NUREG/CR-6142

ANL-93/35

Tensile-Property Characterization
of Thermally Aged Cast
Stainless Steels

Argonne National Laboratory

U.S. Nuclear Regulatory Commission

Office of Nuclear Regulatory Research
Washington, DC 20555-0001
 NUREG/CR-6142
ANL-93/35

Tensile-Property Characterization
of Thermally Aged Cast
Stainless Steels

Manuscript Completed: January 1994

Date Published: February 1994

Prepared by
W.F. Michaud, P.T. Toben, W.K. Soppet, O.K. Chopra

Argonne National Laboratory

9700 South Cass Avenue
Argonne, IL 60439

Prepared for
Division of Engineering
Office of Nuclear Regulatory Research
U.S. Nuclear Regulatory Commission
Washington, DC 20555-0001
NRC FIN A2243
Previous Documents in Series
Initial Assessment of the Mechanisms and Significance of Low–Temperature Embrittlement of
Cast Stainless Steels in LWR Systems, NUREG/CR–5385, ANL–89/17 (August 1990).

Estimation of Fracture Toughness of Cast Stainless Steels During Thermal Aging in LWR
Systems, NUREG/CR–4513, ANL–90/42 (June 1991).

ii
 T e n s i l e – P r o p e r t y Ch a r a c t e r i z a t i o n o f
T h e r m a l l y A g e d C a s t St a i n l e s s St e e l s

by

W. F. Michaud, P. T. Toben,
W. K. Soppet, and O. K. Chopra

Abstract

The effect of thermal aging on tensile properties of cast stainless steels during service in
light water reactors has been evaluated. Tensile data for several experimental and commercial
heats of cast stainless steels are presented. Thermal aging increases the tensile strength of
these steels. The high–C Mo–bearing CF–8M steels are more susceptible to thermal aging than
the Mo–free CF–3 or CF–8 steels. A procedure and correlations are presented for predicting the
change in tensile flow and yield stresses and engineering stress–vs.–strain curve of cast stain-
less steel as a function of time and temperature of service. The tensile properties of aged cast
stainless steel are estimated from known material information, i.e., chemical composition and
the initial tensile strength of the steel. The correlations described in this report may be used
for assessing thermal embrittlement of cast stainless steel components.

iii
iv
Contents
Nomenclature ........................................................................................................... viii

Executive Summary ................................................................................................... 1

1 Introduction ....................................................................................................... 3

2 Mechanism of Thermal Embrittlement ................................................................... 3

3 Experimental Procedure ....................................................................................... 6

3.1 Material Procurem ent ................................................................................. 6

3.2 Material Characterization ............................................................................ 6

3.3 Tensile Tests ............................................................................................. 9

4 Effect of Thermal Aging ...................................................................................... 19

4.1 Tensile Strength ........................................................................................ 19

4.2 Engineering Stress–Strain Behavior ............................................................. 34

5 Estimation of Tensile Properties ........................................................................... 39

5.1 Flow Stress ............................................................................................... 39

5.2 Ramberg–Osgood Parameters ..................................................................... 52

6 Conclusions........................................................................................................ 59

Acknowledgments ..................................................................................................... 59

References ............................................................................................................... 59

Appendix ................................................................................................................. A–1

List of Figures
1. Decrease in Charpy–impact energy for various heats of cast stainless steels
aged at 400°C ............................................................................................... 4

2. Grain structure along the axial and circumferential sections of centrifugally

cast pipes P1 and P2...................................................................................... 8

v
3. Grain structure of various static–cast slabs ...................................................... 8

4. Ferrite morphology from three locations across the thickness of static–cast

slabs of CF–3 (Heat 69), CF–8 (Heats 73 and 68), and CF–8M (Heats 74, 70,
and 75)......................................................................................................... 10

5. Ferrite morphology along the three orientations of the centrifugally cast pipes
(Heats P1, P2, and P3) and the static–cast pump impeller (Heat I) .................... 13

6. Orientation and location of the mechanical–test specimens taken from (a) and
(b) pipe sections and (c) slabs........................................................................ 18

7. Orientation and location of the mechanical–test specimens taken from KRB

pump cover plate........................................................................................... 18

8. Configuration of tensile test specimen ............................................................. 19

9. Effect of thermal aging on engineering stress vs. strain curves for Heat 69 ........ 27

10. Effect of ther mal aging on engineering stress vs. strain curves for Heat P2 ........ 28

11. Effect of thermal aging on engineering stress vs. strain curves for Heat 68 ........ 29

12. Effect of thermal aging on engineering stress vs. strain curves for Heat P1 ........ 30

13. Effect of thermal aging on engineering stress vs. strain curves for Heat 74 ........ 31

14. Effect of thermal aging on engineering stress vs. strain curves for Heat 75 ........ 32

15. Ratio of yield and ultimate stress of aged and unaged cast stainless steel as a
function of the aging parameter P ................................................................... 33

16. Fracture surface of tensile specimens of unaged and aged Heat P1 tested at
room temperature and 290°C ......................................................................... 35

17. Fracture surface of tensile specimens of unaged and aged Heat 68 tested at
room temperature and 290°C ......................................................................... 36

18. Fracture surface of tensile specimens of unaged and aged Heat 75 tested at
room temperature and 290°C ......................................................................... 37

19. Values of yield and ultimate stress estimated from Charpy–impact data and
those obtained from tensile tests for Heats 69, 68, 74, and 75 ........................ 38

20. Examples of ROFIT analysis of tensile stress–vs.–strain curves at room

temperature and 290°C for cast stainless steels using flow stress as the
reference stress............................................................................................. 40

vi
21. Flow stress ratio of aged cast stainless steels at RT and 290°C as a function of
the normalized aging parameter. The solid lines represent correlations
obtained by subtracting σ from the best–fit curve. ........................................... 50

22. Experimental and estimated flow stress of aged cast stainless steel at 290°C
and RT .......................................................................................................... 52

23. Experimental and estimated yield stress of aged cast stainless steel at 290°C
and RT .......................................................................................................... 53

24. Correlation between the Ramberg/Osgood parameter α 1 and flow stress at RT

and 290°C for cast stainless steels.................................................................. 54

25. Engineering stress–vs.–strain curve at RT and 290°C, estimated from the

chemical composition and initial tensile strength and determined
experimentally for thermally aged CF–3, CF–8, and CF–8M steels ....................... 57

List of Tables
1. Product form, chemical composition, hardness, and ferrite morphology of
various heats of cast stainless steel ................................................................ 7

2. Ferrite content and grain structure of various cast stainless steel pipes ............. 7

3. Tensile test results for cast stainless steels ..................................................... 20

4. Best–fit values of the Ramberg–Osgood constants for unaged and aged cast
stainless steels at room temperature............................................................... 43

5. Best–fit values of the Ramberg–Osgood constants for unaged and aged cast
stainless steels at 290°C ................................................................................ 47

6. Values of constants in Eq. 8 for estimating tensile flow stress of aged cast
stainless steels .............................................................................................. 51

7. Values of constants in Eq. 10 for estimating tensile yield stress of aged cast
stainless steels .............................................................................................. 52

8. Values of Ramberg/Osgood parameter n1 and the constants in Eq. 11 for

estimating parameter α 1 for aged cast stainless steels ..................................... 53

vii
 Nomenclature
b Uncracked ligament of Charpy–impact specimen (mm).
B Thickness of Charpy–impact specimen (mm).
E Modulus of elasticity (MPa).
P Aging parameter, i.e., the log of the time of aging at 400°C.
Py Yield load for an instrumented Charpy–impact test (N).
Q Activation energy for the process of thermal embrittlement (kJ/mole).
n Ramberg–Osgood parameter.
Rf Ratio of the tensile flow stress of aged and unaged cast stainless steel.
Ry Ratio of the tensile yield stress of aged and unaged cast stainless steel.
t Service or aging time (h).
Ts Service or aging temperature (°C).
W Width of Charpy–impact specimen (mm).
α Ramberg–Osgood parameter.
ε Engineering strain.
εο Reference strain in Ramberg–Osgood equation.
θ Aging behavior at 400°C, i.e., the log of the time to achieve β reduction in impact energy
at 400°C.
σ Engineering stress (MPa).
σf Engineering flow stress (MPa).
σo Reference stress in Ramberg–Osgood equation (MPa).
σy Engineering yield stress (MPa).

SI units of measure have been used in this report. Conversion factors for measurements in
British units are as follows:

To convert to multiply by
in. mm 25.4
J* ft·lb 0.7376
kJ/m 2 in.–lb/in.2 5.71015
kJ/mole kcal/mole 0.239

* When impact energy is expressed in J/cm 2 , first multiply by 0.8 to obtain impact energy of a standard
Charpy–V notch specimen in J.

viii
Executive Summary
Cast duplex stainless steels used in light water reactor (LWR) systems for primary pres-
sure–boundary components are susceptible to thermal embrittlement at reactor operating tem-
peratures. Thermal aging of cast stainless steels at these temperatures causes an increase in
hardness and tensile strength and a decrease in ductility, impact strength, and fracture tough-
ness of the material and the Charpy transition curve shifts to higher temperatures.
Investigations at Argonne National Laboratory have shown that thermal embrittlement of cast
stainless steel components may occur within the reactor design lifetime of 40 yr. Various
grades and heats of cast stainless steel exhibit varying degrees of thermal embrittlement. In
general, the low–C CF–3 steels are the most resistant t o thermal embrittlement, and the Mo–
bearing, high–C CF–8M steels are the least resistant. An assessment of mechanical–property
degradation due to thermal embrittlement is therefore required to evaluate the performance of
cast stainless steel components during prolonged exposure to service temperatures, because
rupture of the primary pressure boundary could lead to a loss–of–coolant accident and possible
exposure of the public to radiation.

This report presents tensile–property data on several heats of cast stainless steels aged up
to 58,000 h at temperatures between 290 and 450°C (554 and 752°F). The tensile data are
analyzed to establish the effects of thermal aging on tensile strength and engineering
stress–strain behavior (represented by the Ramberg–Osgood equation) of cast stainless steels.
A procedure and correlations are presented for predicting the change in tensile flow and yield
stress, and in the engineering stress–vs.–strain curve of cast stainless steel components due to
thermal aging during service in LWRs. The tensile properties of aged cast stainless steel are
estimated from information that is readily available from certified material test records for the
component, i.e., chemical composition and the initial tensile strength of the unaged material.
The correlations described in this report may be used for assessing thermal embrittlement of
cast stainless steel components.

1
2
1 Introduction
Cast duplex stainless steels used in light water reactor (LWR) systems for primary pres-
sure–boundary components, such as valve bodies, pump casings, and primary coolant piping, are
susceptible to thermal embrittlement at reactor operating temperatures, i.e., 280–320°C
(536–608°F). Thermal aging of cast stainless steels (i.e., ASTM Specification A–351 for Grades
CF–3, CF–3A, CF–8, CF–8A, and CF–8M * ) at these temperatures causes an increase in hardness
and tensile strength and a decrease in ductility, impact strength, and fracture toughness of the
material and the Charpy transition curve shifts to higher temperatures. An assessment of
mechanical–property degradation due to thermal embrittlement is therefore required to evaluate
the performance of cast stainless steel components during prolonged exposure to service
temperatures, because rupture of the primary pressure boundary could lead to a loss–of–
coolant accident and possible exposure of the public to radiation.

Investigations at Argonne National Laboratory (ANL) 1–10 and elsewhere11–16 have shown
that thermal embrittlement of cast stainless steel components occurs during the reactor design
lifetime of 40 yr. Various grades and heats of cast stainless steel exhibit varying degrees of
thermal embrittlement. In general, the low–C CF–3 steels are the most resistant to thermal
embrittlement, and the Mo–bearing, high–C CF–8M steels are the least resistant.

A procedure and correlations have been developed at ANL for estimating mechanical prop-
erties of cast stainless steel components under LWR operating conditions from material infor-
mation readily available in certified material test records.5 These correlations were later up-
dated and optimized with an expanded data base and mechanical–property results obtained
from cast stainless steels that were aged up to ≈58,000 h at 290–350°C (554–662°F). 6 , 7
The results are expressed in terms of engineering fracture toughness parameters that can be
used in fitness–for–service analyses, e.g., “NRCPIPE” computer code for analyzing elastic–plastic
fracture mechanics of nuclear power plant piping. However, correlations for estimating tensile
stress–strain behavior of thermally aged cast stainless steels have not been developed.

This report presents tensile–property data on several heats of cast stainless steels aged up
to 58,000 h at temperatures between 290 and 450°C (554 and 752°F). The results are ana-
lyzed to establish the effects of thermal aging on tensile strength and engineering stress–strain
behavior, represented by the Ramberg–Osgood (RO) equation, of cast stainless steels. A proce-
dure and correlations are presented for estimating tensile flow and yield stress and RO param-
eters of aged cast stainless steel from known material information, i.e., composition and initial
tensile strength of the unaged material.

2 Mechanism of Thermal Embrittlement

Thermal embrittlement of cast duplex stainless steels results in brittle fracture associated
with either cleavage of ferrite or separation of the ferrite/austenite phase boundary. Thermal
aging o f cast stainless steels a t temperatures <500°C (932°F) leads t o precipitation o f additional

* In this report, Grades CF–3A and CF–8A are considered equivalent to CF–3 and CF–8, respectively. The
A designation represents high tensile strength. The chemical composition of CF–3A and CF–8A is further
restricted within the composition limits of CF–3 and CF–8, respectively, to obtain a ferrite/austenite ratio that
results in higher ultimate and yield strengths.

3
phases in the ferrite, e.g., formation of a Cr–rich α' phase by spinodal decomposition; nucleation
and growth of α '; precipitation of a Ni– and Si–rich G phase, M23C6 carbide, and γ2 austenite;
and additional precipitation and/or growth of existing carbides at the ferrite/austenite phase
boundaries. 1,2,8–10,17–21 Thermal aging has little or no effect on the austenite phase. The
formation of Cr–rich α ' phase by spinodal decomposition of ferrite is the primary mechanism for
thermal embrittlement. The α ' phase strengthens the ferrite matrix, i.e., it increases strain
hardening and local tensile stress, so that the critical stress level for brittle fracture is achieved
at higher temperatures.

The degree or extent of thermal embrittlement is controlled by the amount of brittle frac-
ture, which depends on both material and aging conditions. In some cast stainless steels, a
fraction of the material may fail in brittle fashion but the surrounding austenite provides duc-
tility and toughness. Such steels have adequate impact strength even after long–term aging.
Predominantly brittle failure occurs when either the ferrite phase is continuous, e.g., in cast
material with a large ferrite content, or the ferrite/austenite phase boundary provides an easy
path for crack propagation, e.g., in high–C or high–N steels that contain phase–boundary car-
bides or nitrides. Consequently, the amount, size, and distribution of ferrite in the duplex
structure and phase–boundary precipitates are important parameters that control the extent of
thermal embrittlement. The decrease in room–temperature (RT) Charpy–impact energy during
thermal aging at 400°C (752°F) of various heats of cast stainless steel4–6,11,15,16 is shown in
Fig. 1. The results indicate that all the materials reach a “saturation” RT impact energy, i.e., a
minimum value that would be achieved by the material after long–term aging. The actual value
of the saturation RT impact energy for a specific cast stainless steel is independent of aging
temperature but depends strongly on the chemical composition of the steel; it is lower for the
Mo–bearing CF–8M steels than for the Mo–free CF–3 or CF–8 steels, and decreases with an in-
crease in ferrite content or the concentration of C or N in the steel.

The time to reach saturation, i.e., the kinetics of thermal embrittlement, depends on both
material and aging parameters. Figure 1 indicates that the time for aging at 400°C for a given
decrease in impact energy varies by more than two orders of magnitude for the various heats,

400
Impact Energy, Cv (J/cm 2 )

Cast SS
Impact Energy, Cv (ft·lb)

Aged at 400°C 200

300
150

200
100

100 ANL
FRA
50
EPRI
GF
0 0
1 2 3 4 5
10 10 10 10 10
Aging Time (h)
Figure 1. Decrease in Charpy–impact energy for various heats of cast
stainless steels aged at 400°C. FRA= Framatome, EPRI=
Electrical Power Research Institute, GF= Georg Fischer Co.

4
ANL and Framatome (FRA) heats, and 10,000–30,000 h for the Georg Fischer Co. (GF) heats.
Activation energies of thermal embrittlement range from 65 to 230 kJ/mole (15 to
55 kcal/mole).4–6,11,13–15,22 These values are well below the 202 kJ/mole (48 kcal/mole)
value associated with Cr bulk diffusion in the Fe–28Cr alloy.23 Small changes in the constituent
elements of the material can cause the kinetics of thermal embrittlement to vary significantly.
The logarithm of the aging time at 400°C for a 50% reduction in RT Charpy–impact energy has
been shown to be an important parameter for characterizing the kinetics of thermal
embrittlement. 5,6

Activation energy is high for steels that show fast embrittlement at 400°C and low for
those that show slow embrittlement at 400°C. Also, materials with the same chemical compo-
sition but differing heat treatment show different kinetics of embrittlement. 11 Microstructural
examination of aged cast stainless steels suggests that slow embrittlement at 400°C and low
activation energy are associated with clusters of Ni–Si, Mo–Si, and Ni–Si–Mo in the ferrite ma-
trix.8–10 These clusters are considered precursors of G–phase nucleation and precipitation.
Cast stainless steels with low activation energy and slow embrittlement at 400°C show G–phase
precipitation after aging, and steels with high activation energy and fast embrittlement at
400°C do not contain a G phase. 8–10,17,18 The presence of Ni–Si–Mo clusters in the ferrite ma-
trix of an unaged material may be considered a signature of steels that are potentially sensitive
to thermal embrittlement, i.e., steels with Ni–Si–Mo clusters in the ferrite matrix show low acti-
vation energy for thermal embrittlement but take longer to embrittle at 400°C.

The kinetics of thermal embrittlement of cast stainless steels are controlled primarily by
the kinetics of ferrite strengthening, e.g., activation energy determined from ferrite hardness
measurements shows very good agreement with that obtained from the Charpy–impact
data. 13,14,22 Microstructural characterization and annealing studies on thermally aged cast
stainless steel show that strengthening of ferrite is caused primarily by spinodal decomposition
of ferrite to form the Cr–rich α ' phase.4,9,10 Consequently, the kinetics of thermal embrittle-
ment should be controlled by the amplitude and frequency of Cr fluctuations produced by
spinodal decomposition, i.e., by the size and spacing of the α ' phase. The low activation ener-
gies of thermal embrittlement are most likely caused by variations in the spacing of Cr fluctua-
tions; atom probe field–ion microscopy studies indicate that the spacing between Cr fluctua-
tions decreases with decreasing temperature.17,21 During thermal aging, production heat
treatment and possibly the casting process, both of which affect ferrite composition and mi-
crostructure of unaged material, can influence microstructural evolution and, therefore, the
kinetics of embrittlement.

For most materials, the kinetics of thermal embrittlement vary with aging temperature. For
a specific heat of cast stainless steel, activation energy of thermal embrittlement is not
constant over the temperature range of 290–450°C (554–842°F), but increases with
decreasing temperature.1–3,13 The increase is particularly significant between 400 and 450°C
(752 and 842°F). In addition, materials aged at 450°C show precipitation of phase–boundary
carbides (also nitrides in high–N steels) and a decrease in ferrite content of the steel. 1 , 2 At
reactor temperatures, such processes either do not occur or their kinetics are extremely slow.
Consequently, data obtained after 450°C aging do not reflect the mechanisms that are active
under reactor operating conditions, and extrapolation of the 450°C data to predict the extent of
thermal embrittlement at reactor temperatures is not valid. The activation energy for thermal
embrittlement may be represented by an average value in the temperature range of 290–400°C
(554–752°F).

5
3 Experimental Procedure

3 . 1 Material Procurement

Material was obtained from various experimental and commercial heats of CF–3, CF–8,
and CF–8M (ASTM Specification A 351) cast stainless steels in differing product forms and sec-
tion thicknesses. Six experimental heats of cast stainless steel were procured in the form of
76–mm–thick slabs. Materials from the commercial heats included sections of four different
centrifugally cast pipes (CF–8 and CF–8M grades), a pump impeller (CF–3 grade), and a pump
casing ring (CF–8 grade). The outer diameter and wall thickness of the cast pipes ranged from
0.6 to 0.9 m and 38.1 to 76.2 mm, respectively.

A cover plate assembly from the recirculating pump of the KRB reactor in
Gundremmingen, Germany was also procured. The cover plate assembly was in service for ap-
proximately eight effective full power years (efpys) at a service temperature of 284°C (543°F).
The plate assembly was decontaminated and samples were obtained from the inner 25–mm–
thick region of the plate. The average temperature of the samples was estimated to be 280°C.

3 . 2 Material Characterization

The various cast materials were characterized to determine their chemical composition, hard-
ness, grain structure, and ferrite content and distribution. All castings were examined in the
three orientations as well as at different locations, namely, material near the center and near
the inner and outer surfaces of the pipes, and top and bottom regions of the slabs. A ferrite
scope (Auto Test FE, Probe Type FSP–1) was used to measure the ferrite content of the cast-
ings. The instrument was calibrated with several weld metal standards (ferrite numbers be-
tween 2.4 and 28.1) obtained from the British Welding Institute. The distribution of ferrite was
determined by the intercept method, i.e., by counting the number of ferrite/austenite phase
boundaries intersected by a superimposed outline. The chemical composition, hardness, and
ferrite content and distribution of the cast materials are given in Table 1. For each material,
the ferrite content calculated from the composition with Hull's equivalent factor24 are also
listed in the table.

Some differences in hardness and ferritic content were observed for material from various
locations in the castings. The ferrite content was lower and the hardness slightly higher toward
the top of the static–cast slabs or the inner surface of the centrifugally cast pipes. This behav-
ior appears to be related to compositional variations, particularly changes in Ni content. In
general, the hardness of the cast material increased with an increase in ferrite content. For the
same ferrite content, the hardness of CF–8 and CF–8M material is comparable, whereas the
hardness of CF–3 material is lower. An increase in N content increases the hardness of cast
stainless steels of all grades.

The grain structures of the various castings were examined along the axial, circumferential,
and radial sections. Descriptions of the structures observed in the four centrifugally cast pipe
sections and the pump casing ring are given in Table 2. Two castings, Heats P1 and P2,
contain equiaxed grains across the entire thickness of the pipe. Grain size and distribution in
the various orientations do not differ significantly, as shown in Fig. 2. The equiaxed grains
were probably produced intentionally by a low pouring temperature or by shear between the

6
Table 1. Product form, chemical composition, hardness, and ferrite morphology of various
heats of cast stainless steel

Ferrite a Hard– Ferrite

Chemical Composition (wt.%) (%) ness Spacing
Heat Grade Mn Si P S Mo Cr Ni N C Calc. Meas. RB (µ m )

76-mm Slabsb
69 CF–3 0.63 1.13 0.015 0.005 0.34 20.18 8.59 0.028 0.023 21.0 23.6 83.7 35

73 CF–8 0.72 1.09 0.028 0.016 0.25 19.43 8.54 0.053 0.070 7.0 7.7 78.8 253
68 CF–8 0.64 1.07 0.021 0.014 0.31 20.64 8.08 0.062 0.063 14.9 23.4 84.6 87

70 CF–8M 0.55 0.72 0.021 0.016 2.30 19.17 9.01 0.049 0.066 14.2 18.9 86.5 96
74 CF–8M 0.54 0.73 0.022 0.016 2.51 19.11 9.03 0.048 0.064 15.5 18.4 85.8 90
75 CF–8M 0.53 0.67 0.022 0.012 2.58 20.86 9.12 0.052 0.065 24.8 27.8 89.5 69

Reactor Componentsc
P3 CF–3 1.06 0.88 0.017 0.014 0.01 18.89 8.45 0.168 0.021 2.8 1.9 82.2 –
P2 CF–3 0.74 0.94 0.019 0.006 0.16 20.20 9.38 0.040 0.019 12.5 15.6 83.8 69
I CF–3 0.47 0.83 0.030 0.011 0.45 20.20 8.70 0.032 0.019 20.4 17.1 81.0 65

C1 CF–8 1.22 1.18 0.033 0.008 0.65 19.00 9.37 0.040 0.039 7.8 2.2 79.5 –
P1 CF–8 0.59 1.12 0.026 0.013 0.04 20.49 8.10 0.056 0.036 17.7 24.1 84.9 90

205 CF–8M 0.93 0.63 0.019 – 3.37 17.88 8.80 – 0.040 21.0 15.9 – 79
758 CF–8M 0.91 0.62 0.018 – 3.36 17.91 8.70 – 0.030 24.2 19.2 – 62

Reactor–Agedd
KRB CF–8 0.31 1.17 – – 0.17 21.99 8.03 0.038 0.062 27.7 34.0 – –

a Calculated from the composition with Hull's equivalent factor.

Measured by ferrite scope AUTO Test FE, Probe Type FSP–1.
b Static Cast Slabs: Foundry ESCO; Size 610 x 610 x 76 mm.
c Centrifugally Cast Pipes:
P3 Foundry SANDUSKY; Size 580 mm O.D.,76 mm wall.
P2 Foundry FAM, France; Size 930 mm O.D., 73 mm wall.
P1 Foundry ESCO; Size 890 mm O.D., 63 mm wall.
205 Size 305 mm O.D., 25 mm wall.
Static Cast:
Elbow 758: Size 305 mm O.D., 30 mm wall.
Pump Impeller I: Foundry ESCO; Size 660 mm diameter.
Pump Casing C1: Foundry ESCO; Size 600 mm O.D., 57 mm wall.
d KRB Reactor Pump Cover Plate: Foundry GF; Size 890 mm diameter.

Table 2. Ferrite content and grain structure of various cast stainless steel pipes

a
o.d. Wall Ferrite Content (%)
Heat (m) (mm) Process Grade o.d. i.d. Grain Structure
C1 0.60 57.1 Static CF–8 2.3 1.7 Banded, columnar/equiaxed radial to
axial growth near ends
P1 0.89 63.5 Centr. CF–8 27.6 19.5 Equiaxed across thickness
P3 0.58 51.6 Centr. CF–3 2.5 0.9 Banded, radially oriented columnar one
equiaxed band (≈4 mm deep) near i.d.
P2 0.93 73.0 Centr. CF–3 15.9 13.2 Equiaxed across thickness

a Ferrite content measured by Ferrite Scope, Auto Test FE, Probe Type FSP–1.

7
 Axial Circum. Axial Circum.
Heat P1 Heat P2
Figure 2. Grain structure along the axial and circumferential sections of centrifugally
cast pipes P1 and P2

Figure 3. Grain structure of various static–cast slabs

liquid and solid; the shear could cause dendrite arms to break and disperse in the liquid–solid
region.

The static–cast slabs and the pump casing ring showed a mixed structure of columnar and
equiaxed grains. The grain structures of the cast slabs are shown in Fig. 3. A change from
horizontal to vertical growth of the columnar grains was observed near the edges of the cast
slabs, e.g., Heat 73. The size of the equiaxed grains in the mixed structure is generally smaller
than that of the columnar grains.

8
 The ferrite morphology of the various materials varied with ferrite content, chemical com-
position, and size of the casting. The ferrite morphology was globular for materials containing
<5% ferrite. Some differences in morphology were observed between the different grades o f cast
stainless steel containing >5% ferrite. The CF–8 and CF–8M steels exhibited a lacy morphol
ogy, i.e., an interlaced network of ferrite islands, whereas the CF–3 cast steel showed a mixture
of lacy and acicular ferrite. The acicular morphology is characterized by fine needle–like ferrite
that is distributed in the austenite matrix. All morphologies were randomly arranged within
the casting. Typical microstructures for the static–cast slabs and pump impeller and centrifu-
gally cast pipes are shown in Figs. 4 and 5.

3 . 3 Tensile Tests

Tensile tests were conducted at ANL and at Materials Engineering Associates (MEA). The
orientation and location of the mechanical–test specimens from pipe sections, slabs, and the
KRB pump cover plate are shown in Figs. 6 and 7. The specimen blanks from the experimental
and commercial heats were aged at 290, 320, 350, 400, and 450°C (554, 608, 662, 752, and
842°F) for times up to 58,000 h. Details of the test procedure and results for the tests at MEA
have been presented earlier.2 5 , 2 6

Tests at ANL were performed according to ASTM Specification E 8 and E 21 in an Instron

tensile test machine with a maximum loading capacity of 90 kN (20 kips). Cylindrical specimens
with a diameter of 5.0 mm (0.2 in.) and a gauge length of 20.3 mm (0.8 in.) were used for all
the tests, Fig. 8. An axial extensometer, with an initial gauge length of 20.3 mm (0.8 in.), was
used for continuous measurement of strain during room–temperature tests. An IBM computer
was used to digitize load, crosshead movement, and axial displacement data, and to store the
data on floppy disks. Analog traces of load–vs.–crosshead displacement and load–vs.–ex-
tensometer displacement were also obtained for each test.

The true stress–strain data were calculated up to the maximum load using the constant–
volume criterion, which assumes a homogeneous distribution of strain along the gauge length.
However, most specimens showed inhomogeneous deformation because of relatively large grain
structure. The specimen surfaces along the gauge length were irregular, and the fracture cross
sections were often elliptical. These factors created some uncertainty in the true stress–strain
data. True fracture stress was obtained from the fracture load and cross–sectional area at frac-
ture. The strain at fracture, i.e., total elongation, was determined from extensometer displace-
ments. Total elongation was also measured from crosshead displacements; the values obtained
from the extensometer were ≈64% of the values determined from crosshead displacement.
Correlations between crosshead displacement and total strain in the specimen gauge length
were also developed from the room–temperature tests. These correlations were used to correct
the data for the elevated–temperature tests.

The tests at 290°C ( ≈ 550°F) were conducted in a forced–air recirculating furnace.

Thermocouples were mounted above and below the specimen gauge length to monitor and con-
trol the temperature within ±2°C. For the tests on samples aged for <10,000 h, an axial exten-
someter was not used for the elevated–temperature tests. Total strain in the specimen gauge
length was determined from correlations developed from the room–temperature tests. The total
elongation was determined from the crosshead displacement multiplied by 0.64.

9
Figure 4. Ferrite morphology from three locations across the thickness of
static–cast slabs of CF–3 (Heat 69), CF–8 (Heats 73 and 68),
and CF–8M (Heats 74, 70, and 75)

10
Figure 4. (Contd.)

11
Figure 4. (Contd.)

12
Figure 5. Ferrite morphology along the three orientations of the
centrifugally cast pipes (Heats P1, P2, and P3) and the
static–cast pump impeller (Heat I)

13
Figure 5. (Contd.)

14
Figure 5. (Contd.)

15
Figure 5. (Contd.)

16
Figure 5. (Contd.)

17
Figure 6. Orientation and location of the mechanical–test specimens taken from (a) and (b)
pipe sections and (c) slabs

Figure 7. Orientation and location of the mechanical–test specimens taken from KRB pump
cover plate

18
 2.400

63

63
.960 .570

.480 7/16
.150 R
C
16 16

A xxx-
xx

SEE NOTE 3
1/16 X 45 A .002

D1 7/16-20 UNF-2A
THREAD
.800
A .002
GAGE LENGTH
A .002 A .002

D2 D2
ALL UNITS ARE INCHES
D1 = .200 .001
D2 = FROM .001 TO .002 > D1
TOLERANCES = .005 UNLESS NOTED.

1. THE .800 INCH GAGE LENGTH TO HAVE UNIFORM SLOPE FROM MAX. DIA. D2 TO MIN. DIA. D1. UNIFORM SLOPE MUST
NOT EXCEED .004 CHANGE IN DIA. PER 1 INCH CHANGE IN LENGTH.

2. ALL RADII MUST BLEND WITHOUT UNDERCUTS OR STEPS.

3. DIMENSIONS AND SPECIFICATIONS TYPICAL BOTH ENDS.

4. ALL SURFACES TO BE FREE OF BURRS.

Figure 8. Configuration of tensile test specimen

Elevated–temperature tests on the long–term–aged samples were conducted with a clip

gauge mounted on the specimen grips. Total strain in the specimen gauge length was deter-
mined from correlations developed from room–temperature tests conducted with clip gauge at-
tached to the specimen grips and the extensometer mounted on the specimen gauge length.

The results for ten commercial and experimental heats aged up to 58,000 h at tempera-
tures between 290 and 450°C are given in Table 3; results from the tests at MEA are also in-
cluded in the table.

4 Effect of Thermal Aging

4 . 1 Tensile Strength

Tensile tests were conducted at room temperature and 290°C (554°F) on three commercial
and five experimental heats aged up t o 58,000 h a t 290–450°C (554–842°F) and on service–
aged material from the KRB pump cover plate. The results from the tests, which were con-
ducted at ANL27 and MEA,25,26 are given in the Appendix. The engineering stress–vs.–strain
curves for six of the heats of CF–3, CF–8, and CF–8M steel aged up to 50,000 h at 320, 350,
and 400°C and tested at room temperature and 290°C are shown in Figs. 9–14. At both test

19
Table 3. Tensile test results for cast stainless steels

Engineering Aging Condition

Test 0.2% Yield Ultimate Fracture Elong–at Red. in
Specimen Orien–t Temp. Stress Stress Stress ion Area Temp. Time
Number ationa Heatb (°C) (MPa) (MPa) (MPa) (%) (%) (°C) ( h ) Ref.b
CF–3 Grade
I1V–01 L I 25 264.8 598.8 1636.6 84.6 79.3 Unaged – 2
I1V–02 L I 25 242.1 583.4 1698.5 78.4 79.5 Unaged – 2
I2V–01 L I 25 251.0 579.9 1274.6 77.4 74.3 Unaged – 2
I2V–02 L I 25 257.7 578.1 1671.8 75.0 80.2 Unaged – 2
I3C–01 L I 25 239.7 517.6 1274.8 66.2 69.5 Unaged – 2
I2V–23 L I 25 235.8 637.3 1387.7 72.5 66.7 320 30000 1
I3C–14 L I 25 278.2 633.9 1411.7 56.9 68.2 320 30000 1
I3V–38 L I 25 255.0 609.6 1432.6 56.6 68.5 320 30000 1
I3V–39 L I 25 282.5 452.7 858.8 12.7 50.5 320 30000 1
I1V–26 L I 25 281.3 615.4 1897.6 60.6 77.4 350 10000 2
I1V–27 L I 25 303.4 644.7 1445.0 – 62.2 350 10000 2
I2V–19 L I 25 314.7 642.0 1296.9 72.0 68.4 350 10000 2
I2V–03 L I 290 169.2 409.2 756.1 – 58.9 Unaged – 2
I2V–06 L I 290 178.5 402.4 837.8 39.4 64.6 Unaged – 2
I3C–02 L I 290 158.6 387.3 819.5 33.0 66.2 Unaged – 2
I2V–24 L I 290 178.6 445.9 710.7 28.9 57.2 320 30000 1
I3C–15 L I 290 163.6 427.2 810.4 27.9 67.2 320 30000 1
I3V–40 L I 290 – 470.5 828.9 18.5 54.7 320 30000 1
I1V–28 L I 290 192.4 381.1 503.0 – 36.0 350 10000 2
I1V–29 L I 290 189.0 442.8 780.5 34.2 59.7 350 10000 2
I2V–20 L I 290 179.1 437.8 756.0 39.0 51.6 350 10000 2
P21T–01 C P2 25 216.3 538.3 1000.4 72.6 59.9 Unaged – 2
P23T–01 C P2 25 238.1 556.8 1568.6 106.0 84.4 Unaged – 2
P22A–01 L P2 25 206.4 561.7 1094.5 73.7 75.7 Unaged – 2
P23A–01 L P2 25 216.7 536.9 887.4 62.4 75.1 Unaged – 2
P22T–16 C P2 25 247.0 580.1 1547.8 65.4 79.9 290 30000 1
P21A–31 L P2 25 242.6 571.1 2017.1 65.9 84.7 290 30000 1
P25A–28 L P2 25 223.9 548.3 1797.3 57.2 87.0 290 30000 1
P21A–36 L P2 25 263.6 583.8 1564.4 58.3 79.3 290 58000 1
P24T–14 C P2 25 229.4 600.0 1944.4 73.1 82.3 320 30000 1
P25T–10 C P2 25 258.1 581.8 1535.3 55.4 75.5 320 30000 1
P22A–36 L P2 25 237.4 603.0 1487.0 77.8 80.5 320 30000 1
P21A–19 L P2 25 249.7 605.2 1673.6 49.4 78.3 320 55000 1
P22T–04 C P2 25 252.3 601.8 2162.5 – 85.3 350 10000 2
P23A–14 L P2 25 249.2 594.3 2783.2 73.6 88.5 350 10000 2
P23A–26 L P2 25 265.2 608.5 1830.3 76.6 78.8 350 10000 2
P22T–11 C P2 25 249.3 628.4 1235.0 68.6 64.4 350 30000 1
P22A–13 L P2 25 245.5 615.4 1598.5 65.5 76.2 350 30000 1
P24A–32 L P2 25 225.4 617.2 1799.8 68.9 79.0 350 30000 1
P24T–05 C P2 25 233.5 603.1 1268.2 – 68.8 400 10000 2
P24A–04 L P2 25 236.2 616.8 2384.5 – 78.0 400 10000 2
P21T–02 C P2 290 161.3 387.1 819.1 44.6 72.2 Unaged – 2
P23T–02 C P2 290 154.2 405.0 688.2 42.4 65.9 Unaged – 2
P22A–02 L P2 290 137.9 406.9 755.7 47.2 65.9 Unaged – 2
P23A–02 L P2 290 144.0 385.1 538.7 39.9 59.6 Unaged – 2
P21A–32 L P2 290 162.3 403.4 830.6 36.8 74.5 290 30000 1
P21A–33 L P2 290 155.2 405.9 740.8 35.0 73.7 290 30000 1
P24T–16 C P2 290 148.2 407.0 389.5 39.9 78.7 290 30000 1
P21A–37 L P2 290 164.2 410.7 1152.1 33.1 72.2 290 58000 1
P22T–17 C P2 290 177.5 422.7 1094.7 37.9 72.3 290 58000 1
P21A–14 L P2 290 153.2 428.9 968.4 31.4 73.0 320 30000 1
P21A–15 L P2 290 163.9 422.7 815.5 30.9 62.9 320 30000 1
P21A–16 L P2 290 152.6 407.7 870.6 28.8 71.9 320 30000 1
P25T–12 C P2 290 171.4 418.4 790.5 31.5 62.5 320 55000 1
P21A–18 L P2 290 168.6 416.4 980.1 31.2 67.9 320 55000 1

20
Table 3. (Contd.)

Engineering Aging Condition

Test 0.2% Yield Ultimate Fracture Elong–at Red. in
Specimen Orien–t Temp. Stress Stress Stress ion Area Temp. Time
Number ationa Heat (°C) (MPa) (MPa) (MPa) (%) (%) (°C) ( h ) Ref.b
P21T–08 C P2 290 155.6 423.5 876.3 49.8 70.7 350 10000 2
P22T–05 C P2 290 153.8 399.0 696.5 43.0 66.9 350 10000 2
P23A–15 L P2 290 161.0 415.4 900.5 – 69.7 350 10000 2
P23A–27 L P2 290 154.1 419.4 970.7 39.6 72.9 350 10000 2
P22T–12 C P2 290 167.0 436.2 740.2 28.2 56.0 350 30000 1
P24A–30 L P2 290 142.4 432.1 828.0 38.5 60.9 350 30000 1
P24A–33 L P2 290 149.1 425.7 463.7 41.5 62.6 350 30000 1
P24T–06 C P2 290 160.4 447.1 818.5 40.2 56.4 400 10000 2
P24A–05 L P2 290 146.6 430.6 655.0 40.2 53.8 400 10000 2
693–40 H 69 25 278.8 606.0 1070.1 57.1 48.9 Unaged – 2
693–41 H 69 25 273.4 583.6 1093.4 54.1 54.4 Unaged – 2
694–30 H 69 25 253.6 592.7 1430.6 50.1 71.8 290 30000 1
694–31 H 69 25 264.1 588.9 1714.0 51.1 76.4 290 30000 1
69–135 V 69 25 244.7 600.6 1617.5 62.8 74.5 290 30000 1
694–21 H 69 25 286.7 624.6 1757.0 52.2 76.1 320 10000 1
694–25 H 69 25 232.1 585.4 1428.3 70.5 75.2 320 10000 1
692–40 H 69 25 289.6 622.0 1516.1 43.6 72.3 320 30000 1
692–41 H 69 25 269.4 604.4 1623.8 38.0 75.2 320 30000 1
69–245 V 69 25 272.5 485.8 – 12.9 25.4 320 30000 1
691–28 H 69 25 291.6 637.9 1484.8 45.7 69.2 320 50000 1
691–29 H 69 25 287.7 650.5 1604.0 50.3 71.7 320 50000 1
69–230 V 69 25 298.8 669.4 1713.1 53.5 71.8 320 50000 1
692–25 H 69 25 285.4 633.4 1483.2 67.7 76.2 350 2570 2
692–26 H 69 25 302.6 648.2 1364.3 62.5 72.4 350 2570 2
694–06 H 69 25 292.1 652.0 1902.3 54.2 76.0 350 10000 1
694–07 H 69 25 266.2 635.5 1480.4 53.5 71.6 350 10000 1
694–08 H 69 25 246.8 619.9 1564.4 54.7 72.7 350 10000 1
69–119 V 69 25 249.6 617.3 1811.6 51.6 78.4 350 10000 1
693–12 H 69 25 270.9 674.0 1795.8 50.6 71.4 350 30000 1
693–13 H 69 25 259.2 655.1 1665.4 49.0 68.9 350 30000 1
69–130 V 69 25 258.4 661.2 1936.1 55.3 74.8 350 30000 1
692–16 H 69 25 253.6 638.8 1358.9 52.4 72.4 400 2570 2
692–17 H 69 25 300.9 683.2 1309.9 44.3 60.6 400 2570 2
692–15 H 69 25 287.8 673.9 1409.6 43.6 56.8 400 10000 1
692–22 H 69 25 278.6 699.1 1727.1 51.2 68.3 400 10000 1
692–23 H 69 25 260.5 664.7 1653.4 53.3 72.0 400 10000 1
69–109 V 69 25 276.7 688.0 1796.6 65.7 73.5 400 10000 1
691–04 H 69 25 271.3 691.9 1476.9 36.5 71.4 450 2570 2
691–05 H 69 25 263.1 664.6 1528.2 56.6 73.2 450 2570 2
693–42 H 69 290 190.8 420.9 908.2 35.9 63.4 Unaged – 2
694–40 H 69 290 177.0 417.0 809.0 33.6 59.7 Unaged – 2
694–32 H 69 290 176.8 401.9 422.9 29.4 67.0 290 30000 1
694–33 H 69 290 173.0 386.7 543.7 21.5 51.3 290 30000 1
69–236 V 69 290 194.1 440.5 818.0 30.8 61.9 290 30000 1
694–26 H 69 290 174.4 408.7 697.5 21.8 60.5 320 10000 1
694–27 H 69 290 183.5 422.8 973.7 20.9 65.3 320 10000 1
692–42 H 69 290 178.5 423.2 709.8 21.6 55.0 320 30000 1
694–39 H 69 290 168.2 413.8 692.4 21.3 51.7 320 30000 1
69–246 V 69 290 165.5 423.0 921.8 27.8 70.6 320 30000 1
692–28 H 69 290 209.1 462.5 895.8 28.1 59.8 320 55000 1
692–29 H 69 290 212.3 464.4 911.6 27.9 58.5 320 55000 1
69–130 V 69 290 204.7 468.0 733.1 29.1 52.8 320 55000 1
692–27 H 69 290 173.1 451.3 752.6 32.3 53.8 350 2570 2
694–09 H 69 290 156.4 413.1 720.9 29.8 52.7 350 10000 1
69–120 V 69 290 179.8 429.8 875.1 23.2 68.8 350 10000 1

