit Contents Hrs Marks

. SL FA SA
Unit- Introduction 4 3 5 5
1 Introduction to Basic Considerations in Process Equipment
Design. Materials of construction: properties, materials, corrosion
and prevention. Symbols for Unit Operation equipment’s,
Instrumentation, Valves as per IS 3232, working and specific
applications of Gate Valve, Globe valve, Ball Valve, Swing
Check & Lift Check valves, Safety Valve.

Unit- Design Considerations 5 3 6 6

2 Introduction, Stresses and Strains, fatigue, brittle fracture, creep,
temperature effects, radiation effects, effects of fabrication
methods. Design of elements: couplings, bearings, joints: type
of joints, threaded fasteners, packing and gaskets, flanges.
Unit- Supports 6 4 9 9
3 Introduction, support for pipes, Leg, bracket and skirt
support, Saddle support
Storage Tanks
Loss mechanism in storage tanks, volume of storage tanks,
design of storage tank, types of storage tank-Atmospheric
storage tanks (types of floating roofs) and pressure storage
tanks (spherical storage tank)
Unit- process equipment 8 4 - 14
4 Design of Double pipe, shell and tube heat exchanger;
evaporators and crystallisers.
Design of Distillation column and absorbers – plate type and
packed columns. Types of packings, Trays.

13
Unit-5 Principles and Design of Reactors 6 3 - 11
Concepts of reaction vessels design
Batch Reactor, continuous flow reactor, semi-batch reactor,
Types of heads, jackets, coils, agitators, baffles, stuffing box,
nozzles.

Unit-6 Develop skill of drawing process flow diagram from process 7 3 - 15

description, for any given chemical process, develop – block
diagram, Process Flow Diagram, Process Instrumentation
Diagram, Tank Farm Layout.

Total 36 20 20 60

Reference Books
1. Peters M., Timmer Haus K., West R., Plant Design and Economics for Chemical Engineers, 5th
ed., McGraw Hill, USA, 2017.

2. Kemp I.C., Pinch Analysis and Process Integration: A User Guide on Process Integration for
Efficient Use of Energy, 2nd ed., Butterworth-Heinemann, USA, 2007.

3. Joshi. M.V., Mahajan. V.V., Process Equipment Design, 5th ed., Mc-Millan India Ltd., India,
2000.

4.Richard A. Turton, Richard C. Bailie, Wallace B. Whiting, Joseph A. Shaeiwitz, Debangsu

Bhattacharyya, Analysis, Synthesis and Design of Chemical Processes, 4th ed., Prentice Hall, USA,
2013.

5. R.W. ZAPPE., valve selection handbook 4th edition.

6 Amir Razmi, Storage Tank Farms Layout and Piping

14
 ELECTIVE – I
Course Title BIOCHEMICAL Course Code DCH 3205
ENGINEERING
Learning Scheme Assessment Scheme: Credits- 4
Classroom Learning CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) - Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) -Hrs/Week Summative Assessment (SA) 60 Marks
. Impart the basic knowledge and overview of biotechnology covering the principles of cell and kinetics, bioreactor
design, sterilization agitation and aeration 2. Understand the physical processes involved in bio-systems 3. Apply
the knowledge of chemical engineering principles to biological processes
Course Outcomes:
After successful completion of course, the students will be able to:
1 Understand significance and scope of biochemical processes
2. Classify microorganisms and cell functions for industrial biochemical processes, enzyme and kinetics for
bioprocesses
3. Apply Chemical Engineering Principles to develop kinetic models for bioprocesses
4. Make use of theoretical basics of chemical engineering and unit operations in designing bioprocess equipment
5. Analyse bioreactor performance
6. Distinguish downstream processing and biological Sewage treatment in solving open ended chemical problems
using biochemical route.

Unit Contents Hrs Marks

SL FA SA
Unit-1 Introduction to Biochemical Engineering 06 4 3 8
1.1 An overview of industrial biochemical processes with typical
examples comparing chemical and biochemical processes –
development and scope of biochemical engineering as a discipline.

Unit-2 Basic microbiology and Biochemistry 07 3 3 9

2.1 Industrially important microbial strains, their classification – structure –
cellular genetics – typical examples of microbial synthesis of biologicals
Unit-3 Enzymes & Applications 05 2 3 10
3.1 Enzymes - in industry, medicine and food – their classification with
typical examples of industrially important enzymes; Mechanism of enzymatic
reactions – Michaelis Menten Kinetics – enzymes inhibition factors affecting
the reaction rates.
3.2Industrial production, purification and immobilization – enzyme reactors
with typical examples.

15
 Unit-4 Kinetics of Cell Growth: 06 3 4 10
4.1Typical growth characteristics of microbial cells – factors affecting growth
Monod model; Modelling of batch and continuous cell growth;
4.2 Immobilized whole cells and their characteristics – free cell and
immobilized cell reactors; Typical industrial examples – transport in cells.

Unit-5 Unit Operations in Biochemical engineering: 06 3 3 11

5.1Newtonian and non-Newtonian behaviour of broth – agitation and mixing
power consumption; Gas/liquid transport in cells – transfer resistances – mass
transfer coefficients & their role in scale up of equipment.
5.2 transfer; Heat transport in microbial systems – Heat transfer correlation’s;
Sterilization cycles; Heat addition & removal during biological production.

Unit-6 Downstream and effluent treatment processes: 06 5 4 12

6.1Downstream processes and effluent treatment: Different Unit operations in
down streaming with special reference to membrane separations, extractive
fermentation;
6.2 Anaerobic and aerobic treatment of effluents – typical industrial examples
for downstream processing and effluent disposal.

Total 36 20 20 60

Sr.no REFERENCE BOOKS: Author Publication

01 Introduction to Biochemical Engineering Rao D.G 1 st ed., Tata McGraw

Hill, India, 2009
02 Bioprocess Engineering Principles, Doran P.M 3 rd ed., Academic Press,
United Kingdom,.2013
03 Biochemical Engineering Aiba A, , 2 nd ed., Academic
Humphrey A.E., Press,.USA, 2004.
Milli. N.R.

16
 ELECTIVE – I
Course Title Membrane Course Code DCH 3205
Technology
Learning Scheme Assessment Scheme: Credits- 4
Classroom Learning CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) -Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) -Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
Develop ideas in dimensional analysis and to be familiar with different unit systems and conversion from
one set of system to another. Understand the various unit operations and unit processes performed in a
chemical industry. Learn fundamentals of stoichiometry and apply the material balance concept Learn to
calculate the amount of materials required to carry out the suitable unit operation or process.
Course Outcomes:
After successful completion of course, the students will be able to:
1. Understand the basic principle of membrane separation processes

2. Describe different technics available for membrane characterization.

3. Derive various transport models for membrane flux and concentration polarization for various
membrane systems.
4. Compute membrane flux, concentration polarization and fouling using various transport models for
various membrane systems
Unit Contents Hrs Marks
SL FA SA
Unit-1 Membrane Materials, Preparation and Characterization 06 4 3 8
1.2 Introduction, Historical development of membranes, types of
membrane processes, types of synthetic membranes, membrane
materials, membrane module.
1.3 Membrane preparation, Phase inversion process, casting methods.
1.4 Membrane characterization, Measurement of pore size, solute
properties, visual methods, bubble point method, liquid
displacement.
Unit-2 Microfiltration and Ultrafiltration. 07 3 3 9
2.1 Microfiltration: Introduction and history, applications; Recent
trends and progress in MF/UF technology.
2.2 Ultra-filtration: Introduction and history; characterization of
ultrafiltration membranes, concentration polarization and
membrane fouling, membrane cleaning, membrane and
modules, system design, application.
2.3 Nanofiltration: Introduction, process principles, application of
application of nanofiltration for the production of drinking
water and process water, solvent resistance nanofiltration.

