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Chemistry Practical 1

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194 views23 pages

Chemistry Practical 1

Uploaded by

aryan86ya
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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peRTePeseS Rao: GECERIEALSEBESESISEALS Name: HARSH RAT sunrma Class: 1°'Sem Roll No: jg- \coz0 Exam No: Institution _S-G s.7.7.3. ho This is certified to be the bonafide work of the student in the a Laboratory during the academic year 20/20 No. of practicals certified 2 out of io in the subject of _ Chem a Teacher In-charge Examiner's Signature Principal Date;.... Institution Rubber Stamp (N.B: ‘The candidate is expected to retain his/her. journal till he/she passes in the subject.) Stes pany pans REED ESE BIOS RAO PIERS BIST BOOT EGS BIO ET ETE ES B SASS OSI ES SS SE I EE OST OS BS OT EET ESE ERES ERE fe No. P51, auaalon g | uoaten. E07 mmathed. | 2)| Detoxminabion i cost” 501 coy b_telal_ahraliniy y= acaler Semple. oe ma —1aon altar -by Ankexnol ___ |_| indicalex mained. ‘Name an ee hordneys La Dekoxminalion a vices Hf '@ j—sbricalion, 948 “hy fedusooa |_| viscometen to: |_5)| Debxmination © No. Experiment Submission jallovjae. |2ifor]22 - @. Peete I WBaeof ined |. pemans. | 3} Dedeminghon f antine ont Jo ——|9} 2 giveta Ac 10}, “Deleamindlion 4 drep point oe A derai-n Solid —bubricowd ee UD Sgercq esas esc std BOOS RIES BIOS RIES OSES ESE EO ESEAESERESESEST IES SI [ees aia : BD SEBS ORES EE I ESOS ESET ESE EHS ESET EET TERRIERS OES a ‘ bg EDTA method i Apporstun— Comical Moale piprite burette, ele + Solution | dem! Eriochrome Blark T- indicdor EDTA § hikion Butter. dolution ee oll > TThestuy'= sl isclex cow be detexmined by complen, te care G | #2 ynobsct Hisate lene - diamine tetvoacehe gud Cent) | | 1s yo well known Jemprening ngout , which 1s widely red a ie Oe es | the Jock hal siete = ee ee bic acid CEDTA) jocs pee S a ei i f + \ aust, di A polyps ent makals _ Pe | | a he > | | Funckon of 20TA! BCA ydec J. | A « | a a ea Te The fo moy be obbxeviated 4 dhe doke 4 donop city v As Nag | Be foes erte encase EA heeft ieee | | mofeesinee m0 tampletwohidh tx_ictt—tlshie tise ———__ ‘ Teacher's Signature fo | ° ° Noe oA NAN ANC o on + 2H, 0 ON® Cherwico stouidine stat teh — | Expt. No. = ) j [She weldlive stabi bi Ne a estab F | | = at dit complones. 40 fase Lonaidened Gq- DTA Semper Mga € orn fomplon 7 M4 -Sndicdley Compden Famdon of indfeatoy : ult 1 peaisead = dhe indieslor Evfochrom blak=T yi a dibasic _| 2 ‘ a | - - i stodug Aslored ions | 4} vorious pH 24 dolor = Sras : = | eter > ne | ey [aes Hin 27 In | | Red (below pH ¢) Blue (pH 4-14) Orange Cobove pH iz) | 1 | r t 1 ia] 4 ht bivolewt ble colored indicdlor jon hich Quidled about pl 10 pes a hn dA tolow = | ae ees Mg nek ai | free indicates abe Complen i | L_ | (Rise) Colortesa) Cine xed) Se. an deo al bai added Te Jesse 2dr taneple J See [- pee fel ain a C ee nh NOS ae Ee SoM Chemical stxucture re nx i e mekal- EDTA compen os OP eS N s? $03 No~ Cueisal structare 