21
Table 3. (Contd.)

Engineering Aging Condition

Test 0.2% Yield Ultimate Fracture Elong–at Red. in
Specimen Orien–t Temp. Stress Stress Stress ion Area Temp. Time
Number ationa Heat (°C) (MPa) (MPa) (MPa) (%) (%) (°C) ( h ) Ref.b
693–14 H 69 290 186.4 457.6 832.1 28.0 58.0 350 30000 1
693–15 H 69 290 195.8 444.0 639.2 32.5 46.9 350 30000 1
69–270 V 69 290 193.6 462.4 739.4 27.7 49.4 350 30000 1
692–18 H 69 290 163.9 444.8 556.4 21.8 33.2 400 2570 2
692–24 H 69 290 173.3 494.5 785.1 23.4 44.8 400 10000 1
69–110 V 69 290 196.9 481.6 802.3 26.1 51.5 400 10000 1
691–06 H 69 290 177.7 479.7 683.6 28.5 44.9 450 2570 2
692–09 H 69 290 175.7 477.1 793.4 27.4 51.0 450 2570 2
CF–8 Grade
18–11 C KRB 25 306.2 554.9 1348.9 56.8 67.0 280 68000 1
18–12 C KRB 25 288.5 555.9 1426.1 35.0 70.2 280 68000 1
18–22 C KRB 25 291.9 568.9 1162.3 40.4 59.2 280 68000 1
13–12 C KRB 25 317.3 567.4 1285.7 57.4 6 7 . 7 Reannealed – 1
13–21 C KRB 25 289.2 575.2 1209.1 43.4 6 7 . 0 Reannealed – 1
13–22 C KRB 25 287.7 531.2 1370.6 44.0 6 9 . 5 Reannealed – 1
15–11 C KRB 290 214.0 469.0 924.1 33.4 62.4 280 68000 1
15–12 C KRB 290 208.4 444.5 774.1 28.9 51.1 280 68000 1
15–21 C KRB 290 199.6 482.5 842.1 38.3 53.3 280 68000 1
15–22 C KRB 290 180.2 434.0 710.1 35.7 51.1 280 68000 1
16–21 C KRB 290 184.0 405.0 605.4 25.9 4 1 . 5 Reannealed – 1
17–21 C KRB 290 171.5 416.2 875.3 42.1 6 6 . 3 Reannealed – 1
P13T–01 C P1 25 244.7 584.5 1221.5 56.5 68.8 Unaged – 2
P13T–03 C P1 25 245.9 579.9 1206.6 54.6 65.9 Unaged – 2
P11A–01 L P1 25 – 584.9 1127.0 57.7 64.0 Unaged – 2
P13A–01 L P1 25 248.5 584.5 1579.5 62.4 72.9 Unaged – 2
P14T–09 C P1 25 266.2 596.2 1561.8 74.6 74.4 290 30000 1
P11A–25 L P1 25 285.7 595.2 1660.1 70.2 71.7 290 30000 1
P14A–26 L P1 25 276.5 575.7 993.2 42.7 61.6 290 30000 1
P11A–28 L P1 25 263.5 536.0 1915.5 68.1 78.3 290 58000 1
P11A–29 L P1 25 266.1 562.0 415.05 63.5 51.9 290 58000 1
P11A–10 L P1 25 279.1 622.6 1625.9 62.5 70.7 320 30000 1
P11T–06 C P1 25 – 569.3 1676.7 48.1 79.6 320 30000 1
P14T–08 C P1 25 – – – 47.7 78.3 320 30000 1
P11A–13 L P1 25 299.0 646.8 1100.7 61.3 53.1 320 55000 1
P12A–25 L P1 25 287.6 688.3 1463.6 60.9 60.3 320 55000 1
P12T–05 C P1 25 276.8 610.8 1315.5 67.2 58.9 350 10000 2
P12T–06 C P1 25 263.4 608.7 864.7 87.2 76.1 350 10000 2
P12A–08 L P1 25 290.5 652.9 1625.9 – 75.2 350 10000 2
P12A–09 L P1 25 271.2 618.0 2322.0 – 80.2 350 10000 2
P12T–11 C P1 25 266.6 617.0 1240.0 47.7 61.0 350 30000 1
P12A–13 L P1 25 285.0 637.0 1068.7 67.8 55.8 350 30000 1
P12A–14 L P1 25 263.5 634.9 1648.8 44.1 70.3 350 30000 1
P13T–07 C P1 25 285.0 660.0 1351.8 46.8 55.8 400 10000 2
P13A–07 L P1 25 286.3 677.7 1429.8 68.6 56.4 400 10000 2
P13T–02 C P1 290 148.5 408.8 642.2 33.3 43.9 Unaged – 2
P14T–01 C P1 290 157.0 437.5 622.3 32.6 46.4 Unaged – 2
P11A–02 L P1 290 159.9 442.7 497.0 35.5 36.7 Unaged – 2
P13A–02 L P1 290 155.0 424.4 850.8 43.0 67.2 Unaged – 2
P14T–10 C P1 290 166.1 415.3 769.1 35.4 64.0 290 30000 1
P11A–26 L P1 290 160.3 394.6 605.7 51.3 73.6 290 30000 1
P14A–27 L P1 290 167.8 421.6 812.5 29.4 60.1 290 30000 1
P11A–27 L P1 290 167.1 388.4 843.0 34.8 60.1 290 58000 1
P11A–30 L P1 290 179.3 445.5 683.6 39.5 46.6 290 58000 1
P11A–09 L P1 290 175.5 435.1 934.6 29.4 59.1 320 30000 1
P12A–19 L P1 290 174.8 456.9 731.1 27.4 51.6 320 30000 1
P12A–22 L P1 290 175.4 418.7 629.7 24.5 46.6 320 30000 1

22
Table 3. (Contd.)

Engineering Aging Condition

Test 0.2% Yield Ultimate Fracture Elong–at Red. in
Specimen Orien–t Temp. Stress Stress Stress ion Area Temp. Time
Number ationa Heat (°C) (MPa) (MPa) (MPa) (%) (%) (°C) ( h ) Ref.b
P11A–12 L P1 290 188.2 424.8 865.0 39.5 56.6 320 55000 1
P12A–26 L P1 290 200.4 472.0 951.8 31.0 58.3 320 55000 1
P12T–08 C P1 290 180.2 454.2 981.5 – 63.4 350 10000 2
P12A–10 L P1 290 173.7 451.3 919.6 43.4 62.8 350 10000 2
P12A–11 L P1 290 180.7 457.7 823.2 42.4 55.8 350 10000 2
P12T–12 C P1 290 194.9 472.7 786.5 24.8 58.0 350 30000 1
P14A–22 L P1 290 185.3 462.3 719.2 25.3 44.5 350 30000 1
P14A–23 L P1 290 198.6 475.6 735.1 25.1 42.0 350 30000 1
P13T–08 C P1 290 167.3 502.2 791.0 – 49.6 400 10000 2
P13A–08 L P1 290 162.9 485.6 881.0 35.6 51.0 400 10000 2
683–40 H 68 25 274.1 530.0 996.8 45.4 53.4 Unaged – 2
683–41 H 68 25 279.4 517.2 811.9 36.4 49.2 Unaged – 2
683–33 H 68 25 263.1 502.3 2242.4 55.7 83.2 290 30000 1
684–31 H 68 25 269.2 531.5 2050.9 42.3 79.7 290 30000 1
68–145 V 68 25 278.0 566.4 1903.0 42.1 78.9 290 30000 1
684–21 H 68 25 304.5 614.1 1291.8 67.8 61.9 320 10000 1
684–22 H 68 25 281.0 571.2 1880.1 76.6 80.7 320 10000 1
682–41 H 68 25 305.7 621.0 1544.6 40.8 71.2 320 30000 1
684–39 H 68 25 358.2 614.4 1716.9 43.4 75.4 320 30000 1
68–264 V 68 25 296.2 572.5 1903.8 65.3 75.6 320 30000 1
681–28 H 68 25 326.9 640.3 1130.7 51.0 66.6 320 50000 1
681–29 H 68 25 303.7 608.4 1666.1 50.7 71.1 320 50000 1
68–230 V 68 25 294.3 578.9 1696.8 47.0 75.8 320 50000 1
682–25 H 68 25 281.5 601.6 1647.2 64.1 75.2 350 5780 2
682–26 H 68 25 294.8 599.4 1620.7 62.0 73.5 350 5780 2
684–06 H 68 25 264.5 606.5 2014.0 53.7 78.3 350 10000 1
684–07 H 68 25 299.7 601.1 1953.4 47.4 76.7 350 10000 1
684–08 H 68 25 296.8 612.0 2084.7 52.6 78.5 350 10000 1
68–129 V 68 25 287.6 595.8 1688.6 58.5 73.5 350 10000 1
684–10 H 68 25 299.0 652.8 2072.9 44.6 74.9 350 30000 1
684–11 H 68 25 281.1 628.2 1342.3 55.0 57.4 350 30000 1
68–139 V 68 25 287.4 639.0 2090.6 44.5 77.0 350 30000 1
682–16 H 68 25 294.1 657.8 1534.6 75.0 64.0 400 2570 2
682–17 H 68 25 289.8 629.5 1313.0 – 64.6 400 2570 2
682–15 H 68 25 313.4 641.0 1526.3 36.8 64.4 400 10000 1
682–22 H 68 25 299.3 650.4 1019.0 43.9 49.4 400 10000 1
682–23 H 68 25 306.0 657.4 941.5 31.8 42.2 400 10000 1
68–119 V 68 25 – 624.3 1926.8 44.0 72.9 400 10000 1
681–04 H 68 25 291.3 653.1 1030.9 41.5 38.7 450 2570 2
681–05 H 68 25 309.4 632.9 1447.0 – 68.7 450 2570 2
683–42 H 68 290 162.7 397.3 815.4 29.2 57.8 Unaged – 2
684–40 H 68 290 156.4 412.3 792.0 37.9 60.6 Unaged – 2
684–32 H 68 290 149.5 333.2 513.0 27.7 62.2 290 30000 1
684–33 H 68 290 155.0 399.6 784.0 43.8 62.6 290 30000 1
68–246 V 68 290 170.6 390.7 522.1 28.4 51.5 290 30000 1
684–23 H 68 290 173.4 416.6 1048.7 26.8 72.7 320 10000 1
684–24 H 68 290 164.4 442.8 869.9 32.6 58.2 320 10000 1
682–40 H 68 290 174.3 440.8 853.5 36.6 62.3 320 30000 1
682–42 H 68 290 176.9 451.6 788.3 38.1 59.6 320 30000 1
68–263 V 68 290 165.6 450.3 758.2 37.2 48.0 320 30000 1
682–28 H 68 290 203.3 479.0 1132.6 32.6 64.0 320 50000 1
682–29 H 68 290 205.3 485.6 824.2 41.4 47.1 320 50000 1
68–130 V 68 290 201.3 475.2 699.1 38.9 46.2 320 50000 1
682–27 H 68 290 185.1 452.4 826.3 41.7 57.8 350 5780 2
684–09 H 68 290 164.3 500.3 765.7 30.5 51.9 350 10000 1
68–130 V 68 290 168.9 447.2 765.4 27.0 49.9 350 10000 1

23
Table 3. (Contd.)

Engineering Aging Condition

Test 0.2% Yield Ultimate Fracture Elong–at Red. in
Specimen Orien–t Temp. Stress Stress Stress ion Area Temp. Time
Number ationa Heat (°C) (MPa) (MPa) (MPa) (%) (%) (°C) ( h ) Ref.b
684–12 H 68 290 216.0 485.7 888.0 29.6 53.9 350 30000 1
684–15 H 68 290 190.4 427.3 671.2 25.3 41.7 350 30000 1
68–140 V 68 290 170.2 479.0 482.8 31.6 53.6 350 30000 1
682–18 H 68 290 161.3 463.1 711.3 32.1 47.1 400 2570 2
682–24 H 68 290 176.7 475.6 800.8 34.4 47.6 400 10000 1
68–120 V 68 290 193.9 484.4 734.0 27.8 37.1 400 10000 1
681–06 H 68 290 169.7 486.8 700.4 – 36.8 450 2570 2
682–09 H 68 290 191.6 503.8 769.0 35.5 42.6 450 2570 2
733–40 H 73 25 254.3 557.0 882.9 46.5 41.3 Unaged – 1
733–41 H 73 25 249.5 530.8 988.8 54.9 55.1 Unaged – 1
734–23 H 73 25 221.9 475.4 1835.0 62.7 78.0 320 10000 1
734–24 H 73 25 228.2 521.4 1675.1 72.3 78.0 320 10000 1
732–25 H 73 25 244.0 526.5 1453.0 57.3 74.2 350 2570 1
732–26 H 73 25 244.4 528.4 1109.6 45.5 65.4 350 2570 1
734–06 H 73 25 228.0 536.9 1885.1 53.5 78.0 350 10000 1
734–07 H 73 25 219.1 529.3 2005.0 67.1 79.0 350 10000 1
73–119 H 73 25 212.8 488.1 2084.8 50.8 83.0 350 10000 1
732–16 H 73 25 240.8 541.8 1390.9 59.5 72.4 400 2570 1
732–17 H 73 25 252.6 555.7 1419.0 56.1 72.1 400 2570 1
732–15 H 73 25 235.3 563.3 2183.2 58.5 79.2 400 10000 1
732–22 H 73 25 215.8 530.3 1298.3 58.4 63.6 400 10000 1
73–109 V 73 25 222.2 534.0 1719.7 69.0 74.4 400 10000 1
731–04 H 73 25 256.5 493.1 944.5 34.4 53.1 450 2570 1
731–05 H 73 25 234.0 570.4 1511.4 75.2 69.3 450 2570 1
733–42 H 73 290 138.9 366.6 970.1 40.5 75.8 Unaged – 1
734–40 H 73 290 133.9 365.0 599.5 33.0 54.0 Unaged – 1
734–19 H 73 290 130.4 354.0 426.4 33.6 33.8 320 10000 1
734–22 H 73 290 131.3 365.2 743.5 45.7 61.1 320 10000 1
732–27 H 73 290 139.6 419.8 833.9 44.3 62.0 350 2570 1
734–08 H 73 290 127.7 377.7 964.3 40.7 68.6 350 10000 1
734–09 H 73 290 165.0 417.5 725.9 28.9 53.3 350 10000 1
73–120 V 73 290 136.7 386.4 835.4 35.5 69.0 350 10000 1
732–18 H 73 290 – 444.1 700.7 38.0 59.3 400 2570 1
732–23 H 73 290 138.5 408.5 683.8 39.7 50.0 400 10000
732–24 H 73 290 143.0 424.1 649.8 32.7 40.2 400 10000
73–110 V 73 290 139.4 395.8 696.5 37.4 51.7 400 10000
731–06 H 73 290 144.1 411.2 596.6 24.8 39.2 450 2570 1
732–09 H 73 290 136.2 436.1 730.6 43.6 51.2 450 2570 1
CF–8M Grade
205–26 L 205 25 248.5 670.6 1227.7 36.3 65.0 400 18000 1
205–27 L 205 25 254.0 642.4 1694.1 49.0 71.2 400 18000 1
205–30 L 205 25 248.7 646.1 1576.7 41.8 70.6 400 18000 1
205–25 L 205 290 179.4 505.9 744.1 23.6 44.6 400 18000 1
205–28 L 205 290 177.3 507.8 790.3 27.0 49.2 400 18000 1
205–29 L 205 290 168.2 495.1 700.7 24.6 44.2 400 18000 1
743–40 H 74 25 273.5 542.4 1356.5 – 65.4 Unaged – 1
743–41 H 74 25 273.0 531.3 1362.7 63.0 68.3 Unaged – 1
743–36 H 74 25 282.2 555.6 2157.5 42.5 83.2 290 30000 1
744–34 H 74 25 292.9 601.2 1509.6 38.1 72.1 290 30000 1
74–135 V 74 25 259.0 570.4 1832.2 55.6 77.6 290 30000 1
744–21 H 74 25 273.1 551.0 1848.3 49.9 78.1 320 10000 1
744–25 H 74 25 270.5 565.3 2107.4 69.9 80.8 320 10000 1
742–42 H 74 25 312.7 589.9 1418.6 40.2 66.4 320 30000 1
744–39 H 74 25 326.4 663.6 1400.8 39.2 63.6 320 30000 1
74–245 V 74 25 278.8 617.0 1579.6 44.4 76.7 320 30000 1

24
Table 3. (Contd.)

Engineering Aging Condition

Test 0.2% Yield Ultimate Fracture Elong–at Red. in
Specimen Orien–t Temp. Stress Stress Stress ion Area Temp. Time
Number ationa Heat (°C) (MPa) (MPa) (MPa) (%) (%) (°C) ( h ) Ref.b
741–28 H 74 25 309.1 668.1 1056.7 42.2 52.7 320 50000 1
741–29 H 74 25 304.5 638.1 1506.5 48.3 62.9 320 50000 1
74–230 V 74 25 299.4 631.6 1623.1 47.1 68.7 320 50000 1
742–25 H 74 25 269.0 575.1 1380.5 58.9 68.1 350 2570 1
742–26 H 74 25 261.0 536.8 1517.5 62.5 72.0 350 2570 1
744–07 H 74 25 281.7 606.1 1498.4 57.1 63.8 350 10000 1
744–08 H 74 25 278.2 619.2 1903.6 38.7 74.0 350 10000 1
74–119 V 74 25 267.5 587.8 2081.4 49.3 80.9 350 10000 1
743–13 H 74 25 265.8 647.2 1198.4 55.6 51.8 350 30000 1
743–14 H 74 25 260.3 613.5 1375.6 39.5 63.8 350 30000 1
74–130 V 74 25 272.3 624.8 1334.6 37.6 60.0 350 30000 1
742–16 H 74 25 268.6 602.3 1409.4 44.1 70.8 400 2570 1
742–17 H 74 25 267.7 579.7 1308.7 41.7 71.8 400 2570 1
742–22 H 74 25 269.8 626.3 991.8 40.7 69.1 400 10000 1
742–23 H 74 25 267.7 624.3 1170.2 46.4 72.6 400 10000 1
74–110 V 74 25 259.2 607.9 1429.6 48.5 69.6 400 10000 1
741–04 H 74 25 257.5 620.5 1293.5 43.5 60.5 450 2570 1
741–05 H 74 25 259.1 616.7 1176.2 58.8 52.9 450 2570 1
744–40 H 74 290 171.8 412.3 557.7 25.3 58.7 Unaged – 1
743–42 H 74 290 164.6 442.8 674.7 35.4 42.1 Unaged – 1
744–35 H 74 290 193.8 424.7 1061.2 42.8 69.9 290 30000 1
744–36 H 74 290 165.2 424.1 810.8 35.1 54.9 290 30000 1
74–236 V 74 290 179.9 436.3 1433.8 29.2 76.4 290 30000 1
744–26 H 74 290 192.7 440.1 890.9 36.3 62.6 320 10000 1
744–27 H 74 290 181.0 420.6 831.2 35.8 56.9 320 10000 1
742–40 H 74 290 153.7 452.7 915.5 31.5 57.3 320 30000 1
742–41 H 74 290 190.3 483.3 748.7 24.0 42.5 320 30000 1
74–246 V 74 290 184.4 481.7 839.4 33.5 52.5 320 30000 1
742–28 H 74 290 203.5 473.3 884.5 33.7 53.1 320 50000 1
742–29 H 74 290 215.2 474.4 743.6 24.3 41.2 320 50000 1
74–130 V 74 290 235.4 517.7 741.1 29.5 34.2 320 50000 1
742–27 H 74 290 174.9 454.3 787.2 31.5 65.9 350 2570 1
744–06 H 74 290 185.4 448.0 677.7 28.0 38.7 350 10000 1
744–09 H 74 290 197.8 507.2 889.6 34.2 52.4 350 10000 1
74–120 V 74 290 176.6 453.8 751.0 33.3 48.3 350 10000 1
744–18 H 74 290 228.5 510.5 791.9 27.6 40.3 350 30000 1
743–15 H 74 290 180.0 503.8 830.7 34.0 49.9 350 30000 1
74–270 H 74 290 182.2 495.0 729.9 31.2 40.2 350 30000 1
742–18 H 74 290 166.2 485.1 695.0 28.5 57.1 400 2570 1
742–15 H 74 290 178.9 516.0 – 33.7 – 400 10000 1
742–24 H 74 290 184.2 509.1 848.8 29.9 48.9 400 10000 1
74–109 V 74 290 172.0 476.8 546.4 33.3 48.7 400 10000 1
741–06 H 74 290 172.0 500.7 678.6 22.9 45.5 450 2570 1
742–09 H 74 290 170.3 485.2 697.5 21.3 35.8 450 2570 1
753–40 H 75 25 313.5 610.4 1056.6 47.4 67.9 Unaged – 1
753–41 H 75 25 330.5 589.8 931.7 39.9 74.9 Unaged – 1
753–30 H 75 25 315.6 609.0 1668.9 37.2 75.0 290 30000 1
754–28 H 75 25 321.7 619.2 1140.2 48.3 70.5 290 30000 1
75–135 V 75 25 310.6 630.4 1448.9 48.3 69.7 290 30000 1
754–21 H 75 25 355.9 693.7 1822.9 58.5 75.0 320 10000 1
754–25 H 75 25 406.3 706.0 1763.9 46.4 71.2 320 10000 1
752–41 H 75 25 357.9 726.8 1224.7 38.8 52.4 320 30000 1
754–39 H 75 25 395.1 722.5 1203.2 39.2 52.5 320 30000 1
75–245 V 75 25 323.1 691.3 1418.1 47.5 62.2 320 30000 1
751–28 H 75 25 334.7 689.5 1118.9 28.1 40.8 320 50000 1
751–29 H 75 25 352.0 729.8 1166.6 27.0 43.2 320 50000 1

25
Table 3. (Contd.)

Engineering Aging Condition

Test 0.2% Yield Ultimate Fracture Elong–at Red. in
Specimen Orien–t Temp. Stress Stress Stress ion Area Temp. Time
Number ationa Heat (°C) (MPa) (MPa) (MPa) (%) (%) (°C) ( h ) Ref.b
75–230 V 75 25 378.4 759.5 1179.8 32.7 38.6 320 50000 1
752–25 H 75 25 – 667.8 1677.6 37.5 68.4 350 2570 1
752–26 H 75 25 346.5 688.9 1522.3 37.6 64.6 350 2570 1
754–06 H 75 25 332.7 741.1 1543.1 41.4 59.6 350 10000 1
754–07 H 75 25 352.5 728.5 1159.6 39.5 54.2 350 10000 1
754–08 H 75 25 308.6 718.8 1455.1 42.3 56.1 350 10000 1
75–119 V 75 25 354.0 742.8 1437.7 44.4 53.6 350 10000 1
753–10 H 75 25 316.1 766.4 1256.0 31.5 41.4 350 30000 1
753–11 H 75 25 344.3 748.2 1051.8 26.3 31.6 350 30000 1
75–130 V 75 25 300.8 711.0 1061.3 30.5 34.9 350 30000 1
752–16 H 75 25 326.7 703.6 1531.0 38.5 64.3 400 2570 1
752–17 H 75 25 353.1 731.5 1441.4 33.5 64.0 400 2570 1
752–15 H 75 25 405.3 777.1 1305.1 36.4 45.0 400 10000 1
752–22 H 75 25 – 749.1 1093.5 28.1 37.6 400 10000 1
752–23 H 75 25 338.9 726.6 1328.9 26.7 53.6 400 10000 1
75–109 V 75 25 359.0 736.8 1171.8 38.1 46.3 400 10000 1
751–04 H 75 25 311.7 721.2 1094.2 25.1 38.4 450 2570 1
751–05 H 75 25 314.7 746.4 1217.2 32.0 41.6 450 2570 1
754–40 H 75 290 196.8 470.8 652.0 26.1 63.1 Unaged – 1
753–42 H 75 290 191.5 474.8 620.7 30.5 45.0 Unaged – 1
754–29 H 75 290 193.3 528.3 1051.1 33.5 60.5 290 30000 1
754–30 H 75 290 202.6 495.3 784.9 31.1 58.5 290 30000 1
75–236 V 75 290 211.8 486.2 924.1 32.0 58.2 290 30000 1
754–26 H 75 290 205.6 538.0 945.5 28.9 64.7 320 10000 1
754–27 H 75 290 212.2 534.3 957.8 29.2 64.6 320 10000 1
752–40 H 75 290 231.7 589.3 852.7 26.0 38.4 320 30000 1
752–42 H 75 290 268.5 575.8 893.6 22.9 46.0 320 30000 1
75–246 V 75 290 213.0 521.8 881.3 26.7 54.2 320 30000 1
752–28 H 75 290 258.9 587.9 933.6 24.4 43.2 320 50000 1
752–29 H 75 290 264.1 581.7 969.4 23.2 48.5 320 50000 1
75–130 V 75 290 239.6 557.8 889.5 24.7 38.9 320 50000 1
752–27 H 75 290 204.7 528.8 843.9 25.8 49.4 350 2570 1
754–09 H 75 290 219.8 614.1 918.6 24.5 44.8 350 10000 1
75–120 V 75 290 209.9 595.6 854.7 32.7 35.4 350 10000 1
753–12 H 75 290 264.4 615.9 809.3 23.0 30.2 350 30000 1
754–12 H 75 290 227.2 613.8 839.4 24.2 31.2 350 30000 1
75–270 V 75 290 209.0 584.6 823.5 26.2 32.9 350 30000 1
752–18 H 75 290 203.2 591.1 799.6 26.4 41.0 400 2570 1
752–24 H 75 290 208.2 630.4 858.4 23.7 31.4 400 10000 1
75–110 V 75 290 206.7 593.1 884.1 25.3 42.4 400 10000 1
751–06 H 75 290 218.7 598.2 749.6 24.3 24.7 450 2570 1
752–09 H 75 290 197.7 606.2 888.1 25.5 33.0 450 2570 1
a Designation L = longitudinal or axial direction, C = circumferential direction, H = horizontal direction in the
plane of the slab, and V = vertical direction transverse to the plane of the slab.
b Heats I, P2, P1, KRB, and 205 are commercial and Heats 69, 68, 73, 74, and 75 are experimental.
c 1: Argonne National Laboratory
2: Materials Engineering Associates

26
 800
Heat 69 CF–3 Heat 69 CF–3
Engineering Stress (MPa)

δ = 21% δ = 21% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
200 Room Temp. 290°C
Unaged Unaged
20
2,570 h at 400°C 2,570 h at 400°C
10,000 h at 400 10,000 h at 400°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat 69 CF–3 Heat 69 CF–3
Engineering Stress (MPa)

δ = 21% δ = 21% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
Room Temp. 290°C
200 Unaged Unaged
2,570 h at 350°C 2,570 h at 350°C 20
10,000 h at 350 10,000 h at 350°C
30,000 h at 350 30,000 h at 350°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat 69 CF–3 Heat 69 CF–3
Engineering Stress (MPa)

δ = 21% δ = 21% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
Room Temp. 290°C
200 Unaged Unaged
10,000 h at 320°C 10,000 h at 320°C
20
30,000 h at 320°C 30,000 h at 320°C
50,000 h at 320°C 50,000 h at 320°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
Figure 9. Effect of thermal aging on engineering stress vs. strain curves for Heat 69

27
 800
Heat P2 CF–3 Heat P2 CF–3
Engineering Stress (MPa)

δ = 13% δ = 13% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
200
Room Temp. 290°C
20
Unaged Unaged
10,000 h at 400 10,000 h at 400°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat P2 CF–3 Heat P2 CF–3
Engineering Stress (MPa)

δ = 13% δ = 13% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
200 Room Temp. 290°C
Unaged Unaged 20
10,000 h at 350 10,000 h at 350°C
30,000 h at 350 30,000 h at 350°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat P2 CF–3 Heat P2 CF–3
Engineering Stress (MPa)

δ = 13% δ = 13% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
200 Room Temp. 290°C
Unaged Unaged 20
30,000 h at 320 30,000 h at 320°C
55,000 h at 320 55,000 h at 320°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
Figure 10. Effect of thermal aging on engineering stress vs. strain curves for Heat P2

28
 800
Heat 68 CF–8 Heat 68 CF–8
Engineering Stress (MPa)

δ = 15% δ = 15% 100

Engineering Stress (ksi)

c c
600
80

400 60

Room Temp. 40
200 Unaged 290°C
2,570 h at 400°C Unaged
10,000 h at 400° 20
2,570 h at 400°C
10,000 h at 400°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat 68 CF–8 Heat 68 CF–8
Engineering Stress (MPa)

δ = 15% δ = 15% 100

Engineering Stress (ksi)

c c
600
80

400 60

Room Temp. 40
290°C
200 Unaged Unaged
5,780 h at 350°C 3,000 h at 350°C 20
10,000 h at 350°C 10,000 h at 350°C
30,000 h at 350°C 30,000 h at 350°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat 68 CF–8 Heat 68 CF–8
Engineering Stress (MPa)

δ = 15% δ = 15% 100

Engineering Stress (ksi)

c c
600
80

400 60

Room Temp. 40
290°C
200 Unaged Unaged
10,000 at 320°C 10,000 h at 320°C20
30,000 h at 320°C 30,000 h at 320°C
50,000 h at 320°C 50,000 h at 320°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
Figure 11. Effect of thermal aging on engineering stress vs. strain curves for Heat 68

29
 800
Heat P1 CF–8 Heat P1 CF–8
Engineering Stress (MPa)

δ = 18% δ = 18% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
200
Room Temp. 290°C
20
Unaged Unaged
10,000 h at 400 10,000 h at 400°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat P1 CF–8 Heat P1 CF–8
Engineering Stress (MPa)

δ = 18% δ = 18% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
200 Room Temp. 290°C
Unaged Unaged 20
10,000 h at 350 10,000 h at 350°C
30,000 h at 350 30,000 h at 350°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat P1 CF–8 Heat P1 CF–8
Engineering Stress (MPa)

δ = 18% δ = 18% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
200 Room Temp. 290°C
Unaged Unaged 20
30,000 h at 320 30,000 h at 320°C
55,000 h at 320 55,000 h at 320°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
Figure 12. Effect of thermal aging on engineering stress vs. strain curves for Heat P1

30
 800
Heat 74 CF–8M Heat 74 CF–8M
Engineering Stress (MPa)

δ = 16% δ = 16% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
200 Room Temp. 290°C
Unaged Unaged
20
2,570 h at 400°C 2,570 h at 400°C
10,000 h at 400° 10,000 h at 400°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat 74 CF–8M Heat 74 CF–8M
Engineering Stress (MPa)

δ = 16% δ = 16% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
Room Temp. 290°C
200 Unaged Unaged
2,570 h at 350°C 2,570 h at 350°C 20
10,000 h at 350° 10,000 h at 350°C
30,000 h at 350° 30,000 h at 350°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat 74 CF–8M Heat 74 CF–8M
Engineering Stress (MPa)

δ = 16% δ = 16% 100

Engineering Stress (ksi)

c c
600
80

400 60

40
Room Temp. 290°C
200 Unaged Unaged
10,000 h at 320° 10,000 h at 320°C20
30,000 h at 320° 30,000 h at 320°C
50,000 h at 320° 50,000 h at 320°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
Figure 13. Effect of thermal aging on engineering stress vs. strain curves for Heat 74

31
 800
Heat 75 CF–8M
Engineering Stress (MPa)

δ = 25% 100

Engineering Stress (ksi)

c
600
80

400 Heat 75 CF–8M 60

δ = 25%
c
40
200 Room Temp. 290°C
Unaged Unaged 20
2,570 h at 400°C 3,000 h at 400°C
10,000 h at 400°C 10,000 h at 400°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat 75 CF–8M
Engineering Stress (MPa)

100
δ = 25%

Engineering Stress (ksi)

c
600
80

400 Heat 75 CF–8M 60

δ = 25%
c
Room Temp. 290°C 40
200 Unaged Unaged
2,570 h at 350°C 3,000 h at 350°C 20
10,000 h at 350°C 10,000 h at 350°C
30,000 h at 350°C 30,000 h at 350°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
800
Heat 75 CF–8M
Engineering Stress (MPa)

100
δ = 25%

Engineering Stress (ksi)

c
600
80

400 Heat 75 CF–8M 60

δ = 25%
c
Room Temp. 40
290°C
200 Unaged Unaged
10,000 h at 320°C 10,000 h at 320°C20
30,000 h at 320°C 30,000 h at 320°C
50,000 h at 320°C 50,000 h at 320°C
0 0
0 10 20 30 40 50 60 0 10 20 30 40 50 60
Engineering Strain (%) Engineering Strain (%)
Figure 14. Effect of thermal aging on engineering stress vs. strain curves for Heat 75

32
 1.4
Room Temp. 290°C
Yield Ratio (aged/unaged)

1.3 CF–3 CF–3

CF–8 CF–8
CF–8M
CF–8M
1.2

1.1

1.0

0.9
Open Symbols: ANL
Closed Symbols: FRA
0.8
0 1 2 3 4 5 0 1 2 3 4 5
Aging Parameter P Aging Parameter P

1.4
Room Temp. 290°C
Ultimate Ratio (aged/unaged)

1.3 CF–3 CF–3

CF–8 CF–8
CF–8M
CF–8M
1.2

1.1

1.0

0.9
Open Symbols: ANL
Closed Symbols: FRA
0.8
0 1 2 3 4 5 0 1 2 3 4 5
Aging Parameter P Aging Parameter P
Figure 15. Ratio of yield and ultimate stress of aged and unaged cast stainless steel as a
function of the aging parameter P

temperatures, thermal aging led to an increase in yield and ultimate stress and a slight decrease
in ductility. For all heats, the increase in ultimate stress is substantially greater than the
increase in yield stress. The Mo–bearing CF–8M steels are the most sensitive to thermal
aging and Mo–free low–C CF–3 steels the least sensitive. Some heats show no change in yield
stress. Furthermore, specimens aged for short times at high temperatures, e.g., ≈3,000 h at
400 (752°F), often show a decrease in yield stress.

The ratios of the yield and ultimate stress of aged and unaged cast stainless steels at room
temperature and 290°C (554°F) are plotted as a function of the aging parameter P in Fig. 15.
The results from tensile tests conducted at FRA15 are also shown in the figure. The aging pa-
rameter P is determined from the equation

1000Q ⎡ 1 1 ⎤
P = log10 [t ] – – , (1)
19.143 ⎢⎣ Ts + 273 673 ⎥⎦

where Q is the activation energy and t and Ts are the time and temperature of aging, respec-
tively. Equation 1 considers aging at 400°C as the baseline aging behavior for the material and

33
parameter P is the log of the aging time at 400°C. Activation energies for the various heats of
cast stainless steel were obtained from room–temperature Charpy–impact data for materials
that were aged up to 30,000 h at 290–400°C.5,6

The data show considerable scatter, particularly for the yield stress. However, for the vari-
ous heats of cast stainless steel, increases in yield and ultimate stress are observed for P values
of 1.5–2.5, which correspond to aging times of 30–300 h at 400°C. The increase in ultimate
stress is substantially greater than the increase in yield stress. The changes in yield and ulti-
mate stress range from –10 to 20% and from –5 t o 25%, respectively. These results are consis-
tent with the Charpy data, i.e., for a specific heat, an increase in tensile stress corresponds to a
decrease in impact energy.

Photomicrographs of the fracture surface of unaged and aged Heats P1, 68, and 75, tested
at room temperature and 290°C, are shown in Figs. 16–18. In most cases, the fracture mode
was predominantly a dimpled ductile failure, particularly for the unaged materials. The aged
materials showed some cleavage and, in addition, the high–C steels, e.g., Heats 68 and P1, ex-
hibit phase boundary separation.

Tensile properties of the cast materials can also be obtained from Charpy–impact data.
For a Charpy specimen, the yield stress is estimated from the expression

σ y = CPy B / Wb 2 , (2)

taken from Ref. 28, where Py is the yield load, W is the specimen width, B is the specimen
thickness, b is the uncracked ligament, and C is a constant. The yield load was obtained from
load–time traces of the Charpy tests. Deviation from linearity in the load–time traces occurred
a t 125–150 µ s for the various heats. The load at 2 0 0 µs was estimated t o represent 0.2% yield
stress. Ultimate stress was also obtained from impact data by means of Eq. 2 and the maxi-
mum load. The constant C was determined by comparing tensile and Charpy–impact data. The
best values of the constant were 1.50 and 2.36 for yield stress and ultimate stress, respec-
tively. The estimated values of tensile stress are based on the assumption that strain rate ef-
fects are approximately the same for all heats and aging conditions. The estimated values of
tensile stress are not accurate at temperatures corresponding to lower–shelf and transition re-
gions. The estimated values of yield and ultimate stress for Heats 68, 69, 74, and 75, along
with the values obtained from actual tensile tests, are shown in Fig. 19. The estimated tensile
properties are in good agreement with the measured values.

4 . 2 Engineering Stress–Strain Behavior

Thermal aging increases the strain–hardening rate of all grades of cast stainless steel. The
increase is greater at room temperature than at 290°C, and CF–8M steels show a larger increase
than do Mo–free grades of steel (Figs. 9–14). The influence of thermal aging on tensile
stress–strain behavior of cast stainless steels was evaluated by fitting the engineering stress ( σ )
vs. strain (ε) data with the RO equation

n
ε σ ⎛ σ ⎞
= + α⎜ ⎟ , (3)
εo σo ⎝ σo ⎠

34
Figure 16. Fracture surface of tensile specimens of unaged and aged
Heat P1 tested at room temperature and 290°C

35
Figure 17. Fracture surface of tensile specimens of unaged and aged
Heat 68 tested at room temperature and 290°C

36
Figure 18. Fracture surface of tensile specimens of unaged and aged
Heat 75 tested at room temperature and 290°C

37
 Temperature (°F) Temperature (°F)
-500 -300 -100 100 300 500 700 -500 -300 -100 100 300 500 700
800 800
Estimated Tensile Stress (MPa)

Estimated Tensile Stress (ksi)

CF–3 Steel CF–8 Steel
Heat 69 Ultimate Stress 100 Heat 68 Ultimate Stress 100
600 600
80 80

400 60 400 60

Yield Stress Yield Stress

40 40
200 Unaged 200 Unaged
o
10,000 h at 400 C 20 10,000 h at 400oC 20
Closed Symbols: Tensile Tests Closed Symbols: Tensile Tests
0 0 0 0
-300 -200 -100 0 100 200 300 400 -300 -200 -100 0 100 200 300 400

-500 -300 -100 100 300 500 700 -500 -300 -100 100 300 500 700
800 800
Estimated Tensile Stress (MPa)

Estimated Tensile Stress (ksi)

CF–8M Steel CF–8M Steel Ultimate Stress
Heat 74 Ultimate Stress 100 Heat 75 100

600 600
80 80

400 60 400 60
Yield Stress
Yield Stress 40 40
200 Unaged 200 Unaged
10,000 h at 400°C
10,000 h at 400oC 20 20
Closed Symbols: Tensile Tests Closed Symbols: Tensile Tests

0 0 0 0
-300 -200 -100 0 100 200 300 400 -300 -200 -100 0 100 200 300 400
Temperature (°C) Temperature (°C)

Figure 19. Values of yield and ultimate stress estimated from Charpy–impact data and those
obtained from tensile tests for Heats 69, 68, 74, and 75

where σ o is an arbitary reference stress, often assumed to be equal to flow or yield stress; the
reference strain ε o = σ o /E; α and n are RO parameters; and E is elastic modulus. The RO
equation can be rearranged to the form

n
Eε – σ ⎛ σ ⎞
= α⎜ ⎟ , (4)
σo ⎝ σo ⎠

which is more convenient for fitting stress vs. strain data; α can be determined at σ /σ o = 1 and
n can be obtained from the slope of the log–log plot of Eq. 4. For each test, the RO parameters
were obtained from the best–fit of the tensile data to Eq. 4, with flow stress σ f as the reference
stress

n
Eε – σ ⎛ σ ⎞ 1
= α1 ⎜ ⎟⎟ , (5)
σf ⎜σ
⎝ f ⎠

38
and also with yield stress σ y as the reference stress
n2
Eε – σ ⎛ σ ⎞
= α2 ⎜ ⎟ . (6)
σy ⎝ σy ⎠

The ROFIT computer program developed by Battelle* was used for the analyses. For each ref-
erence stress, three different sets of values of the RO parameters were obtained from the best
fit of the engineering stress–vs.–strain data for <5% strain, <15% strain, and the entire strain
range of the test. Typical examples of the ROFIT analyses with σ f as the reference stress are
shown in Fig. 20. The best–fit values of the constant for all the tensile tests are given in
Tables 4 and 5. As expected, the exponents n1 and n2 are the same from the two analyses,
where σ f or σ y are used as the reference stress. The parameters α 1 and α 2 follow the relation-
ship
n1 –1
⎛ σy ⎞
α 2 = α1 ⎜ ⎟ (7)
⎜σ ⎟
⎝ f⎠

and can be determined from one another. The results indicate that the exponent n1 or n 2 does
not change with thermal aging and differs for the three grades of steel. The parameters α 1 and
α 2 decrease with thermal aging.

5 Estimation of Tensile Properties

5 . 1 Flow Stress

Tensile flow stress of aged cast stainless steels can be estimated from the correlation be-
tween the ratio of the tensile flow stress of aged and unaged cast stainless steels and a normal-
ized aging parameter. Correlations have been developed for estimating the tensile flow stress o f
aged cast stainless steels from the kinetics of thermal embrittlement.6 The ratio of the tensile
flow stress of aged and unaged cast stainless steels at room temperature and 290°C (554°F) is
plotted as a function of a normalized aging parameter in Fig. 21. Flow stress is characterized
as the mean of the 0.2% yield stress and ultimate stress, and the aging parameter is normalized
with respect to a θ value of 2.9. The aging parameter P was determined from Eq. 1 and
experimental values of activation energy. At both temperatures, the flow stress ratio increased
with thermal aging; the increase in flow stress of CF–3 steels was the smallest and that of CF–
8M steels the largest. The correlations (shown as solid lines in Fig. 21) were obtained by sub-
tracting one times the standard deviation for the fit to the data from the best–fit curve. The
tensile–flow–stress ratio R f = (σfaged/σfunaged), is given by

R f = a1 + b1P (1.00 ≤ R f )
≤ c1 . (8)

Values of the constants a1 , b1 , and c1 for various grades of steel and test temperatures are
given in Table 6. Equation 8 is valid for R f values between 1 and c1, service temperatures

* ROFIT (Version 1.0) computer program for IBM PC developed by Battelle Columbus for the U.S. Nuclear
Regulatory Commission. Contact N. D. Ghadiali.

39
 6 6
Heat P2 CF–3 Steel Heat P2 CF–3 Steel
4 y = 4.92 + 11.96 x R= 0.96 4 Best–fit curves for
<5% stress vs. strain data
ln (E ε - σ ) / σf

ln (E ε - σ ) / σf
y = 3.47 + 6.45 x R= 0.99
290°C
2 y = 3.72 + 5.17 x R= 0.96 2

P21A-36 P21A-14
0 0
P22A-13 P21A-33
P25A-28 P24A-33
-2 -2
y = 3.27 + 6.52 x R= 0.99
Best–fit curves for
<5% stress vs. strain data y = 3.73 + 6.28 x R= 0.98
-4 -4
25°C
y = 4.86+ 7.95 x R= 0.96

-6 -6
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )

6 6
Heat 68 CF–8 Steel Heat 68 CF–8 Steel
4 y = 3.36 + 6.29 x R= 0.98 4
682-24
ln (E ε - σ ) / σf

ln (E ε - σ ) / σf
y = 2.58 + 5.43 x R= 0.96
681-06
2 y = 3.22 + 6.70 x R= 1.00
2 683-42

0 0
68-145 Best–fit curves for
<5% stress vs. strain data
681-28 290°C
-2 -2
684-11
y = 3.45 + 6.34 x R= 0.98
Best–fit curves for
-4 <5% stress vs. strain data -4 y = 3.55 + 5.38 x R= 1.00
25°C y = 3.72 + 5.17 x R= 0.96

-6 -6
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )

6 6
Heat 75 CF–8M Steel Heat 75 CF–8M Steel
4 y = 1.98 + 4.44 x R= 0.99 4 y = 2.79 + 6.00 x R= 0.99
y = 3.19 + 6.90 x R= 0.98
ln (E ε - σ ) / σf

ln (E ε - σ ) / σf

y = 2.33 + 5.23 x R= 0.99

2 y = 2.25 + 5.79 x R= 0.98
2 y = 2.91 + 6.59 x R= 0.99

Best–fit curves for Best–fit curves for

<5% stress vs. strain data <5% stress vs. strain data
0 0 290°C
25°C

-2 -2
751-05 752-18
-4 752-25 -4 754-40
753-40 752-40

-6 -6
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )
Figure 20. Examples of ROFIT analysis of tensile stress–vs.–strain curves at room temperature
and 290°C for cast stainless steels using flow stress as the reference stress

40
 6 6
Heat P2 CF–3 Steel Heat P2 CF–3 Steel
4 Best–fit curves for 4
Best–fit curves for
<15% stress vs. strain data
ln (E ε - σ ) / σf

ln (E ε - σ ) / σf
<15% stress vs. strain data
25°C 290°C
2 2

0 P25A-28 0 P21A-33
P22A-13 P24A-33
P21A-36 P21A-14
-2 -2
y = 3.59 + 6.74 x R= 0.99 y = 3.32 + 5.23 x R= 0.99
y = 3.34 + 6.18 x R= 0.99 y = 3.51 + 5.45 x R= 0.95
-4 -4
y = 3.75 + 9.027 x R= 0.96
y = 2.94 + 5.48 x R= 0.99

-6 -6
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )

6 6
Heat 68 CF–8 Steel Heat 68 CF–8 Steel
4 y = 2.96 + 6.04 x R= 0.98 4 Best–fit curves for
<15% stress vs. strain data
ln (E ε - σ ) / σf

ln (E ε - σ ) / σf
y = 3.12 + 6.67 x R= 1.00 290°C
2 y = 3.22 + 5.50 x R= 0.99
2

681-06
0 0
681-28 683-42
684-11 682-24
-2 68-145 -2
y = 3.32 + 4.90 x R= 1.00
Best–fit curves for
-4 <15% stress vs. strain data -4 y = 3.67 + 5.05 x R= 0.98
25°C y = 3.45 + 6.34 x R= 0.98

-6 -6
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )

6 6
Heat 75 CF–8M Steel Heat 75 CF–8M Steel
4 y = 2.68 + 6.65 x R= 0.98 y = 2.63 + 5.84 x R= 0.99
4
y = 2.99 + 6.49 x R= 0.99
ln (E ε - σ ) / σf

ln (E ε - σ ) / σf

y = 2.60 + 5.70 x R= 0.99

2 y = 2.16 + 4.78 x R= 0.99
y = 2.63 + 5.68 x R= 0.99
2 Best–fit curves for
<15% stress vs. strain data
0 290°C
753-40
0
752-25
-2
751-05
752-40
Best–fit curves for -2 754-40
-4 <15% stress vs. strain data
25°C 752-18

-6 -4
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )
Figure 20. (Contd.)