17
 Unit-3 Reverse Osmosis: 05 2 3 10
3.1 Introduction – membrane categories, membrane selectivity,
membrane.
3.2 Transport concentration polarization, membrane modules,
membrane fouling control, membrane cleaning application.

Unit-4 Membrane Transport Theory 06 3 - 10

4.1Membrane transport theory – Introduction, solution-diffusion
model.
4.2Structure-permeability relationship in solution diffusion
membranes; Pore-flow membranes.
Unit-5 Concentration Polarization 06 3 - 11
5.1 Concentration polarization, Introduction, boundary layer film
model.
5.2 Concentration polarization in liquid separation process, Cross-
flow.
Unit-6 Recent development in Membrane Processes 06 5 - 12
5.1 Recent material and module configurations for Microfiltration and
ultrafiltration.
5.2 Thin film composite membranes; Biofouling protection; Integrated
membrane systems.
5.3 Gas separation - Hydrogen separation; oxygen and oxygen
enriched air; Membrane distillation and Ceramic membranes.

Total 36 20 20 60

Sr.no REFERENCE BOOKS: Author Publication

01 Principles of Mass transfer and Separation Dutta B. K 1 st ed., Prentice Hall of
Processes. India, 2007.

02 Basic Principles of Membrane Technology Mulder M., 2 nd ed., Springer

Science, USA, 1991.
03 K.N., Membrane Separation Process, Kaushik K.N., 1st ed., Prentice Hall
of India, India, 2008.

18
 SEMESTER
Course Title MOMENTUM Course Code DCH 3205
TRANSFER

Learning Scheme Assessment Scheme: Credits- 3

Classroom Learning CL) 3 Hrs/Week SL 20Marks
Tutorial Learning (TL) - Hrs/Week FA 20Marks
Self-Learning (SL) - Hrs/Week SA 60Marks
Course Objectives:
1. Understand the fluid properties, the fundamental principles and theorem related to momentum transfer
2. Apply the physical and mathematical models to analyse the fluid flow phenomena
in engineering applications
3. Solve the steady state and un-steady state momentum transfer problems
Unit Contents Hrs. Marks
SL FA SA
Unit-1 Basic Concept of Momentum Transfer 5 4 3 8
Introduction and Significance of Momentum Transfer in Chemical
Engineering. Definition of
fluid - Classification of fluids – Newtonian fluid – Characteristic
properties of fluids – Non -
Newtonian Fluids and their classification. Fluid statics: Pascal’s law
and Hydrostatic law of
equilibrium; Pressure and its measurement- Manometers
Unit-2 Concept of Fluid Flow Phenomena 6 3 3 10
Kinematics of fluid flow, Dynamics of fluid flow – Basic equations
governing fluid flow types of fluid flow. Equation of Continuity and its
application, Equation of motion Derivation of Euler’s equation,
Bernoulli’s equation and its application in fluid flow
Unit-3 Flow Measuring Devices 4 2 3 10
Importance of metering – Classification flow measuring devices,
Principle and working of Orifice meter, Venturi meter, Pitot tube,
Variable area meters: Rotameter
Unit-4 Flow through Circular Pipes and Dimensional Analysis 7 3 - 10
Flow of fluids in Laminar regime – Velocity Profile, Shear Stress
Distribution – Hagen–Poiseuille equation - Concept of average velocity
– Concept of Kinetic energy correction factor, Concept of Fluid friction
– Skin friction – Form friction – Factors affecting friction – Friction
factor –Application of Moody’s diagram, Minor losses and major
losses during flow.
Dimensional homogeneity – Raleigh and Buckingham π theorems –
Non-dimensional numbers, model laws

19
Unit-5 Fluid Flow through Packed and Fluidized Bed 7 3 - 11
Flow past immersed bodies – Significance of form friction - Concept of
Drag, Drag Coefficients and Particle Reynolds number - Drag
Coefficient vs. Particle Reynolds number curves for regular and irregular
shaped solid particles. Flow of fluids through packed beds – Packing and
types of packing -Pressure drop across packed beds – Kozeny Carman
equation – Ergun’s equation - Loading and Flooding Packed Beds.
Concept of Fluidization – Condition for Solid particles to be in a
suspended condition in a flowing fluid – minimum fluidization velocity
Unit-6 Transportation of Fluids 7 4 - 11
Transportation Components -Pipe, Fittings and Valves, Types of
Fittings, valves -Stuffing Boxes, Mechanical Seals – Estimation of head
loss from fittings and valves, Concept of minor losses types of minor
losses. Fluid Moving Machinery: Pumps – Classification and working of
Centrifugal Pumps and Positive Displacement Pumps Basic Principles of
Centrifugal Pumps – Pump Characteristics – Concept of Specific Speed,
Net Positive Suction Head – Factors influencing selection of pump

Total 36 20 20 60

Reference Books

1. Fox R.W., McDonald A.T., Pritchard P.J., Mitchell J. W., Introduction to Fluid
Mechanics, 9th ed., Wiley Publications, 2015.

2. Cengel Y.A., Cimbala J.M., Fluid Mechanics (SIE): Fundamentals and Applications, 3rd ed.,
McGraw Hill, New York, 2014.

3. Mc Cabe, Smith, Harriot, Unit Operations of Chemical Engineering 7th ed., McGraw Hill, USA,
2014.

4. Som S.K., Biswas G., Chakraborty S., Introduction to Fluid Mechanics and Fluid Machines, 3rd
ed., Tata McGraw Hill, India, 2011.

5. Welty J. Rorrer G.L. Foster D.G. Fundamentals of momentum, heat and mass transfer 6ed 2015.

20
 SEMESTER-V
Course Title ENTREPRENEURSHIP Course DCH 3105
DEVELOPMENT and Code
MANAGEMENT SKILLS
Learning Scheme Assessment Scheme: Credits- 4
Classroom Learning CL) 2 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) - Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
The students should be able to understand the process of formation & promotion of industry,
organizational structure, necessary management, supervisory skills, leadership required by the
technical students. The students will be stimulated thought & creativity in management of work.
Course Outcomes:
After successful completion of course, the students will be able to:
1. Understand the basic principle of membrane separation processes
2. Describe different technics available for membrane characterization.
3. Derive various transport models for membrane flux and concentration polarization for various membrane
systems.
4. Compute membrane flux, concentration polarization and fouling using various transport models for
various membrane systems
5. Analyse a membrane process and design components to carry out a specific separation
6. Select membranes for gas and bio separation applications.
Unit Contents Hrs Marks
SL FA SA
Unit-1 Management Process and Organisational Management: 06 4 3 8

1.1 What is Management? : Evolution ,Various definitions of

management, Concept of management, Levels of management,
Administration & management, Scientific management by
F.W.Taylor ; Principles of Management (14 principles of Henry
Fayol) ; Functions of Management: Planning Organizing ,Directing,
Controlling ,Decision Making.
1.2 Organization- Definition, Steps in organization;Type organization
:Line ,Line & staff,Functional, Project ; Departmentation :By product
,By process , By function ; Principles of Organisation:Authority &
Responsibility, Span of Control, Effective Delegation : Balance
,stability and flexibility, Communication.