4 secure eee acto © Win” + 1 pipe ren Free indicaley — AnSly te Comp den Calue) Ccolorters) Cusine sed) Es ~ tee, ch Uae mepel 4 Han? in, ned Blue Date | Ao Jo Hh solution, yf COTA radu added ik sill Hommove, |_gakduet don “pat because Co- EpvA fomplen te more Stable, | A allo iow one ted up tncein EDN, eels bs ald Mg At _Mg - Indicalos phon became __/ | mg = £078 Wore lable tnow ta indicdler Complen | | [Ging bivalent indicator i we, Which bal «ux folows ye roduce blue oure i 2 (tus predict ble coloured solubian, Tous o Chouge fron desk is | Lioloun te blue toler unk indice, Volume “e4 otloy solubon | Va! ® Volume of Jintexmediale solution _| iwi Lenknown dolubion I Ny= ag > WE 20mt Va = 17-2 mL 4o | No> Bessy f. D_NN2= NeVg > 1 43 B= Nex 20 Zook iwe | 34-4 Suu a = 3:3 (34-4) (20) torvenk at ivlo toto} Colo. ieee EINES Ey ivalent woth a ato, = erne given Wakn Seep oR, Strong on 9/L 4 Cat og aie by mn a 1G volar contacts op" Cato, Ud co aoe yx toe — = BYYxK20 2 py —Shengtnn y% 403 2 Hardness 4 ae wacko sample an ppm | oP /ayye ge x fot > 605.2 ppra —# Result - The Ep1h anders vow cosky_Samp le cs 603.2 poem. Teacher's Signature a sim - Debomiralion of thu carbonate , bicarbonate £ total | Alkobini iven welt domple by neutralization e ian 4 4 & P d Lx Soluti 1 x On oui Hed Nig0° ui ee Eston, en se ——_ydinchloric_acid Solution. , phenol phithal jee Prt esaime tediedden A Tory Shu. wodkadiiti 2} raliscal wale i gussally due iB ets lad tine ne | js) Hedon ich =e 12) Gobo nalen oxy — Betieereriennis ep be 4 Bicasl ee! sibidi iden ish ee A | (pee follow a car ae bol of 4 the gt ee as ee i Teacher's Signature | OH 4 HUQ > CoqamenaO hysomde combines Wie bicarbonate SOM eit a ese) + tat fT > Hog meee te Ga > anes) ** Wh 2 i alc dachabes tt. | 3. Ane i | Teacher's Signature | Observobtions as breum Aslulion :- SNe. Veluwe ¢ Kren | Vibimaag, Selina [etal Volumel f | delulion (mL) 4 vol) | of Intnl {dritial Reading rol Pading| Ee Mo’ (rd) bay, 20 mo} ee a is Bord O ml Ve-Bmt | I6-3mh) WS 20 mt Ort 16-3 mt { zt ss | Obarrvation a abnor telublen 3 - LS NO. Volume § bream Volume Sy sea otal Volume bation (mt) fen Gol) oe $atiol dedi Pieal a ‘ wl ei oe ded Onn me ie aa Od atm] (a-tn Ee ae Od WL mt 1 | Expt.No. Page No, #& Calculations >= a aaa given: “/30 (Known solution’) N= Normality of noon solution. Ni = Volume oe Nat Normality of intexmediate Solution Nae Nolume Cindeemaltale: dolusbon. N= Nav Yeo%20 + Nox 63 2 Ny? 0,04989 + Pheulpitalin dion, = | nln = Normality of jntexmediale Solution, T éd | Ni3> Volume aden Solution > No => Normality 3 unknown Selidion (>) s Teacher's Signature { Naxp = NpxVa Na | 0-04085 K4 + Npx20 e | eu 2 0, OORI78 s | Sse Mek 9 “THyolion: = | eee ———__—_—_—_—_ Na> Nowmalily ef intsemedicle Solution ee 0 - Na = Volume Unknown Solution. Nm: coe ui unknown solution Cm) | | m= Volume. of Intermediate soliton with ‘erg range indicalor | | N2*M= NaxV3 | Nm- Naxym Na E | 2 oot. a~ N.. x20 | | lente Non + 0° 02422845 | ae _ weight sf Calogxio> | Phendphthelein Nop X “4, ue a = O-00BIZB X so 1903 2 408.3 ppm. Teacher's Signature Date _ Page No, @) | saad | Net ormige = Maar ton aoe E SEA + 0-0.2U428 ° 103 + Results: — . ~ a ae 7 tee | “Total otalinty ET)! Pama = {1236-9 4 4OB:S \ pom FF = [645.8 pra (orbondle alkalinity = Pp Cs 2%_408-9 pom } = 817-8 pow | Biearbonale alkalinity = 2p. | : =(Is4s.