41
 6 6
Heat P2 CF–3 Steel Heat P2 CF–3 Steel
4 Best–fit curves for 4 Best–fit curves for
entire stress vs. strain data entire stress vs. strain data
ln (E ε - σ ) / σf

ln (E ε - σ ) / σf
25°C 290°C
2 2

P21A-36 P21A-14
0 P22A-13 0
P21A-33
P25A-28 P24A-33
-2 y = 3.26 + 7.041 x R= 0.96 -2
y = 2.90 + 5.30 x R= 0.99
y = 3.25 + 5.93 x R= 1.00
y = 3.25 + 4.99 x R= 0.99
-4 y = 3.44 + 6.40 x R= 0.99 -4
y = 3.33 + 4.95 x R= 0.96

-6 -6
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )

6 6

Heat 68 CF–8 Steel Heat 68 CF–8 Steel

4 y = 3.21 + 5.91 x R= 0.99 y = 3.19 + 5.56 x R= 0.99
4
y = 3.55 + 4.83 x R= 0.98
ln (E ε - σ ) / σf

y = 2.97 + 6.07 x R= 0.98

ln (E ε - σ ) / σf
2 y = 3.22 + 4.68 x R= 1.00
y = 3.11 + 6.69 x R= 1.00
2 Best–fit curves for
entire stress vs. strain data
0 68-145 290°C
681-28 0
684-11
-2
Best–fit curves for 682-24
entire stress vs. strain data -2 683-42
-4 o
25 C 681-06

-6 -4
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )

6 6
Heat 75 CF–8M Steel Heat 75 CF–8M Steel
4 4
y = 2.33 + 5.18 x R= 0.99 y = 2.56 + 5.52 x R= 0.99
ln (E ε - σ ) / σf

ln (E ε - σ ) / σf

y = 2.75 + 5.98 x R= 0.99 y = 2.84 + 6.16 x R= 0.99

2 2
y = 2.82 + 6.98 x R= 0.99 y = 2.57 + 5.63 x R= 0.99

0 0 752-18
751-05 754-40
752-25 752-40
-2 -2
753-40
Best–fit curves for Best–fit curves for
-4 entire stress vs. strain data -4 entire stress vs. strain data
25°C 290°C

-6 -6
-1.5 -1.0 -0.5 0.0 0.5 -1.5 -1.0 -0.5 0.0 0.5
σ /σ
ln (σ σf ) σ /σ
ln (σ σf )
Figure 20. (Contd.)

42
Table 4. Best–fit values of the Ramberg–Osgood constants for unaged and aged cast stainless
steels at room temperature

Stress–Strain Data <5% Strain Stress–Strain Data <15% Strain

Aging Aging Flow Yield Flow Stress Yield Stress Flow Stress Yield Stress
Specimen Temp. Time Stress Stress Reference Reference Reference Reference
Id (°C) (h) (MPa) (MPa) α1 n1 α2 n2 α1 n1 α2 n2

I1V–01 – Unaged – – – – – – – – – –
I1V–02 – Unaged – – – – – – – – – –
I2V–01 – Unaged – – – – – – – – – –
I2V–02 – Unaged – – – – – – – – – –
I3C–01 – Unaged – – – – – – – – – –
I2V–23 320 30000 – – – – – – – – – –
I3C–14 320 30000 – – – – – – – – – –
I3V–38 320 30000 – – – – – – – – – –
I3V–39 320 30000 – – – – – – – – – –
I1V–26 350 10000 – – – – – – – – – –
I1V–27 350 10000 – – – – – – – – – –
I2V–19 350 10000 – – – – – – – – – –

P21T–01 Unaged 383.9 216.3 159.990 9.444 1.260 9.457159.990 9.444 1.260 9.457
P23T–01 Unaged 383.9 238.1 40.424 5.683 4.337 5.741 85.369 7.176 4.585 7.167
P22A–01 Unaged 383.9 206.4 – – – – – – – –
P23A–01 Unaged 383.9 216.7 215.760 9.724 1.487 9.574 215.760 9.724 1.487 9.574
P22T–16 290 30000 402.2 247.0 32.593 7.114 1.668 7.139 25.473 6.437 1.835 6.402
P21A–31 290 30000 402.2 242.6 22.849 4.613 3.701 4.645 33.167 5.341 3.778 5.307
P25A–28 290 30000 402.2 223.9 51.289 7.584 1.087 7.616 36.499 6.778 1.222 6.799
P21A–36 290 58000 423.7 263.6 72.661 9.374 1.365 9.374 37.263 7.274 1.897 7.274
P24T–14 320 30000 420.6 229.4 40.476 6.737 1.312 6.718 33.034 6.226 1.457 6.200
P25T–10 320 30000 420.6 258.1 35.647 5.582 3.913 5.640 33.573 5.429 4.028 5.396
P22A–36 320 30000 420.6 237.4 33.190 7.072 1.079 7.058 27.017 6.515 1.209 6.486
P21A–19 320 55000 420.6 249.7 38.413 7.061 1.630 7.061 26.214 5.977 1.956 5.977
P22T–04 350 10000 428.6 252.3 54.343 7.512 1.725 7.583 37.351 6.682 1.863 6.661
P23A–14 350 10000 428.6 249.2 – – – – – – – –
P23A–26 350 10000 428.6 265.2 25.764 5.133 3.614 5.236 34.435 5.571 3.835 5.609
P22T–11 350 30000 430.2 249.3 26.955 5.275 2.633 5.282 27.933 5.291 2.809 5.217
P22A–13 350 30000 430.2 245.5 36.711 6.805 1.435 6.797 28.308 6.128 1.559 6.167
P24A–32 350 30000 430.2 225.4 39.929 6.309 1.291 6.309 37.118 6.148 1.332 6.148
P24T–05 400 10000 422.4 233.5 24.690 4.656 2.851 4.697 28.145 4.865 2.897 4.842
P24A–04 400 10000 422.4 236.2 28.971 4.915 3.007 4.955 29.521 4.936 3.059 4.912

693–40 – Unaged 435.5 278.8 – – – – – – – –

693–41 – Unaged 435.5 273.4 – – – – – – – –
694–30 290 30000 424.1 253.6 30.555 4.728 4.698 4.745 43.951 6.190 3.200 6.213
694–31 290 30000 424.1 264.1 24.789 5.776 2.512 5.776 27.213 5.920 2.574 5.920
69–135 290 30000 424.1 244.7 22.763 4.376 3.694 4.399 30.069 5.419 2.759 5.441
694–21 320 10000 432.2 286.7 17.925 4.851 3.713 4.869 20.988 5.264 3.717 5.224
694–25 320 10000 432.2 232.1 44.791 6.399 1.567 6.418 44.623 6.370 1.620 6.334
692–40 320 30000 424.0 289.6 15.853 5.845 2.512 5.846 15.988 5.837 2.555 5.820
692–41 320 30000 424.0 269.4 18.531 7.844 0.823 7.864 14.921 6.909 0.978 6.996
69–245 320 30000 424.0 272.5 26.978 6.855 2.047 6.829 24.139 6.386 2.204 6.411
691–28 320 50000 472.7 291.6 22.045 6.877 1.289 6.877 20.545 6.661 1.334 6.661
691–29 320 50000 472.7 287.7 21.561 6.549 1.371 6.549 20.691 6.421 1.402 6.421
69–230 320 50000 472.7 298.8 13.510 4.912 2.261 4.939 17.249 5.845 1.865 5.883
692–25 350 2570 467.4 285.4 15.553 4.340 3.026 4.367 26.148 5.012 3.654 5.006
692–26 350 2570 467.4 302.6 26.449 7.724 1.421 7.724 23.675 7.446 1.436 7.446
694–06 350 10000 447.4 292.1 17.587 5.489 2.633 5.467 19.035 5.746 2.601 5.673
694–07 350 10000 447.4 266.2 21.273 5.627 1.929 5.642 21.923 5.677 1.968 5.649
694–08 350 10000 447.4 246.8 35.089 5.691 2.174 5.710 43.789 6.389 1.783 6.394
69–119 350 10000 447.4 249.6 23.819 5.233 2.042 5.221 25.712 5.393 2.048 5.341
693–12 350 30000 463.1 270.9 10.841 3.606 2.693 3.631 14.585 4.623 2.089 4.646
693–13 350 30000 463.1 259.2 0.221 6.764 0.008 6.801 0.310 5.892 0.017 5.950
69–130 350 30000 463.1 258.4 0.170 6.811 0.006 6.809 0.229 6.114 0.011 6.180
692–16 400 2570 469.1 253.6 19.126 4.302 2.529 4.359 27.997 4.819 2.745 4.781
692–17 400 2570 469.1 300.9 13.736 5.709 1.706 5.727 14.780 5.816 1.769 5.790
692–15 400 10000 478.7 287.8 19.665 4.433 3.448 4.433 22.398 4.730 3.412 4.698
692–22 400 10000 478.7 278.6 14.768 3.925 3.078 3.906 18.461 4.490 2.867 4.447

43
Table 4. (Contd.)

Stress–Strain Data <5% Strain Stress–Strain Data <15% Strain

Aging Aging Flow Yield Flow Stress Yield Stress Flow Stress Yield Stress
Specimen Temp. Time Stress Stress Reference Reference Reference Reference
Id (°C) (h) (MPa) (MPa) α1 n1 α2 n2 α1 n1 α2 n2
692–23 400 10000 478.7 260.5 0.052 9.372 0.000 9.364 0.101 7.372 0.002 7.372
69–109 400 10000 478.7 276.7 15.407 3.777 3.422 3.763 20.840 4.475 3.211 4.422
691–04 450 2570 472.7 271.3 16.603 5.109 1.713 5.120 17.980 5.230 1.749 5.202
691–05 450 2570 472.7 263.1 15.329 4.617 1.833 4.676 21.304 5.129 1.938 5.094
13–12 Reannealed 428.0 317.3 11.427 5.877 2.680 5.931 19.503 7.339 2.968 7.326
13–21 Reannealed 428.0 289.2 14.418 6.371 1.775 6.388 16.916 6.855 1.739 6.805
13–22 Reannealed 428.0 287.7 21.342 6.146 2.787 6.179 29.837 6.952 2.854 6.923
18–11 280 68000 427.7 306.2 10.625 5.530 2.348 5.566 19.999 7.231 2.517 7.239
18–12 280 68000 427.7 288.5 10.993 4.205 3.137 4.219 18.607 5.475 3.254 5.445
18–22 280 68000 427.7 291.9 14.229 4.033 4.495 4.065 22.943 5.087 4.860 5.087
P13T–01 – Unaged 414.7 244.7 – – – – – – – –
P13T–03 – Unaged 414.7 245.9 18.390 4.811 2.558 4.811 – – – –
P11A–01 – Unaged 414.7 – – – – – – – – –
P13A–01 – Unaged 414.7 248.5 13.941 3.592 3.735 3.641 13.941 3.592 3.735 3.641
P14T–09 290 30000 432.6 266.2 38.307 7.901 1.371 7.881 30.932 7.239 1.561 7.157
P11A–25 290 30000 432.6 285.7 19.437 5.851 2.637 5.982 41.052 7.222 3.163 7.197
P14A–26 290 30000 432.6 276.5 32.047 8.186 1.284 8.242 25.783 7.626 1.382 7.551
P11A–28 290 58000 406.9 263.5 54.999 7.121 3.893 7.176 119.150 10.061 2.328 10.098
P11A–29 290 58000 406.9 266.1 47.780 7.616 2.915 7.694 85.846 10.007 1.875 10.023
P11A–10 320 30000 437.5 279.1 21.692 5.411 3.020 5.462 37.846 7.781 1.801 7.808
P11T–06 320 30000 437.5 279.1 10.098 6.872 0.742 6.902 18.305 8.368 0.712 8.281
P14T–08 320 30000 437.5 279.1 28.733 6.122 2.922 6.167 30.281 6.185 3.048 6.133
P11A–13 320 55000 480.4 299.0 52.974 9.220 1.075 9.220 33.964 7.887 1.297 7.887
P12A–25 320 55000 480.4 287.6 35.501 7.301 1.233 7.301 26.832 6.632 1.366 6.632
P12T–05 350 10000 449.0 276.8 21.132 5.215 2.776 5.269 31.762 5.947 2.949 5.930
P12T–06 350 10000 449.0 263.4 – – – – – – – –
P12A–08 350 10000 449.0 290.5 16.002 6.087 1.767 6.131 18.882 6.406 1.817 6.387
P12A–09 350 10000 449.0 271.2 23.598 5.539 2.416 5.571 31.778 6.061 2.504 6.049
P12T–11 350 30000 450.7 266.6 – – – – – – – –
P12A–13 350 30000 450.7 285.0 – – – – – – – –
P12A–14 350 30000 450.7 263.5 18.527 4.510 2.843 4.531 27.212 5.877 1.984 5.914
P13T–07 400 10000 477.3 285.0 16.824 5.017 2.132 5.108 23.356 5.687 2.064 5.733
P13A–07 400 10000 477.3 286.3 – – – – – – – –
683–40 – Unaged 400.2 274.1 18.111 6.157 2.626 6.256 35.382 7.344 3.307 7.302
683–41 – Unaged 400.2 279.4 207.510 14.167 1.829 14.167 46.484 8.900 2.720 8.900
683–33 290 30000 401.8 263.1 42.422 5.875 5.444 5.922 97.246 9.132 3.121 9.194
684–31 290 30000 411.3 269.2 44.741 7.984 2.317 7.984 29.922 6.728 2.640 6.728
68–145 290 30000 411.3 278.0 36.767 8.380 2.042 8.380 23.922 6.864 2.406 6.864
684–21 320 10000 442.7 304.5 26.407 6.045 4.024 6.147 33.866 6.667 4.124 6.635
684–22 320 10000 442.7 281.0 29.172 6.156 2.817 6.253 45.705 7.056 2.951 7.053
682–41 320 30000 461.3 305.7 24.772 7.692 1.614 7.707 21.104 7.180 1.713 7.149
684–39 320 30000 461.3 358.2 11.773 7.925 2.091 7.942 13.833 8.705 2.041 8.664
68–264 320 30000 461.3 296.2 64.084 8.442 2.416 8.497 57.662 8.112 2.533 8.105
681–28 320 50000 458.8 326.9 21.643 8.739 1.571 8.739 18.528 8.083 1.680 8.083
681–29 320 50000 458.8 303.7 37.068 9.573 1.047 9.575 24.331 8.088 1.213 8.211
68–230 320 50000 458.8 294.3 51.050 8.868 1.534 8.905 39.151 8.325 1.438 8.395
682–25 350 5780 444.3 281.5 17.455 5.151 2.659 5.216 34.164 6.178 3.259 6.169
682–26 350 5780 444.3 294.8 19.928 6.556 2.062 6.604 25.623 6.943 2.279 6.939
684–06 350 10000 445.5 264.5 28.948 5.701 2.521 5.718 30.160 5.763 2.562 5.732
684–07 350 10000 445.5 299.7 20.265 5.926 2.907 5.940 22.413 6.206 2.912 6.158
684–08 350 10000 445.5 296.8 31.405 7.795 1.992 7.822 22.691 6.769 2.120 6.826
68–129 350 10000 445.5 287.6 28.106 6.786 2.255 6.817 30.560 6.971 2.313 6.911
684–10 350 30000 464.6 299.0 17.031 5.158 2.753 5.164 19.141 5.366 2.890 5.314
684–11 350 30000 464.6 281.1 28.202 6.988 1.392 6.988 27.810 6.920 1.420 6.920
68–139 350 30000 464.6 287.4 17.838 4.824 2.867 4.829 20.368 5.068 2.966 5.025
682–16 400 2570 467.8 294.1 12.724 4.995 2.019 5.046 23.999 5.842 2.612 5.821
682–17 400 2570 467.8 289.8 58.392 8.607 1.551 8.742 40.401 7.823 1.602 7.762
682–15 400 10000 474.8 313.4 13.800 3.938 4.105 3.938 20.428 4.786 4.345 4.743
682–22 400 10000 474.8 299.3 19.582 5.423 2.559 5.443 24.375 5.914 2.576 5.872

44
Table 4. (Contd.)

Stress–Strain Data <5% Strain Stress–Strain Data <15% Strain

Aging Aging Flow Yield Flow Stress Yield Stress Flow Stress Yield Stress
Specimen Temp. Time Stress Stress Reference Reference Reference Reference
Id (°C) (h) (MPa) (MPa) α1 n1 α2 n2 α1 n1 α2 n2
682–23 400 10000 474.8 306.0 22.124 8.130 0.980 8.155 15.832 7.263 1.077 7.150
68–119 400 10000 474.8 306.0 11.958 6.646 1.041 6.640 18.501 7.864 0.982 7.718
681–04 450 2570 471.7 291.3 12.073 4.417 2.340 4.437 19.187 5.741 1.990 5.705
681–05 450 2570 471.7 309.4 23.584 8.151 1.151 8.147 15.286 6.787 1.285 6.855
733–40 – Unaged 397.9 254.3 43.198 5.265 6.497 5.358 65.118 5.911 7.280 5.950
733–41 – Unaged 397.9 249.5 42.120 4.949 6.744 5.031 66.565 5.680 7.556 5.687
734–23 320 10000 361.7 221.9 82.088 5.642 8.583 5.740 136.890 7.082 7.003 7.213
734–24 320 10000 361.7 228.2 78.605 6.508 6.307 6.600 235.190 10.357 3.163 10.418
732–25 350 2570 385.8 244.0 31.340 4.668 5.909 4.741 53.655 5.476 6.962 5.489
732–26 350 2570 385.8 244.4 39.039 5.082 6.108 5.162 51.467 5.553 6.481 5.556
734–06 350 10000 369.0 228.0 37.056 4.636 6.482 4.662 50.353 5.766 5.093 5.805
734–07 350 10000 369.0 219.1 92.682 7.376 3.370 7.431 161.510 9.453 1.954 9.440
73–119 350 10000 369.0 212.8 77.572 5.914 5.223 5.979 160.750 8.181 3.088 8.212
732–16 400 2570 397.7 240.8 45.420 4.952 6.315 5.012 58.294 5.303 6.786 5.313
732–17 400 2570 397.7 252.6 30.895 4.551 6.243 4.650 53.262 5.458 7.143 5.445
732–15 400 10000 383.5 235.3 79.137 7.745 2.961 7.812 138.690 9.914 1.775 9.899
732–22 400 10000 383.5 215.8 59.208 5.429 4.664 5.478 108.370 7.384 2.776 7.397
73–109 400 10000 383.5 222.2 141.470 7.653 3.769 7.714 231.090 9.089 2.801 9.124
731–04 450 2570 388.5 256.5 26.147 2.851 12.319 2.896 51.846 3.799 16.259 3.812
731–05 450 2570 388.5 234.0 39.084 4.884 5.495 4.965 54.330 5.445 5.781 5.447
205–26 4 0 0 18000 451.7 248.5 16.608 5.582 1.083 5.572 15.368 5.245 1.187 5.277
205–27 4 0 0 18000 451.7 254.0 26.983 6.041 1.482 6.041 21.881 5.480 1.660 5.480
205–30 4 0 0 18000 451.7 248.7 18.630 5.929 1.038 5.826 17.727 5.702 1.106 5.655
743–40 – Unaged 405.1 273.5 28.508 7.143 2.567 7.242 28.508 7.143 2.567 7.242
743–41 – Unaged 405.1 273.0 32.577 7.243 2.790 7.338 41.016 7.732 2.907 7.733
743–36 290 30000 426.9 282.2 19.449 4.611 4.389 4.633 26.229 6.060 3.252 6.083
744–34 290 30000 426.9 292.9 17.663 4.946 4.026 4.980 24.788 6.879 2.729 6.912
74–135 290 30000 426.9 259.0 39.152 6.521 2.484 6.543 49.329 7.376 2.042 7.397
744–21 320 10000 415.0 273.1 22.149 4.989 4.217 4.983 29.442 6.601 2.857 6.585
744–25 320 10000 415.0 270.5 22.929 6.195 2.513 6.233 36.461 8.431 1.518 8.437
742–42 320 30000 464.7 312.7 27.934 7.079 2.521 7.092 26.811 6.934 2.588 6.908
744–39 320 30000 464.7 326.4 13.424 6.229 2.126 6.223 13.100 6.043 2.217 6.033
74–245 320 30000 464.7 278.8 28.997 6.733 1.558 6.727 26.061 6.360 1.715 6.329
741–28 320 50000 475.1 309.1 29.442 8.931 0.964 8.869 29.442 8.931 0.964 8.869
741–29 320 50000 475.1 304.5 32.513 8.929 0.953 8.917 32.513 8.929 0.953 8.917
74–230 320 50000 475.1 299.4 24.334 7.678 1.113 7.643 24.334 7.678 1.113 7.643
742–25 350 2570 410.5 269.0 16.928 6.393 1.742 6.435 19.907 6.785 1.753 6.755
742–26 350 2570 410.5 261.0 16.973 5.303 2.418 5.303 30.084 6.277 2.758 6.277
744–07 350 10000 440.1 281.7 14.788 4.524 3.085 4.549 21.009 6.194 2.070 6.226
744–08 350 10000 440.1 278.2 18.690 6.054 1.840 6.054 19.480 6.119 1.860 6.119
74–119 350 10000 440.1 267.5 15.903 4.226 3.211 4.245 21.691 5.414 2.418 5.439
743–13 350 30000 447.3 265.8 0.107 7.431 0.004 7.431 0.150 6.635 0.008 6.635
743–14 350 30000 447.3 260.3 0.133 7.107 0.005 7.106 0.172 6.494 0.009 6.494
74–130 350 30000 447.3 272.3 13.905 4.037 3.101 4.053 17.690 4.985 2.460 5.014
742–16 400 2570 429.6 268.6 15.782 5.485 1.932 5.490 18.142 5.828 1.918 5.786
742–17 400 2570 429.6 267.7 22.234 5.711 2.414 5.732 25.045 5.974 2.425 5.943
742–22 400 10000 442.5 269.8 24.153 5.520 2.613 5.526 26.238 6.263 1.961 6.248
742–23 400 10000 442.5 267.7 11.307 3.804 2.768 3.828 15.704 4.972 2.134 5.005
74–110 400 10000 442.5 259.2 17.082 4.036 3.367 4.065 24.402 5.308 2.440 5.349
741–04 450 2570 438.5 257.5 15.295 4.821 2.000 4.821 17.999 5.130 1.998 5.130
741–05 450 2570 438.5 259.1 13.906 4.944 1.746 4.944 17.690 5.404 1.744 5.404
753–40 – Unaged 461.1 313.5 12.147 6.574 1.416 6.604 16.941 7.444 1.434 7.415
753–41 – Unaged 461.1 330.5 13.029 6.095 2.403 6.128 18.803 6.940 2.622 6.921
753–30 290 30000 467.8 315.6 20.617 6.962 1.974 6.962 19.834 6.823 2.005 6.823
754–28 290 30000 467.8 321.7 8.964 4.374 2.557 4.398 12.731 5.985 1.979 6.026
75–135 290 30000 467.8 310.6 9.692 3.836 3.057 3.858 12.318 4.842 2.565 4.877
754–21 320 10000 540.5 355.9 16.380 4.536 3.772 4.544 21.684 5.353 3.588 5.313
754–25 320 10000 540.5 406.3 10.041 4.754 3.470 4.807 16.288 6.161 3.776 6.136

45
Table 4. (Contd.)

Stress–Strain Data <5% Strain Stress–Strain Data <15% Strain

Aging Aging Flow Yield Flow Stress Yield Stress Flow Stress Yield Stress
Specimen Temp. Time Stress Stress Reference Reference Reference Reference
Id (°C) (h) ( M P a ) (MPa α1 n1 α2 n2 α1 n1 α2 n2
)

752–41 320 30000 536.1 357.9 11.926 5.252 2.149 5.248 14.048 5.626 2.201 5.595
754–39 320 30000 536.1 395.1 14.744 6.116 3.119 6.095 14.412 5.957 3.196 5.942
75–245 320 30000 536.1 323.1 17.781 5.545 1.797 5.527 19.716 5.861 1.715 5.828
751–28 320 50000 540.7 334.7 13.731 6.386 1.026 6.403 14.226 6.494 1.007 6.515
751–29 320 50000 540.7 352.0 11.023 7.021 0.822 7.049 10.240 6.687 0.888 6.695
75–230 320 50000 540.7 378.4 7.784 6.904 0.977 6.834 7.787 6.874 0.990 6.811
752–25 350 2570 512.4 346.5 13.535 6.380 1.650 6.380 14.776 6.639 1.627 6.639
752–26 350 2570 512.4 346.5 9.653 5.484 1.680 5.494 12.560 6.161 1.694 6.130
754–06 350 10000 534.9 332.7 10.717 4.126 2.404 4.116 14.558 4.927 2.244 4.893
754–07 350 10000 534.9 352.5 11.133 4.345 2.713 4.349 14.696 5.132 2.615 5.088
754–08 350 10000 534.9 308.6 15.351 5.636 1.157 5.640 16.361 5.792 1.156 5.761
75–119 350 10000 534.9 354.0 10.874 2.987 4.750 2.983 16.013 3.991 4.666 3.953
753–10 350 30000 531.1 316.1 8.290 4.609 1.275 4.609 9.648 5.005 1.208 5.005
753–11 350 30000 531.1 344.3 7.949 4.105 2.147 4.102 10.552 4.779 2.188 4.737
75–130 350 30000 531.1 300.8 29.721 6.819 1.200 6.840 19.201 5.492 1.541 5.581
752–16 400 2570 528.7 326.7 12.535 5.422 1.501 5.428 14.879 5.862 1.461 5.823
752–17 400 2570 528.7 353.1 9.051 5.123 1.723 5.125 10.847 5.620 1.707 5.587
752–15 400 10000 557.6 405.3 7.764 3.164 3.893 3.164 11.286 3.990 4.348 3.990
752–22 400 10000 557.6 367.7 3.568 3.125 1.473 3.125 7.472 5.128 1.340 5.128
752–23 400 10000 557.6 338.9 11.999 5.662 1.178 5.662 12.404 5.745 1.168 5.745
75–109 400 10000 557.6 359.0 16.151 3.879 4.547 3.879 19.749 4.616 4.018 4.616
751–04 450 2570 523.5 311.7 8.651 4.794 1.233 4.763 10.631 5.384 1.134 5.331
751–05 450 2570 523.5 314.7 7.661 4.949 1.027 4.949 8.863 5.447 0.922 5.447

46
Table 5. Best–fit values of the Ramberg–Osgood constants for unaged and aged cast stainless
steels at 290°C

Stress–Strain Data <5% Strain Stress–Strain Data <15% Strain

Aging Aging Flow Yield Flow Stress Yield Stress Flow Stress Yield Stress
Specimen Temp. Time Stress Stress Reference Reference Reference Reference
Id (°C) (h) (MPa) (MPa) α1 n1 α2 n2 α1 n1 α2 n2
I2V–03 – Unaged – – – – – – – – – –
I2V–06 – Unaged – – – – – – – – – –
I3C–02 – Unaged – – – – – – – – – –
I2V–24 320 30000 – – – – – – – – – –
I3C–15 320 30000 – – – – – – – – – –
I3V–40 320 30000 – – – – – – – – – –
I1V–28 350 10000 – – – – – – – – – –
I1V–29 350 10000 – – – – – – – – – –
I2V–20 350 10000 – – – – – – – – – –
P21T–02 – Unaged 273.3 161.3 30.130 3.599 7.750 3.602 40.384 4.108 8.083 4.076
P23T–02 – Unaged 273.3 154.2 9.867 2.779 3.629 2.833 9.867 2.779 3.629 2.833
P22A–02 – Unaged 273.3 137.9 28.481 2.892 7.894 2.928 28.481 2.892 7.894 2.928
P23A–02 – Unaged 273.3 144.0 – – – – – – – –
P21A–32 290 30000 280.3 162.3 133.790 8.911 1.745 8.902 62.867 6.959 2.255 7.108
P21A–33 290 30000 280.3 155.2 40.329 6.136 1.901 6.160 27.515 4.876 2.619 4.966
P24T–16 290 30000 280.3 148.2 593.540 9.612 2.439 9.593 119.110 6.359 3.760 6.417
P21A–37 290 58000 293.8 164.2 114.150 8.300 1.630 8.300 35.770 5.800 2.202 5.800
P22T–17 290 58000 293.8 177.5 14.069 3.600 3.860 3.600 25.090 4.000 5.470 4.000
P21A–14 320 30000 288.2 153.2 25.048 6.266 0.867 6.336 19.474 5.115 1.290 5.262
P21A–15 320 30000 288.2 163.9 62.046 7.180 1.864 7.194 40.888 6.076 2.211 6.174
P21A–16 320 30000 288.2 152.6 32.615 5.864 1.451 5.895 23.481 4.847 1.871 4.956
P25T–12 320 55000 293.7 171.4 100.920 9.045 1.283 9.057 55.847 7.457 1.572 7.652
P21A–18 320 55000 293.7 168.6 62.313 7.568 1.589 7.590 44.166 6.695 1.782 6.786
P21T–08 350 10000 285.2 155.6 74.163 6.743 2.271 6.737 32.202 4.799 3.100 4.860
P22T–05 350 10000 285.2 153.8 45.695 4.933 4.095 4.955 35.083 4.366 4.567 4.311
P23A–15 350 10000 285.2 161.0 30.569 2.874 10.639 2.927 30.569 2.874 10.639 2.927
P23A–27 350 10000 285.2 154.1 37.588 4.893 3.464 4.905 29.679 4.349 3.930 4.290
P22T–12 350 30000 292.1 167.0 21.989 6.231 1.165 6.258 17.282 5.227 1.529 5.313
P24A–30 350 30000 292.1 142.4 42.270 6.000 1.160 6.000 28.880 5.100 1.550 5.100
P24A–33 350 30000 292.1 149.1 129.200 7.900 1.210 7.900 33.430 5.400 1.680 5.400
P24T–06 400 10000 296.2 160.4 34.062 5.237 2.550 5.237 24.125 4.335 2.995 4.392
P24A–05 400 10000 296.2 146.6 58.077 5.333 2.742 5.335 34.889 4.173 3.602 4.228
693–42 – Unaged 301.4 190.8 64.420 8.800 1.850 8.800 26.940 6.600 2.045 6.600
694–40 – Unaged 301.4 177.0 36.631 5.468 3.337 5.588 31.210 5.066 3.738 4.998
694–32 290 30000 295.5 176.8 67.208 7.773 2.108 7.783 46.935 6.781 2.302 6.868
694–33 290 30000 295.5 173.0 57.898 7.371 1.869 7.409 41.700 6.490 2.115 6.575
69–236 290 30000 295.5 194.1 28.885 6.811 2.609 6.756 29.038 7.918 1.499 8.056
694–26 320 10000 297.4 174.4 23.782 6.627 1.177 6.631 18.479 5.606 1.464 5.722
694–27 320 10000 297.4 183.5 17.580 6.625 1.192 6.574 14.487 5.633 1.453 5.730
692–42 320 30000 295.4 178.5 22.021 6.693 1.235 6.719 15.351 5.404 1.590 5.476
694–39 320 30000 295.4 168.2 31.424 6.043 1.830 6.043 21.323 4.957 2.224 5.004
69–246 320 30000 295.4 165.5 31.758 6.747 1.121 6.774 21.168 5.392 1.580 5.467
692–28 320 55000 336.8 209.1 39.539 8.602 1.019 8.653 19.246 5.899 1.681 6.069
692–29 320 55000 336.8 212.3 28.152 7.328 1.495 7.350 18.314 5.679 1.975 5.795
69–130 320 55000 336.8 204.7 26.381 6.390 1.998 6.414 19.024 5.279 2.354 5.359
692–27 350 2570 312.2 173.1 28.175 5.109 2.513 5.115 22.891 4.661 2.716 4.622
694–09 350 10000 294.8 156.4 27.831 6.155 1.047 6.175 23.302 5.524 1.237 5.618
69–120 350 10000 294.8 179.8 16.671 5.960 1.444 5.954 14.764 5.268 1.697 5.343
693–14 350 30000 323.3 186.4 – – – – – – – –
693–15 350 30000 323.3 195.8 87.807 9.618 1.147 9.608 27.180 5.664 2.344 5.856
69–270 350 30000 323.3 193.6 18.280 4.700 2.720 4.700 19.780 4.800 2.830 4.800
692–18 400 2570 304.4 163.9 20.517 5.282 1.433 5.301 17.262 4.704 1.667 4.759
692–24 400 10000 336.6 173.3 15.209 5.798 0.644 5.764 13.451 5.224 0.772 5.289
69–110 400 10000 336.6 196.9 16.846 5.161 1.828 5.144 15.834 4.894 2.008 4.865
691–06 450 2570 326.4 177.7 – – – – – – – –
692–09 450 2570 326.4 175.7 16.753 3.488 3.552 3.498 20.567 3.857 3.580 3.821
16–21 Reannealed 2 9 4 . 2 1 8 4 . 0 23.371 6.542 1.730 6.606 22.522 6.420 1.791 6.398
17–21 Reannealed 2 9 4 . 2 1 7 1 . 5 43.387 7.274 1.472 7.304 35.599 6.830 1.515 6.841

47
Table 5. (Contd.)

Stress–Strain Data <5% Strain Stress–Strain Data <15% Strain

Aging Aging Flow Yield Flow Stress Yield Stress Flow Stress Yield Stress
Specimen Temp. Time Stress Stress Reference Reference Reference Reference
Id (°C) (h) ( M P a ) (MPa α1 n1 α2 n2 α1 n1 α2 n2
)

15–11 280 68000 329.0 214.0 29.798 7.548 1.787 7.613 21.419 6.753 1.817 6.742
15–12 280 68000 329.0 208.4 21.457 6.952 1.421 7.022 21.433 6.907 1.469 6.878
15–21 280 68000 329.0 199.6 22.500 6.800 1.220 6.800 21.210 6.700 1.240 6.700
15–22 280 68000 329.0 180.2 50.791 6.420 1.946 6.442 41.359 6.012 2.015 6.012

P13T–02 – Unaged 291.7 148.5 – – – – – – – –

P14T–01 – Unaged 291.7 157.0 20.036 2.770 6.687 2.816 20.036 2.770 6.687 2.816
P11A–02 – Unaged 291.7 159.9 130.600 7.798 2.178 7.765 64.764 6.068 2.963 6.126
P13A–02 – Unaged 291.7 155.0 24.299 2.653 8.647 2.690 24.299 2.643 8.647 2.690
P14T–10 290 30000 287.6 166.1 83.677 7.080 3.004 7.117 75.153 7.366 2.160 7.467
P11A–26 290 30000 287.6 160.3 742.000 11.368 1.730 11.288 207.350 8.505 2.528 8.505
P14A–27 290 30000 287.6 167.8 39.270 6.400 2.180 6.400 26.540 5.200 2.770 5.200
P11A–27 290 58000 295.1 167.1 753.280 12.183 1.280 12.164 68.354 6.036 3.321 6.330
P11A–30 290 58000 295.1 179.3 232.720 11.102 1.511 11.031 118.910 9.452 1.697 9.523
P11A–09 320 30000 306.1 175.5 – – – – – – – –
P12A–19 320 30000 306.1 174.8 53.610 9.400 0.476 9.400 20.100 6.700 0.824 6.700
P12A–22 320 30000 306.1 175.4 31.422 6.518 1.466 6.506 23.289 5.486 1.788 5.591
P11A–12 320 55000 321.4 188.2 377.120 11.330 1.490 11.275 242.300 10.361 1.620 10.280
P12A–26 320 55000 321.4 200.4 0.054 9.398 0.001 9.404 42.068 7.541 1.910 7.540
P12T–08 350 10000 316.3 180.2 21.398 1.649 15.041 1.649 37.036 2.324 18.183 2.280
P12A–10 350 10000 316.3 173.7 – – – – – – – –
P12A–11 350 10000 316.3 180.7 39.146 5.859 2.591 5.949 27.387 5.042 2.955 4.988
P12T–12 350 30000 331.6 194.9 30.730 8.900 0.451 8.900 15.200 6.600 0.757 6.600
P14A–22 350 30000 331.6 185.3 22.602 5.908 1.334 5.861 19.391 5.348 1.499 5.390
P14A–23 350 30000 331.6 198.6 21.591 5.568 2.096 5.549 18.855 4.988 2.432 4.994
P13T–08 400 10000 329.5 167.3 22.393 4.175 2.616 4.173 21.854 4.106 2.719 4.084
P13A–08 400 10000 329.5 162.9 – – – – – – – –

683–42 – Unaged 282.2 162.7 57.263 5.759 4.194 5.807 40.128 5.162 3.907 5.220
684–40 – Unaged 282.2 156.4 62.480 5.337 4.858 5.403 53.141 5.302 4.082 5.341
684–32 290 30000 266.4 149.5 491.100 9.472 3.677 9.472 236.650 7.794 4.673 7.794
684–33 290 30000 266.4 155.0 217.630 8.564 3.619 8.564 58.224 4.643 8.098 4.643
68–246 290 30000 266.4 170.6 56.87 7.726 2.838 7.726 28.580 4.748 5.379 4.748
684–23 320 10000 299.3 173.4 46.251 7.541 1.282 7.560 27.077 5.768 1.881 5.875
684–24 320 10000 299.3 164.4 59.073 7.845 0.966 7.847 28.686 5.800 1.492 5.922
682–40 320 30000 309.9 174.3 60.509 6.851 2.081 6.897 38.295 5.861 2.297 5.889
682–42 320 30000 309.9 176.9 69.293 7.621 1.698 7.628 38.098 6.263 1.945 6.298
68–263 320 30000 309.9 165.6 82.173 7.451 1.442 7.471 39.230 5.869 1.791 5.916
682–28 320 50000 341.6 203.3 137.850 10.900 0.830 10.900 29.530 6.600 1.590 6.600
682–29 320 50000 341.6 205.3 17.860 3.600 4.790 3.600 31.420 4.100 6.510 4.100
68–130 320 50000 341.6 201.3 125.980 9.000 1.840 9.000 45.340 6.600 2.330 6.600
682–27 350 5780 318.8 185.1 51.555 6.211 3.053 6.289 40.384 5.749 3.106 5.725
684–09 350 10000 320.2 164.3 33.154 7.169 0.592 7.030 19.014 5.249 1.101 5.269
68–130 350 10000 320.2 168.9 38.779 6.331 1.326 6.269 29.055 5.464 1.581 5.546
684–12 350 30000 328.1 216.0 114.470 12.559 0.931 12.610 18.874 7.681 0.960 8.042
684–15 350 30000 328.1 190.4 97.984 7.516 2.854 7.586 141.680 9.247 1.569 9.249
68–140 350 30000 328.1 170.2 65.242 6.344 1.935 6.337 32.437 4.625 2.714 4.765
682–18 400 2570 312.2 161.3 59.088 5.578 2.872 5.608 37.567 4.714 3.224 4.718
682–24 400 10000 332.7 176.7 31.480 6.300 1.075 6.300 27.610 6.000 1.180 6.000
68–120 400 10000 332.7 193.9 29.554 6.209 1.796 6.187 23.117 5.235 2.254 5.302
681–06 450 2570 338.0 169.7 34.810 5.400 1.700 5.400 27.530 4.900 1.870 4.900
682–09 450 2570 338.0 191.6 8.430 2.600 3.460 2.600 15.580 3.100 4.840 3.100

733–42 – Unaged 251.1 138.9 124.230 7.000 3.530 7.000 110.930 6.800 3.500 6.800
734–40 – Unaged 251.1 133.9 51.330 4.600 5.210 4.600 70.480 5.000 5.790 5.000
734–19 320 10000 245.2 130.4 – – – – – – – –
734–22 320 10000 245.2 131.3 – – – – – – – –
732–27 350 2570 419.8 139.6 – – – – – – – –
734–08 350 10000 268.5 127.7 – – – – – – – –
734–09 350 10000 268.5 165.0 – – – – – – – –
73–120 350 10000 268.5 136.7 – – – – – – – –
732–18 400 2570 – – – – – – – – – –

48
Table 5. (Contd.)

Stress–Strain Data <5% Strain Stress–Strain Data <15% Strain

Aging Aging Flow Yield Flow Stress Yield Stress Flow Stress Yield Stress
Specimen Temp. Time Stress Stress Reference Reference Reference Reference
Id (°C) (h) (MPa) (MPa) α1 n1 α2 n2 α1 n1 α2 n2

732–23 400 10000 274.9 138.5 534.550 9.356 1.740 9.282 188.970 7.213 2.626 7.225
732–24 400 10000 274.9 143.0 231.760 8.357 1.888 8.318 126.800 7.114 2.282 7.136
73–110 400 10000 274.9 139.4 116.310 7.000 2.044 7.000 87.390 6.300 2.440 6.300
731–06 450 2570 281.9 144.1 104.410 6.497 2.607 6.549 52.000 5.311 2.829 5.327
732–09 450 2570 281.9 136.2 232.370 7.535 2.001 7.566 80.969 5.958 2.157 5.965

205–25 4 0 0 18000 339.0 179.4 18.003 5.151 1.286 5.155 15.687 4.713 1.419 4.763
205–28 4 0 0 18000 339.0 177.3 21.084 5.212 1.381 5.212 17.382 4.646 1.555 4.712
205–29 4 0 0 18000 339.0 168.2 – – – – – – – –

744–40 Unaged 297.9 171.8 86.188 9.360 0.861 9.291 30.450 7.111 1.023 7.154
743–42 Unaged 297.9 164.6 60.021 7.722 1.113 7.722 30.750 6.220 1.390 6.220
744–35 290 30000 304.0 193.8 190.681 8.199 7.462 8.199 60.370 4.883 10.511 4.883
744–36 290 30000 304.0 165.2 230.811 8.266 2.746 8.266 62.633 4.985 5.511 4.985
74–236 290 30000 304.0 179.9 75.777 7.258 2.842 7.258 32.967 5.001 4.041 5.001
744–26 320 10000 308.6 192.7 88.686 8.381 2.744 8.381 36.606 5.100 5.311 5.100
744–27 320 10000 308.6 181.0 228.170 9.397 2.586 9.397 59.216 5.424 5.588 5.424
742–40 320 30000 324.4 153.7 75.219 7.633 0.530 7.633 37.604 5.823 1.025 5.823
742–41 320 30000 324.4 190.3 26.614 5.765 2.110 5.765 21.063 5.072 2.343 5.115
74–246 320 30000 324.4 184.4 34.808 5.726 2.431 5.721 26.416 4.989 2.715 5.025
742–28 320 50000 353.3 203.5 37.451 5.691 2.850 5.700 32.175 5.317 3.085 5.258
742–29 320 50000 353.3 215.2 40.274 7.600 1.547 7.594 23.492 5.886 2.265 5.744
74–130 320 50000 353.3 235.4 36.297 8.371 1.876 8.349 23.087 6.896 2.267 6.755
742–27 350 2570 314.6 174.9 42.692 7.360 1.020 7.321 23.367 6.086 1.159 6.109
744–06 350 10000 328.1 185.4 85.841 7.577 2.010 7.577 40.650 5.450 3.206 5.450
744–09 350 10000 328.1 197.8 42.453 7.166 1.873 7.166 23.848 4.967 3.204 4.967
74–120 350 10000 328.1 176.6 – – – – – – – –
744–18 350 30000 350.0 228.5 40.940 5.910 5.046 5.910 26.472 4.790 5.259 4.790
743–15 350 30000 350.0 180.0 58.921 6.192 1.866 6.192 32.411 4.759 2.662 4.759
74–270 350 30000 350.0 182.2 65.448 6.614 1.677 6.600 32.197 4.747 2.580 4.856
742–18 400 2570 325.7 166.2 16.677 5.443 0.827 5.459 20.211 5.959 0.711 5.977
742–15 400 10000 339.5 178.9 46.860 6.366 1.487 6.377 27.495 4.658 2.422 4.777
742–24 400 10000 339.5 184.2 52.170 6.733 1.544 6.746 42.964 6.243 1.677 6.311
74–109 400 10000 339.5 172.0 67.830 6.166 2.023 6.166 41.190 5.005 2.705 5.005
741–06 450 2570 332.1 172.0 18.336 6.049 0.638 6.089 12.885 5.196 0.760 5.279
742–09 450 2570 332.1 170.3 19.035 5.811 0.767 5.795 15.463 5.218 0.899 5.252

754–40 – Unaged 333.5 196.8 25.078 7.034 1.040 7.034 19.523 6.425 1.116 6.425
753–42 – Unaged 333.5 191.5 44.831 8.314 0.773 8.288 20.357 6.686 0.825 6.756
754–29 290 30000 352.9 193.3 115.040 7.768 1.964 7.814 62.860 6.575 2.218 6.567
754–30 290 30000 352.9 202.6 75.568 7.828 1.724 7.844 29.391 5.103 2.723 5.265
75–236 290 30000 352.9 211.8 43.168 6.026 3.321 6.052 41.021 6.001 3.206 6.003
754–26 320 10000 372.5 205.6 22.520 6.684 0.773 6.674 16.004 5.552 0.997 5.652
754–27 320 10000 372.5 212.2 21.898 6.555 0.995 6.486 16.625 5.537 1.208 5.639
752–40 320 30000 400.0 231.7 16.985 6.141 1.019 6.151 13.869 5.279 1.276 5.356
752–42 320 30000 400.0 268.5 16.575 5.834 2.432 5.819 13.848 4.971 2.762 5.024
75–246 320 30000 400.0 213.0 29.906 5.645 1.617 5.636 23.927 5.066 1.807 5.097
752–28 320 50000 415.0 258.9 19.436 7.167 1.033 7.214 13.178 5.627 1.404 5.716
752–29 320 50000 415.0 264.1 16.035 6.185 1.559 6.171 12.815 5.647 1.482 5.744
75–130 320 50000 415.0 239.6 27.785 6.506 1.350 6.506 19.445 5.525 1.619 5.525
752–27 350 2570 366.8 204.7 16.335 6.493 0.673 6.481 13.486 6.028 0.722 6.021
754–09 350 10000 409.9 219.8 14.071 5.518 0.856 5.493 12.665 5.075 0.982 5.098
75–120 350 10000 409.9 209.9 – – – – – – – –
753–12 350 30000 419.1 264.4 15.076 6.979 0.960 6.979 10.962 5.711 1.251 5.711
754–12 350 30000 419.1 227.2 17.526 5.072 1.449 5.072 14.936 4.645 1.604 4.645
75–270 350 30000 419.1 209.0 24.102 4.891 1.608 4.891 20.895 4.573 1.739 4.573
752–18 400 2570 397.2 203.2 17.324 6.207 0.525 6.207 13.672 5.555 0.624 5.601
752–24 400 10000 409.6 208.2 10.689 5.217 0.629 5.189 10.518 5.073 0.694 5.033
75–110 400 10000 409.6 206.7 15.317 5.431 0.750 5.415 14.238 5.113 0.841 5.130
751–06 450 2570 405.2 218.7 10.515 5.089 0.840 5.045 11.424 5.293 0.798 5.268
752–09 450 2570 405.2 197.7 13.264 4.882 0.783 4.891 12.952 4.829 0.789 4.850

49
Flow Stress Ratio (aged/unaged)
1.4
CF–3 Steel CF–3 Steel
1.3 Room Temp. 290°C
ANL ANL
1.2 FRA

1.1

1.0

Ratio = 0.90 + 0.05(P– Θ +2.9)

0.9 Ratio = 0.87 + 0.06(P– θ +2.9)
1.00 ≤ Ratio ≤ 1.10
1.00 ≤ Ratio ≤ 1.08
0.8
0 1 2 3 4 5 0 1 2 3 4 5
Normalized Aging Parameter (P – Θ + 2.9) Normalized Aging Parameter (P – θ + 2.9)
Flow Stress Ratio (aged/unaged)

1.4
CF–8 Steel CF–8 Steel
1.3 Room Temp. 290°C
ANL ANL
1.2 FRA

1.1

1.0

Ratio = 0.83 + 0.09(P– θ +2.9)

0.9 Ratio = 0.84 + 0.08(P– θ +2.9)
1.00 ≤ Ratio ≤ 1.14
1.00 ≤ Ratio ≤ 1.16
0.8
0 1 2 3 4 5 0 1 2 3 4 5
Normalized Aging Parameter (P – θ + 2.9) Normalized Aging Parameter (P – θ + 2.9)
Flow Stress Ratio (aged/unaged)

1.4
CF–8M Steel CF–8M Steel
1.3 Room Temp. 290°C
ANL ANL
1.2 FRA

1.1

1.0

Ratio = 0.69 + 0.14(P– θ +2.9)

Ratio = 0.77 + 0.10(P– θ +2.9)
0.9
1.0 ≤ Ratio ≤ 1.19 1.00 ≤ Ratio ≤ 1.24

0.8
0 1 2 3 4 5 0 1 2 3 4 5
Normalized Aging Parameter (P – θ + 2.9) Normalized Aging Parameter (P – θ + 2.9)

Figure 21. Flow stress ratio of aged cast stainless steels at RT and 290°C as a function of the
normalized aging parameter. The solid lines represent correlations obtained by
subtracting σ from the best fit curve.