21
Unit-2 Financial Management (No Numerical)- 07 3 3 9
2.1 Objectives & Functions ; Capital Generation & Management
;Types of Capitals - Fixed & Working Sources of raising Capital -
Features of Short term, Medium Term & Long Term Sources
;Budgets and accounts , Types of Budgets Fixed & Variable Budget -
Concept Production Budget - Sample format , Labour Budget -
Sample format , Profit & Loss Account & Balance Sheet - Meaning,
sample format, meaning of different terms involved; Meaning &
Examples of - Excise Tax, Service Tax, Income Tax , Value Added
Tax,Custom Duty (new taxation system- GST etc.)

Unit-3 Materials Management (No Numerical): 05 2 3 10

3.1nventory Concept, its classification, functions of inventory, ABC
Analysis - Necessity & Steps, Economic Order Quantity Concept,
graphical representation, determination of EOQ; Standard steps in
Purchasing;
3.2 Modern Techniques of MaterialManagement: Material Resource
Planning (MRP) - Functions of MRP, Input to MRP, Benefits of
MRP; Enterprise Resource Planning (ERP) - Concept, list of modules,
advantages & disadvantages of ERP.
Unit-4 Introduction: 06 3 4 10
4.1Objective of the course; what is entrepreneurship; Need and scope
for entrepreneurship; Risks and Rewards in entrepreneurship;
Characteristics of an entrepreneur; Relevance and benefits of small
Scale industry.Business Idea Methods and techniques to generate
business idea. 4.2Transforming Ideas in to opportunities
transformation involves, Assessment of idea &Feasibility of
opportunity, SWOT Analysis.
Unit-5 5.1Setting-up an industry: Forms of business 06 3 3 11
organizations/ownership - their merits and demerits; Formation of a
company; Procedures and formalities for setting up of a new industry;
Sources of information, Marketing-Concept and Importance,Market
Identification, Survey Key components,Market Assessment
5.2Business Finance & Accounts: Business Finance , Cost of Project
Sources of Finance , Assessment of working capital , Product costing
, Profitability , Break Even Analysis , Financial Ratios and
Significance , Business Account , Accounting Principles,
Methodology, Book Keeping , Financial Statements Concept of Audit.

22
 Unit-6 Project planning 06 5 4 12
6.1 Identification of opportunities; Market survey;
Techno-economic feasibilitystudies,Business plan steps
involved from concept to commissioning Activity
Recourses, Time, Cost Project Report , Meaning and
Importance ,Components of project report/profile, Project
Appraisal 1) Meaning and definition2) Technical,
Economic feasibility 3) Cost benefit Analysis.
6.2 Enterprise Management and Modern Trends:
Enterprise Management: Essential roles of Entrepreneur in
managing enterprise, Product Cycle: Concept and
importance, Probable Causes Of Sickness, Quality
Assurance: Importance of Quality, Importance of testing,
E-Commerce: Concept and Process

Total 36 20 20 60

Sr.no REFERENCE BOOKS: Author Publication

01 Industrial Engineering & Management Dr. O.P. Khanna Dr. O.P. Khanna

02 Plant Design &Economics for Chemical Peter M.S. & Third1991 McGraw
Engineer Timmerhaus Hill; Auckland.
K.D
03 Entrepreneurship Theory and Practice J.S. Saini Wheeler Publisher,
B.S.Rathore, New Delhi

23
 SEMESTER-V
Course Title Heat Transfer Operation (Lab) Course Code DCH3106
Learning Scheme Assessment Scheme: Credits- 02
Laboratory Learning (LL) 02 Hrs./Week Formative Assessment (FA) 60Marks
Summative Assessment (SA) 40Marks
Course Objectives:
To understand processes & operations involve the exchange of heat and need to calculate the
amount of heat transferred. This lab is designed to develop among the students the skills to perform
experiments related to the application of heat transfer concepts is conduction, convection and
radiation. The students learn about operation of heat exchangers and evaporators. The students
learn to record and present their observations in reports.
Course Outcomes:
After successful completion of the course, the student will be able to:
1.This lab will provide practical knowledge on various heat transfer process and equipment like heat
exchangers and evaporators.
2.Learn basic Heat transfer principles.
3.Impart the knowledge in heat transfer measurements and different heat transfer equipment.
4.Learn how the convection takes place in natural and forced convection and gain knowledge of the
heat transfer taking place in different heat exchangers.
Sr. No List of Experiments
1 To determine heat flow rate through the lagged pipe and compare it with the heater for
known value of thermal conductivity of lagging material.
2 To determine thermal conductivity of liquid (oil) and gas.
3 To estimate the film heat transfer coefficient between the medium in which body is
heated
4 To demonstrate the super thermal conducting heat pipe and to compare its working with
that of the best conductor
5 Shell and tube, HE: To study the following at various flow rates:
(i) LMTD
(ii) Heat transfer rate
(iii) Overall Heat Transfer Co-efficient.
6 To calculate overall heat transfer coefficient for cross flow heat exchanger

7 To determine the thermal conductivity of a good conductor material

24
8 To determine the thermal conductivity of a liquid.
9 To find out total thermal resistance and total thermal conductivity of composite wall
10 To determine the mean emissivity of aluminium plate at different temperature
11 Natural Convection
i)To determine the convective heat transfer coefficient for heated vertical cylinder losing
heat to the ambient by free or natural convection. Ii) To find the theoretical convective heat
transfer coefficient and to compare with the experimental value
12 To verify Boltzmann constant
13 To visualized the pool boiling over the heater wire in different regions up to the
critical heat flux point at which the wire melts.
14 To determine the heat transfer coefficient in forced convection set up.
15 Pin Fin set up: i)To draw the variation of temperature along the length of pin fin under
forced
16 To determine the experimental and theoretical heat transfer coefficient for drop wise and
film wise condensation.
17 To study the heat transfer phenomena in parallel / counter flow arrangements.
18 To study the evaporator and determine the capacity of evaporator.
19 Double pipe HE To study the following at various flow rates:

25
Course Title :-PROCESS ENGINEERING DRAWING LAB Course Code:- DCH3108
Teaching Scheme and credits Examination scheme

Practical :- 02 TW :- 25
Tutorial :- 1* PR/OR :- 25
Credit :- 02 TOTAL:- 50

Laboratory Experiments
Draw minimum five half-empirical size sheet on following:-
NOTE- All drawing sheets must be drawn using drafter

1. Basics of 3D drawing and applications

2. Extrusion of surfaces and geometries
3. Design and drawing of Pressure vessel to dimensions
4. Design and drawing of a Shell and Tube heat Exchanger
5. Design and drawing of a bubble cap tray
6. Design and drawing of Rotary Louvre dryer
7. Design of Distillation Column
8. Dynamic simulation experiment on distillation column
9. Symbols (IS-3232)
10. Systematic sectional views of gate, globe, ball and needle valve
11. Supports - Hanger, roller support for steam pipes. Leg, bracket and skirt supports, Saddle support.
12. Pipe joints - Bend, Elbow. Nipple, Socket, Reducer, Expander, Union Joint, Tee, Cross, Plug, Blind,
Flanged Joints- CI, Welded neck, Hub type, welded flange type, Screwed flange
13. Pipe joints - Socket & Spigot Joint, Hydraulic Joint, Expansion Joints
14. Plant utility block & line diagram,
15. Process control systems,
16. Process flow sheet design using process block, process flow, utility line, P & I, ELD,
17. Plant layout & tank farm on one process plant,