@-~ 219 2) ppm | = 38. ptt * Precautions! Se re 1) Sin dhe mixture will 0 lesa gods od Teacher's Signaiyes |__| Sie = “ sclederanine _poteentay kage 4 PaaS | | intemal inci ccifsr method + ~ Apposecttina? — fentcol Hoar, pipette » busette ale _- % Solutions seated *~ lao focus balphele tution. 5 diphenyloraine aR etal Ruiraione potassium Senet Solubion, | a 9. al an Concentration 4y/c) ba Eee KeCro09 Contains oe avai table foe anidotion whith dopa dhe and pest ri joneus jong PHssent in ro dolution ae |_| paint of hs neath cats be deteclad using | ; _ ee Yoo ive jee ag amine on Sotenteden. sulphuric atid 2a ard Jou oe otassium~ dichro: g olition . Teacher's Signature * Fesog (ung, so4 .GH,0 —> fesoy + (wna), S04 1 O20 : + GFeS0q 4 Katt 0g +FHS0g —> 88%, Go4) 1 Cre Cody + KeS0y + THO 2 KOSS iy ©) diphanytbenatne. Ceobres) (AE) Diphenzlamine Ccotortess ) CS (ez ) Diphenytbenciaine Cufelet ) Date by biphenyl _bertdine iad Pe ee Hl rs never onidizech | Av_u__guinonotd form Cutolet cols), As it shee ag” t | Habe ue tecced 2 onilieed, forse 1 oh on 0. adem | indicates + i | Red-On polentiol el In (0:5-1 mM u.S0¢ + O-S mtg Poy) medium ,!— aed . Fy, = = 0 76 |The onidotion polential of ne Tse system. in ai ean! . 2s jon a Or ad + RT, Towta.") iva (Rec. } And he formal petrol cl syle a = | | fe? _Y £234 ts o6sy | ee dhe oxidation | Teacher's Signature + Formal Potential Syke | fe OS Se oe } + Hypo, + fe2? ——» [fexifog)? + 2H™ | Creen Cobred tormpierw Date | petit before Abe actual snd_poin (ale AES oe aa ica he _ ferro potential ri enon — 5 Pipette out 20 mb 4 dhe known solution ive the contend peak |__| sla ae nly Bey mintuve A 2 drops oh diphenylonine ial [-—4anterdunt observab’ona . \. alo. ph Sit lea Hepeat dhe BNE ee 2) Now, titrate it Against Ko C03 Aotution FW dAplution becom blue. | : ae eecl_Ahe_sapuriment ee * + Seleelaliga.” = __ = i a ll ge ae —ollou sot? | Na+ Nos. of jntenmediale solution. __Va!> Volurne of“intormediale | j—Ne: Volume At UT sormediale Solattibn, __ Sel wid. ol Teacher's Signature | Bhstavedion fpr revs solution 2 - | SNO, | Yelama of Frown] Ware of Kaley (re) Petal Va aelalion (mt) FSi di nl nly {ey 7 Ab: ; 2 ROrnk 0 wf 1B-brJ } 2 20 wh O mt [B-Gmf 86, hea 20 mt, Ok | 1B-bmt be Satea | | Obdevablon fi turkmeum Sedublen 2- | SNo_| Volant ¢ Kmeurrt| Volume jet Tel Velen | Aeluiten (rt) Bs G 8S m ts Lets (o- e- ag oo 10-5 mp [Sex 3° 20 rl. Gel 10 <5 wf Date Page No. oe en ae Me NN: 1 x20K 10 | j \2 Boxire } 1 | Homce, Nyt 0-035" ' i | road Nav2! : N3Va 4 PORT oe Novel Sorte ky jn | Va lox20 a | Heuce Nz 2 0-018 | Yooh Tron wv given abl 2 x50g x PY | = 0-0/8 xSS-8x25 | = AaSjr | #& Trecoukions )— | f Joees 1) Mate sure Io ol i | T | ea Teacher's Signature

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