50
 Table 6. Values of constants in Eq. 8 for estimating tensile flow
stress of aged cast stainless steels

Room Temp. 290°C

Grade a1 b1 c1 a1 b1 c1

CF–3 0.90 0.05 1.10 0.87 0.06 1.08

CF–8 0.84 0.08 1.16 0.83 0.09 1.14
CF–8M 0.77 0.10 1.19 0.69 0.14 1.24

between 280 and 330°C (536 and 626°F), and ferrite content >7% for CF–8M steel and >10%
for CF–3 and CF–8 steels. Thermal aging has little or no effect on the tensile strength of cast
stainless steels with low ferrite content. The available data base is inadequate for estimating
the tensile properties at service temperatures <280°C (<536°F).

The flow stress for a specific composition of cast stainless steel, as a function of time and
temperature of aging, is estimated from Eqs. 8 and 1. The activation energy Q in Eq. 1 is de-
termined from the composition of the steel6,7 expressed as

[ ( ) ]
Q = 10 74.52 – 7.20θ – 3.46Si – 1.78Cr – 4.35I1Mn + 148 – 125I1 N – 61I2 C , (9)

where the indicators I1 I2 are o and 1, respectively, for CF–3 or CF–8 steels and assume the
values of 1 and 0, respectively, for CF–8M steels, and θ is a constant. Parametric studies show
that the aging response at reactor temperatures is relatively insensitive to the values of θ . 5 , 6
A θ value of 2.9 (i.e., mean value of the experimental data) is used to estimate thermal aging
effects at 280–330°C (536–626°F), a value of 3.3 is used at temperatures <280°C (<536°F),
and 2.5 at 330–360°C (626–680°F). Tensile flow stress of aged material can be determined
from R f and the initial tensile flow stress. The minimum value of 1 and maximum value of c1 for
the tensile–flow–stress ratio Rf is assumed, respectively, when the ratio calculated from Eq. 8 is
<1 or >c1 .

Experimental and estimated tensile flow stress at 290°C (554°F) and at RT for various
heats of aged cast stainless steel are shown in Fig. 22. For each heat, the aging parameter and
activation energy were obtained from Eqs. 1 and 9 and a θ value of 2.9. Tensile flow stress was
then estimated from Eq. 8 and the initial flow stress of the materials. The estimated values are
either accurate or conservative for all materials and aging conditions.

The data on tensile properties of cast stainless steels indicate that the increase in yield
stress due to thermal aging is much lower than the increase in ultimate stress. The
tensile–yield–stress ratio Ry = (σyaged/σyunaged), is given by

Ry = a2 + b2 P (1.00 ≤ Ry ≤ c2 ). (10)

Values of the constants a2 , b2 , and c2 for different grades of steel and test temperatures are
given in Table 7. Equation 10 is valid for R y values between 1 and c2 , service temperatures
between 280 and 330°C (536 and 626°F), and ferrite content >7% for CF–8M steel and >10%
for CF–3 and CF–8 steels.

51
 500 600
290°C Room Temp.
Estimated Flow Stress (MPa)

CF–3 CF–3
CF–8 CF–8
CF–8M CF–8M
400 500

300 400

Open Symbols: ANL

Closed Symbols: FRA
200 300
200 300 400 500 300 400 500 600
Measured Flow Stress (MPa) Measured Flow Stress (MPa)

Figure 22. Experimental and estimated flow stress of aged cast stainless steel at 290°C
and RT

Table 7. Values of constants in Eq. 10 for estimating tensile yield

stress of aged cast stainless steels

Room Temp. 290°C

Grade a2 b2 c2 a2 b2 c2

CF–3 0.873 0.048 1.07 0.844 0.058 1.05

CF–8 0.798 0.076 1.10 0.788 0.086 1.09
CF–8M 0.708 0.092 1.10 0.635 0.129 1.14

Experimental and estimated tensile yield stress at 290°C (554°F) and at RT for various
heats of aged cast stainless steel are shown in Fig. 23. The aging parameter and activation en-
ergy were obtained from Eqs. 1 and 9 and a θ value of 2.9. Tensile yield stress was then esti-
mated from Eq. 10 and the initial yield stress of the materials. The estimated values are con-
servative for most materials and aging conditions.

5 . 2 Ramberg–Osgood Parameters

The engineering stress vs. strain behavior of aged cast stainless steel can also be obtained from
the estimated flow stress. For all grades of cast stainless steel, the RO parameter n1 does not
change with thermal aging. The parameter α 1 decreases with aging and shows good correlation
with the flow stress σ f of the material, Fig. 24. The RO parameter is correlated to flow stress σ f
by the expression
α1 = a3 + b3σ f . (11)

The RO parameter n1 and values of the constants a3 and b3 for different grades of steel, test
temperatures, and range of engineering strain are given in Table 8. Examples of engineering

52
 350 450
290°C Room Temp.
Estimated Yield Stress (MPa)

300 CF–3 400 CF–3

CF–8 CF–8
CF–8M CF–8M
250 350

200 300

150 250

100 200
Open Symbols: ANL
Closed Symbols: FRA
50 150
50 100 150 200 250 300 350 150 200 250 300 350 400 450
Measured Yield Stress (MPa) Measured Yield Stress (MPa)

Figure 23. Experimental and estimated yield stress of aged cast stainless steel at 290°C
and RT

Table 8. Values of Ramberg/Osgood parameter n1 and the constants in

Eq. 11 for estimating parameter α 1 for aged cast stainless steels

Strain Room Temp. 290°C

% Grade a3 b3 n1 a3 b3 n1

<5 CF–3 143.9 –0.267 6.1 102.1 –0.235 6.2

CF–8 157.9 –0.300 6.4 153.3 –0.373 7.1
CF–8M 50.9 –0.072 5.6 145.9 –0.314 6.6

<15 CF–3 104.5 –0.176 6.0 91.3 –0.221 5.3

CF–8 149.0 –0.271 6.9 137.5 –0.336 5.9
CF–8M 65.7 –0.097 6.1 103.3 –0.217 5.4

>15 CF–3 76.2 –0.116 6.0 95.5 –0.233 5.1

CF–8 122.0 –0.216 6.2 124.2 –0.303 5.5
CF–8M 44.6 –0.056 5.8 81.4 –0.162 5.4

stress–vs.–strain curves determined from estimated flow stress and Eq. 11 and those observed
experimentally for several heats of aged CF–3, CF–8, and CF–8M steels, are shown in Fig. 25.
The estimated curves are essentially conservative.

If required, the engineering stress–vs.–strain curve can also be obtained from Eq. 6, i.e.,
when yield stress is used as the reference stress. The RO parameter α 2 is determined from es-
timated values of α 1 , σ f, σ y , and Eq. 7. The parameter n2 is same as n1.

53
 100
CF–3 Steel CF–3 Steel
Room Temp. 290°C
α 1 (<5% Strain)

75

α 1 = 143.9 – 0.267σf
50 α 1 = 102.1 – 0.235σf

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

100
CF–8 Steel CF–8 Steel
Room Temp. 290°C
α 1 (<5% Strain)

75
α 1 = 157.9 – 0.300σf
α 1 = 153.3 – 0.373σf
50

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

100
CF–8M Steel CF–8M Steel
Room Temp. 290°C
α 1 (<5% Strain)

75

α 1 = 145.9 – 0.314σf

50 α 1 = 50.9 – 0.072σf

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

Figure 24. Correlation between the Ramberg/Osgood parameter α 1 and flow stress at RT and
290°C for cast stainless steels

54
 100
CF–3 Steel CF–3 Steel
Room Temp. 290°C
α 1 (<15% Strain)

75

α 1 = 104.5 – 0.176σf α 1 = 91.3 – 0.221σf

50

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

100
CF–8 Steel CF–8 Steel
Room Temp. 290°C
α 1 (<15% Strain)

75
α 1 = 137.5 – 0.336σf
α 1 = 149.0 – 0.271σf

50

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

100
CF–8M Steel CF–8M Steel
Room Temp. 290°C
α 1 (<15% Strain)

75

α 1 = 65.7 – 0.097σf α 1 = 103.3 – 0.217σf

50

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

Figure 24. (Contd.)

55
 100
CF–3 Steel CF–3 Steel
Room Temp. 290°C
α 1 (Entire Data)

75

α 1 = 76.2 – 0.116σf
50
α 1 = 95.5 – 0.233σf

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

100
CF–8 Steel CF–8 Steel
Room Temp. 290°C
α 1 (Entire Data)

75
α 1 = 122.0 – 0.216σf α 1 = 124.2 – 0.303σf

50

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

100
CF–8M Steel CF–8M Steel
Room Temp. 290°C
α 1 (Entire Data)

75

α 1 = 44.6 – 0.056σf α 1 = 81.4 – 0.162σf

50

2 5

0
350 400 450 500 550 250 300 350 400 450
Flow Stress, σ f (MPa) Flow Stress, σ f (MPa)

Figure 24. (Contd.)

56
Engineering Stress (MPa) 800
Heat 68 CF–8 Heat 68 CF–8

Engineering Stress (ksi)

100
δ = 15% δ = 15% Unaged
c c
600 Room Temp. 290°C Aged 53,000 h at 320°C
80
Predicted Unaged
Predicted Aged
400 60

40
Unaged
200 Aged 53,000 h at 320°C
Predicted Unaged
20
Predicted Aged

0 0
0 1 2 3 4 5 6 0 1 2 3 4 5 6
Engineering Strain (%) Engineering Strain (%)

800
Engineering Stress (MPa)

Heat 69 CF–3 Heat 69 CF–3

Engineering Stress (ksi)

100
δ = 21% δ = 21% Unaged
c c
600 Room Temp. 290°C Aged 53,000 h at 320°C
Predicted Unaged 80
Predicted Aged

400 60

40
Unaged
200 Aged 53,000 h at 320°C
Predicted Unaged 20
Predicted Aged

0 0
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6
Engineering Strain (%) Engineering Strain (%)

800
Engineering Stress (MPa)

Heat 75 CF–8M Heat 75 CF–8M

Engineering Stress (ksi)

100
δ = 25% δ = 25%
c c
600 Room Temp. 290°C
80

400 60

Unaged 40
Aged 53,000 h at 320°C
200 Unaged
Predicted Unaged Aged 53,000 h at 320°C
Predicted Aged Predicted Unaged 20
Predicted Aged
0 0
0 1 2 3 4 5 6 0 1 2 3 4 5 6
Engineering Strain (%) Engineering Strain (%)
Figure 25. Engineering stress–vs.–strain curve at RT and 290°C, estimated from the chemical
composition and initial tensile strength and determined experimentally for thermally
aged CF–3, CF–8, and CF–8M steels

57
 800
Engineering Stress (MPa)

Heat P2 CF–3 Heat P2 CF–3

Engineering Stress (ksi)

100
δ = 13% δ = 13%
c c
600 Room Temp. 290°C Unaged
80
Aged 55,000 h at 320°C
Predicted Unaged
Predicted Aged 60
400

40
Unaged
200 Aged 55,000 h at 320°C
Predicted Unaged 20
Predicted Aged

0 0
0 1 2 3 4 5 6 0 1 2 3 4 5 6
Engineering Strain (%) Engineering Strain (%)

800
Engineering Stress (MPa)

Heat P1 CF–8 Heat P1 CF–8

Engineering Stress (ksi)

100
δ = 18% δ = 18% Unaged
c c
600 Room Temp. 290°C Aged 55,000 h at 320°C
Predicted Unaged 80
Predicted Aged

400 60

40
Unaged
200 Aged 55,000 h at 320°C
Predicted Unaged 20
Predicted Aged

0 0
0 1 2 3 4 5 6 0 1 2 3 4 5 6
Engineering Strain (%) Engineering Strain (%)

800
Engineering Stress (MPa)

KRB Reactor Pump Cover KRB Reactor Pump Cover

Engineering Stress (ksi)

100
CF–8 CF–8
600 δ = 28% δ = 28% Annealed
c c
68,000 h service at 284°C 80
Room Temp. 290°C Predicted Unaged
Predicted Aged
400 60

40
Annealed
200 68,000 h service at 284°C
Predicted Unaged 20
Predicted Aged

0 0
0 1 2 3 4 5 6 0 1 2 3 4 5 6
Engineering Strain (%) Engineering Strain (%)
Figure 25. (Contd.)

58
6 Conclusions
The effect of thermal aging on tensile properties of cast stainless steels has been evalu-
ated. Tensile data for several experimental and commercial heats of cast stainless steels are
presented. The materials were thermally aged up to 58,000 h at temperatures between 290
and 450°C (554 and 842°F). Aging at these temperatures increases the tensile strength of
these steels. The high–C Mo–bearing CF–8M steels are the most and the low–C Mo–free CF–3
steels least susceptible to thermal aging.

A procedure and correlations are presented for predicting the change in tensile flow and
yield stress and engineering stress–vs.–strain curve (represented by the Ramberg/Osgood
equation) of cast stainless steel components that is due to thermal aging during service in
LWRs at 280–330°C (535–625°C). The tensile properties of aged cast stainless steel are esti-
mated from information that is readily available from certified material test records for the
component, i.e., chemical composition and the initial tensile strength of unaged material. The
correlations described in this report may be used to assess thermal embrittlement of cast
stainless steel components. The estimated tensile properties may be used as input to a struc-
tural analysis code, such as leak–before–break analysis of nuclear power plant piping, or for
performing fitness–for–service evaluations of safety–related components in support of plant life
extension and license renewal.

Acknowledgments
This work was supported by the Office of the Nuclear Regulatory Research in the U.S.
Nuclear Regulatory Commission. The author are grateful to T. M. Galvin, A. Sather, and W. F.
Burke for their contributions to the experimental effort. The authors also thank W. J. Shack and
T. F. Kassner for their helpful discussions. This work was sponsored by the Office of Nuclear
Regulatory Research, U.S. Nuclear Regulatory Commission, under FIN A2243; Project Manager:
Dr. J. Muscara.

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61
62
Appendix
Introduction
Tensile tests were conducted according to ASTM Specification E 8 and E 21 in an Instron
tensile test machine with a maximum loading capacity of 90 kN (20 kips). Cylindrical specimens
with a diameter of 5.08 mm (0.2 in.) and a gauge length of 20.3 mm (0.8 in.) were used for all
the tests. An axial extensometer, with an initial gauge length of 20.3 mm (0.8 in.), was used
for continuous measurement of strain during room–temperature tests. An IBM computer was
used to digitize load, crosshead movement, and axial displacement data, and to store the data
on floppy disks. Analog traces of load–vs.–crosshead displacement and load–vs.–extensometer
displacement were also obtained for each test.

The tests at 290°C ( ≈ 550°F) were conducted in a forced–air recirculating furnace.

Thermocouples were mounted above and below the specimen gauge length to monitor and con-
trol the temperature within ±2°C. For the tests on samples aged for <10,000 h, an axial exten-
someter was not used for the elevated–temperature tests. Total strain in the specimen gauge
length was determined from correlations developed from the room–temperature tests. The total
elongation was determined from the crosshead displacement multiplied by 0.64. Elevated–
temperature tests on the long–term–aged samples were conducted with a clip gauge mounted
on the specimen grips. Total strain in the specimen gauge length was determined from correla-
tions developed from room–temperature tests conducted with clip gauge attached to the speci-
men grips and the extensometer mounted on the specimen gauge length.

The engineering stress vs. strain data for ten commercial and experimental heats aged up
to 58,000 h at temperatures between 290 and 450°C are presented in this appendix; results
from the tests at Materials Engineering Associates (MEA) are also included.

A–2
Table 1. Test data for specimen I1V–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 264.8 MPa Ultimate Stress : 598.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

23.72 0.0001 298.27 0.0101 530.28 0.2536

24.20 0.0001 304.13 0.0116 539.31 0.2763
51.30 0.0002 306.47 0.0130 546.48 0.2990
87.22 0.0002 312.06 0.0144 553.99 0.3222
122.52 0.0002 314.68 0.0159 560.41 0.3454
160.44 0.0002 353.15 0.0365 566.82 0.3691
194.02 0.0003 384.38 0.0579 572.54 0.3930
222.29 0.0007 410.44 0.0792 575.99 0.4172
242.63 0.0015 433.82 0.1006 581.64 0.4418
255.86 0.0024 452.09 0.1221 585.64 0.4668
268.07 0.0035 469.46 0.1436 588.54 0.4922
277.93 0.0047 485.12 0.1652 592.12 0.5182
283.51 0.0060 497.25 0.1870 593.91 0.5451
289.37 0.0073 509.52 0.2090 596.12 0.5730
296.34 0.0088 520.76 0.2311 597.29 0.6027

Table 2. Test data for specimen I1V–02

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 242.1 MPa Ultimate Stress : 583.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.75 0.0000 302.20 0.0146 525.79 0.2703

69.09 0.0004 305.44 0.0160 534.34 0.2921
105.42 0.0006 309.44 0.0175 541.38 0.3142
145.82 0.0009 311.44 0.0189 546.75 0.3362
179.06 0.0013 349.01 0.0390 554.55 0.3589
207.67 0.0019 377.56 0.0599 558.41 0.3816
228.22 0.0027 403.48 0.0808 562.41 0.4049
245.52 0.0037 423.48 0.1015 566.34 0.4286
258.21 0.0049 442.02 0.1225 570.13 0.4526
269.31 0.0062 459.12 0.1434 572.95 0.4771
276.41 0.0075 472.84 0.1642 576.06 0.5021
282.41 0.0088 486.22 0.1852 578.19 0.5278
288.27 0.0102 496.63 0.2062 579.99 0.5544
293.10 0.0117 507.73 0.2273 581.09 0.5820
297.23 0.0131 517.59 0.2488 582.19 0.6116

A–3
Table 3. Test data for specimen I2V–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Y 1.0 MPa Ultimate Stress : 579.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.75 0.0001 303.92 0.0151 519.66 0.2644

78.26 0.0004 307.99 0.0166 527.52 0.2855
117.07 0.0006 309.92 0.0180 534.76 0.3068
158.23 0.0009 313.50 0.0195 540.62 0.3283
192.36 0.0012 347.91 0.0396 544.41 0.3501
220.15 0.0018 375.21 0.0604 550.82 0.3723
239.80 0.0027 399.00 0.0808 557.37 0.3946
254.42 0.0037 419.13 0.1011 560.47 0.4175
266.07 0.0050 436.85 0.1214 563.99 0.4406
274.20 0.0063 452.50 0.1417 567.99 0.4643
282.20 0.0077 466.84 0.1620 570.47 0.4882
287.72 0.0091 479.88 0.1822 573.64 0.5129
292.54 0.0106 490.63 0.2026 575.30 0.5384
297.58 0.0121 502.01 0.2230 577.64 0.5650
300.75 0.0136 510.69 0.2436 579.09 0.5934

Table 4. Test data for specimen I2V–02

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 257.7 MPa Ultimate Stress : 578.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

21.65 0.0001 307.71 0.0150 519.73 0.2586

65.84 0.0004 311.30 0.0165 526.76 0.2789
103.63 0.0006 313.71 0.0181 534.69 0.2992
142.51 0.0008 316.88 0.0196 539.86 0.3199
178.64 0.0010 350.12 0.0394 546.27 0.3409
212.08 0.0015 377.14 0.0600 551.10 0.3620
236.83 0.0022 401.48 0.0802 555.92 0.3835
254.76 0.0033 421.27 0.1003 560.75 0.4054
267.52 0.0044 438.02 0.1203 563.51 0.4276
276.96 0.0058 452.99 0.1400 567.37 0.4502
284.06 0.0073 465.40 0.1597 568.96 0.4732
289.30 0.0088 481.53 0.1793 572.33 0.4969
294.96 0.0104 492.35 0.1990 573.85 0.5212
299.65 0.0119 501.11 0.2188 574.75 0.5463
301.09 0.0134 511.66 0.2387 575.09 0.5735

A–4
Table 5. Test data for specimen I3C–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 239.7 MPa Ultimate Stress : 517.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

21.79 0.0001 292.20 0.0149 462.57 0.2234

70.46 0.0004 294.68 0.0164 468.64 0.2410
109.97 0.0006 298.41 0.0180 475.60 0.2589
148.44 0.0008 300.89 0.0195 480.22 0.2768
182.71 0.0012 327.23 0.0356 486.56 0.2951
209.53 0.0018 347.01 0.0525 491.73 0.3135
229.11 0.0026 365.49 0.0692 495.87 0.3323
244.42 0.0037 381.56 0.0860 499.39 0.3513
254.97 0.0049 395.35 0.1028 503.52 0.3707
262.35 0.0061 408.79 0.1197 506.49 0.3903
268.90 0.0075 419.89 0.1368 509.11 0.4105
274.14 0.0089 429.82 0.1540 511.94 0.4314
279.24 0.0104 438.64 0.1711 514.21 0.4528
283.65 0.0119 448.09 0.1884 516.35 0.4752
288.13 0.0134 454.92 0.2058 516.49 0.4987

Table 6. Test data for specimen I2V–23

Test Number : 119 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 235.8 MPa Ultimate Stress : 637.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.00 384.59 0.0324 603.57 0.3157

43.6040 0.00 386.62 0.0330 605.86 0.3371
190.25 0.0015 436.18 0.0642 611.71 0.3616
274.48 0.0042 457.78 0.0815 615.35 0.3771
296.47 0.0056 479.29 0.0983 619.50 0.3984
303.00 0.0063 486.13 0.1062 631.01 0.4890
333.23 0.0116 534.59 0.1614 634.39 0.5164
360.34 0.0208 574.76 0.2402 637.33 0.5749

A–5
Table 7. Test data for specimen I3C–14

Test Number : 121 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 278.2 MPa Ultimate Stress : 633.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

1.04 0.0000 430.45 0.0536 590.35 0.2479

68.95 0.0005 451.69 0.0731 606.17 0.2892
196.77 0.0028 474.35 0.0867 606.87 0.2891
283.55 0.0054 482.80 0.0930 613.18 0.3155
311.96 0.0082 492.80 0.0997 623.97 0.3807
324.49 0.0099 526.96 0.1350 624.47 0.3806
356.89 0.0172 562.69 0.1863 631.93 0.4557
378.50 0.0253 564.45 0.1916 633.91 0.5043
414.69 0.0429

Table 8. Test data for specimen I3V–38

Test Number : 215 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 255.0 MPa Ultimate Stress : 609.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.31 0.0001 343.18 0.0197 512.07 0.1530

58.64 0.0005 358.13 0.0259 519.27 0.1633
91.12 0.0008 370.99 0.0320 532.16 0.1839
127.95 0.0010 382.74 0.0381 544.08 0.2045
152.36 0.0013 393.50 0.0443 556.49 0.2295
176.22 0.0015 403.34 0.0504 567.12 0.2547
188.00 0.0017 412.73 0.0565 577.22 0.2819
199.29 0.0019 421.62 0.0626 587.01 0.3138
219.44 0.0024 429.86 0.0687 594.55 0.3440
242.09 0.0032 441.64 0.0780 601.63 0.3814
259.00 0.0043 451.14 0.0861 606.43 0.4150
272.01 0.0053 460.27 0.0943 608.93 0.4501
285.98 0.0067 468.83 0.1025 607.43 0.4928
297.47 0.0082 476.91 0.1107 588.07 0.5213
310.53 0.0105 487.33 0.1222 554.04 0.5400
321.27 0.0129 496.22 0.1325 508.75 0.5549
332.68 0.0161 504.19 0.1428 451.10 0.5656

A–6
Table 9. Test data for specimen I3V–39

Test Number : 120 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 282.5 MPa Ultimate Stress : 452.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.44 0.0000 364.62 0.0269

58.55 0.0009 389.67 0.0413
210.64 0.0036 409.75 0.0553
276.76 0.0058 430.67 0.0701
309.50 0.0089 443.50 0.0803
323.52 0.0115 450.68 0.0874
344.97 0.0180

Table 10. Test data for specimen I1V–26

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 281.3 MPa Ultimate Stress : 615.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.34 0.0001 347.91 0.0144 557.72 0.2101

31.65 0.0002 352.25 0.0159 565.99 0.2270
64.74 0.0004 356.46 0.0174 573.44 0.2439
103.42 0.0006 359.98 0.0188 579.44 0.2612
143.27 0.0009 391.35 0.0337 585.30 0.2787
184.43 0.0012 417.68 0.0495 590.05 0.2964
222.36 0.0016 440.92 0.0652 594.95 0.3145
252.42 0.0022 460.09 0.0809 598.67 0.3329
274.20 0.0032 477.32 0.0968 603.08 0.3518
290.48 0.0044 492.70 0.1126 605.91 0.3710
303.23 0.0057 505.73 0.1286 609.43 0.3908
314.47 0.0071 518.76 0.1447 611.56 0.4114
323.09 0.0085 529.10 0.1609 612.74 0.4330
330.53 0.0099 540.76 0.1771 613.22 0.4560
336.46 0.0114 549.58 0.1936 613.22 0.4813
341.98 0.0128

A–7
Table 11. Test data for specimen I1V–27

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 303.4 MPa Ultimate Stress : 644.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.82 0.0001 374.25 0.0113 593.22 0.2240

33.72 0.0002 379.76 0.0126 600.40 0.2404
65.98 0.0003 384.11 0.0139 605.91 0.2568
103.90 0.0005 390.73 0.0152 611.84 0.2735
143.41 0.0007 421.34 0.0303 616.18 0.2903
184.02 0.0009 448.30 0.0466 619.63 0.3075
222.98 0.0013 471.33 0.0628 623.98 0.3248
257.31 0.0018 489.67 0.0789 627.01 0.3422
283.24 0.0025 508.01 0.0950 630.32 0.3599
303.44 0.0034 523.38 0.1110 633.35 0.3779
320.68 0.0044 536.21 0.1270 634.94 0.3962
333.64 0.0054 548.48 0.1431 637.97 0.4149
344.60 0.0066 559.16 0.1591 639.28 0.4337
353.49 0.0077 569.44 0.1753 641.76 0.4529
361.63 0.0089 579.78 0.1916 642.18 0.4723
367.01 0.0101 587.64 0.2078 643.83 0.4919

Table 12. Test data for specimen I2V–19

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 314.7 MPa Ultimate Stress : 642.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

23.79 0.0001 360.04 0.0100 592.47 0.2152

36.75 0.0002 365.49 0.0114 600.67 0.2344
71.08 0.0004 372.94 0.0129 605.50 0.2538
107.08 0.0004 376.38 0.0144 612.74 0.2736
144.24 0.0006 380.59 0.0159 617.56 0.2939
182.99 0.0008 418.10 0.0331 620.60 0.3144
220.63 0.0010 445.61 0.0510 627.56 0.3352
250.69 0.0013 470.91 0.0689 629.22 0.3567
278.55 0.0019 491.04 0.0867 632.59 0.3786
297.92 0.0028 509.80 0.1045 634.80 0.4009
314.75 0.0038 541.58 0.1226 637.97 0.4240
326.47 0.0049 554.48 0.1408 638.59 0.4480
338.39 0.0060 564.54 0.1591 639.97 0.4728
347.01 0.0073 575.30 0.1775 640.18 0.4988
355.42 0.0086 583.64 0.1962 640.32 0.5265

A–8
Table 13. Test data for specimen I2V–03

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 169.2 MPa Ultimate Stress : 409.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

35.99 0.0001 203.12 0.0108 358.94 0.1225

35.44 0.0001 205.67 0.0119 365.28 0.1303
36.40 0.0001 208.36 0.0130 369.63 0.1372
39.44 0.0001 225.11 0.0202 374.18 0.1472
59.29 0.0002 240.97 0.0283 381.00 0.1534
85.15 0.0004 255.24 0.0362 381.62 0.1643
108.32 0.0007 268.14 0.0440 386.93 0.1751
128.10 0.0011 279.58 0.0518 391.76 0.1779
145.76 0.0016 292.06 0.0596 393.83 0.1911
160.17 0.0023 303.71 0.6750 398.03 0.1995
170.44 0.0031 312.26 0.0752 397.90 0.2061
177.68 0.0040 320.54 0.0830 401.55 0.2118
184.16 0.0051 331.43 0.0909 403.89 0.2261
189.67 0.0062 339.43 0.0988 405.76 0.2345
194.16 0.0073 346.67 0.1066 406.10 0.2451
196.85 0.0084 353.15 0.1145 407.76 0.2464
202.15 0.0096

Table 14. Test data for specimen I2V–06

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 178.5 MPa Ultimate Stress : 402.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

21.44 0.0002 200.43 0.0101 332.19 0.0994

21.93 0.0002 202.71 0.0113 341.01 0.1090
42.20 0.0003 205.26 0.0125 349.22 0.1187
69.43 0.0005 207.26 0.0137 355.84 0.1289
97.49 0.0007 210.57 0.0148 362.32 0.1386
128.38 0.0009 210.98 0.0158 370.59 0.1459
156.51 0.0011 228.91 0.0243 373.42 0.1578
168.37 0.0019 246.90 0.0339 378.25 0.1660
175.33 0.0029 262.76 0.0435 382.04 0.1801
182.64 0.0041 277.10 0.0527 383.76 0.1921
185.74 0.0053 291.79 0.0620 391.42 0.2000
189.81 0.0064 302.75 0.0713 395.21 0.2108
193.95 0.0077 313.23 0.0808 396.79 0.2269
197.05 0.0089 324.12 0.0900 401.62 0.2296

A–9
Table 15. Test data for specimen I3C–02

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 158.6 MPa Ultimate Stress : 387.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

35.16 0.0003 192.85 0.0113 324.88 0.0940

36.06 0.0003 195.88 0.0123 333.02 0.1021
57.23 0.0003 198.71 0.0135 340.39 0.1101
84.32 0.0005 201.40 0.0146 346.19 0.1185
109.70 0.0008 202.64 0.0156 353.08 0.1266
128.38 0.0013 218.49 0.0228 358.25 0.1353
145.27 0.0018 233.87 0.0308 363.28 0.1441
155.27 0.0026 248.69 0.0385 365.01 0.1539
163.54 0.0035 262.35 0.0464 371.49 0.1614
169.68 0.0045 274.69 0.0542 377.76 0.1728
176.16 0.0056 285.24 0.0621 377.49 0.1832
180.78 0.0068 297.78 0.0701 383.97 0.1869
183.40 0.0079 307.85 0.0781 384.38 0.2002
187.40 0.0090 315.02 0.0861 386.73 0.2136
190.36 0.0102

Table 16. Test data for specimen I2V–24

Test Number : 090 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 178.6 MPa Ultimate Stress : 445.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

145.28 0.0011 248.73 0.0102 350.28 0.0706

165.45 0.0018 255.47 0.0126 361.52 0.0803
170.86 0.0020 261.78 0.0148 373.89 0.0909
176.52 0.0023 268.08 0.0173 377.04 0.0939
181.88 0.0027 273.89 0.0201 388.48 0.1034
186.90 0.0031 278.61 0.0224 395.83 0.1118
192.32 0.0036 288.66 0.0276 405.30 0.1248
197.14 0.0041 293.19 0.0301 411.18 0.1355
200.83 0.0043 298.51 0.0332 419.91 0.1487
203.93 0.0045 304.37 0.0368 423.28 0.1560
208.75 0.0048 310.28 0.0406 427.33 0.1655
214.56 0.0051 314.66 0.0435 432.37 0.1787
221.25 0.0055 318.95 0.0464 435.88 0.1861
227.85 0.0059 323.97 0.0501 437.63 0.1982
232.77 0.0063 329.34 0.0542 437.74 0.2033
238.04 0.0071 485.56 0.0585 440.28 0.2202
241.93 0.0080 340.13 0.0626 441.22 0.2253

A–1 0
Table 17. Test data for specimen I3C–15

Test Number : 089 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 163.6 MPa Ultimate Stress : 427.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

135.46 0.0010 290.05 0.0352 389.27 0.1184

140.82 0.0012 293.13 0.0374 393.63 0.1243
166.39 0.0022 296.36 0.0392 398.03 0.1307
184.42 0.0035 299.43 0.0416 403.25 0.1394
193.07 0.0044 309.75 0.0487 407.55 0.1466
200.97 0.0054 315.76 0.0531 409.39 0.1497
226.12 0.0074 323.77 0.0594 410.97 0.1528
233.47 0.0081 485.56 0.0717 419.81 0.1723
241.11 0.0099 346.25 0.0783 420.88 0.1743
244.69 0.0112 348.99 0.0805 423.02 0.1809
247.82 0.0125 355.71 0.0863 424.34 0.1860
250.90 0.0138 362.14 0.0916 425.25 0.1888
254.62 0.0156 364.72 0.0942 425.76 0.1916
257.80 0.0170 367.02 0.0962 425.83 0.1943
261.08 0.0185 369.00 0.0985 426.28 0.1977
284.03 0.0315 386.36 0.1142 427.03 0.2017
286.92 0.0333 387.86 0.1162 427.24 0.2045

Table 18. Test data for specimen I3V–40

Test Number : 088 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Y – MPa Ultimate Stress : 470.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

212.71 0.0017 380.70 0.0127 437.61 0.0570

224.61 0.0019 384.77 0.0143 442.37 0.0625
235.42 0.0020 388.73 0.0160 445.21 0.0676
246.68 0.0022 392.05 0.0174 448.56 0.0720
258.83 0.0024 394.94 0.0189 452.66 0.0794
271.47 0.0026 485.56 0.0205 454.44 0.0826
288.43 0.0029 402.90 0.0238 453.98 0.0874
298.12 0.0032 408.90 0.0280 454.42 0.0916
308.54 0.0035 411.34 0.0299 456.78 0.0958
318.12 0.0038 417.04 0.0347 457.92 0.0982
329.87 0.0043 420.85 0.0378 459.79 0.1004
334.79 0.0047 422.94 0.0396 461.50 0.1053
341.12 0.0052 424.50 0.0416 462.96 0.1100
346.43 0.0056 426.73 0.0440 463.79 0.1144
355.36 0.0068 429.70 0.0472 464.36 0.1164
361.00 0.0078 432.42 0.0507 465.60 0.1235
367.97 0.0090 434.51 0.0529

A–1 1
Table 19. Test data for specimen I1V–28

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 192.4 MPa Ultimate Stress : 381.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.82 0.0002 225.39 0.0091 329.78 0.0585

28.06 0.0002 229.39 0.0101 333.22 0.0618
46.54 0.0003 233.11 0.0110 339.02 0.0652
66.60 0.0004 240.76 0.0134 342.60 0.0686
95.22 0.0006 251.31 0.0170 346.81 0.0719
122.11 0.0007 259.31 0.0205 351.56 0.0753
146.24 0.0009 268.27 0.0240 356.39 0.0784
160.23 0.0012 274.96 0.0275 360.18 0.0816
173.33 0.0018 282.89 0.0310 362.32 0.0846
183.88 0.0024 288.96 0.0345 364.39 0.0876
191.61 0.0032 294.27 0.0379 368.59 0.0903
198.57 0.0040 301.99 0.0414 371.83 0.0932
204.36 0.0048 309.09 0.0448 373.35 0.0959
209.74 0.0056 314.26 0.0482 374.73 0.0984
215.19 0.0065 318.54 0.0516 377.90 0.1007
218.43 0.0073 324.81 0.0551 380.66 0.1021
222.36 0.0082

Table 20. Test data for specimen I1V–29

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 189.0 MPa Ultimate Stress : 442.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.55 0.0001 211.46 0.0057 375.21 0.0873

21.17 0.0001 214.77 0.0065 384.66 0.0953
21.79 0.0001 219.80 0.0074 391.62 0.1035
38.13 0.0002 224.15 0.0082 398.52 0.1117
55.71 0.0003 226.84 0.0090 405.27 0.1201
78.19 0.0004 246.00 0.0150 409.55 0.1286
102.80 0.0006 265.93 0.0219 414.86 0.1372
126.45 0.0008 281.10 0.0290 421.41 0.1458
148.38 0.0011 296.47 0.0362 424.72 0.1547
164.30 0.0015 311.09 0.0434 429.89 0.1639
175.40 0.0021 324.26 0.0506 432.58 0.1731
185.40 0.0027 334.95 0.0578 434.99 0.1829
192.71 0.0034 344.88 0.0650 436.92 0.1925
199.26 0.0041 357.36 0.0724 438.92 0.2046
205.74 0.0049 366.53 0.0798 442.02 0.2140

A–1 2
Table 21. Test data for specimen I2V–20

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 179.1 MPa Ultimate Stress : 437.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

24.06 0.0001 215.74 0.0090 383.28 0.1135

24.41 0.0001 221.11 0.0100 390.66 0.1231
38.20 0.0002 222.29 0.0111 397.55 0.1331
56.88 0.0004 226.42 0.0123 402.17 0.1432
81.01 0.0005 229.11 0.0135 408.79 0.1534
106.73 0.0008 252.42 0.0218 413.75 0.1636
129.48 0.0010 270.62 0.0309 417.55 0.1743
148.51 0.0015 288.61 0.0398 423.27 0.1854
163.34 0.0021 305.44 0.0487 424.99 0.1966
174.37 0.0029 319.85 0.0576 429.54 0.2086
183.61 0.0037 333.29 0.0667 430.85 0.2210
192.36 0.0047 344.32 0.0758 432.23 0.2336
199.88 0.0057 354.74 0.0852 435.89 0.2483
204.15 0.0067 365.28 0.0945 436.30 0.2624
209.74 0.0078 373.42 0.1039 436.78 0.2795

Table 22. Test data for specimen P21T–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 216.3 MPa Ultimate Stress : 538.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

75.77 0.0002 225.73 0.0031 263.10 0.0101

95.56 0.0003 232.84 0.0038 267.31 0.0110
112.94 0.0004 239.59 0.0047 267.93 0.0120
133.55 0.0005 245.38 0.0055 271.93 0.0130
154.30 0.0007 248.90 0.0063 272.62 0.0141
171.47 0.0010 253.38 0.0073 275.38 0.0152
189.81 0.0014 257.59 0.0082 279.31 0.0164
204.64 0.0018 259.66 0.0091 280.13 0.0174
215.53 0.0025

A–1 3
Table 23. Test data for specimen P23T–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 238.1 MPa Ultimate Stress : 556.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 342.95 0.0845 358.18 0.2337

59.50 0.0004 347.50 0.0975 358.18 0.2444
136.45 0.0010 349.08 0.1064 358.18 0.2560
212.36 0.0024 350.46 0.1406 358.18 0.2653
226.56 0.0032 350.46 0.1474 358.18 0.2736
246.14 0.0052 350.46 0.1587 358.18 0.2837
256.35 0.0064 349.08 0.1633 358.18 0.2953
268.90 0.0094 350.94 0.1683 361.97 0.3024
282.34 0.0142 352.87 0.1755 361.97 0.3118
294.41 0.0198 353.15 0.1798 365.22 0.3214
304.06 0.0263 354.46 0.1848 365.22 0.3297
313.44 0.0330 356.32 0.1901 368.66 0.3373
321.99 0.0398 357.70 0.1973 368.66 0.3398
332.19 0.0504 356.87 0.2048 368.66 0.3472
337.84 0.0584 358.18 0.2124 368.66 0.3547
342.95 0.0687 358.18 0.2225

Table 24. Test data for specimen P22A–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 206.4 MPa Ultimate Stress : 561.7 MPa

Experimental Data Not Available.