26
Course Title Minor Project / Seminar Course Code DCH 3109

PROJECT WORK:

➢ The project work is training in chemical engineering. The knowledge gained by studying
various subjects separately utilized as a single task. A group of maximum 04 students will
have to work on assigned work.
➢ The topic could be on plant design, specific equipment, process development, manufacturing
process, live industrial problem etc. The project work involves experimental /theoretical /
computational work. A preliminary work to be completed during this semester. It is expected
to do necessary literature survey by referring current journals belonging to chemical
engineering, reference books & internet.
➢ The title of the project is to be registered. The requisites like equipment’s, data, chemicals
etc. are too arranged.

Project Selection:
➢ The department Head / Incharge/Co-ordinator will form the balanced groups of maximum
four students per group. The project groups are to form within first week of the beginning of
academics semester & faculty will assign as project guide to each group.
➢ The project group should interact with the guide, who is turn advice the group in selecting a
project based on the group – potential. The project is to select & registered within two weeks
on the group formation & a brief synopsis of the project to be submitted to the HOD &
guide.
➢ Guide should closely monitor the work & help the students from time to time. The guide
should also maintain a record of continuous assessment of project work progress on weekly
basis.
Project Examination:
➢ The guide should maintain the record of continuous assessment of each member of the group
on weekly basis. Concern guide, External examiner & faculty of the department will assess
the project work during project examination. Group will have to prepare project report in
multiple copies.
➢ One copy for department, one for concern guide & one each for individual. Group should
have to prepare overhead project/ power point presentation for 15 minutes to explain their
project. 15 minutes question & answer session will be taken on each project

27
SEMINAR REPORT & ASSESMENT:
➢ The term work shall consist of a seminar report containing the literature survey in the field
of chemical engineering or allied fields & technical details of seminar topic in all respect.
The concerned guide for continuous activity done by student to prepare seminar report will
assess the term work.
➢ The student will have to prepare seminar report in multiple copies. One copy for
department, one for concern guide & one each for individual. Student should have to
prepare overhead project/ power point presentation for 10 minutes to explain his topic.
➢ 5 minutes question & answer session will be taken on each student. Concern guide,
External examiner & faculty of the department will assess the performance during
presentation combine

28
Course Title Industrial Training Course Code DCH 3110

Teaching Scheme and Credits Examination Scheme:

Practical Credit TW / PR ORAL Total
02 25 25 50

Objectives:
The students should be able to do the observations of actual chemical plant operations to learn what
goes on in a typical chemical process industry. They will understand how the basic knowledge
comes in use to design, development & to run the process plant.

Training Report:
Each student should spend four weeks in any one factory/project/workshop. Here he/she will
observe layout, working, & use of various equipment’s, plants, tools, instruments etc. under the
general supervision of the supervisor, operator, supervisor, engineer of the factory etc. Students are
required to submit a typed report of industrial implant training in systematic technical format during
fifth semester.
The report should contain information about the major field of the factory, particularly about the
section/department where he/she has received the training giving the details of equipment,
machinery, materials, tools with their detailed specifications, use etc. The training report & field
experience will be assessed by two internal examination appointed by the head of the department&
appropriate grade will be awarded. In case he has not attended, he will have to repeat such training
& will not declare pass in corresponding semester until his re-assessment & obtaining grade.

29
SEMESTER :VI

30
 SEMESTER-VI
Course Title Chemical Reaction Course Code DCH3201
Engineering
Learning Scheme Assessment Scheme: Credits- 4
Classroom Learning CL) 3Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) 1 Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
The students should be able to understand basics of reaction engineering, chemical thermodynamics,
and kinetics of homogenous & heterogeneous reactions, types of reactors, steps in design & operation
of chemical reactors. They should be able to compare reactors for best fit, catalysis& its application.
Course Outcomes:
After completion of this course the students are expected to be able to demonstrate following
knowledge, skills and attitudes:
7. Use the concept of equilibrium in chemical thermodynamic process.
8. List the variables affecting the rate of the given reaction.
9. Determine the order and rate constant of the reaction from the given data.
10. Distinguish different types of reactor.
11. Compare the specified types of reactors according to the given parameters.
12. Use proper catalyst for various chemical reactions.
Unit Contents Hrs Marks
SL FA SA
Unit-1 Introduction to Chemical reaction Engineering 6 3 3 7
1.5 Kinetics, classification of chemical reactions, rate of reaction,
factors affecting reaction rate, molecularity & order of reaction
1.6 pseudo molecularity of reaction, zero order reaction, chemical
equilibrium, Le-chatelier’s principle
1.7 first & second law, system, surroundings, intensive & extensive
properties, thermodynamics properties like internal energy,
enthalpy, entropy, free energy
1.8 chemical potential, fugacity, & activity., feasibility of chemical
reaction from the free energy change
Unit-2 Kinetics of Homogeneous Reaction 6 4 4 9
2.5 Rate of reaction, rate equation/law, factors affecting the rate
of reaction, classification of reactions, reaction rate, rate
constant, Concentration dependent term of a rate equation
2.6 elementary and non-elementary reactions, molecularity and
31
 order of reaction, chain and non-chain reactions, Types of
intermediate in non-chain reactions
2.7 Temperature dependency of rate constant based on Arrhenius
theory, Collision state theory, Transition state theory,
Comparison of different theories, Problem based on
Arrhenius’ law – calculation of k and E and rate of reaction
Unit-3 Introduction to Batch Reactor data 7 4 4 9
3.5 Constant volume batch reactor& analysis of total pressure data
obtained in a constant volume system
3.6 Analysis of kinetic data by integral & by differential method for
first order, second order, zero order, nth order, parallel,
autocatalytic, irreversible reactions, & first order reversible
reaction, Half-life method
3.7 Variable volume batch reactor, integral method of analysis of
reactions for variable volume, Temperature & reaction rate
Unit-4 Introduction to Reactor Design 6 3 3 11
4.5 General view of reactor design, classification of chemical
reactor, single ideal reactors, ideal batch reactor
4.6 performance equations for ideal batch reactor, steady state mixed
flow reactor
4.7 space-time & space velocity
4.8 plug flow reactor, holding time & space-time for flow system,
Numerical
Unit-5 Types of Reactors & Size Comparison 6 3 3 12
5.5 Size comparison of a single reactors, multiple reactor system
5.6 plug flow reactor in series, equal sized mixed reactor in series
5.7 mixed flow reactor of different sizes in series, autocatalytic
reactions
Unit-6 Catalysis 5 3 3 12
6.5 Nature of the catalyst, catalyst in homogeneous &
heterogeneous system
6.6 classification of catalysis, catalyst preparation, promoters &
inhibitors, catalyst poisoning (deactivation)
6.7 Introduction to packed and fluidized bed reactor: - Construction
& operation
Total 36 20 20 60
Sr.no REFERENCE BOOKS: Author Publication

01 Principles of Mass transfer and Separation Dutta B. K 1 st ed., Prentice

Processes. Hall of India, 2007.

32
02 Mass-Transfer Operations(1,3,4,5,6) Treybal, R.E 3 rd. ed, McGraw-
Hill 1981.

03 Transport processes and Unit Christie J 4 th ed, Prentice

Operations(2) Geankoplis, Hall India Pvt.Ltd,
2003

04 Mass Transfer in Fluid Systems Cussler, E.L, Cambridge

Diffusion university
press,2017
05 Mass Transfer-Theory and practice Anantharaman N, PrenticeHall of
Meera Sheriffa India, New Delhi,
Begum K.M 2011.

33
 SEMESTER-VI
Course Title Mass Transfer Course Code DCH3202
Operation
Learning Scheme Assessment Scheme: Credits- 4
Classroom Learning CL) 3Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) 1 Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) 1 Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
Solve molecular diffusion in fluids and solids using correlation and theories. Compare various mass
transfer coefficients and analogies for various Chemical Engineering applications. Interpret the theories
of mass transfer for individual and overall mass transfer coefficients. Design of humidification and
dehumidification equipment’s based on material and energy balances. Estimate the Psychometric
properties of air-water system using charts and equations. Discuss different types of mass transfer
equipment’s cooling tower, drier, crystallizer used for Industrial applications.
Course Outcomes:
After completion of this course the students are expected to be able to demonstrate following
knowledge, skills and attitudes:
1. Solve molecular diffusion in fluids and solids using correlation and theories
2. Compare various mass transfer coefficients and analogies for various Chemical Engineering applications
3. Interpret the theories of mass transfer for individual and overall mass transfer coefficients
4. Design of humidification and dehumidification equipment’s based on material and energy balances
5. Estimate the Psychometric properties of air-water system using charts and equations
6. Discuss different types of mass transfer equipment’s cooling tower, drier, crystallizer used for Industrial
applications.
Unit Contents Hrs Marks
SL FA SA
Unit-1 Diffusion: 6 3 3 7
1.1 Introduction to Mass transfer operation, Fick's law of diffusion,
Steady state molecular diffusion in fluids under stagnant and laminar
flow conditions, Diffusion coefficient measurement and prediction.
1.2 Molecular diffusion in Fluids: Molecular diffusion in gas and
Liquids, Multicomponent diffusion, Diffusion through variable cross-
sectional area, Diffusivity in solids and its applications.

Unit-2 Mass transfer coefficients: 6 4 4 9

2.1 Introduction to mass transfer coefficient, Correlation for

convective mass transfer coefficient, Correlation of mass transfer
coefficients for single cylinder, Packed column, flow over a flat plate.

34
 2.2 Theories of mass transfer Penetration theory, Surface Renewal
Theory, Interphase mass transfer, two film theory, Overall mass
transfer coefficients.

Unit-3 Distillation: 7 4 4 9

3.1 Distillation column - Types of contact – Tray Vs Packed Column;

Derivation of operating line equation for different section and parts of
distillation column - rectification section - stripping section - feed
tray location - condenser - reboiler - efficiency of distillation column.
3.2Determination of theoretical trays - McCabe-Thiele method -
Ponchon- Savarit method.

Unit-4 Gas absorption: - 6 3 3 11

4.1 Definition, Characteristics of ideal liquid solutions, choice of

solvent for absorption, equilibrium solubility of gas in liquid,
different applications of gas absorption, equipment for gas liquid
operation such as gas dispersed & liquid dispersed equipment’s.
Packed column.
4.2 Types of packing, Calculation of absorption tower height NTU &
HTU.
Unit-5 Drying: 6 3 3 12

5.1 Principles of Drying-Definitions of moisture and other terms on

Drying, Classification of Drying operations. Rate of Drying -Constant
and Falling Rate Drying. Moisture movement in solids -Through
Circulation Drying - Rate of drying for Continuous Direct heat
Driers.
5.2 Types of Dryers used in practice and their operation-Batch and
Continuous Dryers.
Unit-6 Humidification: 5 3 3 12

6.1 Basic concepts, Principles of Humidification –Definitions Wet

Bulb Temperature &Adiabatic Saturation Temperatures –Air/Water
System psychrometric and Psychrometric Charts – Utilization of
Psychrometric Charts – Dehumidification – Cooling Towers –
Mechanical Draft Towers: forced draft towers and induced draft
towers.

Crystallization:
6.2 Principles of Crystallization- Super Saturation-Nucleation-
Crystal growth -Material & Energy Balance applied to Crystallizers-
35
 Types of Crystallizers used in Practice, Mier’s super Saturation
Theory.

Total 36 20 20 60

Sr.no REFERENCE BOOKS: Author Publication

01 Principles of Mass transfer and Separation Dutta B. K 1 st ed., Prentice

Processes. Hall of India, 2007.

02 Mass-Transfer Operations(1,3,4,5,6) Treybal, R.E 3 rd. ed, McGraw-

Hill 1981.

03 Transport processes and Unit Christie J 4 th ed, Prentice

Operations(2) Geankoplis, Hall India Pvt.Ltd,
2003

04 Mass Transfer in Fluid Systems Cussler, E.L, Cambridge

Diffusion university
press,2017
05 Mass Transfer-Theory and practice Anantharaman N, PrenticeHall of
Meera Sheriffa India, New Delhi,
Begum K.M 2011.

36
 ELECTIVE – II
Course Title POLYMER TECHNOLOGY Course Code DCH 3203
Learning Scheme Assessment Scheme: Credits-4
Classroom Learning (CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) -- Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) -Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
Understand different types of polymers. Identify the various technologies and types of polymerization techniques.
Analyze the polymer processing techniques and polymer additives.

Course Outcomes: After completion of the course, students will be able:

1. Classify and characterize polymers and polymeric reactions
2. Explain the different methods of polymerization
3. Identify the processing technologies for different polymer synthesis and their additives
4. Identify suitable polymer for specific application
5. Distinguish different type of polymers for various applications
6. Demonstrate the novel biopolymers and their applications.

Unit Contents Hrs Marks

SL FA SA
Unit-1 Introduction to polymer : 7 4 8 5
1.1Monomer; polymers and their classification: Degree of
polymerization.
1.2Polymeric reaction: addition; condensation and copolymerization
Unit-2 Methods of polymerization 5 3 6 8
2.1Bulk, solution, emulsion and suspension polymerization.
Structure and size of polymer:
2.1 Structure of polymers, Characterization of polymers: Molecular
weight, Crystallinity, Glass transition temperature and mechanical
properties: testing of polymers.
Unit-3 6 3 6 7
Polymer processing additives:

3.1Fillers, plasticizers, Anti-oxidants, colorants, stabilizers, and

other related additives.
Unit-4 6 2 -- 6
Polymer processing additives

4.1Fillers, plasticizers, Anti-oxidants, colorants, stabilizers, and

other related additives.

Polymer processing techniques:

4.2 Injection and compression transfer moulding methods;

calendaring, extrusion, thermoforming, powder coating.

37
Unit-5 6 4 -- 16
Polymeric materials

5.1 Polyethylene; polypropylene; polymethyl methacrylate;

polyvinyl chloride; polytetra-fluoroethylene, polyacrylate,
polyesters; Polymeric foams – Polyurethane, polystyrene.