Table 25. Test data for specimen P23A–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 216.7 MPa Ultimate Stress : 536.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

33.72 0.0000 210.84 0.0025 260.28 0.0105

49.92 0.0002 218.70 0.0031 262.97 0.0113
66.47 0.0003 225.94 0.0037 265.17 0.0123
97.77 0.0004 232.56 0.0045 268.28 0.0132
118.04 0.0005 237.73 0.0053 270.62 0.0141
139.14 0.0007 243.45 0.0061 272.83 0.0151
156.44 0.0009 246.83 0.0070 275.31 0.0160
171.06 0.0011 250.56 0.0078 277.10 0.0170
185.47 0.0014 254.42 0.0087 280.00 0.0180
199.53 0.0019 257.24 0.0096

A–1 4
Table 26. Test data for specimen P22T–16

Test Number : 116 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 247.0 MPa Ultimate Stress : 580.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

43.91 0.0000 342.66 0.0248 481.02 0.1430

189.97 0.0015 363.69 0.0376 485.81 0.1553
201.17 0.0018 388.73 0.0551 508.05 0.1923
223.14 0.0021 421.22 0.0830 526.44 0.2290
261.09 0.0032 448.33 0.1060 541.88 0.2665
275.55 0.0042 468.51 0.1272 562.32 0.3484
303.36 0.0088 475.56 0.1355 576.12 0.4433
323.48 0.0172 477.51 0.1399 580.05 0.5090

Table 27. Test data for specimen P21A–31

Test Number : 114 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 242.6 MPa Ultimate Stress : 571.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 373.76 0.0571 514.47 0.2440

48.35 0.0003 394.21 0.0734 531.02 0.2859
203.54 0.0031 427.78 0.1008 530.23 0.2862
227.32 0.0036 451.32 0.1276 560.39 0.4079
259.89 0.0049 465.92 0.1452 560.29 0.4077
276.22 0.0068 465.92 0.1455 565.28 0.4623
292.42 0.0101 478.12 0.1651 568.19 0.4721
314.12 0.0183 484.73 0.1799 571.09 0.5044
315.90 0.0196 487.58 0.1871 570.99 0.5495
332.18 0.0273

A–1 5
Table 28. Test data for specimen P25A–28

Test Number : 111 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 223.9 MPa Ultimate Stress : 548.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 321.89 0.0234 476.75 0.1723

86.41 0.0002 347.19 0.0401 483.95 0.1925
155.03 0.0009 368.69 0.0567 504.89 0.2369
194.51 0.0016 383.86 0.0691 511.41 0.2558
213.11 0.0023 405.18 0.0880 512.94 0.2598
241.77 0.0025 419.23 0.0991 529.77 0.3109
261.95 0.0042 436.03 0.1167 536.79 0.3411
269.65 0.0052 447.42 0.1308 543.63 0.3742
287.33 0.0090 457.87 0.1450 548.27 0.4148
301.36 0.0135 458.27 0.1448

Table 29. Test data for specimen P21A–36

Test Number : 286 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 58,000 h
Yield Stress : 263.6 MPa Ultimate Stress : 583.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

18.696 0.0001 427.554 0.0875 548.057 0.2827

24.618 0.0001 440.192 0.1004 557.686 0.3122
39.860 0.0001 455.767 0.1178 562.137 0.3283
134.443 0.0005 464.743 0.1290 565.863 0.3422
215.831 0.0011 466.431 0.1312 573.991 0.3795
253.721 0.0024 494.156 0.1706 574.572 0.3819
275.165 0.0041 495.511 0.1728 578.927 0.4081
361.799 0.0360 513.365 0.2038 580.330 0.4189
365.350 0.0382 514.574 0.2060 583.281 0.4486
387.177 0.0531 535.041 0.2491 583.475 0.4507
400.952 0.0638 535.864 0.2514 583.813 0.4631

A–1 6
Table 30. Test data for specimen P24T–14

Test Number : 118 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 229.4 MPa Ultimate Stress : 600.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

1.08 0.0000 368.40 0.0424 521.97 0.2166

72.59 0.0001 395.11 0.0601 542.22 0.2682
207.27 0.0022 421.93 0.0814 560.21 0.3171
241.78 0.0027 444.92 0.1003 571.16 0.3615
272.19 0.0048 467.12 0.1241 579.92 0.4024
285.75 0.0067 474.79 0.1323 594.04 0.5004
307.05 0.0117 486.37 0.1514 599.32 0.5632
326.49 0.0178 500.36 0.1771 600.04 0.6237
340.41 0.0239

Table 31. Test data for specimen P25T–10

Test Number : 109 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Y .1 MPa Ultimate Stress : 581.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 414.63 0.0790 534.40 0.2365

64.28 0.0003 443.49 0.0996 537.07 0.2424
164.98 0.0022 452.36 0.1085 540.08 0.2500
198.69 0.0024 466.92 0.1227 541.90 0.2527
213.37 0.0029 469.64 0.1279 547.20 0.2668
219.84 0.0030 478.91 0.1372 566.01 0.3318
249.13 0.0040 484.19 0.1494 567.78 0.3355
251.89 0.0043 493.73 0.1618 572.87 0.3572
275.62 0.0069 499.40 0.1732 572.56 0.3660
287.20 0.0091 501.58 0.1740 574.42 0.3763
300.95 0.0124 505.86 0.1857 574.32 0.3757
320.76 0.0189 511.37 0.1946 576.85 0.3951
339.21 0.0279 517.49 0.2045 579.98 0.4058
366.24 0.0431 526.82 0.2223 581.80 0.4462
394.74 0.0629 531.63 0.2313

A–1 7
Table 32. Test data for specimen P22A–36

Test Number : 113 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 237.4 MPa Ultimate Stress : 603.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 437.15 0.0830 521.86 0.1973

67.86 0.0001 455.92 0.0989 541.57 0.2361
195.99 0.0015 465.90 0.1055 563.14 0.2942
220.01 0.0020 471.02 0.1109 563.62 0.2993
260.93 0.0031 481.35 0.1347 577.37 0.3565
283.12 0.0050 484.70 0.1395 582.02 0.3841
295.07 0.0065 497.55 0.1568 583.56 0.3885
312.40 0.0099 504.35 0.1669 590.65 0.4283
330.98 0.0152 510.57 0.1782 601.19 0.5273
361.40 0.0298 516.28 0.1882 602.66 0.5777
391.84 0.0483 521.81 0.1946 602.98 0.6590
414.44 0.0649

Table 33. Test data for specimen P21A–19

Test Number : 283 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 55,000 h
Yield Stress : 249.7 MPa Ultimate Stress : 605.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.30 0.0001 351.39 0.0260 523.10 0.1626

19.83 0.0001 372.83 0.0360 524.69 0.1646
57.42 0.0003 376.63 0.0380 530.32 0.1726
68.12 0.0003 398.34 0.0500 538.61 0.1846
127.65 0.0006 401.60 0.0520 546.12 0.1966
140.24 0.0007 404.98 0.0540 556.47 0.2146
152.69 0.0008 420.58 0.0640 563.74 0.2287
207.14 0.0015 426.26 0.0679 564.75 0.2307
223.63 0.0020 443.08 0.0802 571.49 0.2450
259.10 0.0039 445.53 0.0822 577.56 0.2593
266.89 0.0046 462.18 0.0963 581.56 0.2695
273.90 0.0053 473.10 0.1064 582.28 0.2715
308.66 0.0113 487.57 0.1207 594.80 0.3112
314.87 0.0129 500.52 0.1347 599.37 0.3304

A–1 8
Table 34. Test data for specimen P22T–04

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 252.3 MPa Ultimate Stress : 601.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

59.78 0.0003 314.81 0.0148 546.62 0.2670

91.70 0.0004 320.54 0.0163 552.41 0.2844
125.00 0.0006 362.39 0.0358 559.72 0.3022
160.85 0.0008 404.72 0.0641 564.40 0.3201
196.16 0.0011 424.99 0.0808 570.20 0.3379
217.81 0.0017 441.82 0.0974 575.16 0.3561
239.45 0.0024 457.81 0.1139 579.16 0.3743
254.35 0.0033 470.64 0.1306 583.37 0.3926
268.28 0.0044 482.98 0.1474 584.61 0.4112
277.24 0.0056 494.84 0.1641 588.33 0.4299
285.86 0.0068 506.70 0.1811 589.98 0.4487
290.41 0.0081 517.52 0.1982 592.81 0.4679
298.41 0.0094 524.62 0.2154 596.67 0.4868
302.13 0.0107 533.38 0.2325 596.05 0.5056
306.82 0.0121 541.10 0.2496 597.36 0.5240
314.88 0.0134

Table 35. Test data for specimen P23A–14

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 249.2 MPa Ultimate Stress : 594.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.82 0.0002 288.48 0.0086 537.79 0.2465

43.37 0.0003 294.27 0.0096 545.58 0.2655
66.26 0.0004 297.51 0.0107 552.96 0.2845
93.22 0.0005 302.68 0.0119 557.85 0.3039
121.28 0.0006 342.53 0.0278 565.85 0.3237
149.00 0.0008 374.73 0.0461 570.82 0.3436
175.54 0.0010 402.93 0.0655 571.92 0.3637
199.81 0.0014 437.27 0.1004 579.85 0.3844
220.63 0.0019 458.85 0.1176 580.61 0.4054
238.08 0.0027 474.22 0.1356 585.02 0.4267
250.28 0.0035 486.49 0.1538 588.54 0.4487
259.24 0.0044 498.63 0.1720 588.61 0.4714
270.14 0.0054 510.56 0.1904 590.74 0.4951
275.03 0.0064 521.38 0.2090 592.40 0.5204
285.10 0.0075 529.79 0.2277

A–1 9
Table 36. Test data for specimen P23A–36

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 265.2 MPa Ultimate Stress : 608.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

3.17 0.0002 298.20 0.0106 548.34 0.2622

33.58 0.0002 301.30 0.0119 556.82 0.2838
61.98 0.0004 306.13 0.0131 564.13 0.3057
94.32 0.0005 308.13 0.0144 571.44 0.3279
130.66 0.0008 311.92 0.0157 576.61 0.3503
166.03 0.0010 355.42 0.0359 581.64 0.3732
203.81 0.0012 388.17 0.0576 585.92 0.3961
237.66 0.0015 418.30 0.0798 590.19 0.4196
254.76 0.0024 455.95 0.1164 593.50 0.4435
262.21 0.0034 474.29 0.1365 597.57 0.4676
271.24 0.0045 490.22 0.1572 600.12 0.4922
279.10 0.0057 504.35 0.1778 602.19 0.5174
282.82 0.0069 517.18 0.1986 603.91 0.5429
289.44 0.0081 528.48 0.2196 606.33 0.5689
292.96 0.0093 539.17 0.2409 607.98 0.5955

Table 37. Test data for specimen P22T–11

Test Number : 110 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 249.3 MPa Ultimate Stress : 628.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 437.70 0.0736 578.79 0.2605

63.87 0.0003 459.69 0.0898 582.98 0.2690
203.91 0.0025 471.05 0.0973 587.96 0.2787
222.66 0.0028 484.95 0.1108 589.58 0.2852
229.32 0.0029 497.35 0.1235 592.32 0.2982
249.74 0.0036 518.00 0.1476 594.90 0.3027
286.31 0.0062 521.30 0.1541 597.52 0.3136
300.38 0.0080 527.36 0.1624 603.41 0.3340
333.68 0.0158 536.88 0.1732 607.02 0.3542
370.93 0.0297 540.59 0.1816 610.92 0.3707
377.32 0.0333 549.45 0.1968 614.92 0.3913
388.17 0.0403 563.77 0.2188 621.68 0.4432
403.38 0.0502 564.52 0.2301 623.50 0.4576
417.59 0.0575 569.11 0.2389 625.01 0.4709
432.23 0.0689 573.91 0.2496 628.40 0.5554

A–2 0
Table 38. Test data for specimen P22A–13

Test Number : 112 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 245.5 MPa Ultimate Stress : 615.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 382.98 0.0400 570.86 0.2623

92.46 0.0003 402.17 0.0535 580.24 0.2911
194.32 0.0016 424.97 0.0691 581.92 0.2985
216.44 0.0019 451.94 0.0896 583.79 0.3018
228.12 0.0021 474.33 0.1065 589.03 0.3270
266.02 0.0036 479.54 0.1115 590.51 0.3272
281.00 0.0048 484.08 0.1211 601.41 0.3777
301.46 0.0076 509.21 0.1497 602.22 0.3855
321.99 0.0124 509.31 0.1496 607.76 0.4254
335.17 0.0174 537.42 0.1913 614.32 0.4766
358.57 0.0266 554.68 0.2264 615.39 0.5406

Table 39. Test data for specimen P24A–32

Test Number : 115 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 225.4 MPa Ultimate Stress : 617.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 359.05 0.0305 528.87 0.1818

187.93 0.0013 382.89 0.0445 561.70 0.2462
204.63 0.0014 421.03 0.0707 580.29 0.2982
216.16 0.0017 444.60 0.0878 591.20 0.3395
254.69 0.0030 476.19 0.1127 602.95 0.3998
285.18 0.0065 484.47 0.1257 612.92 0.4005
306.94 0.0101 510.06 0.1561 617.20 0.5470
336.38 0.0197

A–2 1
Table 40. Test data for specimen P24T–05

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 233.5 MPa Ultimate Stress : 603.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

20.13 0.0000 301.65 0.0126 534.27 0.1735

40.20 0.0003 306.54 0.0138 542.62 0.1860
74.95 0.0005 311.02 0.0149 549.72 0.1985
112.38 0.0007 314.61 0.0162 558.41 0.2112
147.27 0.0010 345.36 0.0276 565.23 0.2240
176.64 0.0014 373.01 0.0399 571.64 0.2369
201.53 0.0020 395.90 0.0521 575.99 0.2497
220.91 0.0028 415.34 0.0643 580.68 0.2629
237.25 0.0037 433.40 0.0763 585.09 0.2763
250.28 0.0047 449.81 0.0884 590.60 0.2898
261.17 0.0057 466.09 0.1004 592.88 0.3034
269.86 0.0068 479.32 0.1124 595.57 0.3171
277.51 0.0079 492.42 0.1246 599.43 0.3312
284.34 0.0090 504.63 0.1368 600.46 0.3455
292.13 0.0102 513.80 0.1489 601.77 0.3599
296.96 0.0114 525.38 0.1613

Table 41. Test data for specimen P24A–0 4

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 236.2 MPa Ultimate Stress : 616.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

23.72 0.0002 284.41 0.0091 528.07 0.1661

33.44 0.0002 287.86 0.0101 536.89 0.1786
62.74 0.0004 294.96 0.0111 544.69 0.1912
93.01 0.0005 237.66 0.0122 551.30 0.2036
124.45 0.0007 303.51 0.0133 558.27 0.2160
150.58 0.0009 339.15 0.0247 565.16 0.2283
177.47 0.0012 365.70 0.0374 573.78 0.2406
197.88 0.0016 388.31 0.0498 578.54 0.2530
218.15 0.0023 410.17 0.0625 582.19 0.2652
232.35 0.0031 430.09 0.0757 586.95 0.2776
246.21 0.0041 447.61 0.0892 594.26 0.2894
255.31 0.0050 476.77 0.1165 596.60 0.3015
263.66 0.0060 493.87 0.1285 600.74 0.3135
272.96 0.0070 504.35 0.1410 602.33 0.3252
276.82 0.0080 515.73 0.1535 606.46 0.3367

A–2 2
Table 42. Test data for specimen P21T–02

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Y .3 MPa Ultimate Stress : 387.1 MPa
Engr. Engr. Engr.
Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.07 0.0000 181.95 0.0074 247.11 0.0423

25.86 0.0005 194.16 0.0097 250.56 0.0465
36.68 0.0007 204.02 0.0125 253.52 0.0509
67.84 0.0012 211.53 0.0153 256.14 0.0551
83.63 0.0016 217.60 0.0182 259.59 0.0594
100.66 0.0020 224.56 0.0217 261.73 0.0639
117.90 0.0026 230.97 0.0257 264.28 0.0682
135.00 0.0032 235.32 0.0299 267.52 0.0726
152.37 0.0043 240.01 0.0340 269.45 0.0772
167.20 0.0056 243.52 0.0381

Table 43. Test data for specimen P23T–02

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 154.2 MPa Ultimate Stress : 405.0 MPa
Engr. Engr. Engr.
Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

4.48 0.0001 53.71 0.0005 140.17 0.0022

10.20 0.0001 70.40 0.0008 148.51 0.0029
14.89 0.0002 86.80 0.0009 154.58 0.0037
20.55 0.0003 101.70 0.0011 159.13 0.0045
29.99 0.0003 117.69 0.0013 163.61 0.0056
41.71 0.0004 130.59 0.0017 166.99 0.0064

Table 44. Test data for specimen P22A–02

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 137.9 MPa Ultimate Stress : 406.9 MPa
Engr. Engr. Engr.
Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

10.69 0.0002 61.78 0.0009 154.37 0.0079

12.41 0.0002 74.12 0.0011 156.58 0.0089
14.27 0.0002 89.01 0.0013 159.82 0.0099
15.38 0.0002 102.32 0.0015 161.61 0.0107
16.27 0.0002 113.63 0.0019 164.16 0.0117
17.37 0.0003 123.07 0.0024 166.92 0.0125
18.48 0.0003 131.07 0.0030 168.09 0.0134
19.72 0.0003 136.31 0.0037 170.37 0.0144
21.03 0.0003 141.00 0.0045 172.78 0.0152
25.65 0.0004 144.86 0.0053 174.44 0.0161
31.65 0.0004 148.51 0.0062 176.37 0.0171

A–2 3
Table 45. Test data for specimen P23A–02

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 144.0 MPa Ultimate Stress : 385.1 MPa

Experimental Data Not Available.

Table 46. Test data for specimen P21A–32

Test Number : 267 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 162.3 MPa Ultimate Stress : 403.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

44.672 0.0002 242.806 0.0422 371.405 0.1684

46.773 0.0002 259.901 0.0536 372.644 0.1705
102.361 0.0003 283.979 0.0711 381.782 0.1884
111.518 0.0004 292.211 0.0774 382.837 0.1905
120.420 0.0005 312.492 0.0948 387.358 0.2027
127.914 0.0006 319.388 0.1015 396.616 0.2282
165.299 0.0031 332.218 0.1146 397.642 0.2353
170.403 0.0042 338.126 0.1215 400.346 0.2485
186.100 0.0097 345.534 0.1300 402.929 0.2595
191.021 0.0117 355.655 0.1437 402.216 0.2615
218.343 0.0270 360.315 0.1504 403.421 0.2727

Table 47. Test data for specimen P21A–33

Test Number : 070 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 155.2 MPa Ultimate Stress : 405.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

126.22 0.0010 231.75 0.0186 351.63 0.1175

159.63 0.0024 237.87 0.0205 354.16 0.1213
164.81 0.0030 242.83 0.0232 362.63 0.1327
168.80 0.0036 250.06 0.0283 365.60 0.1367
172.02 0.0041 254.96 0.0320 368.00 0.1402
179.21 0.0057 260.16 0.0359 374.97 0.1516
184.07 0.0069 266.55 0.0410 381.91 0.1652
187.40 0.0082 275.01 0.0476 384.64 0.1709
192.53 0.0102 286.24 0.0572 388.73 0.1803
197.56 0.0123 297.42 0.0666 393.29 0.1924
202.25 0.0132 307.75 0.0757 396.45 0.2015
204.73 0.0139 318.13 0.0850 399.57 0.2143
208.74 0.0145 328.51 0.0948 401.57 0.2232
212.31 0.0151 336.87 0.1013 403.44 0.2319
217.96 0.0161 340.72 0.1052 405.35 0.2407
226.73 0.0177 345.13 0.1101 405.91 0.2449

A–2 4
Table 48. Test data for specimen P24T–16

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 148.2 MPa Ultimate Stress : 407.0 MPa

Experimental Data Not Available.

Table 49. Test data for specimen P21A–37

Test Number : 316 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 58,000 h
Yield Stress : 164.2 MPa Ultimate Stress : 410.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

24.800 0.000 190.360 0.009 360.330 0.134

59.530 0.000 196.230 0.011 390.370 0.183
70.650 0.000 235.510 0.031 394.480 0.192
81.700 0.000 246.880 0.038 396.880 0.199
112.760 0.001 261.030 0.047 400.100 0.208
121.120 0.001 267.710 0.051 400.920 0.211
128.690 0.001 280.710 0.060 409.240 0.243
135.470 0.001 298.400 0.073 409.740 0.246
154.940 0.002 333.400 0.104 409.940 0.248
161.630 0.003 335.600 0.106 410.590 0.257
167.120 0.003 351.350 0.123 410.590 0.259

Table 50. Test data for specimen P22T–17

Test Number : 317 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 58,000 h
Y 177.5 MPa Ultimate Stress : 422.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.930 0.000 252.800 0.035 406.590 0.200

20.250 0.000 256.530 0.037 409.090 0.207
34.980 0.000 260.240 0.039 411.600 0.216
46.610 0.000 305.830 0.070 414.150 0.225
58.520 0.000 319.660 0.081 414.850 0.227
92.410 0.000 322.270 0.083 416.820 0.239
103.720 0.000 324.820 0.085 417.460 0.241
151.770 0.001 374.050 0.137 418.280 0.245
177.440 0.003 384.420 0.153 418.920 0.252
195.040 0.006 398.700 0.179 419.580 0.254
200.220 0.008 399.640 0.182 420.160 0.256

A–2 5
Table 51. Test data for specimen P21A–14

Test Number : 075 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 153.2 MPa Ultimate Stress : 428.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 240.59 0.0126 339.96 0.0811

126.47 0.0007 247.15 0.0151 351.42 0.0912
140.94 0.0010 251.64 0.0176 364.20 0.1004
153.12 0.0015 257.87 0.0214 376.09 0.1122
161.24 0.0019 262.91 0.0242 390.12 0.1303
168.47 0.0023 268.07 0.0276 397.02 0.1402
179.44 0.0032 275.15 0.0318 404.68 0.1528
188.51 0.0046 280.09 0.0349 409.96 0.1637
197.32 0.0062 285.05 0.0386 414.54 0.1735
205.07 0.0073 291.29 0.0429 418.00 0.1823
212.49 0.0082 297.23 0.0470 419.93 0.1911
218.37 0.0089 302.06 0.0503 422.02 0.2012
223.76 0.0094 316.65 0.0616 424.43 0.2107
228.26 0.0100 323.63 0.0675 426.22 0.2229
233.74 0.0108 332.60 0.0748 428.89 0.2429

Table 52. Test data for specimen P21A–15

Test Number : 268 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 163.9 MPa Ultimate Stress : 422.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

41.587 0.0002 181.122 0.0053 352.778 0.1018

57.834 0.0002 202.641 0.0119 368.889 0.1170
67.757 0.0002 207.981 0.0142 371.000 0.1192
87.450 0.0002 212.072 0.0162 390.322 0.1413
97.436 0.0003 221.866 0.0205 398.230 0.1522
106.786 0.0003 267.526 0.0440 403.850 0.1608
115.687 0.0004 274.437 0.0481 410.038 0.1718
123.186 0.0006 282.514 0.0526 415.142 0.1827
130.199 0.0006 292.529 0.0586 419.248 0.1936
169.039 0.0033 302.756 0.0651 420.728 0.1997
175.526 0.0042 318.588 0.0756 421.191 0.2021

A–2 6
Table 53. Test data for specimen P21A–16

Test Number : 068 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 152.6 MPa Ultimate Stress : 407.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

117.51 0.0008 276.83 0.0394 369.41 0.1158

129.27 0.0011 288.36 0.0476 372.84 0.1193
139.60 0.0014 297.98 0.0550 378.80 0.1272
151.74 0.0020 305.49 0.0606 381.74 0.1318
162.95 0.0028 312.11 0.0658 385.80 0.1367
175.68 0.0043 317.36 0.0701 388.53 0.1428
186.25 0.0062 323.09 0.0746 392.00 0.1497
195.49 0.0086 329.66 0.0803 393.84 0.1562
202.07 0.0098 334.76 0.0849 396.52 0.1628
207.07 0.0106 340.40 0.0894 399.06 0.1698
218.81 0.0121 346.73 0.0946 401.88 0.1771
230.35 0.0137 351.53 0.0993 403.67 0.1841
243.26 0.0183 357.51 0.1028 405.27 0.1916
252.14 0.0232 362.26 0.1077 407.10 0.2028
264.26 0.0310 365.54 0.1113 407.71 0.2095

Table 54. Test data for specimen P25T–12

Test Number : 313 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 55,000 h
Yield Stress : 171.4 MPa Ultimate Stress : 418.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

13.831 0.0001 218.952 0.0175 357.126 0.1115

19.288 0.0001 231.905 0.0240 361.320 0.1158
100.535 0.0001 244.707 0.0308 363.373 0.1180
124.689 0.0003 256.660 0.0375 376.516 0.1334
131.517 0.0005 267.876 0.0440 378.208 0.1355
156.203 0.0015 278.688 0.0506 384.704 0.1445
174.466 0.0033 292.401 0.0593 390.576 0.1532
180.836 0.0044 311.206 0.0723 406.128 0.1819
192.530 0.0072 325.432 0.0831 409.751 0.1909
198.021 0.0090 330.782 0.0875 410.687 0.1931
202.908 0.0108 348.084 0.1027 418.378 0.2268

A–2 7
Table 55. Test data for specimen P21A–18

Test Number : 312 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 55,000 h
Yield Stress : 168.6 MPa Ultimate Stress : 416.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

20.303 0.0001 173.689 0.0032 319.676 0.0756

24.643 0.0001 196.740 0.0079 322.429 0.0777
64.311 0.0002 202.251 0.0096 338.256 0.0910
74.931 0.0002 228.815 0.0206 345.495 0.0973
86.046 0.0002 242.470 0.0274 350.063 0.1019
96.464 0.0003 250.870 0.0319 364.845 0.1172
123.313 0.0006 263.030 0.0386 377.614 0.1326
136.832 0.0008 270.539 0.0429 385.520 0.1439
142.711 0.0011 288.505 0.0539 397.627 0.1640
160.977 0.0021 295.124 0.0582 408.518 0.1883
167.872 0.0026 304.744 0.0648 415.626 0.2158

Table 56. Test data for specimen P21T–08

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 155.6 MPa Ultimate Stress : 423.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

37.65 0.0002 202.84 0.0139 359.91 0.1300

60.05 0.0003 206.57 0.0155 371.56 0.1418
85.01 0.0005 209.88 0.0170 379.90 0.1537
112.80 0.0008 212.77 0.0184 385.14 0.1657
132.66 0.0014 233.04 0.0288 393.00 0.1780
150.31 0.0024 252.97 0.0402 397.34 0.1906
162.79 0.0036 270.96 0.0513 402.24 0.2035
171.82 0.0049 288.41 0.0624 407.55 0.2168
179.47 0.0064 303.78 0.0735 411.13 0.2305
185.47 0.0079 316.68 0.0847 414.86 0.2448
190.16 0.0094 330.26 0.0958 417.48 0.2593
195.19 0.0109 341.64 0.1071 417.75 0.2756
198.84 0.0125 352.39 0.1184 420.37 0.2938

A–2 8
Table 57. Test data for specimen P22T–05

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 153.8 MPa Ultimate Stress : 399.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.55 0.0002 195.60 0.0136 338.12 0.1086

26.75 0.0002 200.36 0.0151 345.15 0.1180
50.06 0.0003 202.91 0.0164 353.84 0.1275
80.46 0.0005 206.08 0.0178 360.60 0.1370
113.97 0.0008 208.50 0.0191 366.46 0.1468
135.48 0.0016 224.91 0.0271 372.87 0.1567
150.17 0.0026 241.73 0.0362 377.35 0.1668
161.13 0.0038 256.90 0.0452 381.14 0.1773
168.58 0.0051 271.52 0.0542 386.73 0.1881
173.82 0.0065 283.86 0.0632 388.59 0.1993
180.64 0.0079 296.20 0.0723 391.83 0.2110
184.37 0.0094 307.78 0.0813 396.10 0.2236
189.47 0.0108 318.12 0.0904 397.48 0.2380
193.33 0.0122 328.33 0.0995 398.79 0.2563

Table 58. Test data for specimen P23A–15

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 161.0 MPa Ultimate Stress : 415.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

10.69 0.0002 61.78 0.0009 154.37 0.0079

12.41 0.0002 74.12 0.0011 156.58 0.0089
14.27 0.0002 89.01 0.0013 159.82 0.0099
15.38 0.0002 102.32 0.0015 161.61 0.0107
16.27 0.0002 113.63 0.0019 164.16 0.0117
17.37 0.0003 123.07 0.0024 166.92 0.0125
18.48 0.0003 131.07 0.0030 168.09 0.0134
19.72 0.0003 136.31 0.0037 170.37 0.0144
21.03 0.0003 141.00 0.0045 172.78 0.0152
25.65 0.0004 144.86 0.0053 174.44 0.0161
31.65 0.0004 148.51 0.0062 176.37 0.0171
39.85 0.0006 151.55 0.0071 178.51 0.0179
49.64 0.0007

A–2 9
Table 59. Test data for specimen P23A–27

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 154.1 MPa Ultimate Stress : 419.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

21.99 0.0002 205.19 0.0138 359.35 0.1180

31.44 0.0002 207.60 0.0151 366.94 0.1275
63.57 0.0004 211.94 0.0164 374.11 0.1371
98.73 0.0006 215.05 0.0177 380.73 0.1469
121.69 0.0012 217.94 0.0190 387.76 0.1568
141.07 0.0020 234.15 0.0271 392.52 0.1668
154.03 0.0029 251.18 0.0361 396.72 0.1770
164.99 0.0039 266.07 0.0450 402.93 0.1875
172.51 0.0050 281.58 0.0542 406.38 0.1983
178.85 0.0062 296.13 0.0632 409.34 0.2094
185.47 0.0074 308.40 0.0721 413.34 0.2204
188.78 0.0086 319.64 0.0813 415.68 0.2333
194.98 0.0099 330.53 0.0902 417.62 0.2471
197.40 0.0112 340.74 0.0993 418.24 0.2568
200.91 0.0125 350.67 0.1086

Table 60. Test data for specimen P22T–12

Test Number : 066 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 167.0 MPa Ultimate Stress : 436.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

130.91 0.0009 268.41 0.0233 395.75 0.1236

153.22 0.0015 277.06 0.0282 399.34 0.1286
163.93 0.0019 285.77 0.0337 403.47 0.1335
174.58 0.0026 296.03 0.0405 407.24 0.1393
183.67 0.0034 304.54 0.0461 411.61 0.1450
195.59 0.0050 315.14 0.0538 414.86 0.1495
203.53 0.0058 320.76 0.0580 418.07 0.1533
211.42 0.0063 325.59 0.0620 421.65 0.1645
218.28 0.0069 333.05 0.0683 424.69 0.1706
224.89 0.0074 341.35 0.0749 428.54 0.1836
230.92 0.0080 350.28 0.0819 430.45 0.1904
239.05 0.0098 357.50 0.0881 432.49 0.1978
244.67 0.0121 365.29 0.0947 434.25 0.2047
253.04 0.0154 376.10 0.1022 435.40 0.2131
261.70 0.0198 387.44 0.1140 436.23 0.2183

A–3 0
Table 61. Test data for specimen P24A–30

Test Number : 072 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 142.4 MPa Ultimate Stress : 432.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

131.1300 0.0010 256.7900 0.0283 375.0100 0.1331

140.8100 0.0014 260.6500 0.0311 381.8400 0.1423
150.2400 0.0020 264.3600 0.0336 389.1000 0.1534
157.8500 0.0025 269.0900 0.0375 395.7200 0.1641
164.8200 0.0033 273.1500 0.0401 400.1100 0.1726
178.3500 0.0056 283.6000 0.0478 404.0900 0.1813
184.0400 0.0069 289.0800 0.0517 408.2200 0.1913
190.3500 0.0091 294.0900 0.0561 412.8200 0.2031
196.1700 0.0115 301.9000 0.0625 416.9400 0.2131
204.0100 0.0131 314.8300 0.0730 420.8400 0.2262
209.8700 0.0140 327.0800 0.0861 422.4100 0.2322
220.8700 0.0158 334.2300 0.0925 426.1600 0.2507
228.2500 0.0170 341.9300 0.0989 428.3100 0.2628
233.0900 0.0180 345.6800 0.1004 430.0600 0.2746
239.4400 0.0202 361.3300 0.1163 431.4700 0.2825
251.7600 0.0252 364.5300 0.1201 432.1300 0.2978

Table 62. Test data for specimen P24A–33

Test Number : 266 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 149.1 MPa Ultimate Stress : 425.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

40.469 0.0002 174.335 0.0071 377.208 0.1414

62.385 0.0002 191.185 0.0125 387.253 0.1546
72.151 0.0002 224.120 0.0276 391.765 0.1609
99.523 0.0004 228.372 0.0300 403.010 0.1784
107.616 0.0005 255.185 0.0450 404.316 0.1805
114.890 0.0005 274.007 0.0561 411.705 0.1958
120.765 0.0007 316.520 0.0848 415.330 0.2043
125.966 0.0009 324.415 0.0910 415.990 0.2064
134.208 0.0013 345.233 0.1085 422.545 0.2264
141.149 0.0018 347.565 0.1106 424.256 0.2331
169.298 0.0057 370.991 0.1344 425.780 0.2460

A–3 1
Table 63. Test data for specimen P24T–06

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 160.4 MPa Ultimate Stress : 447.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

40.40 0.0002 215.12 0.0125 371.63 0.1019

64.26 0.0004 219.32 0.0138 381.56 0.1110
90.32 0.0005 223.46 0.0151 389.90 0.1202
113.35 0.0008 226.98 0.0163 398.52 0.1296
131.69 0.0014 244.56 0.0239 405.83 0.1391
147.00 0.0021 263.10 0.0324 412.86 0.1488
160.37 0.0030 280.69 0.0409 420.37 0.1588
170.99 0.0040 297.03 0.0494 425.27 0.1691
180.99 0.0051 310.95 0.0580 430.23 0.1796
187.95 0.0062 324.88 0.6670 434.58 0.1905
192.85 0.0073 339.08 0.0754 439.06 0.2019
199.53 0.0086 349.70 0.0841 440.92 0.2138
204.71 0.0099 361.70 0.0930 443.82 0.2269
209.19 0.0112

Table 64. Test data for specimen P24A–05

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Y : 146.6 MPa Ultimate Stress : 430.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

56.54 0.0003 207.05 0.0169 365.42 0.1241

87.77 0.0006 212.70 0.0184 374.52 0.1340
115.07 0.0011 215.19 0.0198 381.62 0.1442
133.07 0.0020 218.22 0.0212 389.14 0.1546
146.58 0.0030 236.83 0.0300 395.07 0.1650
157.48 0.0041 255.45 0.0395 401.69 0.1757
166.30 0.0053 271.58 0.0489 406.79 0.1868
173.47 0.0066 287.24 0.0581 411.69 0.1980
180.37 0.0080 299.16 0.0673 416.37 0.2096
186.02 0.0095 312.95 0.0767 420.37 0.2218
190.09 0.0109 325.02 0.0860 423.34 0.2342
195.60 0.0124 336.46 0.0953 425.41 0.2470
200.15 0.0139 347.50 0.1048 427.75 0.2608
202.91 0.0154 357.42 0.1144 428.92 0.2753

A–3 2
Table 65. Test data for specimen 693–40

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 278.8 MPa Ultimate Stress : 606.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.62 0.0001 360.73 0.0266 562.20 0.3066

34.27 0.0002 389.00 0.0449 570.20 0.3265
73.77 0.0004 412.44 0.0630 573.02 0.3465
118.45 0.0007 433.40 0.0811 578.88 0.3669
143.34 0.0008 450.64 0.0991 583.23 0.3876
195.81 0.0012 464.64 0.1172 586.61 0.4084
219.46 0.0015 481.32 0.1356 590.95 0.4294
239.87 0.0020 492.84 0.1539 592.88 0.4509
258.35 0.0026 505.25 0.1725 597.02 0.4728
274.20 0.0034 515.11 0.1912 599.50 0.4952
288.27 0.0043 523.45 0.2099 600.88 0.5182
296.89 0.0053 532.07 0.2289 601.98 0.5421
305.85 0.0064 541.79 0.2480 605.98 0.5671
312.13 0.0075 551.17 0.2675 604.26 0.5947
316.95 0.0088 555.37 0.2869 580.26 0.6277

Table 66. Test data for specimen 693–41

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 273.4 MPa Ultimate Stress : 583.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

20.55 0.0001 316.12 0.0103 543.86 0.2884

63.98 0.0004 354.46 0.0275 546.89 0.3056
112.25 0.0006 380.66 0.0443 559.44 0.3421
136.86 0.0008 399.62 0.0609 564.06 0.3600
166.37 0.0010 418.79 0.0772 564.89 0.3780
192.78 0.0012 434.30 0.0935 567.44 0.3963
218.08 0.0016 448.71 0.1096 572.13 0.4150
241.52 0.0021 462.71 0.1258 572.47 0.4339
255.80 0.0028 472.98 0.1419 576.06 0.4531
273.38 0.0037 485.18 0.1581 578.61 0.4727
283.24 0.0046 492.63 0.1742 579.02 0.4830
294.06 0.0056 503.87 0.1903 580.54 0.5144
299.09 0.0067 511.45 0.2065 579.99 0.5383
305.78 0.0079 518.83 0.2227 530.90 0.5798
310.54 0.0091 532.07 0.2553

A–3 3
Table 67. Test data for specimen 694–30

Test Number : 213 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 253.6 MPa Ultimate Stress : 592.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.064 0.0001 304.492 0.0131 471.595 0.1353

28.651 0.0002 309.672 0.0149 486.665 0.1520
39.172 0.0003 325.290 0.0214 503.595 0.1729
83.755 0.0006 357.123 0.0389 511.477 0.1834
95.319 0.0007 370.342 0.0475 534.831 0.2191
106.981 0.0008 385.662 0.0581 546.581 0.2396
156.728 0.0013 417.769 0.0835 559.996 0.2673
168.547 0.0014 427.478 0.0919 569.543 0.2912
201.697 0.0020 442.337 0.1053 570.326 0.2934
211.739 0.0022 457.774 0.1206 585.602 0.3471
275.974 0.0063 469.930 0.1331 592.701 0.4041

Table 68. Test data for specimen 694–31

Test Number : 214 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 264.1 MPa Ultimate Stress : 588.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.244 0.0001 353.863 0.0233 490.937 0.1322

30.299 0.0002 371.853 0.0323 508.542 0.1564
75.004 0.0004 376.140 0.0346 514.150 0.1651
86.479 0.0005 387.844 0.0413 529.756 0.1913
134.548 0.0008 391.394 0.0436 537.120 0.2055
146.345 0.0009 405.317 0.0527 538.046 0.2075
202.168 0.0015 424.102 0.0663 541.167 0.2142
266.385 0.0037 443.453 0.0823 557.456 0.2551
288.237 0.0056 453.475 0.0915 561.650 0.2671
293.641 0.0062 467.432 0.1053 574.865 0.3158
316.566 0.0103 477.244 0.1161 586.472 0.3843

A–3 4
Table 69. Test data for specimen 69–135

Test Number : 212 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 244.7 MPa Ultimate Stress : 600.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.941 0.0001 373.098 0.0399 537.746 0.2300

28.372 0.0002 395.391 0.0539 559.708 0.2875
39.164 0.0003 401.251 0.0579 560.534 0.2896
82.127 0.0006 427.169 0.0780 561.166 0.2916
93.196 0.0007 443.763 0.0931 564.956 0.3041
162.694 0.0014 463.539 0.1132 567.920 0.3145
201.857 0.0022 488.281 0.1438 578.707 0.3584
244.583 0.0039 506.308 0.1703 581.234 0.3689
250.010 0.0042 514.908 0.1846 590.514 0.4220
286.788 0.0077 515.880 0.1867 599.746 0.5053
310.806 0.0127 522.828 0.1990 600.670 0.5351

Table 70. Test data for specimen 694–21

Test Number : 129 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 286.7 MPa Ultimate Stress : 624.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 337.70 0.0100 516.64 0.1202

25.29 0.0001 355.85 0.0139 540.48 0.1493
25.78 0.0001 375.32 0.0230 563.50 0.1909
202.11 0.0028 401.68 0.0314 562.73 0.1925
220.67 0.0031 423.52 0.0439 587.68 0.2523
220.47 0.0032 456.54 0.0688 609.91 0.3300
278.46 0.0047 478.25 0.0847 624.63 0.4169
314.64 0.0073 492.58 0.0976

A–3 5
Table 71. Test data for specimen 694–25

Test Number : 138 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 232.1 MPa Ultimate Stress : 585.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 345.97 0.0272 489.97 0.1759

63.76 0.0002 367.11 0.0422 511.55 0.2187
196.90 0.0020 391.60 0.0609 528.74 0.2605
216.59 0.0026 423.07 0.0910 559.66 0.3535
270.79 0.0047 458.08 0.1248 578.29 0.4746
286.44 0.0066 478.44 0.1529 578.29 0.4747
310.53 0.0112 483.92 0.1637 585.42 0.5537
329.69 0.0183

Table 72. Test data for specimen 692–40

Test Number : 169 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 289.6 MPa Ultimate Stress : 622.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 359.36 0.0145 519.97 0.1109

167.41 0.0011 380.55 0.0207 549.61 0.1450
259.45 0.0032 416.48 0.0366 587.78 0.2024
296.75 0.0050 464.10 0.0662 606.17 0.2396
318.41 0.0069 488.56 0.0849 624.50 0.3420
336.94 0.0094

Table 73. Test data for specimen 692–41

Test Number : 158 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 269.4 MPa Ultimate Stress : 604.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 360.37 0.0128 490.75 0.0851

216.85 0.0011 375.03 0.0172 500.69 0.0948
249.30 0.0017 395.81 0.0250 542.63 0.1332
281.66 0.0029 410.58 0.0325 571.23 0.1713
302.70 0.0058 436.92 0.0470 591.06 0.2121
312.62 0.0049 454.19 0.0585 603.15 0.2525
323.14 0.0060 470.45 0.0702 604.40 0.2857
342.94 0.0091

A–3 6
Table 74. Test data for specimen 69–245

Test Number : 160 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 272.5 MPa Ultimate Stress : 485.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 341.82 0.0144 450.74 0.0793

124.00 0.0006 360.03 0.0205 469.20 0.0961
250.85 0.0030 381.06 0.0299 480.46 0.1091
292.97 0.0059 394.62 0.0379 483.88 0.1156
314.66 0.0086 409.01 0.0475 485.82 0.1185
330.39 0.0113 426.91 0.0601

Table 75. Test data for specimen 691–28

Test Number : 290 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 291.6 MPa Ultimate Stress : 637.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

20.217 0.0001 285.141 0.0031 513.943 0.0884

49.211 0.0002 291.618 0.0034 529.028 0.1031
59.313 0.0003 319.590 0.0049 531.148 0.1053
103.425 0.0005 327.870 0.0055 549.125 0.1258
114.924 0.0005 371.732 0.0111 559.101 0.1388
126.683 0.0006 438.943 0.0350 560.643 0.1410
197.707 0.0011 442.567 0.0370 572.643 0.1583
208.454 0.0012 469.498 0.0532 603.488 0.2156
218.725 0.0013 472.467 0.0553 610.958 0.2338
263.449 0.0023 489.364 0.0676 623.247 0.2704
271.030 0.0026 492.111 0.0697 635.055 0.3245

A–3 7
Table 76. Test data for specimen 691–29

Test Number : 291 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 287.7 MPa Ultimate Stress : 650.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

18.324 0.0001 299.056 0.0040 549.087 0.1246

32.816 0.0001 304.902 0.0043 562.486 0.1418
64.389 0.0003 342.600 0.0072 571.594 0.1548
74.794 0.0003 354.210 0.0087 585.186 0.1767
110.034 0.0005 382.322 0.0140 591.499 0.1877
133.886 0.0006 393.706 0.0172 606.777 0.2188
181.445 0.0009 448.784 0.0407 611.645 0.2300
192.641 0.0010 475.489 0.0572 620.031 0.2518
203.393 0.0012 495.205 0.0718 638.007 0.3117
249.839 0.0021 510.290 0.0844 640.658 0.3235
258.027 0.0024 528.122 0.1013 650.490 0.3993

Table 77. Test data for specimen 69–230

Test Number : 292 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 298.8 MPa Ultimate Stress : 669.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

20.574 0.0001 401.408 0.0192 550.954 0.1236

67.134 0.0004 407.220 0.0213 567.002 0.1424
78.055 0.0004 431.264 0.0317 578.039 0.1570
89.323 0.0005 435.510 0.0338 595.389 0.1823
174.631 0.0011 447.375 0.0401 601.702 0.1929
186.713 0.0012 461.207 0.0484 615.293 0.2182
230.179 0.0018 471.063 0.0547 623.245 0.2351
295.588 0.0037 486.085 0.0651 633.992 0.2607
301.988 0.0040 505.073 0.0797 649.511 0.3080
390.983 0.0158 526.230 0.0984 652.450 0.3190
396.420 0.0175 537.074 0.1088 669.415 0.4275

A–3 8
Table 78. Test data for specimen 692–25

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 285.4 MPa Ultimate Stress : 633.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

17.03 0.0002 315.99 0.0060 575.44 0.2356

30.96 0.0003 326.54 0.0069 582.26 0.2567
48.61 0.0003 332.19 0.0078 588.74 0.2782
69.15 0.0004 337.15 0.0088 597.09 0.2997
93.77 0.0006 397.28 0.0281 600.95 0.3215
116.52 0.0007 430.58 0.0488 606.33 0.3434
143.89 0.0009 457.81 0.0694 611.70 0.3655
168.58 0.0011 479.94 0.0899 615.43 0.3878
195.19 0.0014 501.25 0.1105 617.98 0.4106
222.70 0.0018 516.14 0.1311 622.18 0.4338
243.38 0.0023 529.10 0.1518 624.67 0.4572
262.97 0.0029 543.65 0.1725 625.91 0.4813
279.79 0.0035 553.92 0.1934 629.35 0.5058
292.96 0.0043 565.85 0.2145 631.01 0.5310
305.92 0.0051

Table 79. Test data for specimen 692–26

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 2,570
Yield Stress : 302.6 MPa Ultimate Stress : 648.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

56.26 0.0002 342.05 0.0068 599.71 0.2514

77.77 0.0003 348.46 0.0077 607.43 0.2711
100.32 0.0005 403.96 0.0252 612.39 0.2911
126.93 0.0006 438.30 0.0441 619.15 0.3113
156.37 0.0007 464.91 0.0628 624.46 0.3319
184.30 0.0009 489.53 0.0815 629.08 0.3527
209.12 0.0012 506.42 0.1000 631.01 0.3740
235.18 0.0015 522.69 0.1187 635.49 0.3957
252.90 0.0019 536.21 0.1374 639.28 0.4179
273.31 0.0024 550.96 0.1561 641.76 0.4405
288.48 0.0030 561.85 0.1749 643.97 0.4642
302.61 0.0036 573.92 0.1938 643.83 0.4884
317.09 0.0043 582.26 0.2128 693.74 0.5142
326.33 0.0051 591.71 0.2320 693.51 0.5423
334.60 0.0059

A–3 9
Table 80. Test data for specimen 694–06

Test Number : 130 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 292.1 MPa Ultimate Stress : 652.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 424.24 0.0347 586.25 0.1890

52.67 0.0002 446.83 0.0477 598.94 0.2068
205.14 0.0024 472.38 0.0649 613.91 0.2894
300.54 0.0049 479.82 0.0705 627.40 0.2075
333.72 0.0076 490.91 0.0808 635.87 0.3284
352.83 0.0102 516.46 0.0999 643.32 0.3695
374.54 0.0151 539.41 0.1211 651.98 0.4355
397.47 0.0223 567.83 0.1593 652.00 0.4794
397.98 0.0225

Table 81. Test data for specimen 694–07

Test Number : 131 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 266.2 MPa Ultimate Stress : 635.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 351.64 0.0125 522.00 0.1168

48.83 0.0000 375.73 0.0192 521.61 0.1170
190.46 0.0014 394.91 0.0266 546.67 0.1430
205.90 0.0019 413.76 0.0361 575.73 0.1892
219.80 0.0021 432.19 0.0471 600.01 0.2344
224.58 0.0021 457.56 0.0635 616.14 0.2782
282.30 0.0038 479.87 0.0794 625.95 0.3272
311.61 0.0063 490.93 0.0897 635.48 0.3858
336.66 0.0096

A–4 0
Table 82. Test data for specimen 694–08

Test Number : 224 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 246.8 MPa Ultimate Stress : 619.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

29.804 0.0001 251.978 0.0037 489.372 0.1201

57.140 0.0003 257.323 0.0040 505.084 0.1375
69.410 0.0003 290.110 0.0073 529.567 0.1677
114.844 0.0006 295.546 0.0081 540.362 0.1829
126.319 0.0007 300.549 0.0090 580.171 0.2557
139.722 0.0008 323.287 0.0140 584.943 0.2668
151.033 0.0009 356.050 0.0254 600.606 0.3117
193.474 0.0015 383.049 0.0383 609.329 0.3458
202.824 0.0016 387.059 0.0405 615.161 0.3782
211.624 0.0019 428.034 0.0664 615.547 0.3805
246.493 0.0033 450.503 0.0840 619.932 0.4381

Table 83. Test data for specimen 69–119

Test Number : 134 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 249.6 MPa Ultimate Stress : 617.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.15 0.0000 371.71 0.0220 517.93 0.1238

61.59 0.0002 398.15 0.0329 540.92 0.1492
198.49 0.0023 418.93 0.0460 567.66 0.1938
212.81 0.0025 443.63 0.0641 584.92 0.2359
288.30 0.0051 468.44 0.0800 602.70 0.3007
318.24 0.0090 474.73 0.0861 605.60 0.2987
338.72 0.0117 475.41 0.0858 617.30 0.3745
358.66 0.0183 487.14 0.0970

A–4 1
Table 84. Test data for specimen 693–12

Test Number : 194 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 270.9 MPa Ultimate Stress : 674.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

12.191 0.0001 302.570 0.0057 598.040 0.1585

56.631 0.0005 311.152 0.0063 599.509 0.1606
78.604 0.0006 319.010 0.0070 627.808 0.2077
89.895 0.0007 354.996 0.0113 647.783 0.2552
149.801 0.0011 372.959 0.0147 648.713 0.2574
161.836 0.0012 423.485 0.0298 652.826 0.2706
173.532 0.0013 428.640 0.0318 659.240 0.2929
184.754 0.0015 502.373 0.0696 662.863 0.3086
240.357 0.0027 550.452 0.1062 663.205 0.3109
247.857 0.0030 579.534 0.1354 666.143 0.3245
292.043 0.0050 584.919 0.1417 673.683 0.4037

Table 85. Test data for specimen 693–13

Test Number : 195 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 259.2 MPa Ultimate Stress : 655.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.518 0.0001 306.978 0.0074 557.880 0.1354

29.428 0.0002 341.770 0.0124 583.972 0.1679
39.967 0.0003 352.485 0.0145 593.580 0.1824
82.031 0.0006 358.620 0.0160 603.382 0.1991
92.775 0.0007 392.335 0.0267 615.038 0.2223
103.705 0.0008 413.189 0.0350 622.500 0.2394
183.741 0.0016 451.464 0.0536 629.231 0.2582
193.934 0.0017 482.282 0.0718 630.157 0.2604
242.138 0.0030 501.307 0.0850 641.667 0.2995
284.841 0.0054 523.790 0.1026 642.155 0.3017
292.874 0.0060 545.883 0.1229 649.860 0.3381

A–4 2
Table 86. Test data for specimen 69–130

Test Number : 196 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 258.4 MPa Ultimate Stress : 661.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

13.002 0.0001 527.036 0.1119 628.924 0.2825

56.794 0.0005 544.148 0.1288 632.775 0.2970
67.314 0.0006 548.340 0.1335 635.798 0.3095
125.726 0.0009 594.653 0.1979 641.355 0.3369
231.806 0.0023 596.846 0.2019 642.135 0.3390
276.315 0.0043 601.234 0.2105 644.280 0.3541
334.991 0.0091 607.815 0.2248 646.961 0.3694
370.451 0.0159 612.739 0.2358 648.424 0.3825
397.157 0.0254 617.468 0.2479 652.275 0.4205
407.375 0.0300 618.930 0.2519 653.543 0.4434
511.631 0.0982 627.608 0.2784 654.566 0.4810

Table 87. Test data for specimen 692–16

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 253.6 MPa Ultimate Stress : 638.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

5.35 0.0003 308.82 0.0080 579.50 0.2027

57.02 0.0004 318.06 0.0091 589.16 0.2191
78.12 0.0005 323.50 0.0101 595.98 0.2352
102.04 0.0006 378.80 0.0250 601.84 0.2514
123.90 0.0007 416.99 0.0412 609.01 0.2676
148.65 0.0009 444.57 0.0573 614.05 0.2839
174.09 0.0011 468.36 0.0734 618.46 0.3000
198.84 0.0015 487.87 0.0893 621.91 0.3161
218.70 0.0020 507.11 0.1054 624.39 0.3320
237.52 0.0027 521.86 0.1215 629.15 0.3478
253.59 0.0035 538.69 0.1377 632.04 0.3634
268.21 0.0043 551.51 0.1540 635.15 0.3787
279.93 0.0052 560.61 0.1702 635.83 0.3935
291.37 0.0061 571.30 0.1865 636.52 0.4076
300.20 0.0070

A–4 3
Table 88. Test data for specimen 692–17

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570
Yield Stress : 300.9 MPa Ultimate Stress : 683.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

37.16 0.0002 338.33 0.0061 619.98 0.1643

57.09 0.0003 347.08 0.0070 630.73 0.1774
77.36 0.0004 356.18 0.0080 637.28 0.1907
98.80 0.0005 409.76 0.0198 643.56 0.2042
124.24 0.0006 446.57 0.0330 650.45 0.2178
147.75 0.0007 474.22 0.0459 658.38 0.2318
174.71 0.0009 497.53 0.0586 661.48 0.2462
201.88 0.0011 520.07 0.0714 665.83 0.2608
226.35 0.0014 538.83 0.0840 670.86 0.2761
249.93 0.0017 554.82 0.0967 673.62 0.2915
267.38 0.0022 571.30 0.1093 676.38 0.3074
285.93 0.0028 584.88 0.1221 677.89 0.3253
300.89 0.0036 597.22 0.1397 680.72 0.3420
315.57 0.0043 607.08 0.1517 681.41 0.3592
325.98 0.0051

Table 89. Test data for specimen 692-15

Test Number : 132 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 287.8 MPa Ultimate Stress : 673.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 402.17 0.0234 588.75 0.1456

48.36 0.0003 422.54 0.0303 614.28 0.1803
204.28 0.0028 440.75 0.0392 637.49 0.2198
220.26 0.0030 459.56 0.0486 639.37 0.2202
280.31 0.0050 474.81 0.0582 656.16 0.2726
310.80 0.0067 484.83 0.0662 669.09 0.3230
336.12 0.0089 522.63 0.0900 673.06 0.3595
356.52 0.0123 554.65 0.1125 673.92 0.3920
380.47 0.0170

A–4 4
Table 90. Test data for specimen 692–22

Test Number : 133 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 278.6 MPa Ultimate Stress : 699.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 436.88 0.0271 623.56 0.1674

38.38 0.0003 463.13 0.0381 640.99 0.1934
208.64 0.0027 478.68 0.0460 659.25 0.2328
221.35 0.0030 490.47 0.0543 671.26 0.2732
307.54 0.0057 532.36 0.0824 690.36 0.3315
360.78 0.0101 561.09 0.0998 697.69 0.3936
395.49 0.0154 585.36 0.1218 699.13 0.4474
417.65 0.0208 597.45 0.1338

Table 91. Test data for specimen 692–23

Test Number : 230 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 260.5 MPa Ultimate Stress : 664.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

33.299 0.0002 338.892 0.0101 586.626 0.1587

49.029 0.0003 361.067 0.0140 589.529 0.1629
74.030 0.0004 393.989 0.0228 599.642 0.1780
85.676 0.0005 454.954 0.0488 611.060 0.1975
147.160 0.0009 458.695 0.0508 618.851 0.2128
159.290 0.0010 486.807 0.0673 627.753 0.2327
171.333 0.0011 516.370 0.0877 633.076 0.2460
245.169 0.0028 536.450 0.1042 642.172 0.2731
252.088 0.0031 543.418 0.1104 657.656 0.3407
277.017 0.0044 564.078 0.1313 661.188 0.3663
287.836 0.0051 578.449 0.1481 664.043 0.4000

A–4 5
Table 92. Test data for specimen 69–109

Test Number : 135 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 276.7 MPa Ultimate Stress : 688.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 431.75 0.0220 627.12 0.2021

43.64 0.0003 461.67 0.0470 651.41 0.2642
203.61 0.0031 479.14 0.0574 665.36 0.3196
305.80 0.0065 492.48 0.0667 674.17 0.3623
344.05 0.0100 542.45 0.0988 678.09 0.3952
377.06 0.0149 573.46 0.1271 685.21 0.4499
405.86 0.0221 601.41 0.1597 688.02 0.5581

Table 93. Test data for specimen 691–04

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 271.3 MPa Ultimate Stress : 691.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

37.58 0.0000 325.78 0.0068 606.46 0.1622

54.19 0.0003 387.69 0.0158 615.01 0.1738
73.43 0.0004 424.23 0.0267 622.60 0.1854
94.80 0.0005 452.99 0.0378 629.22 0.1970
118.73 0.0006 475.26 0.0489 632.39 0.2085
143.20 0.0007 494.56 0.0601 641.35 0.2203
169.47 0.0010 514.14 0.0712 646.73 0.2322
192.98 0.0012 530.69 0.0824 649.56 0.2442
213.46 0.0016 199.67 0.0728 656.59 0.2559
233.87 0.0021 543.38 0.0936 658.59 0.2669
251.66 0.0026 558.75 0.1049 663.48 0.2779
266.55 0.0032 571.30 0.1162 666.65 0.2894
282.06 0.0039 579.78 0.1278 97.19 0.3008
294.13 0.0045 589.57 0.1392 97.74 0.3109
305.78 0.0053 599.02 0.1507 97.83 0.3197
316.47 0.0060

A–4 6
Table 94. Test data for specimen 691–05

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570
Yield Stress : 263.1 MPa Ultimate Stress : 664.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

2.86 0.0000 307.37 0.0058 612.53 0.2132

5.20 0.0002 315.02 0.0065 620.25 0.2318
55.09 0.0003 324.54 0.0073 628.25 0.2505
76.95 0.0004 334.19 0.0081 634.18 0.2695
101.77 0.0004 402.17 0.0217 639.97 0.2886
126.52 0.0006 441.68 0.0379 643.69 0.3080
150.65 0.0007 470.22 0.0547 647.42 0.3275
173.95 0.0009 496.84 0.0718 652.11 0.3474
197.33 0.0013 518.07 0.0890 655.55 0.3674
216.77 0.0017 539.38 0.1064 657.69 0.3880
236.83 0.0023 554.61 0.1238 659.83 0.4089
253.66 0.0029 569.02 0.1414 660.10 0.4303
269.59 0.0036 582.06 0.1591 661.00 0.4525
281.17 0.0042 594.60 0.1770 662.10 0.4761
296.13 0.0050 603.36 0.1950

Table 95. Test data for specimen 693–42

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 190.8 MPa Ultimate Stress : 420.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

38.40 0.0002 221.11 0.0099 367.35 0.1210

62.81 0.0003 223.25 0.0111 374.66 0.1298
88.25 0.0004 225.67 0.0122 382.25 0.1407
116.38 0.0006 244.35 0.0204 386.04 0.1510
143.76 0.0009 261.66 0.0296 391.14 0.1606
162.03 0.0013 277.17 0.0386 397.69 0.1704
175.33 0.0019 290.34 0.0477 399.96 0.1792
186.50 0.0026 304.27 0.0568 402.38 0.1917
193.74 0.0035 315.50 0.0658 409.00 0.1998
201.60 0.0045 327.29 0.0748 409.76 0.2107
206.22 0.0055 337.84 0.0837 410.17 0.2202
209.95 0.0066 346.88 0.0928 412.10 0.2340
213.19 0.0076 352.87 0.1024 415.00 0.2410
217.87 0.0088 360.66 0.1113 416.31 0.2581

A–4 7
Table 96. Test data for specimen 694–40

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 177.0 MPa Ultimate Stress : 417.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

5.84 0.0002 217.12 0.0120 364.80 0.1259

62.05 0.0003 217.46 0.0134 369.70 0.1357
86.12 0.0003 223.11 0.0143 380.18 0.1476
110.25 0.0006 224.91 0.0156 382.38 0.1598
130.59 0.0009 242.97 0.0248 388.52 0.1707
148.72 0.0014 262.83 0.0351 393.48 0.1830
166.03 0.0021 278.69 0.0451 399.62 0.1924
178.92 0.0030 293.30 0.0551 402.03 0.2047
188.50 0.0040 306.13 0.0652 405.20 0.2206
195.74 0.0051 318.88 0.0753 407.48 0.2323
198.71 0.0065 330.60 0.0853 409.20 0.2450
206.43 0.0078 338.12 0.0950 411.55 0.2557
206.77 0.0093 347.43 0.1052 411.13 0.2715
214.22 0.0106 356.46 0.1155 413.62 0.2897

Table 97. Test data for specimen 694–32

Test Number : 255 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 176.8 MPa Ultimate Stress : 401.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

92.1209 0.0003 196.3262 0.0070 335.6876 0.0945

101.7914 0.0004 201.4223 0.0085 365.2161 0.1293
112.1934 0.0005 207.0842 0.0108 368.0202 0.1315
131.3247 0.0006 243.0889 0.0287 379.9242 0.1488
147.5982 0.0008 255.0904 0.0352 378.3051 0.1510
154.0403 0.0012 258.7821 0.0373 388.0293 0.1683
159.5851 0.0014 266.2142 0.0419 391.2138 0.1726
167.7292 0.0019 289.8515 0.0572 397.4559 0.1860
174.1713 0.0024 305.3058 0.0684 395.7735 0.1931
190.5912 0.0054 313.5523 0.0748 400.2844 0.2048
326.3536 0.0858 401.8791 0.2168

A–4 8
Table 98. Test data for specimen 694-33

Test Number : 256 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 173.0 MPa Ultimate Stress : 386.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

40.677 0.0002 183.059 0.0043 311.235 0.0687

77.338 0.0001 188.797 0.0053 314.099 0.0708
86.362 0.0002 193.883 0.0065 327.536 0.0815
105.077 0.0003 199.723 0.0080 346.024 0.0987
114.923 0.0005 205.021 0.0097 355.618 0.1093
139.343 0.0007 210.938 0.0119 366.011 0.1221
145.909 0.0011 221.791 0.0164 370.124 0.1287
151.739 0.0012 231.511 0.0210 375.045 0.1351
156.810 0.0015 264.427 0.0384 377.498 0.1415
164.711 0.0020 279.195 0.0470 385.428 0.1618
176.450 0.0031 296.023 0.0579 386.580 0.1705

Table 99. Test data for specimen 69-236

Test Number : 254 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 194.1 MPa Ultimate Stress : 440.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

29.931 0.0002 260.447 0.0256 402.820 0.1400

128.317 0.0004 278.262 0.0348 416.634 0.1681
153.637 0.0006 293.774 0.0434 422.237 0.1748
160.551 0.0008 314.841 0.0562 427.859 0.1856
177.960 0.0015 327.460 0.0649 427.540 0.1966
185.697 0.0019 336.252 0.0711 428.628 0.1989
191.963 0.0026 354.730 0.0862 430.196 0.2013
208.602 0.0053 368.481 0.0989 435.668 0.2148
214.752 0.0069 379.193 0.1098 438.387 0.2264
220.210 0.0085 393.975 0.1292 437.134 0.2355
236.327 0.0145 395.983 0.1313 437.841 0.2444

A–4 9
Table 100. Test data for specimen 694–26

Test Number : 093 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 174.4 MPa Ultimate Stress : 408.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

138.84 0.0010 265.70 0.0209 356.35 0.0886

160.95 0.0016 269.89 0.0232 359.43 0.0914
167.45 0.0019 274.99 0.0261 368.11 0.0972
173.71 0.0021 278.60 0.0284 370.90 0.1000
179.57 0.0025 283.15 0.0313 378.15 0.1079
185.44 0.0030 291.95 0.0367 380.44 0.1108
197.02 0.0044 299.03 0.0418 388.90 0.1219
207.49 0.0053 303.34 0.0449 394.34 0.1299
217.36 0.0060 307.25 0.0478 396.33 0.1330
227.69 0.0070 312.20 0.0518 399.83 0.1394
236.43 0.0083 323.14 0.0601 401.68 0.1426
242.41 0.0101 332.16 0.0677 404.39 0.1490
248.98 0.0127 335.03 0.0702 405.75 0.1522
252.15 0.0140 344.10 0.0777 406.52 0.1557
257.29 0.0163 346.68 0.0800 407.38 0.1584
260.90 0.0183 353.77 0.0861 408.66 0.1643

Table 101. Test data for specimen 694–27

Test Number : 094 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 183.5 MPa Ultimate Stress : 422.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

146.2500 0.0011 272.5800 0.0190 382.9700 0.0966

165.8300 0.0016 276.2900 0.0207 391.2300 0.1026
192.3000 0.0030 289.1900 0.0275 398.8000 0.1111
204.5200 0.0039 293.6400 0.0300 406.0500 0.1209
217.7800 0.0045 303.1800 0.0355 410.6100 0.1286
224.7300 0.0050 311.4900 0.0408 412.9100 0.1319
235.6900 0.0060 464.0200 0.0456 416.2700 0.1375
241.1200 0.0070 326.2900 0.0506 418.5200 0.1408
246.4500 0.0087 334.9000 0.0571 419.8900 0.1488
252.7700 0.0108 342.1100 0.0623 420.7900 0.1547
257.1700 0.0124 348.4300 0.0671 421.5300 0.1583
261.1700 0.0139 355.2700 0.0726 422.4500 0.1621
265.0200 0.0155 365.4400 0.0809 422.8100 0.1716
268.6800 0.0172 375.4200 0.0895

A–5 0
Table 102. Test data for specimen 692–42

Test Number : 173 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 178.5 MPa Ultimate Stress : 423.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 220.77 0.0069 328.14 0.0550

32.82 0.0000 225.25 0.0079 335.92 0.0603
87.60 0.0003 232.51 0.0096 343.22 0.0654
122.11 0.0007 244.00 0.0129 356.66 0.0752
147.65 0.0012 246.99 0.0140 365.52 0.0821
166.30 0.0017 251.47 0.0153 373.47 0.0883
174.93 0.0020 255.50 0.0169 380.38 0.0937
178.85 0.0022 259.44 0.0185 383.34 0.0965
187.88 0.0027 264.02 0.0202 389.76 0.1002
194.33 0.0033 279.22 0.0272 398.90 0.1098
198.16 0.0037 289.34 0.0326 406.36 0.1197
202.33 0.0041 297.11 0.0367 412.27 0.1287
208.24 0.0049 310.43 0.0442 416.28 0.1365
213.17 0.0056 319.00 0.0493 420.05 0.1444
215.60 0.0060 321.95 0.0514 423.15 0.1633

Table 103. Test data for specimen 694–39

Test Number : 179 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 168.2 MPa Ultimate Stress : 413.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 221.61 0.0109 342.46 0.0788

38.24 0.0000 225.99 0.0124 356.38 0.0897
77.18 0.0003 230.03 0.0137 362.54 0.0945
118.92 0.0009 233.81 0.0153 370.79 0.0999
142.34 0.0014 242.89 0.0185 377.89 0.1069
154.72 0.0018 246.67 0.0203 386.27 0.1162
166.44 0.0024 255.09 0.0238 391.19 0.1222
177.42 0.0031 263.06 0.0277 399.65 0.1348
183.21 0.0037 267.79 0.0302 403.16 0.1411
188.10 0.0043 275.61 0.0344 406.77 0.1481
197.17 0.0055 281.19 0.0374 409.33 0.1544
202.51 0.0065 286.87 0.0411 411.89 0.1614
207.90 0.0076 301.45 0.0499 413.02 0.1666
212.68 0.0085 311.21 0.0560 413.54 0.1712
217.02 0.0096 328.38 0.0683 413.84 0.1796

A–5 1
Table 104. Test data for specimen 69–246

Test Number : 180 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 165.5 MPa Ultimate Stress : 423.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 226.65 0.0109 333.06 0.0719

38.39 0.0000 233.55 0.0131 336.77 0.0751
88.32 0.0003 241.50 0.0160 342.78 0.0801
125.36 0.0008 251.71 0.0205 353.04 0.0882
151.10 0.0014 263.56 0.0261 366.00 0.0976
164.85 0.0020 273.17 0.0310 380.33 0.1127
175.80 0.0025 281.62 0.0363 388.44 0.1227
184.49 0.0031 285.82 0.0389 397.96 0.1349
190.74 0.0036 291.13 0.0422 402.18 0.1416
198.19 0.0045 300.58 0.0482 408.70 0.1540
203.84 0.0054 304.64 0.0512 412.71 0.1631
210.14 0.0065 307.84 0.0535 418.09 0.1773
212.44 0.0070 312.19 0.0568 419.24 0.1818
216.34 0.0080 318.80 0.0616 422.96 0.1947
220.29 0.0091 322.65 0.0645 423.02 0.1987

Table 105. Test data for specimen 692–28

Test Number : 322 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 55,000 h
Yield Stress : 209.1 MPa Ultimate Stress : 462.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

40.830 0.0001 231.050 0.0052 404.400 0.0993

107.640 0.0002 248.300 0.0089 422.080 0.1191
118.020 0.0003 253.150 0.0102 430.380 0.1302
127.670 0.0004 274.850 0.0178 437.620 0.1412
153.380 0.0006 300.340 0.0291 442.680 0.1501
161.060 0.0007 318.020 0.0380 448.180 0.1612
168.070 0.0009 337.670 0.0490 452.890 0.1724
187.220 0.0016 348.550 0.0556 453.660 0.1746
197.770 0.0020 368.160 0.0687 456.090 0.1812
220.280 0.0038 382.460 0.0795 459.530 0.1923
225.950 0.0044 387.760 0.0839 462.410 0.2119

A–5 2
Table 106. Test data for specimen 692–29

Test Number : 323 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 55,000 h
Yield Stress : 212.3 MPa Ultimate Stress : 464.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.50 0.0001 313.79 0.0358 436.19 0.1390

52.59 0.0002 330.08 0.0447 441.32 0.1479
107.64 0.0002 348.55 0.0556 442.68 0.1501
153.38 0.0006 355.38 0.0598 447.10 0.1590
187.22 0.0016 368.16 0.0687 449.08 0.1634
197.77 0.0020 374.18 0.0730 452.89 0.1724
220.28 0.0038 382.46 0.0795 453.66 0.1746
225.95 0.0044 387.76 0.0839 456.09 0.1812
231.05 0.0052 395.23 0.0905 456.81 0.1835
248.30 0.0089 404.40 0.0993 459.07 0.1901
253.15 0.0102 412.71 0.1081 459.53 0.1923
269.03 0.0155 414.79 0.1102 461.46 0.2002
274.85 0.0178 422.08 0.1191 461.52 0.2026
290.71 0.0246 423.95 0.1212 462.28 0.2096
300.34 0.0291 430.38 0.1302 462.41 0.2119

Table 107. Test data for specimen 69–130

Test Number : 321 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 55,000 h
Yield Stress : 209.1 MPa Ultimate Stress : 468.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.9900 0.0001 297.9800 0.0256 442.2700 0.1422

51.6000 0.0002 316.5400 0.0345 444.7000 0.1465
82.8700 0.0003 329.1100 0.0410 448.3000 0.1534
137.9900 0.0007 348.1400 0.0519 450.4400 0.1577
164.9200 0.0011 361.8000 0.0606 451.5000 0.1599
193.2100 0.0019 368.2400 0.0650 453.4500 0.1644
199.1900 0.0021 380.1900 0.0738 456.9800 0.1734
204.5900 0.0025 391.1000 0.0825 457.7800 0.1757
224.7700 0.0042 396.1400 0.0870 460.0000 0.1824
236.0400 0.0056 398.6300 0.0891 461.3400 0.1870
242.8700 0.0067 405.5600 0.0956 462.8300 0.1937
260.3900 0.0111 414.1800 0.1044 463.0500 0.1957
266.0500 0.0127 427.2600 0.1198 464.1600 0.2028
271.3400 0.0146 433.7100 0.1288 464.3300 0.2052
287.6800 0.0210 436.8000 0.1332

A–5 3
Table 108. Test data for specimen 692–27

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 173.1 MPa Ultimate Stress : 451.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

30.96 0.0002 218.91 0.0095 396.24 0.1123

53.09 0.0003 224.15 0.0107 402.79 0.1220
78.81 0.0005 229.60 0.0118 411.62 0.1316
100.80 0.0006 230.77 0.0129 418.44 0.1416
122.04 0.0010 254.55 0.0213 420.92 0.1519
139.62 0.0015 276.89 0.0305 426.30 0.1607
154.79 0.0021 295.79 0.0395 433.68 0.1711
168.65 0.0027 312.68 0.0485 435.96 0.1819
180.44 0.0035 328.95 0.0574 437.47 0.1949
191.47 0.0044 341.84 0.0663 443.26 0.2042
198.29 0.0054 354.46 0.0754 444.16 0.2147
204.36 0.0064 366.53 0.0844 445.40 0.2278
209.81 0.0074 376.66 0.0936 448.23 0.2386
214.98 0.0084 386.52 0.1029

Table 109. Test data for specimen 694–09

Test Number : 084 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 156.4 MPa Ultimate Stress : 413.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

123.82 0.0008 285.16 0.0396 384.24 0.1428

135.09 0.0011 288.91 0.0425 388.55 0.1516
145.72 0.0014 292.03 0.0451 392.78 0.1621
179.65 0.0034 297.24 0.0497 396.40 0.1704
184.07 0.0039 318.71 0.0680 399.99 0.1807
187.95 0.0044 322.01 0.0713 402.35 0.1886
197.82 0.0059 328.13 0.0044 404.54 0.1971
209.48 0.0070 331.83 0.0064 405.67 0.2006
250.46 0.0161 334.79 0.0835 410.36 0.2219
254.22 0.0183 342.03 0.0902 410.65 0.2254
257.59 0.0205 351.67 0.0984 411.35 0.2291
261.58 0.0233 354.18 0.1012 411.80 0.2324
264.56 0.0251 362.98 0.1120 412.14 0.2359
271.69 0.0300 368.77 0.1199 413.13 0.2504
278.33 0.0344 370.36 0.1223

A–5 4
Table 110. Test data for specimen 69–120

Test Number : 085 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 179.8 MPa Ultimate Stress : 429.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

136.20 0.0012 280.83 0.0234 384.06 0.0967

155.69 0.0017 288.57 0.0269 386.73 0.0978
163.40 0.0020 292.45 0.0293 388.24 0.0997
169.57 0.0023 300.51 0.0341 394.84 0.1057
181.02 0.0028 321.25 0.0472 400.41 0.1116
190.90 0.0035 327.47 0.0516 404.27 0.1186
200.80 0.0042 332.17 0.0563 406.32 0.1205
213.12 0.0047 336.71 0.0598 417.53 0.1375
223.46 0.0051 341.63 0.0630 418.61 0.1406
233.17 0.0058 347.16 0.0666 423.94 0.1475
237.09 0.0064 352.21 0.0711 424.93 0.1505
241.80 0.0075 357.79 0.0753 426.86 0.1582
245.58 0.0089 359.94 0.0773 427.76 0.1623
268.51 0.0176 374.46 0.0886 428.79 0.1649
272.59 0.0200 379.16 0.0925 429.62 0.1680

Table 111. Test data for specimen 693–14

Test Number : 243 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 186.4 MPa Ultimate Stress : 457.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

41.930 0.0002 222.230 0.0082 340.870 0.0606

44.020 0.0002 227.610 0.0095 358.140 0.0714
72.230 0.0002 232.580 0.0110 367.790 0.0779
82.970 0.0002 254.330 0.0181 370.810 0.0800
104.380 0.0003 265.620 0.0227 395.940 0.1000
115.300 0.0004 270.950 0.0249 413.610 0.1151
150.160 0.0008 295.360 0.0360 423.500 0.1263
156.440 0.0011 299.860 0.0382 434.790 0.1416
162.130 0.0014 321.040 0.0492 441.260 0.1783
187.280 0.0029 324.970 0.0513 445.890 0.1869
199.740 0.0044 328.880 0.0536 456.860 0.2177

A–5 5
Table 112. Test data for specimen 693–15

Test Number : 245 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 195.8 MPa Ultimate Stress : 444.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

82.970 0.0002 199.740 0.0044 336.470 0.0582

93.520 0.0003 209.870 0.0059 340.870 0.0606
115.300 0.0004 216.440 0.0071 358.140 0.0714
125.980 0.0005 222.230 0.0082 370.810 0.0800
143.140 0.0007 232.580 0.0110 395.940 0.1000
150.160 0.0008 238.500 0.0129 425.300 0.1285
162.130 0.0014 249.310 0.0163 427.020 0.1307
167.380 0.0016 265.620 0.0227 434.790 0.1416
180.180 0.0025 270.950 0.0249 439.950 0.1761
187.280 0.0029 299.860 0.0382 448.150 0.1914
193.920 0.0036 321.040 0.0492 451.500 0.2004
456.860 0.2177

Table 113. Test data for specimen 69–270

Test Number : 235 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 193.6 MPa Ultimate Stress : 462.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

82.606 0.0001 228.049 0.0085 395.334 0.0963

95.725 0.0002 234.184 0.0103 413.701 0.1135
108.530 0.0002 277.671 0.0264 429.263 0.1313
143.211 0.0003 306.192 0.0395 437.264 0.1421
149.390 0.0005 310.405 0.0415 440.550 0.1470
160.181 0.0006 327.972 0.0507 444.849 0.1536
176.370 0.0014 335.471 0.0551 452.378 0.1682
183.372 0.0019 346.937 0.0616 453.404 0.1704
200.800 0.0036 356.335 0.0677 456.180 0.1769
205.624 0.0043 367.072 0.0747 461.617 0.1955
211.986 0.0052 387.093 0.0896 462.441 0.2042

A–5 6
Table 114. Test data for specimen 692–18

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 163.9 MPa Ultimate Stress : 444.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

86.25 0.0002 233.32 0.0099 384.31 0.0873

108.04 0.0005 237.94 0.0108 391.21 0.0936
127.83 0.0009 257.24 0.0164 397.21 0.1000
145.27 0.0015 274.69 0.0230 403.89 0.1066
160.58 0.0022 290.75 0.0295 410.65 0.1131
173.06 0.0029 304.75 0.0361 414.03 0.1197
184.30 0.0037 316.47 0.0425 420.17 0.1265
194.23 0.0045 328.74 0.0489 424.72 0.1332
203.26 0.0053 340.19 0.0554 429.06 0.1402
210.36 0.0062 349.15 0.0618 430.72 0.1472
216.84 0.0071 357.84 0.0682 435.75 0.1544
223.39 0.0080 367.77 0.0746 437.54 0.1618
228.42 0.0089 376.38 0.0809

Table 115. Test data for specimen 692–24

Test Number : 078 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 173.3 MPa Ultimate Stress : 494.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

140.73 0.0007 317.37 0.0229 461.09 0.1205

156.38 0.0012 322.53 0.0249 466.65 0.1281
172.08 0.0017 327.39 0.0268 468.26 0.1305
207.80 0.0034 334.90 0.0301 474.50 0.1394
226.34 0.0038 342.76 0.0344 475.86 0.1426
238.59 0.0044 349.63 0.0383 486.49 0.1584
245.57 0.0050 367.64 0.0486 486.86 0.1622
255.51 0.0061 375.24 0.0531 489.64 0.1719
264.06 0.0075 392.99 0.0648 491.96 0.1770
268.78 0.0082 403.24 0.0715 492.83 0.1794
299.05 0.0163 416.33 0.0811 493.41 0.1818
303.87 0.0180 439.77 0.0983 493.88 0.1844
308.58 0.0195 448.48 0.1067 494.54 0.1875
313.34 0.0212 456.50 0.1149 494.22 0.1914

A–5 7
Table 116. Test data for specimen 69–110

Test Number : 079 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 196.9 MPa Ultimate Stress : 481.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

160.02 0.0019 289.49 0.0156 435.97 0.1017

167.34 0.0022 296.70 0.0180 446.92 0.1135
180.56 0.0028 302.91 0.0200 452.79 0.1209
198.25 0.0037 317.92 0.0264 460.29 0.1310
211.86 0.0042 329.33 0.0318 463.60 0.1362
225.14 0.0045 341.63 0.0386 466.27 0.1410
243.42 0.0056 352.95 0.0445 470.77 0.1497
248.87 0.0061 357.77 0.0473 473.15 0.1542
256.00 0.0074 362.99 0.0506 475.87 0.1620
260.72 0.0085 378.40 0.0606 478.16 0.1701
266.72 0.0097 394.94 0.0716 480.01 0.1788
272.41 0.0110 407.10 0.0808 481.00 0.1823
277.15 0.0122 416.71 0.0875 481.56 0.1897
282.46 0.0135 426.51 0.0956 481.39 0.1945

Table 117. Test data for specimen 691–06

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 177.7 MPa Ultimate Stress : 479.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

44.40 0.0003 244.83 0.0095 418.30 0.0858

69.36 0.0003 250.49 0.0106 425.89 0.0928
97.15 0.0004 255.73 0.0115 432.71 0.0997
121.28 0.0008 260.83 0.0125 441.06 0.1066
140.31 0.0012 283.24 0.0181 446.37 0.1138
157.48 0.0019 306.27 0.0248 452.71 0.1208
170.09 0.0025 324.19 0.3160 457.40 0.1280
182.78 0.0033 339.50 0.3830 461.26 0.1353
195.67 0.0041 353.98 0.0451 466.43 0.1425
206.22 0.0049 366.73 0.0518 468.43 0.1500
216.22 0.0059 378.38 0.0586 472.36 0.1577
223.60 0.0067 389.76 0.0655 474.22 0.1655
231.11 0.0077 399.69 0.0723 476.77 0.1739
238.08 0.0086 409.76 0.0790

A–5 8
Table 118. Test data for specimen 692–09

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 175.7 MPa Ultimate Stress : 477.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

2.92 0.0002 218.70 0.0074 408.65 0.0914

23.44 0.0002 226.42 0.0084 418.58 0.0998
40.40 0.0004 232.01 0.0094 426.23 0.1086
59.50 0.0005 238.35 0.0105 433.40 0.1176
81.29 0.0007 243.80 0.0115 440.85 0.1268
104.04 0.0009 271.86 0.0180 447.88 0.1361
120.24 0.0014 296.68 0.0261 451.81 0.1457
141.07 0.0019 317.92 0.0340 455.95 0.1553
156.30 0.0025 334.67 0.0421 460.23 0.1653
169.34 0.0032 349.84 0.0500 464.43 0.1755
180.57 0.0040 363.97 0.0580 466.78 0.1861
192.85 0.0047 376.73 0.0661 471.12 0.1971
202.02 0.0056 387.55 0.0744 474.36 0.2090
210.36 0.0065 398.52 0.0828 475.05 0.2219

Table 119. Test data for specimen 18–11

Test Number : 001 Test Temp. : 25°C

Aging Temp. : 280°C Aging Time : 68,000 h
Yield Stress : 306.2 MPa Ultimate Stress : 554.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

48.09 0.0000 287.83 0.0037 424.09 0.0559

84.24 0.0002 293.75 0.0040 442.61 0.0788
107.98 0.0005 303.24 0.0044 457.71 0.0977
131.91 0.0007 307.15 0.0046 464.98 0.1083
155.85 0.0011 312.18 0.0048 469.05 0.1153
179.66 0.0015 317.03 0.0050 473.27 0.1224
203.60 0.0019 321.96 0.0052 482.07 0.1402
215.66 0.0019 326.61 0.0055 499.86 0.1778
227.53 0.0021 336.68 0.0062 515.08 0.2170
233.61 0.0021 348.23 0.0071 525.78 0.2579
239.97 0.0022 357.04 0.0082 531.32 0.2791
249.70 0.0024 363.74 0.0093 532.42 0.3007
256.30 0.0026 373.20 0.0117 546.59 0.3914
265.98 0.0029 378.00 0.0135 553.42 0.4691
275.32 0.0032 383.90 0.0165 553.66 0.4791
278.40 0.0033 394.22 0.0240 554.08 0.4840
283.24 0.0035 410.58 0.0399 554.87 0.4891

A–5 9
Table 120. Test data for specimen 18–12

Test Number : 002 Test Temp. : 25°C

Aging Temp. : 280°C Aging Time : 68,000 h
Yield Stress : 288.5 MPa Ultimate Stress : 555.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.90 0.0000 336.25 0.0074 485.06 0.0940

32.56 0.0001 341.27 0.0080 494.87 0.1032
54.54 0.0003 350.19 0.0090 505.27 0.1157
95.04 0.0008 359.80 0.0099 518.78 0.1330
148.66 0.0017 365.26 0.0112 528.90 0.1481
201.65 0.0024 379.81 0.0154 535.04 0.1613
210.18 0.0025 389.69 0.0190 540.25 0.1711
227.65 0.0027 404.24 0.0258 547.31 0.1880
237.14 0.0033 422.76 0.0380 551.00 0.2022
238.48 0.0033 442.28 0.0532 554.99 0.2214
250.50 0.0034 460.52 0.0701 556.14 0.2421
287.81 0.0048 479.33 0.0888 556.32 0.2550
312.16 0.0059

Table 121. Test data for specimen 18–22

Test Number : 003 Test Temp. : 25°C

Aging Temp. : 280°C Aging Time : 68,000 h
Yield Stress : 291.9 MPa Ultimate Stress : 568.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

23.90 0.0000 313.52 0.0075 419.35 0.0572

48.59 0.0003 323.34 0.0087 457.49 0.0934
97.26 0.0009 332.66 0.0099 481.22 0.1144
145.01 0.0018 337.20 0.0107 484.37 0.1155
193.33 0.0030 347.14 0.0129 512.14 0.1563
241.06 0.0036 356.58 0.0161 537.27 0.2026
265.32 0.0046 365.48 0.0196 552.11 0.2431
289.62 0.0059 380.58 0.0276 558.67 0.2798
304.09 0.0068 394.97 0.0370 568.94 0.3292

A–6 0
Table 122. Test data for specimen 13–12

Test Number : 028 Test Temp. : 25°C

Aging Temp. : Reannealed Aging Time :–
Yield Stress : 317.3 MPa Ultimate Stress : 567.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

59.50 0.0001 352.87 0.0067 496.24 0.1460

99.30 0.0003 357.20 0.0073 510.41 0.1747
133.00 0.0006 361.96 0.0080 522.24 0.2028
163.07 0.0010 367.66 0.0091 529.11 0.2228
193.54 0.0016 372.86 0.0108 536.15 0.2462
201.94 0.0018 378.36 0.0130 542.22 0.2717
215.15 0.0020 385.83 0.0168 547.41 0.2928
229.30 0.0021 398.00 0.0259 552.36 0.3249
237.36 0.0022 415.43 0.0421 558.66 0.3637
280.74 0.0031 434.03 0.0634 562.70 0.4037
300.55 0.0036 449.93 0.0811 566.12 0.4461
319.41 0.0043 464.70 0.0982 567.34 0.4761
332.93 0.0050 474.03 0.1080 567.40 0.4995
346.78 0.0061 478.62 0.1167

Table 123. Test data for specimen 13–21

Test Number : 02 6 Test Temp. : 25°C

Aging Temp. : Reannealed Aging Time :–
Yield Stress : 289.2 MPa Ultimate Stress : 575.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

43.57 0.0000 347.01 0.0081 488.50 0.0968

85.02 0.0002 353.99 0.0092 505.80 0.1120
130.85 0.0006 360.46 0.0107 523.90 0.1343
179.40 0.0014 368.83 0.0131 543.60 0.1667
232.59 0.0022 379.05 0.0167 555.16 0.1962
262.35 0.0028 388.82 0.0210 564.90 0.2333
276.49 0.0032 403.16 0.0286 571.38 0.2689
297.17 0.0040 421.66 0.0407 573.98 0.2871
310.87 0.0046 436.44 0.0518 573.92 0.2947
322.33 0.0053 453.33 0.0654 574.89 0.3157
331.48 0.0062 470.21 0.0788 575.17 0.3364
339.10 0.0070 483.57 0.0905 575.22 0.3509

A–6 1
Table 124. Test data for specimen 13–22

Test Number : 027 Test Temp. : 25°C

Aging Temp. : Reannealed Aging Time :–
Yield Stress : 287.7 MPa Ultimate Stress : 531.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

44.21 0.0000 331.47 0.0081 442.35 0.0957

85.37 0.0003 336.80 0.0093 455.83 0.1097
131.85 0.0008 341.69 0.0105 468.19 0.1252
174.19 0.0014 346.72 0.0124 473.23 0.1269
196.69 0.0019 354.13 0.0158 477.17 0.1347
214.31 0.0022 360.84 0.0195 478.12 0.1390
230.61 0.0024 370.52 0.0259 492.78 0.1656
260.12 0.0031 383.34 0.0361 504.02 0.1894
290.13 0.0042 394.21 0.0455 516.50 0.2247
302.55 0.0048 413.05 0.0640 526.42 0.2619
312.26 0.0056 429.39 0.0806 530.27 0.2926
320.50 0.0064 434.61 0.0856 531.25 0.3066
327.75 0.0074 436.25 0.0876

Table 125. Test data for specimen 15–11

Test Number : 057a Test Temp. : 290°C

Aging Temp. : 280°C Aging Time : 68,000 h
Yield Stress : 214.0 MPa Ultimate Stress : 469.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

48.99 0.0000 278.02 0.0076 438.50 0.1433

83.20 0.0002 281.34 0.0085 443.15 0.1514
122.05 0.0006 284.82 0.0095 452.28 0.1714
162.68 0.0013 287.99 0.0104 460.92 0.1953
189.28 0.0019 294.38 0.0127 466.31 0.2175
195.54 0.0021 319.77 0.0266 468.95 0.2414
201.11 0.0024 333.17 0.0365 468.76 0.2577
213.49 0.0026 348.54 0.0493 460.47 0.2747
220.74 0.0028 365.08 0.0638 434.38 0.2978
235.41 0.0030 380.97 0.0782 387.87 0.3198
245.10 0.0034 390.25 0.0864 308.74 0.3294
252.35 0.0039 402.23 0.0982 269.78 0.3309
260.15 0.0045 410.60 0.1048 213.57 0.3327
265.27 0.0052 420.39 0.1163 166.50 0.3340
271.57 0.0062 429.58 0.1286 156.46 0.3341

A–6 2
Table 126. Test data for specimen 15–12

Test Number : 056 Test Temp. : 290°C

Aging Temp. : 280°C Aging Time : 68,000 h
Yield Stress : 208.4 MPa Ultimate Stress : 444.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.39 0.0000 243.65 0.0045 355.26 0.0853

83.04 0.0003 247.23 0.0052 367.60 0.0977
119.69 0.0007 251.20 0.0060 374.04 0.1017
140.89 0.0010 255.94 0.0073 384.35 0.1144
158.51 0.0014 260.29 0.0086 392.07 0.1237
177.59 0.0019 264.10 0.0100 407.55 0.1429
186.93 0.0022 267.86 0.0116 413.00 0.1531
200.26 0.0026 270.93 0.0131 423.69 0.1712
208.37 0.0028 274.64 0.0149 429.49 0.1877
214.65 0.0029 278.49 0.0171 432.18 0.1915
219.32 0.0031 285.89 0.0220 435.42 0.1987
228.30 0.0033 294.90 0.0285 437.28 0.2026
235.71 0.0036 308.51 0.0400 441.72 0.2144
238.60 0.0039 325.75 0.0560 440.08 0.2189
240.86 0.0042 342.68 0.0724 444.39 0.2366

Table 127. Test data for specimen 15–21

Test Number : 057b Test Temp. : 290°C

Aging Temp. : 280°C Aging Time : 68,000 h
Yield Stress : 199.6 MPa Ultimate Stress : 482.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.08 0.0000 250.40 0.0075 433.07 0.1692

94.79 0.0003 257.78 0.0102 440.72 0.1815
146.04 0.0010 264.58 0.0134 447.58 0.1937
162.41 0.0013 274.87 0.0188 453.33 0.2104
178.43 0.0017 293.17 0.0310 460.34 0.2232
189.53 0.0020 309.98 0.0435 463.99 0.2327
192.57 0.0022 321.99 0.0535 469.40 0.2442
195.81 0.0024 334.15 0.0638 472.72 0.2647
206.61 0.0027 348.83 0.0767 475.88 0.2751
211.14 0.0029 365.16 0.0909 477.68 0.2832
215.98 0.0031 380.65 0.1025 480.52 0.2991
224.75 0.0034 402.73 0.1264 480.74 0.3092
233.03 0.0038 411.79 0.1389 481.60 0.3166
238.07 0.0043 426.78 0.1597 482.51 0.3284
243.35 0.0054

A–6 3
Table 128. Test data for specimen 15–22

Test Number : 058 Test Temp. : 290°C

Aging Temp. : 280°C Aging Time : 68,000 h
Yield Stress : 180.2 MPa Ultimate Stress : 434.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

34.92 0.0000 204.38 0.0055 364.37 0.1249

81.09 0.0003 209.24 0.0059 370.79 0.1328
120.94 0.0009 214.55 0.0065 375.87 0.1406
144.27 0.0014 220.45 0.0072 381.69 0.1491
159.54 0.0019 227.00 0.0080 391.10 0.1642
165.71 0.0021 237.95 0.0098 399.87 0.1797
172.82 0.0024 252.42 0.0181 401.75 0.1814
178.83 0.0027 264.31 0.0273 409.03 0.1954
184.30 0.0032 277.23 0.0387 411.64 0.2005
186.79 0.0034 288.27 0.0491 419.25 0.2181
190.91 0.0038 302.62 0.0627 422.72 0.2286
194.69 0.0043 314.15 0.0741 426.14 0.2408
196.38 0.0045 326.02 0.0859 428.19 0.2480
199.56 0.0050 330.52 0.0903 431.89 0.2636
201.99 0.0053 347.48 0.1053 434.03 0.2816

Table 129. Test data for specimen 16–21

Test Number : 060 Test Temp. : 290°C

Aging Temp. : Reannealed Aging Time :–
Yield Stress : 184.0 MPa Ultimate Stress : 405.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

73.83 0.0002 263.54 0.0096 427.35 0.0939

105.52 0.0006 274.92 0.0124 446.96 0.1061
127.98 0.0009 285.57 0.0155 462.80 0.1199
141.76 0.0012 294.26 0.0185 473.64 0.1309
156.10 0.0016 301.80 0.0212 482.97 0.1419
167.01 0.0020 317.07 0.0277 483.46 0.1437
176.70 0.0024 343.30 0.0410 485.46 0.1484
191.30 0.0033 363.02 0.0523 494.14 0.1610
202.85 0.0039 379.90 0.0624 500.51 0.1719
226.10 0.0048 395.39 0.0723 504.16 0.1812
240.81 0.0057 414.01 0.0844 505.94 0.1900
251.80 0.0072 432.47 0.0972

A–6 4
Table 130. Test data for specimen 17–21

Test Number : 059 Test Temp. : 290°C

Aging Temp. : Reannealed Aging Time :–
Yield Stress : 171.5 MPa Ultimate Stress : 416.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

47.67 0.0000 206.10 0.0063 371.77 0.1798

85.55 0.0003 208.03 0.0065 379.86 0.1942
114.31 0.0007 210.94 0.0070 386.78 0.2092
140.22 0.0012 220.28 0.0086 390.72 0.2216
156.57 0.0017 230.71 0.0105 393.02 0.2293
164.89 0.0020 246.73 0.0207 395.16 0.2356
173.91 0.0024 259.45 0.0331 400.01 0.2503
180.02 0.0028 270.48 0.0460 403.95 0.2639
185.68 0.0033 286.56 0.0643 406.29 0.2704
189.43 0.0039 301.82 0.0830 410.18 0.2900
193.47 0.0045 316.97 0.0985 412.48 0.3016
195.79 0.0050 330.80 0.1155 414.70 0.3139
198.36 0.0056 340.41 0.1284 416.19 0.3330
201.41 0.0059 348.69 0.1405
203.83 0.0061 358.81 0.1550

Table 131. Test data for specimen P13T–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 244.7 MPa Ultimate Stress : 584.5 MPa

Experimental Data Not Available.