Unit-6 Special polymers and bio polymers: 6 4 - 18

6.1Polycarbonates, polysulphones; aromatic polyamides; aromatic
polyester; photo conductive polymers; wool silk and cellulose
derivatives, Protein based polymers and Bio-nano-composites.
Total 36 20 20 60

Sr. No Reference Books

1 Polymer science & Froed J.R., Polymer 1 st ed., Prentice Hall Publishers,
Technology USA, 2014
Introduction to Polymers, Young R.J., Lovell P.A. 1st ed., CRC Press, USA, 2011.
2

Polymer Science and Ebewele R.O., 1st ed ., CRC press, USA, 2000.
3 Technology

38
 ELECTIVE – II
Course Title NUMERICAL METHODS Course Code DCH 3203
Learning Scheme Assessment Scheme: Credits-3
Classroom Learning (CL) 3 Hrs/Week Self Learning (SL) 20 Marks
Tutorial Learning (TL) -- Hrs/Week Formative Assessment (FA) 20 Marks
Self Learning (SL) -Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives: The course is design to equip the students with the necessary mathematical skills
and techniques that are essential for an engineer course.

Course Outcomes: After completion of the course, students will be able:

CO1 : To understand and apply various linear algebraic equations to chemical engineering problems
CO2 : To understand and apply Root finding methods for solution on non-linear algebraic equations
to chemical engineering problems
CO 3: To understand and apply Interpolation and Approximation various methods to
chemical engineering problems
CO4 : To understand and apply various methods of : Numerical integration and numerical
differentiation to chemical engineering problems
CO5 : To understand and apply various Ordinary Differential Equations and Partial Differential
Equations to chemical engineering problems

Unit Contents Hrs Marks

SL FA SA
Unit-1 Linear Algebraic Equations 7 4 8 5
1.1 Introduction, 1.2 Gauss elimination and LU Decomposition ,1.3
Gauss – Jorden elimination ,1.4 Gauss – Seidel and relaxation
methods, 1.5 Case studies; linear Algebraic Equation

Unit-2 5 3 6 8
Nonlinear Algebraic Equation:

2.1 Introduction 2.2 Successive Substitution – Single variable and

Multiple variable 2.3 Newton Raphson Technique – Single variable
and Multiple variable 2.4 Other techniques

Unit-3 6 3 6 7
Numerical Solution of Ordinary Differential Equations (Initial
value problem)

3.1 Introduction 3.2 Runge – kutta Methods, Semi and Implicit

Runge kutta techniques 3.3 Step – size control and estimates of
error 3.4 Stabilitity of Algorithms 3.5 Stiffness and Multi step
Methods.

39
Unit-4 6 2 -- 6
Numerical Solution of Partial Differential Equations

4.1 Introduction, Finite-Difference Technique

4.2Orthogonal collocation, The Galerkin finite element technique.

4.3 Finite element method-one dimentional and two dimention

problem.
Unit-5 6 4 -- 16
Eigenvalues and Eigenvectors of Matrices

5.1 Introduction and problem

5.2 Faddev leverrier method and problem

5.3 Power method and problem

5.4 House holder’s and Given’s Method and problem

Unit-6 Roots of Equation 6 4 - 18
6.1 Bracketing methods – Graphical method Bisection method ,
problems
6.2 Open methods – Newton Raphson Method, Secant method,
Brent’s method, Multiple roots, problem
6.3 Roots of polynomials – Conventional method, Bairtow’s
method, problem
Total 36 20 20 60

Sr. No Reference Books

1 Numerical Analysis and Niyogi, Pradip, Tata McGraw –Hill
Algorithms”,
Numerical Methods for Chapra, S.C. and Canale, R.P. Tata McGraw, Seventh
2 Engineer Edition
Numerical methods for SANTOSH K. GUPTA New age international
3 Engineers limited , publishers, third
edition

40
 ELECTIVE II
Course Title Petroleum Course Code DCH3203
Technology
Learning Scheme Assessment Scheme: Credits- 3
Classroom Learning CL) 3Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) -Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) - Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
Understand the importance of crude oil as source of fuel and the size of refining industry. Interpret the
challenges involved in refining from viewpoint of product specifications, economic considerations and
environmental regulations. Design application of chemical engineering principles to petroleum refining.
Identify the specifications required for good quality petroleum product Exemplify the process of
purification and fractionation of crude oil.
Course Outcomes:
After completion of this course the students are expected to be able to demonstrate following
knowledge, skills and attitudes:
1. Explain the composition of crude oil and its products, along with its properties and characterization
methods
2. Discuss the basic separation and conversion processes used in refining crude oil
3. Implement the chemical engineering principles to the analysis of safe and efficient refinery operations
4. Identify the specifications required for good quality petroleum product
5. Exemplify the process of purification and fractionation of crude oil
6. Interpret the relationship safety and environment in Petroleum Refining Industries.

Unit Contents Hrs Marks

SL FA SA
Unit-1 Petroleum 6 3 3 7
1.1 Exploration Practices Reservoir Rock Properties - Reservoir
types - Reservoir Estimation Origin – Composition -
Classification and constituents of petroleum.
1.2 Dehydration of crude oil, Transportation of crude oil -
Classification of petroleum.
Unit-2 Crude Distillation. 6 4 4 9
2.1 Introduction, Components of crude oil distillation - various
crude oil distillation systems - uses of petroleum products.
Unit-3 Catalytic Cracking 7 4 4 9
3.1 Necessity of cracking - Types of cracking - advantages and
disadvantages of catalytic cracking over thermal cracking, Cracking
reactions.
3.2 Houdrys fixed bed processes - Moving bed processes - Fluid bed
catalytic cracking processes,

41
Unit-4 Reforming and Knocking 6 3 3 11
4.1 Thermal and catalytic Reforming; Polymerization; Alkylation;
Isomerization.
4.2 Reasons for knocking - Additives in petrol - Aviation gasoline -
Aviation turbine fuel (ATF) - Storage and handling of liquid fuels.

Unit-5 Purification of petroleum products 6 3 3 12

5.1 Sweetening processes types –Merox – HDS; Dewaxing; DE
asphalt; Lube oil treatment (blending Stocks).
Unit-6 Properties of Petroleum Products 5 3 3 12
6.1Specific gravity - Vapor pressure – Viscosity - red wood
viscometer Flash point - Fire point - Pour point - Smoke point -
Aniline point - Diesel index - Octane number - Performance number
Cetane number.
6.2 Properties of greases - Drop point of grease.
Total 36 20 20 60

Sr.no REFERENCE BOOKS: Author Publication

01 Petroleum Refining Technology Gary J.H., 6 th ed., CRC Press,

and Economics Handwerk G.E., USA, 2013.
Kaiser M.J.,
02 Petroleum Refining Process Speight J.G., 1st ed., Taylor and
Francis, USA, 2015
03 Fundamentals of Petroleum Mohamed A.F., 1 st ed., Elsevier,
Refining Taher A,Amal E USA, 2010.

04 Petroleum Refinery Engineering Nelson. McGraw Hill, USA,

2010.
05 Modern Petroleum Refining Bhaskara Rao B.K Oxibh, India, 2013
Processess. Reference Books

42
 ELECTIVE III
Course Title CHEMICAL PLANT Course Code DCH 3204
ECONOMICS AND ENERGY
MANAGEMENT
Learning Scheme Assessment Scheme: Credits-3
Classroom Learning (CL) 3 Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) --Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) - Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives: The aim of this course is to help the student to attain the following industry
competency through various teaching learning experiences.