Table 132. Test data for specimen P13T–03

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 245.9 MPa Ultimate Stress : 579.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

10.20 0.0002 136.31 0.0010 263.38 0.0053

18.68 0.0003 156.17 0.0012 270.48 0.0062
28.96 0.0003 175.54 0.0014 275.72 0.0070
37.78 0.0003 192.16 0.0017 279.72 0.0078
54.26 0.0004 210.08 0.0021 285.65 0.0087
68.95 0.0005 224.70 0.0026 288.20 0.0095
84.25 0.0006 236.15 0.0031 291.72 0.0104
100.11 0.0007 247.80 0.0038 296.68 0.0113
118.59 0.0008 256.76 0.0045 298.06 0.0123

A–6 5
Table 133. Test data for specimen P11A–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Y – MPa Ultimate Stress : 584.9 MPa

Experimental Data Not Available.

Table 134. Test data for specimen P13A–01

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 248.5 MPa Ultimate Stress : 584.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

17.93 0.0002 125.42 0.0008 275.79 0.0067

20.96 0.0002 143.20 0.0009 280.62 0.0076
23.44 0.0002 162.65 0.0011 285.79 0.0084
26.89 0.0002 181.81 0.0014 288.20 0.0093
29.30 0.0002 197.95 0.0017 292.06 0.0102
30.89 0.0002 214.36 0.0021 295.92 0.0111
33.09 0.0003 228.63 0.0025 297.16 0.0120
34.89 0.0003 239.11 0.0030 300.96 0.0130
53.57 0.0004 249.93 0.0037 303.30 0.0139
70.95 0.0005 257.45 0.0043 305.51 0.0149
86.32 0.0005 264.55 0.0051 309.44 0.0159
104.39 0.0006 271.52 0.0059 310.40 0.0168

Table 135. Test data for specimen P14T–09

Test Number : 117 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 266.2 MPa Ultimate Stress : 596.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 398.64 0.0486 545.00 0.2716

77.21 0.0002 422.46 0.0680 559.25 0.3307
212.73 0.0018 442.43 0.0858 561.89 0.3462
258.67 0.0025 465.90 0.1064 566.23 0.3725
291.99 0.0042 478.01 0.1209 577.95 0.4433
311.40 0.0062 481.09 0.1354 591.37 0.5609
326.33 0.0093 481.39 0.1361 590.97 0.5612
354.39 0.0201 507.72 0.1791 595.58 0.6312
354.49 0.0204 529.83 0.2271 596.15 0.6717
380.79 0.0348 537.08 0.2433

A–6 6
Table 136. Test data for specimen P11A–25

Test Number : 102 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 285.7 MPa Ultimate Stress : 595.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 327.99 0.0134 485.84 0.1723

68.60 0.0002 330.65 0.0149 503.01 0.2040
147.31 0.0010 391.70 0.0575 524.41 0.2531
181.90 0.0016 395.97 0.0605 546.10 0.3130
205.98 0.0015 410.10 0.0741 557.67 0.3579
222.63 0.0017 420.72 0.0850 564.19 0.3855
258.83 0.0025 431.76 0.0957 575.74 0.4433
283.36 0.0036 445.71 0.1083 582.95 0.4831
299.93 0.0050 445.67 0.1083 590.96 0.5406
307.02 0.0061 467.17 0.1347 595.22 0.6055
311.57 0.0060 483.61 0.1593

Table 137. Test data for specimen P14A–26

Test Number : 104 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 276.5 MPa Ultimate Stress : 575.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

73.86 0.0001 360.33 0.0196 494.94 0.1349

202.47 0.0013 391.83 0.0374 512.42 0.1575
219.88 0.0015 422.46 0.0598 537.40 0.2028
230.30 0.0016 442.39 0.0783 553.09 0.2403
269.71 0.0022 457.87 0.0911 564.42 0.2757
296.90 0.0035 469.61 0.0986 569.81 0.3036
314.51 0.0054 480.19 0.1109 573.78 0.3211
330.05 0.0088 488.72 0.1263 575.68 0.3664
345.39 0.0137

A–6 7
Table 138. Test data for specimen P11A–28

Test Number : 284 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 58,000 h
Yield Stress : 263.5 MPa Ultimate Stress : 536.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

18.772 0.0001 323.730 0.0296 492.111 0.2443

41.505 0.0002 353.702 0.0567 498.424 0.2577
53.992 0.0003 377.558 0.0811 510.328 0.2873
111.117 0.0006 379.486 0.0833 514.377 0.2989
135.575 0.0008 389.501 0.0944 515.051 0.3012
197.871 0.0012 399.024 0.1055 518.666 0.3128
209.283 0.0014 418.340 0.1289 522.281 0.3268
219.264 0.0016 426.745 0.1400 526.040 0.3431
256.470 0.0030 441.324 0.1597 532.642 0.3867
266.986 0.0038 460.765 0.1885 534.233 0.4051
297.088 0.0107 468.973 0.2017 535.968 0.4516

Table 139. Test data for specimen P11A–29

Test Number : 285 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 58,000 h
Yield Stress : 266.1 MPa Ultimate Stress : 562.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.859 0.0001 292.610 0.0071 472.097 0.2052

20.549 0.0001 318.089 0.0177 483.990 0.2298
35.176 0.0002 350.081 0.0412 491.974 0.2477
76.772 0.0004 367.359 0.0571 502.618 0.2745
87.465 0.0004 384.826 0.0751 515.005 0.3103
99.875 0.0005 394.609 0.0864 524.536 0.3420
160.545 0.0008 411.273 0.1068 531.262 0.3672
172.878 0.0009 427.903 0.1300 549.938 0.4652
184.911 0.0010 439.883 0.1481 552.503 0.4836
249.253 0.0025 460.214 0.1828 560.583 0.5582
281.777 0.0050 465.207 0.1917 561.986 0.5795

A–6 8
Table 140. Test data for specimen P11A–10

Test Number : 216 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 279.1 MPa Ultimate Stress : 622.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.015 0.0001 328.678 0.0089 529.516 0.1867

28.397 0.0002 333.701 0.0101 565.073 0.2543
50.324 0.0003 383.033 0.0358 581.929 0.2987
61.112 0.0004 401.113 0.0488 585.086 0.3076
95.717 0.0006 403.974 0.0511 606.216 0.3890
158.146 0.0009 438.987 0.0801 609.713 0.4072
245.309 0.0021 480.820 0.1218 616.368 0.4508
253.270 0.0024 488.276 0.1305 619.088 0.4718
260.644 0.0027 499.011 0.1434 619.137 0.4741
286.243 0.0040 510.523 0.1586 621.274 0.4975
322.655 0.0077 519.558 0.1716 622.537 0.5277

Table 141. Test data for specimen P11T–06

Test Number : 103 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 280.0 MPa Ultimate Stress : 569.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 342.55 0.0035 479.03 0.1020

97.90 0.0002 366.58 0.0043 485.02 0.1088
186.78 0.0011 374.51 0.0049 491.88 0.1191
195.30 0.0013 374.45 0.0048 504.42 0.1376
210.26 0.0016 376.06 0.0061 529.48 0.1813
210.85 0.0017 381.40 0.0094 546.00 0.2204
229.20 0.0017 390.14 0.0159 560.78 0.2703
248.99 0.0020 425.73 0.0470 565.59 0.2916
318.37 0.0029 442.01 0.0635 569.21 0.3316
321.97 0.0031 468.24 0.0982 569.34 0.3603

A–6 9
Table 142. Test data for specimen P14T–08

Test Number : 100 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 279.1 MPa Ultimate Stress : 595.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 379.65 0.0340 515.57 0.1577

130.91 0.0008 393.44 0.0422 521.05 0.1650
195.03 0.0019 404.80 0.0504 528.04 0.1762
218.36 0.0024 416.36 0.0590 536.84 0.1915
242.09 0.0027 426.20 0.0661 543.64 0.2056
251.86 0.0030 431.24 0.0709 485.56 0.2200
261.87 0.0033 451.27 0.0884 560.09 0.2446
271.49 0.0037 460.07 0.0954 570.86 0.2784
280.91 0.0043 465.27 0.0983 581.68 0.3217
295.96 0.0055 471.26 0.1042 583.65 0.3378
314.86 0.0079 478.93 0.1127 585.00 0.3490
329.57 0.0111 492.34 0.1283 585.65 0.3596
339.05 0.0140 498.90 0.1343 587.54 0.3614
354.26 0.0203 506.39 0.1460 588.05 0.3651
367.74 0.0262 509.78 0.1502 589.10 0.3950

Table 143. Test data for specimen P11A–13

Test Number : 281 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 55,000 h
Yield Stress : 299.0 MPa Ultimate Stress : 646.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.902 0.0001 359.101 0.0102 614.679 0.3235

25.967 0.0001 365.251 0.0119 626.149 0.3694
64.721 0.0002 370.441 0.0136 626.631 0.3714
75.416 0.0003 406.347 0.0308 629.764 0.3871
173.574 0.0006 429.615 0.0456 632.222 0.3995
186.428 0.0007 438.753 0.0519 632.752 0.4016
198.896 0.0008 452.705 0.0623 638.632 0.4379
211.070 0.0009 478.162 0.0840 640.994 0.4568
278.813 0.0023 561.231 0.1897 641.524 0.4609
286.481 0.0026 588.172 0.2458 646.006 0.5110
300.163 0.0032 610.534 0.3092 646.777 0.5475

A–7 0
Table 144. Test data for specimen P12A–25

Test Number : 282 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 55,000 h
Yield Stress : 287.6 MPa Ultimate Stress : 688.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

19.268 0.0001 476.490 0.0661 656.994 0.3383

21.177 0.0001 499.011 0.0830 660.127 0.3491
73.420 0.0003 527.735 0.1082 660.657 0.3513
109.798 0.0004 559.062 0.1418 671.067 0.3954
186.235 0.0009 560.845 0.1439 672.465 0.4021
269.237 0.0025 605.956 0.2110 681.333 0.4543
284.794 0.0031 620.848 0.2400 681.622 0.4566
316.501 0.0049 629.330 0.2590 685.333 0.4869
353.028 0.0091 639.451 0.2844 687.261 0.5076
398.963 0.0225 651.259 0.3187 688.032 0.5225
460.710 0.0555 655.259 0.3317 688.321 0.5306

Table 145. Test data for specimen P12T–05

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 276.8 MPa Ultimate Stress : 610.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

49.6422 0.0003 346.8752 0.0156 549.5121 0.2378

82.9439 0.0005 349.8400 0.0172 557.4411 0.2554
121.3477 0.0007 354.0457 0.0188 563.5774 0.2731
161.4062 0.0010 383.6932 0.0355 569.3000 0.2910
197.6727 0.0013 409.3417 0.0526 574.4022 0.3091
229.7333 0.0019 429.8881 0.0690 579.7801 0.3273
255.6576 0.0027 448.2281 0.0853 585.1580 0.3457
276.8245 0.0037 464.0861 0.1019 586.6748 0.3642
294.5440 0.0049 480.0819 0.1184 592.1907 0.3832
307.3683 0.0062 492.0788 0.1352 595.5002 0.4029
316.8141 0.0077 503.7999 0.1520 598.0512 0.4225
325.8462 0.0092 516.0036 0.1690 600.7401 0.4432
330.6036 0.0107 525.1047 0.1860 602.7396 0.4670
337.9810 0.0124 534.6194 0.2031 605.4976 0.4893
341.9799 0.0140 542.3416 0.2204

A–7 1
Table 146. Test data for specimen P12T–06

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 263.4 MPa Ultimate Stress : 608.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

2.42 0.0002 48.37 0.0174 552.27 0.3247

4.53 0.0003 48.85 0.0192 558.20 0.3496
9.51 0.0006 49.33 0.0210 564.82 0.3746
14.84 0.0010 49.67 0.0228 570.89 0.4001
21.36 0.0015 55.26 0.0502 577.64 0.4259
27.03 0.0019 409.62 0.0764 582.47 0.4517
31.95 0.0027 433.89 0.1016 586.67 0.4780
35.57 0.0037 454.50 0.1265 591.23 0.5047
38.61 0.0048 473.81 0.1512 593.78 0.5319
40.95 0.0060 488.56 0.1759 597.71 0.5596
42.94 0.0074 502.35 0.2007 600.88 0.5880
44.43 0.0089 514.28 0.2253 602.95 0.6174
45.41 0.0104 524.69 0.2501 605.43 0.6479
46.52 0.0121 535.38 0.2750 607.01 0.6804
47.03 0.0138 543.31 0.2997 608.74 0.7155
47.88 0.0156

Table 147. Test data for specimen P12A–08

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 290.5 MPa Ultimate Stress : 652.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

33.78 0.0002 357.56 0.0107 590.88 0.2098

64.40 0.0003 361.70 0.0118 599.77 0.2241
98.87 0.0005 366.53 0.0129 605.01 0.2383
135.76 0.0007 398.38 0.0263 612.25 0.2525
171.61 0.0009 427.06 0.0406 617.43 0.2667
207.74 0.0012 449.88 0.0547 621.77 0.2810
238.01 0.0018 469.60 0.0687 626.94 0.2952
262.21 0.0024 487.18 0.0828 629.84 0.3093
282.62 0.0031 503.11 0.0968 633.63 0.3232
298.89 0.0039 519.11 0.1109 637.70 0.3372
311.99 0.0047 533.38 0.1250 640.66 0.3509
324.81 0.0055 545.44 0.1391 643.63 0.3647
334.53 0.0065 555.72 0.1531 645.56 0.3781
341.43 0.0075 567.37 0.1674 646.31 0.3911
347.43 0.0085 576.13 0.1815 649.62 0.4038
353.70 0.0096 584.47 0.1957 649.97 0.4154

A–7 2
Table 148. Test data for specimen P12A–09

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 271.2 MPa Ultimate Stress : 618.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

52.33 0.0003 337.71 0.0125 569.30 0.2471

88.32 0.0005 341.77 0.0135 574.82 0.2621
125.14 0.0007 370.87 0.0289 579.37 0.2771
161.89 0.0010 397.69 0.0458 586.61 0.2918
196.57 0.0013 419.68 0.0624 590.19 0.3064
225.18 0.0018 439.47 0.0785 593.85 0.3209
247.11 0.0025 458.71 0.0944 596.74 0.3352
264.76 0.0033 474.91 0.1099 600.81 0.3494
281.79 0.0042 487.46 0.1255 604.67 0.3632
292.75 0.0052 501.59 0.1408 605.98 0.3770
304.33 0.0063 515.73 0.1561 608.46 0.3905
313.16 0.0074 525.86 0.1714 612.12 0.4034
318.47 0.0084 537.79 0.1866 614.05 0.4159
323.64 0.0093 546.13 0.2017 615.49 0.4278
329.29 0.0103 555.37 0.2169 616.60 0.4387

Table 149. Test data for specimen P12T–11

Test Number : 099 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 266.6 MPa Ultimate Stress : 617.0 MPa

Experimental Data Not Available.

Table 150. Test data for specimen P12A–13

Test Number : 101 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 285.0 MPa Ultimate Stress : 637.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 382.46 0.0223 566.26 0.1812

49.37 0.0000 398.99 0.0318 572.27 0.1902
161.89 0.0009 410.33 0.0397 587.25 0.2119
206.33 0.0016 421.33 0.0475 593.62 0.2245
225.89 0.0019 433.67 0.0575 594.21 0.2286
234.97 0.0019 441.67 0.0635 605.26 0.2540
255.46 0.0024 459.16 0.0774 611.66 0.2733
280.06 0.0031 475.46 0.0900 613.91 0.2805
304.05 0.0042 484.00 0.0975 621.37 0.3072
318.41 0.0052 490.72 0.1026 623.09 0.3087
339.82 0.0081 510.64 0.1197 629.77 0.3427
347.56 0.0094 534.67 0.1421 632.39 0.3721
365.68 0.0148 543.77 0.1509 636.66 0.4754
372.37 0.0177 548.22 0.1572 637.29 0.5645

A–7 3
Table 151. Test data for specimen P12A–14

Test Number : 217 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 263.5 MPa Ultimate Stress : 634.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

10.264 0.0001 342.201 0.0129 596.647 0.2397

50.246 0.0003 394.609 0.0349 597.521 0.2417
95.207 0.0006 415.836 0.0472 602.670 0.2540
109.226 0.0007 451.189 0.0709 610.296 0.2745
122.011 0.0008 467.432 0.0829 615.008 0.2889
184.580 0.0013 480.159 0.0931 621.177 0.3114
206.643 0.0016 489.685 0.1011 623.752 0.3237
241.787 0.0027 529.808 0.1397 630.844 0.3621
262.728 0.0037 531.508 0.1417 632.592 0.3754
281.244 0.0047 546.955 0.1599 632.689 0.3777
291.503 0.0055 562.450 0.1802 637.433 0.4128

Table 152. Test data for specimen P13T–07

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 285.0 MPa Ultimate Stress : 660.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

94.94 0.0004 375.01 0.0145 606.39 0.2093

135.34 0.0005 378.52 0.0159 613.01 0.2243
171.96 0.0006 412.31 0.0281 620.11 0.2396
205.33 0.0010 438.23 0.0417 625.77 0.2551
233.53 0.0015 458.85 0.0552 631.42 0.2708
258.14 0.0022 478.36 0.0687 636.94 0.2868
278.89 0.0031 498.22 0.0823 641.49 0.3033
297.16 0.0042 514.35 0.0957 645.56 0.3200
312.95 0.0053 530.48 0.1094 648.87 0.3370
327.57 0.0064 542.76 0.1232 653.00 0.3544
337.91 0.0077 556.61 0.1371 654.24 0.3724
346.05 0.0089 568.61 0.1512 657.69 0.3907
354.67 0.0103 578.19 0.1655 655.62 0.4099
361.22 0.0117 587.98 0.1797 658.79 0.4301
368.94 0.0131 597.64 0.1944

A–7 4
Table 153. Test data for specimen P13A–07

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 286.3 MPa Ultimate Stress : 677.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

4.14 0.0002 372.59 0.0144 627.49 0.2488

57.36 0.0003 379.00 0.0160 634.39 0.2679
90.39 0.0004 382.93 0.0176 640.66 0.2873
127.55 0.0006 422.79 0.0344 647.69 0.3070
168.03 0.0008 454.99 0.0522 652.52 0.3272
210.15 0.0010 478.36 0.0696 657.07 0.3477
250.56 0.0014 503.80 0.0870 661.41 0.3686
274.07 0.0024 524.97 0.1043 664.10 0.3901
289.37 0.0035 542.76 0.1218 666.59 0.4119
307.09 0.0046 560.20 0.1394 668.17 0.4344
320.88 0.0058 572.82 0.1572 671.55 0.4573
333.84 0.0071 587.30 0.1750 673.14 0.4807
342.88 0.0084 598.88 0.1932 674.24 0.5049
352.32 0.0099 609.36 0.2116 675.69 0.5298
359.15 0.0113 619.22 0.2301 675.96 0.5555
366.66 0.0128

Table 154. Test data for specimen P13T–02

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 148.5 MPa Ultimate Stress : 408.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

19.44 0.0000 119.28 0.0014 179.26 0.0112

22.06 0.0002 130.72 0.0019 181.06 0.0120
25.72 0.0003 140.45 0.0025 183.81 0.0129
29.65 0.0003 146.51 0.0030 185.47 0.0136
35.23 0.0003 152.99 0.0038 186.50 0.0145
39.85 0.0004 156.86 0.0045 188.57 0.0153
40.82 0.0004 161.48 0.0054 189.88 0.0160
45.78 0.0004 164.85 0.0061 191.95 0.0170
51.92 0.0004 166.92 0.0070 192.92 0.0177
57.09 0.0005 170.09 0.0079 195.47 0.0185
62.12 0.0005 172.30 0.0087 196.36 0.0192
67.50 0.0005 174.99 0.0096 198.29 0.0201
83.77 0.0007 176.99 0.0103 199.12 0.0209
102.11 0.0010

A–7 5
Table 155. Test data for specimen P14T–01

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 157.0 MPa Ultimate Stress : 437.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

5.03 0.0000 121.69 0.0024 184.50 0.0096

5.93 0.0002 135.41 0.0031 187.26 0.0103
7.52 0.0002 146.44 0.0039 189.81 0.0112
16.41 0.0003 154.72 0.0044 192.02 0.0121
26.61 0.0005 162.10 0.0050 194.91 0.0129
36.54 0.0006 167.40 0.0055 196.71 0.0138
48.54 0.0008 171.75 0.0063 198.02 0.0147
63.50 0.0010 175.75 0.0071 201.05 0.0156
76.67 0.0012 178.92 0.0078 203.05 0.0166
91.98 0.0015 181.95 0.0087 205.05 0.0173
108.25 0.0019

Table 156. Test data for specimen P11A–02

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 159.9 MPa Ultimate Stress : 442.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

39.99 0.0000 174.37 0.0059 235.32 0.0350

45.16 0.0001 177.61 0.0071 239.32 0.0374
50.68 0.0002 181.26 0.0087 243.45 0.0401
55.36 0.0002 187.12 0.0108 247.04 0.0425
60.88 0.0003 190.43 0.0124 251.18 0.0453
70.26 0.0003 196.02 0.0151 257.52 0.0493
81.36 0.0003 199.81 0.0172 266.76 0.0536
117.42 0.0005 204.64 0.0192 277.86 0.0610
137.76 0.0009 209.67 0.0219 288.82 0.0677
152.72 0.0018 214.01 0.0249 298.96 0.0752
163.61 0.0031 222.56 0.0283 308.40 0.0810
169.06 0.0045 229.60 0.0319

A–7 6
Table 157. Test data for specimen P13A–02

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 155.0 MPa Ultimate Stress : 424.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

4.55 0.0006 139.48 0.0037 179.33 0.0116

9.03 0.0006 148.24 0.0045 181.88 0.0126
19.44 0.0006 155.13 0.0053 184.43 0.0135
33.58 0.0008 160.30 0.0061 186.37 0.0145
50.26 0.0011 164.72 0.0071 188.30 0.0155
65.50 0.0013 168.44 0.0080 190.50 0.0163
83.36 0.0018 171.47 0.0089 192.36 0.0173
99.84 0.0022 174.37 0.0098 194.43 0.0186
113.76 0.0026 177.06 0.0107 196.43 0.0195
128.31 0.0031

Table 158. Test data for specimen P14T–10

Test Number : 263 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 166.1 MPa Ultimate Stress : 415.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

49.686 0.0003 196.581 0.0124 356.289 0.1380

51.137 0.0003 200.884 0.0146 358.380 0.1401
64.981 0.0002 220.424 0.0261 376.128 0.1592
73.645 0.0002 231.175 0.0328 383.481 0.1701
79.114 0.0002 250.488 0.0455 387.668 0.1814
110.354 0.0003 280.509 0.0671 397.185 0.1978
126.569 0.0005 294.898 0.0782 397.773 0.2001
145.661 0.0010 313.219 0.0934 402.525 0.2112
160.219 0.0018 325.714 0.1050 406.577 0.2203
176.655 0.0047 337.274 0.1163 410.779 0.2642
181.604 0.0060 346.762 0.1270 415.188 0.2843

A–7 7
Table 159. Test data for specimen P11A–26

Test Number : 265 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 160.3 MPa Ultimate Stress : 394.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

42.339 0.0002 205.024 0.0281 325.205 0.1856

46.026 0.0002 215.729 0.0372 336.590 0.2027
100.931 0.0004 233.148 0.0528 347.127 0.2183
110.489 0.0005 244.451 0.0633 360.859 0.2450
133.822 0.0008 259.567 0.0782 365.983 0.2559
139.770 0.0010 270.238 0.0891 369.260 0.2627
157.315 0.0022 276.340 0.0955 381.426 0.2957
162.839 0.0029 285.966 0.1060 383.735 0.3046
177.574 0.0089 301.592 0.1241 384.747 0.3067
181.396 0.0109 315.777 0.1397 390.256 0.3254
191.523 0.0175 317.286 0.1419 390.473 0.3319

Table 160. Test data for specimen P14A–27

Test Number : 069 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 167.8 MPa Ultimate Stress : 421.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

134.280 0.0012 265.850 0.0374 376.520 0.1388

146.280 0.0015 277.030 0.0468 381.110 0.1481
161.390 0.0022 287.480 0.0538 383.420 0.1503
169.850 0.0028 302.560 0.0676 393.740 0.1639
181.710 0.0043 313.840 0.0770 401.590 0.1785
194.170 0.0076 326.900 0.0858 403.420 0.1817
197.230 0.0102 339.030 0.0983 408.260 0.1914
204.710 0.0114 350.120 0.1068 412.750 0.2018
212.740 0.0124 360.970 0.1193 417.410 0.2177
239.090 0.0190 366.940 0.1261 420.670 0.2220
243.280 0.0220 368.280 0.1283 421.580 0.2393

A–7 8
Table 161. Test data for specimen P11A–27

Test Number : 315 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 58,000 h
Yield Stress : 167.1 MPa Ultimate Stress : 388.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

42.980 0.0001 204.120 0.0202 328.720 0.1419

54.880 0.0001 229.190 0.0407 336.880 0.1529
97.240 0.0003 236.930 0.0473 347.870 0.1685
107.290 0.0004 249.160 0.0583 353.210 0.1752
116.870 0.0005 251.570 0.0605 361.390 0.1883
145.360 0.0011 263.320 0.0715 362.680 0.1906
150.570 0.0013 272.420 0.0804 370.580 0.2095
158.440 0.0018 285.480 0.0934 372.830 0.2135
182.450 0.0067 294.030 0.1024 378.260 0.2243
187.190 0.0090 312.070 0.1221 382.680 0.2377
191.190 0.0113 323.330 0.1354 387.850 0.2556

Table 162. Test data for specimen P11A–30

Test Number : 314 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 58,000 h
Yield Stress : 179.3 MPa Ultimate Stress : 445.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.878 0.0001 202.720 0.0102 370.226 0.1596

20.989 0.0001 220.071 0.0210 376.627 0.1684
48.486 0.0002 244.253 0.0389 383.251 0.1772
60.940 0.0002 247.113 0.0410 393.064 0.1922
107.906 0.0003 261.265 0.0523 397.907 0.2020
118.106 0.0004 285.056 0.0718 424.204 0.2578
127.299 0.0005 297.408 0.0828 426.516 0.2647
135.616 0.0006 318.571 0.1026 431.229 0.2787
176.196 0.0023 329.685 0.1135 436.938 0.2944
192.908 0.0059 346.387 0.1310 440.770 0.3198
198.148 0.0080 355.396 0.1421 444.927 0.3280

Table 163. Test data for specimen P11A–09

Test Number : 073 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 175.5 MPa Ultimate Stress : 435.1 MPa

Experimental Data Not Available.

A–7 9
Table 164. Test data for specimen P12A–19

Test Number : 074 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 174.8 MPa Ultimate Stress : 456.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

131.38 0.0006 262.30 0.0224 378.76 0.1026

168.14 0.0014 269.07 0.0268 390.99 0.1123
180.81 0.0020 276.04 0.0311 398.61 0.1187
190.28 0.0029 283.06 0.0357 404.47 0.1246
197.47 0.0039 290.72 0.0404 408.04 0.1292
202.65 0.0046 303.47 0.0495 413.26 0.1348
205.37 0.0051 307.01 0.0532 425.04 0.1485
211.97 0.0056 316.34 0.0608 430.30 0.1550
220.18 0.0063 326.74 0.0668 435.21 0.1623
228.18 0.0072 332.58 0.0705 438.72 0.1677
236.77 0.0087 343.90 0.0795 442.50 0.1747
241.73 0.0111 350.90 0.0850 447.03 0.1836
245.57 0.0135 357.43 0.0888 450.03 0.1908
250.99 0.0160 365.46 0.0937 453.65 0.2018
255.46 0.0191 372.84 0.0975 456.90 0.2180

Table 165. Test data for specimen P12A–22

Test Number : 067 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 175.4 MPa Ultimate Stress : 418.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

138.43 0.0011 289.17 0.0404 384.32 0.1234

166.32 0.0019 297.39 0.0463 388.06 0.1280
176.63 0.0025 304.19 0.0518 390.71 0.1316
186.34 0.0033 310.83 0.0574 394.10 0.1367
195.62 0.0045 316.83 0.0621 397.10 0.1411
202.28 0.0052 323.18 0.0673 401.91 0.1495
209.26 0.0059 328.93 0.0720 403.92 0.1535
216.53 0.0065 334.40 0.0771 406.13 0.1583
223.90 0.0072 340.70 0.0821 407.94 0.1627
231.96 0.0082 346.22 0.0872 410.95 0.1687
240.23 0.0102 352.72 0.0925 412.72 0.1736
248.20 0.0138 358.78 0.0979 414.59 0.1791
256.42 0.0183 363.96 0.1009 416.12 0.1842
263.99 0.0229 370.68 0.1078 417.60 0.1905
271.92 0.0278 376.35 0.1139 418.34 0.1961
280.94 0.0344 380.58 0.1187 418.67 0.2057

A–8 0
Table 166. Test data for specimen P12A-22

Test Number : 067 Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 175.4 MPa Ultimate Stress : 418..7MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

138.430 0.0011 240.230 0.0102 380.580 0.1187

154.150 0.0015 248.200 0.0138 384.320 0.1234
166.320 0.0019 256.420 0.0183 388.060 0.1280
176.630 0.0025 263.990 0.0229 390.710 0.1316
186.340 0.0033 271.920 0.0278 399.600 0.1454
195.620 0.0045 280.940 0.0344 401.910 0.1495
202.280 0.0052 297.390 0.0463 410.950 0.1687
209.260 0.0059 323.180 0.0673 412.720 0.1736
216.530 0.0065 328.930 0.0720 414.590 0.1791
223.900 0.0072 352.720 0.0925 416.120 0.1842
231.960 0.0082 367.340 0.1040 418.670 0.2057

Table 167. Test data for specimen P11A-12

Test Number : 310 Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 188.2 MPa Ultimate Stress : 424.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

11.551 0.0001 247.372 0.0335 359.065 0.1530

17.176 0.0001 259.991 0.0440 372.345 0.1731
123.234 0.0002 277.304 0.0595 377.431 0.1816
131.103 0.0003 286.567 0.0685 389.453 0.2048
151.510 0.0007 293.333 0.0751 392.761 0.2117
175.865 0.0017 304.078 0.0860 397.788 0.2230
182.490 0.0022 308.212 0.0905 402.369 0.2343
187.882 0.0030 322.206 0.1061 413.527 0.2687
210.120 0.0090 329.793 0.1148 417.995 0.2912
222.346 0.0154 347.479 0.1371 418.821 0.2935
235.500 0.0246 352.444 0.1437 424.466 0.3186

A–8 1
Table 168. Test data for specimen P12T–08

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 180.2 MPa Ultimate Stress : 454.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

3.19 0.0000 214.63 0.0086 375.49 0.1017

4.50 0.0003 218.63 0.0097 383.56 0.1078
6.80 0.0005 232.90 0.0151 391.07 0.1138
9.48 0.0006 247.73 0.0218 397.00 0.1199
12.72 0.0008 260.90 0.0285 404.10 0.1259
16.01 0.0010 273.17 0.0351 411.34 0.1317
18.54 0.0013 286.68 0.0428 416.24 0.1374
20.88 0.0017 299.72 0.0506 422.03 0.1430
22.77 0.0021 311.37 0.0575 427.06 0.1486
24.28 0.0027 321.50 0.0642 431.82 0.1540
25.76 0.0034 331.36 0.0706 436.85 0.1590
26.99 0.0044 340.95 0.0769 440.58 0.1639
28.23 0.0054 350.39 0.0832 444.16 0.1692
29.46 0.0064 359.01 0.0894 446.44 0.1728
210.57 0.0074 367.90 0.0956 450.23 0.1775

Table 169. Test data for specimen P12A–10

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 173.7 MPa Ultimate Stress : 451.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

3.44 0.0002 33.42 0.0184 389.90 0.1373

7.41 0.0003 33.65 0.0198 397.83 0.1475
12.74 0.0006 34.18 0.0213 406.72 0.1579
18.50 0.0009 253.86 0.0303 412.03 0.1683
22.00 0.0016 270.41 0.0401 418.86 0.1790
24.27 0.0025 284.68 0.0498 425.54 0.1895
25.94 0.0037 299.78 0.0596 430.92 0.2022
27.13 0.0050 313.71 0.0691 434.58 0.2124
28.38 0.0065 326.74 0.0786 438.78 0.2252
29.24 0.0080 339.64 0.0882 442.71 0.2352
30.02 0.0095 350.94 0.0979 443.95 0.2496
30.66 0.0110 362.73 0.1075 448.37 0.2613
31.29 0.0125 371.63 0.1173 449.47 0.2781
31.82 0.0141 381.21 0.1273 450.43 0.2969
32.68 0.0170

A–8 2
Table 170. Test data for specimen P12A–11

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 180.7 MPa Ultimate Stress : 457.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

25.23 0.0002 208.29 0.0076 396.45 0.1291

49.09 0.0002 212.70 0.0083 404.31 0.1391
75.36 0.0003 227.73 0.0120 412.10 0.1491
104.94 0.0005 249.11 0.0217 419.55 0.1594
136.45 0.0006 267.24 0.0311 425.89 0.1698
154.03 0.0011 284.20 0.0409 431.89 0.1805
167.96 0.0016 300.06 0.0501 437.54 0.1914
177.20 0.0022 313.78 0.0594 441.82 0.2009
181.61 0.0030 327.50 0.0690 446.99 0.2133
186.02 0.0038 342.95 0.0802 449.33 0.2265
190.50 0.0045 355.01 0.0905 452.78 0.2358
194.91 0.0053 367.56 0.1003 454.71 0.2503
199.40 0.0060 376.59 0.1095 457.05 0.2700
203.81 0.0068 387.14 0.1193

Table 171. Test data for specimen P12T–12

Test Number : 065 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 194.9 MPa Ultimate Stress : 472.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 285.06 0.0185 418.11 0.1059

160.70 0.0008 292.20 0.0220 428.42 0.1152
177.07 0.0011 300.36 0.0263 433.66 0.1203
193.08 0.0017 307.97 0.0307 442.72 0.1305
203.09 0.0021 314.18 0.0343 447.23 0.1357
210.49 0.0023 323.99 0.0404 451.05 0.1407
218.79 0.0026 333.07 0.0464 455.25 0.1471
227.36 0.0029 340.93 0.0516 459.15 0.1535
236.13 0.0034 349.86 0.0578 462.72 0.1593
243.53 0.0044 358.15 0.0636 465.26 0.1645
251.71 0.0063 366.79 0.0696 468.03 0.1708
257.38 0.0079 375.95 0.0760 470.67 0.1769
264.33 0.0101 383.11 0.0814 472.16 0.1833
271.72 0.0127 402.11 0.0953 472.69 0.1882
278.71 0.0157

A–8 3
Table 172. Test data for specimen P14A–22

Test Number : 071 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 185.3 MPa Ultimate Stress : 462.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

142.29 0.0011 322.47 0.0412 416.55 0.1124

162.23 0.0017 331.01 0.0462 420.31 0.1164
175.77 0.0022 334.55 0.0496 424.96 0.1213
184.78 0.0027 340.61 0.0541 431.85 0.1305
190.30 0.0030 346.03 0.0576 437.80 0.1393
216.79 0.0042 353.29 0.0630 444.69 0.1490
233.27 0.0049 359.55 0.0672 447.63 0.1541
239.75 0.0057 366.71 0.0723 452.41 0.1637
248.93 0.0073 375.77 0.0794 455.58 0.1686
256.89 0.0089 380.67 0.0837 456.88 0.1728
263.22 0.0108 386.30 0.0883 458.33 0.1776
282.83 0.0181 393.80 0.0928 458.58 0.1816
291.04 0.0212 401.42 0.0983 458.98 0.1878
306.67 0.0297 406.60 0.1025 462.34 0.1927
315.65 0.0350 411.50 0.1075

Table 173. Test data for specimen P14A–23

Test Number : 064 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 198.6 MPa Ultimate Stress : 475.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.24 0.0000 316.66 0.0340 447.88 0.1415

148.36 0.0016 324.27 0.0398 452.09 0.1475
161.13 0.0020 330.13 0.0437 454.13 0.1521
185.08 0.0030 343.05 0.0524 459.21 0.1600
204.59 0.0038 352.07 0.0583 462.25 0.1658
215.64 0.0042 363.77 0.0665 466.48 0.1752
229.77 0.0047 375.32 0.0748 468.66 0.1843
244.59 0.0067 385.61 0.0825 468.90 0.1843
255.32 0.0088 394.27 0.0894 471.80 0.1906
265.90 0.0116 403.49 0.0969 473.42 0.1963
272.58 0.0140 414.95 0.1041 474.30 0.2015
281.96 0.0175 417.78 0.1069 475.25 0.2054
292.48 0.0222 423.95 0.1128 475.29 0.2100
300.49 0.0260 433.53 0.1236 475.57 0.2145
307.67 0.0301 443.46 0.1351

A–8 4
Table 174. Test data for specimen P13T–08

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 167.3 MPa Ultimate Stress : 502.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

34.13 0.0002 247.25 0.0129 431.61 0.1201

52.61 0.0004 251.59 0.0141 441.20 0.1294
74.05 0.0005 256.00 0.0151 448.78 0.1388
99.28 0.0007 279.17 0.0226 456.50 0.1487
119.07 0.0012 300.68 0.0317 463.40 0.1586
135.55 0.0017 318.47 0.0402 470.98 0.1697
151.27 0.0023 335.29 0.0491 477.26 0.1807
165.13 0.0031 350.46 0.0577 482.08 0.1909
178.16 0.0040 364.53 0.0665 486.70 0.2012
193.12 0.0056 377.42 0.0752 491.25 0.2116
208.08 0.0072 389.83 0.0841 494.29 0.2223
223.11 0.0089 401.48 0.0930 497.66 0.2331
237.46 0.0105 412.44 0.1019 500.01 0.2441
241.52 0.0116 422.44 0.1109 501.52 0.2545

Table 175. Test data for specimen P13A–08

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 162.9 MPa Ultimate Stress : 485.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

19.93 0.0000 278.96 0.0272 438.09 0.1479

91.98 0.0007 284.34 0.0297 443.88 0.1556
125.97 0.0015 291.92 0.0330 448.92 0.1638
150.86 0.0027 297.58 0.0362 454.50 0.1730
173.20 0.0041 315.23 0.0457 460.16 0.1829
197.60 0.0058 333.29 0.0564 464.71 0.1923
219.46 0.0075 349.84 0.0673 468.43 0.2018
227.80 0.0095 366.11 0.0785 471.81 0.2109
236.77 0.0117 380.66 0.0894 474.64 0.2201
243.73 0.0137 392.86 0.1005 477.46 0.2300
250.62 0.0161 403.48 0.1102 479.88 0.2401
256.69 0.0185 411.69 0.1177 481.25 0.2507
263.52 0.0207 418.58 0.1251 484.43 0.2617
269.45 0.0229 425.41 0.1329 484.29 0.2730
274.00 0.0251 431.89 0.1401 485.39 0.2854

A–8 5
Table 176. Test data for specimen 683–40

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 274.1 MPa Ultimate Stress : 530.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

26.89 0.0002 303.23 0.0074 481.12 0.2244

66.60 0.0003 329.64 0.0206 486.84 0.2387
88.67 0.0004 349.70 0.0356 490.22 0.2528
111.90 0.0005 365.63 0.0507 496.49 0.2669
139.89 0.0006 380.04 0.0658 503.11 0.2809
163.96 0.0007 392.93 0.0807 504.56 0.2948
191.33 0.0009 405.41 0.0954 508.70 0.3086
217.12 0.0012 417.06 0.1099 511.80 0.3223
238.28 0.0017 426.58 0.1244 515.87 0.3357
257.11 0.0023 437.75 0.1389 518.83 0.3489
270.07 0.0030 443.75 0.1532 520.21 0.3620
279.03 0.0038 452.99 0.1675 523.73 0.3746
286.27 0.0046 460.23 0.1818 524.48 0.3869
292.96 0.0054 466.84 0.1961 527.93 0.3983
298.75 0.0064 475.53 0.2104 528.55 0.4082