Course Outcomes:
completion of this course, the students will be able to
1. To learn basic economic concept, to understand and apply this concepts in the project works
undertaken and to chemical engineering situation by solving problem
2.Carry out the primary techno-economic feasibility of project.
3. Select appropriate process for a project. Differentiate the equipment and able to prepare
specification sheet.
4.Provide an overview of renewable and non-renewable energy resources scenarios. Perform energy
audits in various unit operations.
5. Able to understand the principles and technologies involved in alternate sources of energy

Unit Contents Hrs Marks

SL FA SA
Unit-1 Introduction: Basic considerations in chemical engineering 7 4 8 5
plant design, Process Design Development, Plant location,
Plant layout, Selection of the Plant Site, Preparation of layout,
Plant operation and control, Materials handling.

Unit-2 Cost estimation: Cash flow and cumulative cash position for 5 3 6 8
industrial operations, factors affecting estimation of
investment and production cost, breakeven point, total capital
investment, fixed and working capital investment & their
estimations, type of capital invesment, cost indexes, method
for estimating capital investment.
Estimation of total product cost: Estimation of total product
cost: manufacturing cost, general expenses, Manufacturing
cost: direct production cost, fixed charges, plant overhead
cost.
Unit 3 Depreciation: Types of depreciation, Service Life, Salvage 6 3 6 7
43
 value, Present value, Methods for Determining Depreciation-
Straight line method, Declining Balance method, Sum of the
Years Digits Methods, Sinking Fund Method, Single unit and
Group Depreciation.
Unit 4 Taxes, Insurance and Interest 6 2 6
Types of taxes, Investment credit, Taxes and Depreciation,
Excess profit taxes, Tax returns, Other taxes
Insurance- Legal responsibility, Types of Insurance, Self
Insurance
Interest- Types of Interest, Nominal and Effective Interest
rate, Continuous Interest
Unit 5 Introduction 6 4 16
Energy Management, The need of Energy Management,
Energy basic for Energy management, Designing and energy
management program, Starting and energy management
program, Energy audit process- Introduction, The Facilty
Inspection, The energy audit report, The energy action plan.
Unit 6 Alternate source of energy 6 4 18
Renewable Energy sources- Solar Energy, Solar collectors,
Solar thermal storage, Application for Solar thermal systems,
Solar Photovoltaics, Wind energy.
Total 36 20 20 60

Sr. No Reference Books

1 “Guide to energy Barney L. Capehart, Wayne Seventh Edition.
management” C. Turner, William J.
Kennedy
Chemical Engineering plant F.C. Vibrandt and C.E. McGraw Hil, Fifth Edition.
2 Design Dryden
“Plant design and Economics M.S. Peters and Timmer McGraw Hill, Inc. 4th Edition.
3 for Chemical Engineers’’ haus. 1991

44
 ELECTIVE III
Course Title FUELS AND Course Code DCH 3204
COMBUSTION
Learning Scheme Assessment Scheme: Credits- 3
Classroom Learning CL) 3Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) - Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) -Hrs/Week Summative Assessment (SA) 60 Marks
Course Objectives:
Develop the understanding levels of fuels and combustion fundamentals 2. Classify and introduce different types
of fuel and fuel analysis techniques that assists the students to choose most convenient fuel for a process
involving combustion` 3. Engage the students in designing various control techniques for handling various
environmental issues resulting from combustion of fuels.

Course Outcomes:
After completion of this course the students are expected to be able to demonstrate following
knowledge, skills and attitudes:
1.Classify the various types of fuels like liquid, solid and gaseous fuels available for firing in boilers and furnaces
2. Compare various fuel properties and its efficient use
3. Choose the right type of fuel depends on various factors such as availability, storage, handling, pollution and
cost of fuel
4. Differentiate the properties of exhaust and flue gases
5. Execute basic engineering and science concepts for the design of various combustion equipment
Unit Contents Hrs Marks
SL FA SA
Unit-1 Classification and Properties of Fuels 6 3 3 7
1.1 Fuels-Types and characteristics of fuels-Determination of
properties of fuels-Fuel analysisProximate and ultimate
analysis-Calorific value (CV)-Gross and net calorific values
(GCV,NCV)- Bomb Calorimetry-empirical equations for CV
estimation.

Unit-2 Solid Fuels: 6 4 4 9

2.1 Origin of coal-Ranking of coal-Washing, cleaning and storage
of coal-Renewable Solid Fuelscomparative study of Solid, liquid and
gaseous fuels-selection of coal for different industrial applications-
carbonization of coal.
Unit-3 Liquid fuels 7 4 4 9
3.1 Origin of crude oil-composition of crude petroleum-classification of
crude petroleum-Removal of salt from crude oil-processing of crude
petroleum-Fractionation distillation-ADU and VDUCracking-
Hydrotreatment and Reforming.
Gaseous fuels:

45
 3.2 Rich and lean gas-Wobbe index-Natural gas-Dry and wet natural gas-
Foul and sweet NG-LPGLNG-CNG-Methane-Producer Gas-Water gas-
Coal Gasification-Gasification Efficiency.

Unit-4 Combustion: 6 3 3 11
4.1General principles of combustion-types of combustion processes-
Combustion chemistryCombustion Equations-Kinetics of combustion-
combustion of solid fuels-Combustion calculations-air fuel ratio-Excess air
calculations.

Unit-5 Combustion Equipment: 6 3 3 12

5.1Analysis of flue gases by Orsat apparatus-Combustion of solid fuels-
grate firing and pulverized fuel firing system-Fluidized bed combustion-
Circulating fluidized bed boiler-Burners-Factors affecting burners and
combustion

Unit-6 Air Pollution 5 3 3 12

6.1 Types of pollution-Combustion generated air pollution-Effects of air
pollution-Pollution of fossil fuels and its control-Pollution from
automobiles and its control.

Total 36 20 20 60

Sr. No Reference Books

1 The Chemistry and Technology of Speight J.G 3 rd ed., Taylor and Francis Ltd.,
Coal. USA,2016
Principles of Combustion Kenneth K.K 2nd ed., Wiley Publications, USA,
2
2012
Fuels-solid, liquid and gases–Their Phillips H.J 1 st ed., Foster Press, USA, 2010
3 analysis and valuation,

46
 ELECTIVE III
Course Title RHEOLOGY OF Course Code DCH3204
COMPLEX FLUIDS
Learning Scheme Assessment Scheme: Credits- 3
Classroom Learning CL) 3Hrs/Week Self-Learning (SL) 20 Marks
Tutorial Learning (TL) -Hrs/Week Formative Assessment (FA) 20 Marks
Self-Learning (SL) -Hrs/Week Summative Assessment (SA) 60 Marks
Make student aware about complex fluids and structure length scales in polymeric and colloidal systems. Provide
basic knowledge of the physics behind colloidal systems. Impart basic knowledge of the physics behind
polymeric solutions and its rheological behaviour with concentration and temperature.

Course Outcomes:
1. Distinguish among viscous, elastic and viscoelastic behavior of fluids

2. Explain the basic forces that give rise to complex fluid behavior 3. Identify non-linear viscoelastic properties of
materials and their corresponding behavior
4. Measure extensional behavior of complex fluids
5. Apply rheological behavior of colloidal system for various applications 6. Apply rheological behavior of
polymeric system for various application.
Unit Contents Hrs Marks
SL FA SA
Unit-1 Elastic Solid and Viscous liquid 6 3 3 7
Stress tensor - Principal stresses - Finite deformation tensor - Neo-
Hookean solid; Velocity gradient, general viscous fluid, plastic behaviour

Unit-2 Complex fluid and forces 6 4 4 9

Complex fluids – examples, pertinent length scales, common features &
applications; Forces – basics forces that drive the dynamics and behaviour
steric, van der Waals, electrostatic etc.

Unit-3 Linear and Nonlinear Viscoelasticity 7 4 4 9

Introduction, models - Kelvin, Maxwell; Linear viscoelasticity in three
dimensions - differential form; Stress relaxation, creep, oscillation.
Nonlinear Viscoelasticity
Nonlinear phenomenon, normal stress, shear thinning, extensional
thickening; Second order fluid - Upper-Convected Maxwell Equation,
Lodge Integral Equation, Integral Constitutive Equations.

Unit-4 Extensional Viscosity 6 3 3 11

Introduction - Importance, theory; Experimental methods - Homogeneous
stretching method, Constant stress devices; Spinning, Lubricated flows,
Contraction flows, Open-syphon method.

47
Unit-5 Suspension Rheology 6 3 3 12
Introduction, viscosity of suspension of solid particles in Newtonian fluids,
colloidal contribution to viscosity, viscoelastic properties of suspension.

Unit-6 Rheology of Polymeric Liquids 5 3 3 12

Introduction, polymer chain conformation, zero shear viscosity, rheology
of dilute polymer solution; Concentrated Solutions and Melts -
Temperature Dependence.

Total 36 20 20 60

Sr. No Reference Books

1 Rheology of Complex Fluids Despande A.P., Krishnan J.M 1 st ed., Springer-Verlag, USA,
Sunil Kumar P.B., 2010
An Introduction to Rheology Barnes H.A., Hutton J.F., 7th ed., Elsevier, UK, 2011.
2 Walters K.,
The Structure and Rheology of Complex Larson R.G 1 st ed., Oxford University Press,
3 Fluids UK, 1999

48
 SEMESTER-VI
Course Title Chemical Reaction Engineering Course Code DCH3206
(Lab)
Learning Scheme Assessment Scheme: Credits- 02
Laboratory Learning (LL) 02 Hrs./Week Formative Assessment (FA) 60Marks
Summative Assessment (SA) 40Marks
Course Objectives:
The knowledge of the practical helps in selecting the optimum reactor design for any process by
taking into consideration the kinetics of the reaction, heat and mass transfer effects & economics
of the process.
Course Outcomes:
After successful completion of the course, the student will be able to:
1. Ability to understand and analyze the rate kinetics for the given reaction
2. Ability to analyze the properties of solid catalyst particles
3. Determine the order and rate constant of the reaction from the given data.
4. Distinguish different types of reactor.
5. Compare the specified types of reactors according to the given parameters.
6. Use proper catalyst for various chemical reactions

Sr. No List of Experiments

1 To determine specific reaction rate of acid catalyzed hydrolysis of ethyl acetate at room
temperature
2 To calculate the reaction rate constant k for given reaction in batch reactor
3 To determine specific reaction rate of hydrolysis of ethyl acetate by caustic soda
4 To determine activation energy of acid catalyzed hydrolysis of methyl acetate
5 To do qualitative study of effect of concentration & temperature of reactant on rate of
reaction between potassium permanganate & oxalic acid
6 To calculate the reaction rate constant k for given reaction in semi batch reactor
7 To calculate the reaction rate constant k for given reaction in plug flow reactor.
8 To study kinetics of hydrolysis of methyl acetate by strong acid & to study relative strength
of acid
9 To study the kinetics of saponification of methyl acetate with sodium hydroxide
10 To study the kinetics of saponification of ethyl acetate with sodium hydroxide
11 To study kinetics between the reaction between potassium per sulphate & potassium iodide.
12 To study rate of acid catalyzed iodination of acetone in presence of excess acid & acetone at
room temperature,
13 To study performance equation of ideal reactors by taking particular reaction,
14 To study nature & properties of different types of catalyst
15 To calculate the reaction rate constant k for given reaction in continuous stirred tank reactor

49
 in series.
16 Study of packed bed reactor

SEMESTER-VI
Course Title Mass Transfer Operation (Lab) Course Code DCH3207
Learning Scheme Assessment Scheme: Credits- 02
Laboratory Learning (LL) 02 Hrs./Week Formative Assessment (FA) 60Marks
Summative Assessment (SA) 40Marks
Course Objectives:
1. To provide hands-on experience in performance of mass transfer, separations related
processes and equipment.
2. To familiarize students with various methods of data gathering, analysis and reduction.

Sr. No List of Experiments

1 To calculate the individual and overall Mass Transfer Coefficient- Interphase Mass
Transfer Coefficient
2 To determine Diffusion in gas phase.
3 To determine Diffusion in Liquid phase.
4 To find the mass transfer coefficient in a wetted wall Column.
5 To find Vapor-liquid equilibria.
6 To determine Simple distillation.
7 To determine Multi Component distillation.
8 To calculate Liquid-liquid equilibria.
9 To study Liquid-liquid extraction.
10 To study Continuous distillation.
11 To study Adsorption.
12 To study the characteristics- Cooling Tower.
13 To study the Characteristics- Humidifier and Dehumidifier.

14 Process of Crystallization and its Characteristics and Batch Crystallization.

15 To calculate rate of Drying using Tray Dryer and Rotary Dryer.
16 To determine yield of Crystals.

50
 SEMESTER-VI
Course Title Major Project Course Code DCH3208
Learning Scheme Assessment Scheme: Credits- 04
Laboratory Learning (LL) 02 Hrs./Week Term Work (TW) 75 Marks
Practical / Oral (PR/OR) 75 Marks
Course Objectives:
To provide sufficient hands-on learning experience related to the design, development and analysis of
suitable product / process so as to enhance the technical skill sets in the chosen field.
Expected Course Outcome:

At the end of the course the student will be able to

1. Formulate specific problem statements for ill-defined real life problems with reasonable assumptions
and constraints.
2. Perform literature search and / or patent search in the area of interest.
3. Conduct experiments / Design and Analysis / solution iterations and document the results.
4. Perform error analysis / benchmarking / costing
5. Synthesise the results and arrive at scientific conclusions / products / solution
6. Document the results in the form of technical report / presentation
1. Capstone Project may be a theoretical analysis, modelling & simulation, experimentation &analysis,
prototype design, fabrication of new equipment, correlation and analysis of data, software development,
applied research and any other related activities.
2. Project can be for one or two semesters based on the completion of required number of credits as per
the academic regulations.
3. Can be individual work or a group project, with a maximum of 3 students.
4. In case of group projects, the individual project report of each student should specify the individual’s
contribution to the group project.
5. Carried out inside or outside the university, in any relevant industry or research institution.
6. Publications in the peer reviewed journals / International Conferences will be an added advantage
Mode of Evaluation: Periodic reviews, Presentation, Final oral viva, Poster submission

51