Table 177. Test data for specimen 683–41

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 279.4 MPa Ultimate Stress : 517.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

45.37 0.0002 299.92 0.0106 457.61 0.1693

65.43 0.0003 304.06 0.0122 462.16 0.1802
86.67 0.0004 327.43 0.0266 469.67 0.1913
109.49 0.0005 345.08 0.0408 475.81 0.2026
136.59 0.0007 357.15 0.0538 482.91 0.2138
163.82 0.0008 370.46 0.0664 486.01 0.2253
192.16 0.0009 383.00 0.0785 493.60 0.2369
219.60 0.0011 392.59 0.0903 496.35 0.2487
246.63 0.0014 405.55 0.1020 501.87 0.2609
264.41 0.0020 415.48 0.1136 505.66 0.2733
276.48 0.0030 424.30 0.1249 508.83 0.2860
285.17 0.0044 432.58 0.1362 511.66 0.2993
291.03 0.0059 440.16 0.1473 512.97 0.3132
295.03 0.0074 450.16 0.1583 514.07 0.3290
298.61 0.0090

A–8 6
Table 178. Test data for specimen 683-33

Test Number : 206 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 263.1 MPa Ultimate Stress : 502.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.277 0.0001 351.581 0.0596 443.121 0.1839

59.946 0.0004 363.526 0.0726 466.461 0.2323
70.662 0.0005 365.541 0.0747 467.452 0.2344
167.215 0.0011 376.495 0.0875 471.522 0.2452
179.868 0.0012 378.511 0.0896 472.586 0.2473
240.869 0.0023 386.982 0.1002 479.712 0.2668
247.815 0.0027 409.652 0.1302 484.443 0.2821
316.452 0.0264 411.134 0.1323 490.510 0.3043
319.288 0.0287 412.518 0.1344 492.891 0.3156
334.245 0.0421 439.657 0.1776 501.585 0.3781
336.620 0.0443 440.721 0.1797 502.266 0.4007

Table 179. Test data for specimen 684-31

Test Number : 207 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 269.2 MPa Ultimate Stress : 531.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.603 0.0001 360.080 0.0352 481.976 0.1438

28.245 0.0002 394.218 0.0583 497.647 0.1677
49.499 0.0004 397.019 0.0604 499.002 0.1699
92.316 0.0007 405.249 0.0667 511.484 0.1944
186.523 0.0014 425.612 0.0834 512.452 0.1966
197.849 0.0016 435.013 0.0918 516.370 0.2057
227.787 0.0022 437.819 0.0943 519.660 0.2149
283.764 0.0054 455.309 0.1119 525.563 0.2349
289.304 0.0062 463.055 0.1204 527.208 0.2420
312.856 0.0119 468.522 0.1268 527.595 0.2444
349.219 0.0289 470.375 0.1289 531.369 0.2795

A–8 7
Table 180. Test data for specimen 68-145

Test Number : 208 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 278.0 MPa Ultimate Stress : 566.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.767 0.0001 407.302 0.0596 511.435 0.1588

27.509 0.0002 410.232 0.0616 517.459 0.1669
138.852 0.0009 418.155 0.0676 530.809 0.1873
218.478 0.0017 439.177 0.0842 532.014 0.1893
245.500 0.0023 448.344 0.0922 535.628 0.1955
253.019 0.0026 455.192 0.0981 547.436 0.2182
319.555 0.0106 478.504 0.1208 550.183 0.2245
325.097 0.0125 480.605 0.1228 551.677 0.2281
341.088 0.0190 488.109 0.1307 560.737 0.2534
371.687 0.0356 489.940 0.1327 562.328 0.2599
384.323 0.0436 495.097 0.1387 566.376 0.2892

Table 181. Test data for specimen 684–21

Test Number : 122 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 304.5 MPa Ultimate Stress : 614.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.20 0.0000 383.48 0.0356 514.78 0.1775

43.86 0.0001 405.09 0.0528 542.52 0.2325
201.61 0.0025 428.57 0.0739 565.75 0.2918
299.97 0.0052 459.36 0.1004 581.42 0.3475
323.03 0.0077 473.99 0.1162 599.71 0.4324
331.67 0.0093 478.54 0.1220 609.92 0.5201
342.81 0.0127 484.63 0.1342 614.05 0.5901
358.17 0.0193

A–8 8
Table 182. Test data for specimen 684–22

Test Number : 123 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 281.0 MPa Ultimate Stress : 571.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.20 0.0000 322.48 0.0097 485.20 0.1852

32.30 0.0000 334.82 0.0140 485.89 0.1852
205.66 0.0020 353.54 0.0251 511.51 0.2517
206.25 0.0020 386.11 0.0506 539.46 0.3421
222.40 0.0022 420.65 0.0852 560.89 0.4697
279.06 0.0038 450.14 0.1178 570.53 0.5504
297.49 0.0050 466.83 0.1429 571.22 0.6435
311.09 0.0069 478.09 0.1629

Table 183. Test data for specimen 682–41

Test Number : 168 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 305.7 MPa Ultimate Stress : 621.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 379.18 0.0145 509.61 0.0980

232.61 0.0017 401.78 0.0249 539.21 0.1225
291.45 0.0031 434.95 0.0420 570.81 0.1592
306.61 0.0036 464.96 0.0635 607.20 0.2236
331.78 0.0054 488.25 0.0806 621.00 0.2783
354.04 0.0084

Table 184. Test data for specimen 684–39

Test Number : 164 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 358.2 MPa Ultimate Stress : 614.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 416.93 0.0133 532.08 0.1137

69.76 0.0001 434.07 0.0200 566.06 0.1636
298.81 0.0030 457.04 0.0334 595.24 0.2291
347.64 0.0044 477.88 0.0502 612.83 0.3099
379.70 0.0067 495.73 0.0735 614.44 0.3387
400.70 0.0092

A–8 9
Table 185. Test data for specimen 68–264

Test Number : 165 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 296.2 MPa Ultimate Stress : 572.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 355.60 0.0183 447.85 0.1035

261.43 0.0032 355.90 0.0183 467.97 0.1347
291.16 0.0046 363.44 0.0228 491.74 0.1833
306.26 0.0058 376.07 0.0319 503.84 0.2217
315.94 0.0068 391.55 0.0442 535.15 0.3130
325.70 0.0085 410.68 0.0621 563.65 0.4398
336.88 0.0111 432.03 0.0853 572.53 0.5390
345.85 0.0141

Table 186. Test data for specimen 681-28

Test Number : 287 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 326.9 MPa Ultimate Stress : 640.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

13.740 0.0001 440.890 0.0401 568.650 0.1798

16.160 0.0000 446.950 0.0444 576.090 0.1926
73.320 0.0005 476.220 0.0679 577.180 0.1947
84.350 0.0005 478.690 0.0700 594.630 0.2288
133.140 0.0008 481.040 0.0721 600.430 0.2418
222.700 0.0014 512.890 0.1038 613.920 0.2763
286.290 0.0024 522.170 0.1144 619.030 0.2915
346.130 0.0052 523.880 0.1165 628.870 0.3265
370.930 0.0084 538.910 0.1354 633.110 0.3442
392.980 0.0143 548.160 0.1481 634.720 0.3532
412.490 0.0229 567.410 0.1777 640.200 0.4019

A–9 0
Table 187. Test data for specimen 681-29

Test Number : 288 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 303.7 MPa Ultimate Stress : 608.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.690 0.0001 440.540 0.0508 568.460 0.2131

70.570 0.0002 456.880 0.0634 580.810 0.2443
131.820 0.0005 482.840 0.0866 588.550 0.2679
241.370 0.0014 491.090 0.0952 589.270 0.2703
251.140 0.0016 501.010 0.1060 590.700 0.2751
292.890 0.0028 523.550 0.1343 599.450 0.3102
299.860 0.0030 525.140 0.1365 601.830 0.3226
354.120 0.0085 534.260 0.1497 602.240 0.3247
387.160 0.0193 547.790 0.1720 605.580 0.3470
391.690 0.0214 550.470 0.1766 606.700 0.3572
434.680 0.0465 555.190 0.1856 608.430 0.3845

Table 188. Test data for specimen 68-230

Test Number : 289 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 294.3 MPa Ultimate Stress : 578.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

17.980 0.0001 391.280 0.0327 521.840 0.1759

23.600 0.0001 394.710 0.0350 524.540 0.1805
119.640 0.0005 430.170 0.0623 541.250 0.2125
170.980 0.0008 432.620 0.0646 542.450 0.2148
183.760 0.0009 435.270 0.0669 552.460 0.2387
196.100 0.0010 454.540 0.0862 554.310 0.2434
296.600 0.0036 469.050 0.1023 561.180 0.2612
302.200 0.0040 471.040 0.1046 567.420 0.2793
327.610 0.0067 497.960 0.1395 571.500 0.2959
334.490 0.0079 501.210 0.1440 575.950 0.3158
376.020 0.0236 508.950 0.1554 578.850 0.3491

A–9 1
Table 189. Test data for specimen 682–25

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 5780 h
Yield Stress : 281.5 MPa Ultimate Stress : 601.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

40.06 0.0002 324.67 0.0088 557.37 0.2780

59.43 0.0004 331.43 0.0102 564.20 0.3001
80.88 0.0005 335.50 0.0117 572.20 0.3227
105.70 0.0006 376.94 0.0359 577.02 0.3452
130.38 0.0008 406.03 0.0600 582.47 0.3684
156.92 0.0010 431.40 0.0832 588.19 0.3922
183.95 0.0011 451.40 0.1054 591.98 0.4165
211.67 0.0014 469.40 0.1272 593.29 0.4412
235.39 0.0019 487.53 0.1487 595.22 0.4669
255.86 0.0025 501.80 0.1702 596.60 0.4932
274.20 0.0033 515.38 0.1914 599.29 0.5203
288.06 0.0042 527.93 0.2129 599.02 0.5484
300.40 0.0051 538.76 0.2343 600.67 0.5775
309.78 0.0062 548.41 0.2560 598.74 0.6072
318.12 0.0075

Table 190. Test data for specimen 682–26

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 5780 h
Yield Stress : 294.8 MPa Ultimate Stress : 599.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

39.02 0.0002 321.43 0.0059 546.20 0.2054

58.33 0.0003 330.19 0.0070 554.06 0.2226
78.26 0.0004 336.60 0.0081 563.03 0.2402
100.25 0.0005 342.26 0.0091 567.65 0.2580
123.90 0.0007 385.07 0.0281 573.37 0.2762
150.37 0.0008 411.55 0.0472 578.61 0.2947
178.71 0.0009 434.09 0.0658 582.47 0.3139
208.57 0.0011 454.64 0.0839 586.47 0.3334
233.66 0.0014 474.22 0.1017 590.74 0.3538
253.24 0.0019 488.98 0.1192 593.43 0.3747
272.62 0.0025 504.42 0.1367 595.09 0.3967
288.41 0.0033 515.04 0.1538 597.15 0.4199
301.44 0.0041 525.59 0.1710 596.33 0.4447
314.13 0.0049 538.20 0.1882 597.78 0.4715

A–9 2
Table 191. Test data for specimen 684–06

Test Number : 124 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 264.5 MPa Ultimate Stress : 606.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

42.91 0.0002 329.49 0.0112 480.34 0.1036

194.98 0.0024 348.32 0.0163 485.57 0.1118
219.11 0.0030 362.95 0.0227 520.34 0.1500
255.25 0.0039 383.50 0.0335 551.99 0.1962
280.26 0.0050 398.95 0.0434 571.40 0.2367
280.51 0.0049 422.46 0.0602 588.76 0.2865
297.62 0.0062 450.71 0.0811 601.37 0.3393
313.10 0.0081 470.92 0.0973 606.46 0.3925

Table 192. Test data for specimen 684–07

Test Number : 137 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 299.7 MPa Ultimate Stress : 601.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.20 0.0000 359.88 0.0124 483.99 0.0926

44.00 0.0001 379.74 0.0188 525.48 0.1305
207.78 0.0024 402.32 0.0293 552.96 0.1719
282.94 0.0040 426.63 0.0448 581.43 0.2267
320.64 0.0062 452.65 0.0638 592.69 0.2652
341.11 0.0084 475.82 0.0818 601.06 0.3150

A–9 3
Table 193. Test data for specimen 684–08

Test Number : 223 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 296.8 MPa Ultimate Stress : 612.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

39.27 0.0000 425.98 0.0489 562.39 0.1853

61.70 0.0001 444.80 0.0611 573.01 0.2054
132.87 0.0006 465.05 0.0758 575.27 0.2099
168.93 0.0009 470.32 0.0801 580.15 0.2208
224.62 0.0016 482.95 0.0904 585.60 0.2340
241.26 0.0020 494.42 0.1006 589.42 0.2452
286.33 0.0027 498.72 0.1047 593.91 0.2585
322.46 0.0064 509.40 0.1152 594.69 0.2607
333.59 0.0084 513.34 0.1194 597.78 0.2717
355.79 0.0143 524.74 0.1321 602.34 0.2898
361.40 0.0163 533.63 0.1427 602.70 0.2921
366.72 0.0183 536.90 0.1469 605.66 0.3057
371.80 0.0203 544.67 0.1577 608.51 0.3242
393.42 0.0304 547.74 0.1620 610.47 0.3403
401.42 0.0345 554.71 0.1726 611.19 0.3495
419.31 0.0448 557.45 0.1768 612.03 0.3657

Table 194. Test data for specimen 68–129

Test Number : 127 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 287.6 MPa Ultimate Stress : 595.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

43.56 0.0000 383.46 0.0300 545.42 0.2116

196.46 0.0017 400.23 0.0420 568.01 0.2740
223.72 0.0021 424.12 0.0606 585.78 0.3478
284.67 0.0036 446.75 0.0807 594.05 0.4167
319.09 0.0060 468.20 0.0978 594.45 0.4169
332.24 0.0080 480.50 0.1101 595.56 0.4226
345.83 0.0080 489.89 0.1261 595.46 0.4220
358.73 0.0164 515.18 0.1569 595.81 0.5039

A–9 4
Table 195. Test data for specimen 684–10

Test Number : 191 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 299.0 MPa Ultimate Stress : 652.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

9.42 0.0000 412.04 0.0253 581.43 0.1448

34.71 0.0002 426.38 0.0319 596.07 0.1630
99.40 0.0006 456.56 0.0478 601.13 0.1699
136.72 0.0009 464.56 0.0524 604.28 0.1745
234.34 0.0018 468.30 0.0547 615.26 0.1922
244.35 0.0020 497.14 0.0731 619.10 0.1992
253.55 0.0022 507.17 0.0799 621.48 0.2038
269.99 0.0027 513.66 0.0844 629.89 0.2217
277.38 0.0029 533.80 0.1000 633.66 0.2317
332.95 0.0061 542.24 0.1068 639.49 0.2485
346.27 0.0075 544.86 0.1090 640.42 0.2505
351.98 0.0083 547.56 0.1113 642.60 0.2585
356.97 0.0090 551.92 0.1155 643.09 0.2606
363.36 0.0101 571.03 0.1335 647.38 0.2789
368.95 0.0113 575.28 0.1380 647.45 0.2809
406.56 0.0229 577.47 0.1403 652.75 0.3335

Table 196. Test data for specimen 684–11

Test Number : 192 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 281.1 MPa Ultimate Stress : 628.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

9.95 0.0001 480.97 0.0878 587.05 0.2655

38.08 0.0002 485.35 0.0921 589.00 0.2721
59.45 0.0003 498.90 0.1071 595.44 0.2918
153.78 0.0008 502.77 0.1113 597.82 0.3006
202.98 0.0012 519.28 0.1323 601.95 0.3161
265.79 0.0028 529.92 0.1473 602.88 0.3205
279.07 0.0034 534.16 0.1538 608.88 0.3449
327.92 0.0065 543.50 0.1691 609.68 0.3493
340.30 0.0079 554.33 0.1886 615.00 0.3761
379.05 0.0170 556.39 0.1930 615.87 0.3806
393.50 0.0230 557.77 0.1951 616.30 0.3828
401.83 0.0272 564.88 0.2104 619.10 0.4007
425.91 0.0418 567.95 0.2169 621.06 0.4141
429.22 0.0439 574.55 0.2326 621.50 0.4185
439.73 0.0515 576.44 0.2370 624.75 0.4452
458.10 0.0665 579.07 0.2436 628.10 0.4976
462.98 0.0708 585.41 0.2610

A–9 5
Table 197. Test data for specimen 68–139

Test Number : 193 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 287.4 MPa Ultimate Stress : 639.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.50 0.0001 430.18 0.0356 590.30 0.1636

79.76 0.0006 434.81 0.0378 598.00 0.1749
163.03 0.0011 460.58 0.0515 601.84 0.1813
198.39 0.0014 468.51 0.0561 607.28 0.1913
255.48 0.0025 490.56 0.0697 610.59 0.1974
270.00 0.0030 500.67 0.0766 619.13 0.2155
283.13 0.0036 519.54 0.0903 621.46 0.2216
319.14 0.0058 539.11 0.1063 626.71 0.2354
326.46 0.0064 544.20 0.1109 628.58 0.2415
339.28 0.0078 557.24 0.1238 629.28 0.2435
372.47 0.0138 561.93 0.1284 633.18 0.2579
378.08 0.0153 563.95 0.1308 633.52 0.2599
383.14 0.0168 565.68 0.1327 633.89 0.2620
389.09 0.0187 575.40 0.1440 635.40 0.2684
394.44 0.0205 578.95 0.1483 635.76 0.2704
425.35 0.0333 587.76 0.1596 638.85 0.2963

Table 198. Test data for specimen 682–16

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 294.1 MPa Ultimate Stress : 657.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

19.10 0.0002 323.71 0.0054 601.98 0.2667

21.24 0.0002 331.16 0.0063 611.36 0.2940
38.61 0.0002 342.95 0.0072 617.01 0.3216
57.09 0.0003 350.46 0.0081 624.87 0.3493
79.36 0.0004 407.27 0.0300 631.35 0.3774
105.08 0.0005 441.06 0.0529 635.42 0.4055
130.66 0.0007 468.71 0.0749 639.08 0.4341
158.72 0.0008 495.53 0.0966 643.14 0.4627
191.54 0.0010 519.59 0.1185 646.04 0.4916
219.18 0.0012 537.72 0.1408 649.28 0.5206
242.01 0.0017 555.17 0.1640 651.76 0.5497
261.66 0.0022 570.75 0.1881 652.73 0.5789
280.34 0.0029 584.74 0.2136 653.97 0.6084
295.65 0.0036 595.78 0.2397 654.86 0.6382
310.82 0.0045

A–9 6
Table 199. Test data for specimen 682–17

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 289.8 MPa Ultimate Stress : 629.5 MPa
Engr. Engr. Engr.
Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

39.16 0.0002 322.88 0.0075 570.47 0.2032

60.54 0.0002 326.81 0.0085 577.78 0.2165
79.15 0.0003 358.87 0.0204 586.61 0.2300
102.66 0.0004 381.21 0.0337 592.05 0.2434
126.86 0.0005 401.07 0.0468 598.95 0.2570
154.10 0.0006 420.79 0.0599 603.15 0.2705
180.09 0.0007 438.51 0.0727 607.50 0.2839
206.91 0.0009 455.95 0.0856 614.46 0.2973
234.63 0.0012 472.70 0.0985 615.70 0.3105
257.04 0.0016 487.39 0.1114 618.11 0.3233
272.76 0.0022 502.97 0.1244 622.67 0.3361
285.58 0.0029 516.90 0.1374 623.42 0.3482
296.13 0.0037 528.07 0.1505 625.97 0.3602
305.58 0.0046 540.20 0.1635 626.04 0.3717
312.06 0.0055 551.44 0.1767 628.25 0.3824
318.54 0.0065 561.51 0.1899

Table 200. Test data for specimen 682–15

Test Number : 125 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 313.4 MPa Ultimate Stress : 641.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

48.61 0.0003 426.81 0.0265 545.48 0.1063

194.81 0.0025 450.59 0.0376 580.02 0.1369
229.86 0.0032 475.06 0.0526 600.75 0.1625
307.85 0.0052 479.75 0.0561 623.67 0.2002
354.53 0.0084 485.66 0.0635 629.45 0.2148
385.15 0.0131 508.43 0.0787 638.11 0.2498
404.35 0.0184 545.28 0.1038 640.98 0.2785

A–9 7
Table 201. Test data for specimen 682–22

Test Number : 126 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 299.3 MPa Ultimate Stress : 650.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

33.34 0.0000 390.58 0.0178 559.42 0.1414

204.82 0.0018 401.82 0.0220 591.94 0.1803
218.93 0.0021 422.99 0.0333 614.57 0.2202
285.41 0.0040 449.59 0.0501 614.27 0.2202
322.45 0.0058 470.96 0.0666 636.06 0.2756
348.30 0.0084 483.35 0.0783 647.26 0.3307
372.86 0.0131 526.76 0.1082 650.39 0.3705

Table 202. Test data for specimen 682–23

Test Number : 229 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 306.0 MPa Ultimate Stress : 657.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

17.77 0.0001 461.40 0.0430 601.42 0.1524

90.70 0.0004 469.39 0.0475 608.18 0.1611
189.83 0.0008 488.52 0.0585 617.09 0.1742
256.81 0.0017 492.15 0.0608 624.19 0.1852
265.69 0.0019 509.41 0.0718 630.09 0.1962
273.92 0.0022 525.21 0.0828 631.33 0.1984
289.49 0.0027 542.89 0.0959 635.60 0.2072
321.44 0.0041 556.44 0.1068 640.22 0.2182
340.09 0.0054 559.13 0.1090 641.05 0.2204
347.25 0.0060 568.84 0.1177 645.29 0.2314
381.41 0.0111 571.11 0.1199 647.48 0.2382
387.43 0.0125 573.48 0.1221 650.64 0.2494
392.67 0.0140 584.31 0.1329 652.99 0.2584
398.48 0.0158 586.42 0.1351 654.91 0.2693
425.12 0.0256 588.40 0.1372 655.36 0.2715
434.90 0.0299 597.82 0.1481 656.58 0.2806
444.28 0.0343 599.62 0.1502 657.39 0.2942

A–9 8
Table 203. Test data for specimen 68–119

Test Number : 128 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 306.0 MPa Ultimate Stress : 624.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 422.97 0.0206 587.81 0.1922

195.52 0.0016 443.47 0.0336 604.31 0.2298
240.17 0.0021 473.25 0.0576 617.67 0.2781
386.78 0.0049 479.42 0.0625 622.63 0.3245
389.99 0.0052 486.10 0.0718 624.26 0.3521
392.85 0.0064 536.68 0.1179 615.88 0.3758
393.10 0.0066 560.09 0.1484

Table 204. Test data for specimen 681–04

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 291.3 MPa Ultimate Stress : 653.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

18.00 0.0000 338.67 0.0064 593.22 0.1786

45.57 0.0003 348.32 0.0072 599.09 0.1921
65.85 0.0004 356.80 0.0079 606.88 0.2058
86.53 0.0005 401.55 0.0172 612.94 0.2193
110.52 0.0007 430.30 0.0287 617.98 0.2332
137.41 0.0009 454.50 0.0405 623.22 0.2472
163.75 0.0011 475.32 0.0526 626.94 0.2612
190.50 0.0014 493.25 0.0646 632.46 0.2753
214.84 0.0017 508.01 0.0768 634.80 0.2896
237.25 0.0022 521.80 0.0889 638.32 0.3040
256.62 0.0027 534.83 0.1012 641.28 0.3185
274.14 0.0032 548.27 0.1137 642.45 0.3331
291.30 0.0038 559.30 0.1263 645.14 0.3477
306.61 0.0044 565.99 0.1392 646.66 0.3626
317.16 0.0051 577.99 0.1521 648.87 0.3777

A–9 9
Table 205. Test data for specimen 681–05

Test Number : MEA Test Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 309.4 MPa Ultimate Stress : 632.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

61.16 0.0003 351.08 0.0071 554.41 0.1045

86.60 0.0004 380.66 0.0122 562.82 0.1108
114.94 0.0005 405.41 0.0187 570.06 0.1172
142.79 0.0007 422.30 0.0254 576.95 0.1236
172.16 0.0008 437.89 0.0323 583.57 0.1299
200.29 0.0010 453.47 0.0391 589.36 0.1363
225.80 0.0012 466.64 0.0459 596.47 0.1428
247.66 0.0015 477.19 0.0526 600.95 0.1493
267.72 0.0020 489.11 0.0592 605.64 0.1559
283.10 0.0024 501.39 0.0657 611.84 0.1626
298.06 0.0029 510.07 0.0723 614.94 0.1692
309.51 0.0035 520.35 0.0788 619.49 0.1759
320.61 0.0042 530.41 0.0852 623.29 0.1827
337.43 0.0056 537.93 0.0916 627.70 0.1895
348.12 0.0064 547.86 0.0980 628.59 0.1964

Table 206. Test data for specimen 683–42

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 162.7 MPa Ultimate Stress : 397.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

66.74 0.0005 204.43 0.0170 341.29 0.1304

95.91 0.0007 206.91 0.0184 348.12 0.1387
121.28 0.0011 217.87 0.0268 355.36 0.1485
141.20 0.0017 230.77 0.0362 362.39 0.1574
155.20 0.0025 243.04 0.0452 365.28 0.1656
165.61 0.0034 254.21 0.0541 370.87 0.1751
174.16 0.0045 266.96 0.0628 374.32 0.1846
179.82 0.0057 277.72 0.0716 380.45 0.1919
183.88 0.0069 288.75 0.0799 385.42 0.2031
187.40 0.0083 297.03 0.0883 389.55 0.2146
191.81 0.0097 307.51 0.0968 389.21 0.2235
192.36 0.0110 316.33 0.1056 394.04 0.2372
195.88 0.0125 324.67 0.1137 394.93 0.2498
197.40 0.0139 332.81 0.1218 394.93 0.2639
200.22 0.0154

A–1 0 0
Table 207. Test data for specimen 684–40

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 156.4 MPa Ultimate Stress : 412.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

43.02 0.0003 190.57 0.0142 336.12 0.1472

64.33 0.0005 192.29 0.0156 343.15 0.1580
86.32 0.0006 193.81 0.0169 353.22 0.1695
105.15 0.0008 210.01 0.0273 359.91 0.1806
123.28 0.0013 226.77 0.0386 367.42 0.1917
137.96 0.0019 238.63 0.0497 372.73 0.2029
150.44 0.0027 250.97 0.0608 379.28 0.2128
158.86 0.0037 264.83 0.0718 383.56 0.2248
165.89 0.0048 275.58 0.0831 390.17 0.2380
172.37 0.0060 287.51 0.0942 395.83 0.2510
175.61 0.0074 296.27 0.1044 397.90 0.2655
177.88 0.0087 308.68 0.1151 402.45 0.2749
181.88 0.0101 316.68 0.1264 403.34 0.2882
186.16 0.0115 328.26 0.1382 410.10 0.3068
188.23 0.0128

Table 208. Test data for specimen 684-32

Test Number : 251 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 149.5 MPa Ultimate Stress : 333.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

38.035 0.0002 189.629 0.0321 272.081 0.1269

40.376 0.0002 202.477 0.0452 281.043 0.1400
55.969 0.0001 208.233 0.0515 286.391 0.1465
65.557 0.0002 210.259 0.0535 288.174 0.1488
105.987 0.0005 225.677 0.0709 299.143 0.1662
115.819 0.0006 227.751 0.0731 302.679 0.1705
123.596 0.0007 233.046 0.0794 314.764 0.1903
147.480 0.0023 245.258 0.0938 318.349 0.2002
152.702 0.0035 250.596 0.1005 325.917 0.2151
164.710 0.0099 265.256 0.1182 326.063 0.2174
180.375 0.0231 267.287 0.1204 333.170 0.2438

A–1 0 1
Table 209. Test data for specimen 684-33

Test Number : 250 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 155.0 MPa Ultimate Stress : 399.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

36.630 0.0002 224.300 0.0528 332.150 0.1663

68.620 0.0002 231.820 0.0592 343.890 0.1839
78.580 0.0002 250.800 0.0768 347.800 0.1906
106.320 0.0004 253.250 0.0791 350.210 0.1930
115.570 0.0004 260.060 0.0855 368.870 0.2534
135.860 0.0007 279.690 0.1053 377.750 0.2736
143.790 0.0012 285.970 0.1119 380.670 0.2804
164.580 0.0058 302.170 0.1296 388.490 0.3070
190.810 0.0240 303.820 0.1316 390.300 0.3095
199.110 0.0307 311.800 0.1404 393.670 0.3299
201.240 0.0327 324.840 0.1580 395.710 0.3364

Table 210. Test data for specimen 68-246

Test Number : 249 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 170.6 MPa Ultimate Stress : 390.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

41.940 0.0002 209.810 0.0183 326.070 0.1042

64.890 0.0002 235.910 0.0344 342.730 0.1217
75.350 0.0003 245.360 0.0407 348.040 0.1283
117.050 0.0004 248.310 0.0430 363.210 0.1487
126.570 0.0005 267.370 0.0561 364.310 0.1508
134.690 0.0006 270.460 0.0583 369.340 0.1576
161.000 0.0016 273.410 0.0605 376.300 0.1708
166.350 0.0022 290.630 0.0734 380.330 0.1794
172.140 0.0029 293.360 0.0755 387.400 0.1999
201.510 0.0138 296.050 0.0777 388.030 0.2019
205.820 0.0160 316.710 0.0954 390.650 0.2221

A–1 0 2
Table 211. Test data for specimen 684–23

Test Number : 091 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 173.4 MPa Ultimate Stress : 416.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

137.03 0.0009 260.07 0.0280 374.87 0.1304

166.79 0.0017 269.42 0.0354 380.58 0.1373
175.09 0.0022 275.07 0.0400 383.43 0.1413
186.21 0.0035 283.63 0.0476 390.10 0.1497
191.45 0.0045 291.32 0.0545 393.67 0.1555
195.90 0.0055 297.79 0.0619 395.70 0.1583
199.81 0.0064 308.11 0.0690 398.82 0.1641
206.73 0.0072 317.35 0.0771 400.26 0.1673
213.91 0.0081 326.30 0.0847 402.70 0.1721
222.01 0.0093 330.86 0.0889 405.86 0.1791
227.13 0.0101 335.91 0.0934 407.25 0.1823
234.78 0.0114 340.24 0.0972 409.32 0.1862
238.58 0.0132 350.48 0.1044 410.74 0.1903
242.49 0.0148 354.85 0.1088 412.18 0.1934
246.97 0.0181 363.38 0.1176 412.36 0.1993
251.74 0.0216 367.70 0.1221 412.41 0.2025
255.64 0.0245 371.87 0.1266

Table 212. Test data for specimen 684–24

Test Number : 092 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 164.4 MPa Ultimate Stress : 442.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

131.09 0.0007 264.23 0.0338 395.13 0.1571

161.38 0.0016 268.58 0.0370 399.64 0.1631
170.77 0.0021 292.17 0.0571 406.01 0.1727
177.76 0.0028 299.27 0.0630 408.98 0.1772
184.73 0.0039 305.22 0.0682 410.77 0.1804
188.47 0.0047 310.81 0.0730 414.03 0.1871
191.92 0.0056 315.96 0.0778 423.79 0.2067
195.08 0.0065 318.97 0.0805 425.05 0.2100
198.78 0.0076 337.58 0.0967 429.03 0.2167
201.57 0.0081 344.16 0.1001 430.50 0.2207
207.31 0.0088 350.35 0.1059 431.77 0.2260
236.70 0.0140 355.06 0.1103 432.94 0.2311
241.45 0.0167 363.12 0.1186 435.81 0.2386
246.41 0.0201 365.95 0.1218 437.16 0.2448
251.57 0.0236 371.04 0.1273 439.01 0.2497
256.17 0.0270 354.82 0.1306 439.80 0.2544
260.33 0.0305 391.27 0.1513 442.04 0.2608

A–1 0 3
Table 213. Test data for specimen 682–40

Test Number : 178 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 174.3 MPa Ultimate Stress : 440.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.25 0.0000 218.20 0.0109 342.51 0.1025

33.32 0.0001 220.60 0.0120 359.89 0.1192
97.41 0.0007 224.95 0.0139 376.72 0.1375
144.41 0.0015 229.50 0.0160 384.74 0.1472
157.94 0.0018 233.25 0.0182 392.24 0.1570
162.85 0.0021 238.24 0.0210 398.80 0.1659
174.78 0.0026 247.78 0.0270 409.88 0.1835
183.14 0.0033 253.92 0.0312 419.01 0.2008
190.60 0.0041 260.91 0.0365 422.18 0.2068
196.45 0.0049 271.49 0.0448 423.13 0.2086
201.35 0.0058 280.12 0.0523 431.34 0.2305
205.71 0.0069 292.09 0.0622 434.92 0.2482
210.26 0.0080 305.66 0.0731 439.19 0.2666
213.01 0.0091 317.23 0.0832 440.78 0.2804
215.71 0.0099 329.89 0.0936 440.83 0.2903

Table 214. Test data for specimen 682–42

Test Number : 176 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 176.9 MPa Ultimate Stress : 451.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.64 0.0000 226.99 0.0137 376.65 0.1316

30.11 0.0000 236.62 0.0188 383.92 0.1396
95.68 0.0005 244.12 0.0235 393.44 0.1529
134.65 0.0010 249.34 0.0268 401.17 0.1631
161.74 0.0017 255.40 0.0306 409.59 0.1740
167.78 0.0020 261.86 0.0360 413.59 0.1799
178.19 0.0025 269.51 0.0415 417.63 0.1861
186.21 0.0031 279.95 0.0497 422.07 0.1929
189.13 0.0034 285.02 0.0538 429.12 0.2062
194.24 0.0040 297.14 0.0634 433.29 0.2175
198.55 0.0047 306.34 0.0708 437.63 0.2318
206.44 0.0062 314.30 0.0777 442.07 0.2430
209.77 0.0071 326.74 0.0880 447.30 0.2585
214.33 0.0085 338.22 0.0975 448.61 0.2688
217.60 0.0097 360.01 0.1145 450.08 0.2851
221.43 0.0112 369.13 0.1240 451.61 0.3043

A–1 0 4
Table 215. Test data for specimen 68–263

Test Number : 181 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 165.6 MPa Ultimate Stress : 450.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 242.20 0.0266 376.97 0.1490

80.05 0.0003 248.82 0.0312 382.37 0.1557
129.13 0.0010 260.45 0.0401 388.36 0.1647
157.15 0.0019 271.23 0.0491 392.52 0.1710
164.98 0.0022 288.38 0.0639 400.29 0.1824
175.45 0.0027 298.41 0.0723 406.13 0.1928
180.09 0.0031 306.85 0.0799 413.00 0.2067
188.86 0.0039 316.09 0.0880 413.88 0.2070
192.50 0.0045 324.38 0.0952 417.98 0.2174
195.84 0.0051 332.62 0.1006 422.37 0.2266
199.02 0.0058 339.82 0.1078 427.99 0.2419
205.20 0.0072 345.52 0.1134 438.53 0.2735
215.00 0.0109 349.69 0.1175 444.23 0.2983
220.87 0.0135 355.10 0.1231 449.22 0.3216
223.96 0.0151 359.91 0.1288 450.01 0.3315
228.83 0.0178 366.31 0.1352 450.32 0.3464
233.71 0.0207 371.27 0.1413

Table 216. Test data for specimen 682-28

Test Number : 319 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 203.3 MPa Ultimate Stress : 479.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

95.970 0.0002 311.280 0.0498 422.850 0.1422

118.450 0.0002 318.200 0.0543 428.320 0.1489
155.240 0.0005 338.060 0.0673 431.790 0.1533
162.540 0.0007 341.270 0.0695 442.830 0.1689
204.750 0.0029 359.350 0.0826 455.890 0.1911
210.160 0.0037 378.570 0.0979 457.050 0.1933
228.290 0.0075 381.060 0.1001 464.650 0.2116
264.380 0.0231 390.950 0.1090 466.090 0.2139
268.810 0.0253 404.820 0.1223 466.860 0.2159
281.090 0.0320 407.000 0.1245 473.630 0.2382
300.340 0.0432 409.010 0.1268 478.960 0.2689

A–1 0 5
Table 217. Test data for specimen 682-29

Test Number : 320 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 205.3 MPa Ultimate Stress : 485.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

18.870 0.0001 301.950 0.0480 418.900 0.1578

33.340 0.0002 305.100 0.0501 428.130 0.1711
68.280 0.0003 319.730 0.0611 443.810 0.1979
78.920 0.0003 338.970 0.0765 449.360 0.2072
90.140 0.0003 351.940 0.0874 459.460 0.2311
133.150 0.0005 354.440 0.0896 463.780 0.2405
142.130 0.0006 375.810 0.1094 472.960 0.2706
196.750 0.0022 377.910 0.1115 476.600 0.2818
239.890 0.0098 388.780 0.1225 480.990 0.3041
258.450 0.0189 398.960 0.1335 482.860 0.3129
262.340 0.0212 417.320 0.1557 485.580 0.3506

Table 218. Test data for specimen 681-30

Test Number : 318 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 201.3 MPa Ultimate Stress : 475.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

112.840 0.0001 329.750 0.0780 430.620 0.1979

119.940 0.0002 342.440 0.0891 443.920 0.2229
149.250 0.0007 344.740 0.0912 445.330 0.2274
168.720 0.0013 371.180 0.1176 457.120 0.2528
180.220 0.0017 373.300 0.1198 455.730 0.2548
244.130 0.0161 383.200 0.1308 464.740 0.2758
248.410 0.0184 396.060 0.1461 463.810 0.2778
252.380 0.0208 403.040 0.1550 466.760 0.2865
292.290 0.0476 404.700 0.1572 470.830 0.3026
295.130 0.0499 422.660 0.1835 471.970 0.3050
306.500 0.0587 429.590 0.1956 475.140 0.3337

A–1 0 6
Table 219. Test data for specimen 682–27

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 5,780 h
Yield Stress : 185.1 MPa Ultimate Stress : 452.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

36.34 0.0002 213.39 0.0086 389.42 0.1610

57.23 0.0004 216.98 0.0096 396.38 0.1726
77.64 0.0005 220.84 0.0107 404.72 0.1848
98.32 0.0006 241.11 0.0213 411.96 0.1970
117.35 0.0007 257.45 0.0329 416.37 0.2091
136.24 0.0011 273.10 0.0443 423.61 0.2200
150.31 0.0016 289.79 0.0558 427.34 0.2358
162.99 0.0021 301.78 0.0675 430.85 0.2474
174.51 0.0026 316.54 0.0789 436.23 0.2601
185.12 0.0032 327.50 0.0906 442.23 0.2769
190.23 0.0039 340.60 0.1021 444.09 0.2891
198.57 0.0047 349.36 0.1137 447.06 0.3037
203.53 0.0057 360.39 0.1254 449.19 0.3238
207.39 0.0066 370.11 0.1373 450.23 0.3447
209.88 0.0076 378.87 0.1489 450.37 0.3672

Table 220. Test data for specimen 684–09

Test Number : 082 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 164.3 MPa Ultimate Stress : 500.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

112.43 0.0004 319.88 0.0463 451.18 0.1521

136.35 0.0007 330.15 0.0531 458.54 0.1622
153.62 0.0012 338.70 0.0596 462.12 0.1676
188.85 0.0024 345.67 0.0645 465.31 0.1717
199.52 0.0031 369.51 0.0813 474.65 0.1766
216.98 0.0037 377.37 0.0873 477.80 0.1805
234.00 0.0047 385.47 0.0929 479.90 0.1882
240.14 0.0055 392.40 0.0977 482.34 0.1959
244.67 0.0067 399.62 0.1010 487.25 0.2127
248.80 0.0082 407.33 0.1074 492.37 0.2187
254.35 0.0102 416.37 0.1147 494.34 0.2215
283.26 0.0237 433.21 0.1314 494.83 0.2277
293.73 0.0297 438.61 0.1371 495.71 0.2366
305.03 0.0367 442.98 0.1420 497.57 0.2426
315.10 0.0433 447.21 0.1471 500.32 0.2567

A–1 0 7
Table 221. Test data for specimen 68–130

Test Number : 083 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 168.9 MPa Ultimate Stress : 447.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

122.1500 0.0008 266.7200 0.0244 395.3500 0.1314

138.2200 0.0012 273.6900 0.0296 401.0800 0.1385
155.0300 0.0018 280.2500 0.0342 404.1500 0.1428
160.7000 0.0020 288.5200 0.0407 406.9700 0.1467
166.4700 0.0023 293.2500 0.0446 410.0800 0.1509
177.2300 0.0028 301.2700 0.0509 415.3200 0.1584
180.9800 0.0031 308.6000 0.0572 418.6000 0.1637
195.8000 0.0044 313.6800 0.0614 426.7800 0.1772
203.5800 0.0052 322.4600 0.0688 428.7200 0.1812
212.2400 0.0058 327.7500 0.0732 432.8700 0.1894
221.2100 0.0066 334.3400 0.0790 436.2800 0.1970
230.5300 0.0075 340.1700 0.0837 439.6400 0.2044
234.2100 0.0080 364.9600 0.1007 442.6200 0.2129
237.4900 0.0088 372.2600 0.1067 443.5500 0.2161
240.8200 0.0101 377.6200 0.1124 446.0800 0.2243
254.1300 0.0164 385.2900 0.1207 446.8500 0.2301
260.4000 0.0204 392.7400 0.1281 447.1400 0.2333

Table 222. Test data for specimen 684-12

Test Number : 236 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 216.0 MPa Ultimate Stress : 485.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

64.060 0.0004 227.050 0.0060 386.180 0.0998

93.730 0.0005 259.280 0.0181 389.000 0.1024
103.610 0.0006 272.530 0.0251 409.010 0.1188
125.630 0.0007 277.420 0.0276 421.990 0.1310
132.320 0.0007 301.910 0.0421 442.810 0.1500
138.680 0.0008 306.330 0.0447 443.850 0.1536
163.920 0.0009 318.480 0.0521 460.970 0.1797
172.010 0.0010 347.650 0.0713 462.490 0.1817
179.520 0.0011 357.420 0.0783 472.180 0.1991
203.880 0.0021 360.570 0.0806 477.380 0.2102
221.270 0.0046 383.260 0.0975 485.710 0.2388

A–1 0 8
Table 223. Test data for specimen 684-15

Test Number : 261 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 190.4 MPa Ultimate Stress : 427.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

28.682 0.0002 242.204 0.0235 354.865 0.1120

35.020 0.0002 245.934 0.0258 369.129 0.1270
61.873 0.0003 266.270 0.0387 374.891 0.1337
72.445 0.0004 275.565 0.0451 376.827 0.1357
128.096 0.0007 278.526 0.0474 391.284 0.1532
134.391 0.0007 298.421 0.0621 392.876 0.1553
151.378 0.0008 301.189 0.0642 397.980 0.1623
190.100 0.0030 322.623 0.0819 410.957 0.1816
195.833 0.0040 325.153 0.0840 414.474 0.1879
211.355 0.0085 327.582 0.0862 421.804 0.2031
230.795 0.0172 348.338 0.1056 427.262 0.2227

Table 224. Test data for specimen 68-140

Test Number : 244 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 170.2 MPa Ultimate Stress : 479.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

44.260 0.0002 281.450 0.0413 416.300 0.1427

48.740 0.0002 309.740 0.0585 428.390 0.1557
94.850 0.0005 313.120 0.0607 430.280 0.1579
104.690 0.0007 322.910 0.0670 435.920 0.1645
161.360 0.0025 350.440 0.0862 447.870 0.1798
166.450 0.0028 353.360 0.0884 452.540 0.1865
174.850 0.0034 356.220 0.0906 461.470 0.2023
223.280 0.0125 383.360 0.1121 462.660 0.2045
229.230 0.0147 385.840 0.1143 471.640 0.2247
244.580 0.0213 388.320 0.1166 473.380 0.2293
270.070 0.0348 409.670 0.1361 479.000 0.2522

A–1 0 9
Table 225. Test data for specimen 682–18

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 161.3 MPa Ultimate Stress : 463.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

78.53 0.0005 213.74 0.0143 391.21 0.1431

102.18 0.0007 234.35 0.0238 398.72 0.1517
121.76 0.0011 251.59 0.0341 409.48 0.1605
138.38 0.0015 262.41 0.0440 415.34 0.1693
149.13 0.0022 280.27 0.0538 424.17 0.1782
160.17 0.0030 292.41 0.0631 428.65 0.1872
169.82 0.0038 305.30 0.0723 434.78 0.1962
178.09 0.0049 318.40 0.0815 441.47 0.2052
184.37 0.0060 329.98 0.0904 445.13 0.2151
189.95 0.0071 341.36 0.0993 449.74 0.2250
196.02 0.0084 353.49 0.1083 454.57 0.2341
200.57 0.0095 363.15 0.1170 457.95 0.2459
202.09 0.0108 374.52 0.1257 459.47 0.2573
207.19 0.0119 382.59 0.1344 461.88 0.2716
209.95 0.0131

Table 226. Test data for specimen 682–24

Test Number : 076 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 176.7 MPa Ultimate Stress : 475.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

144.63 0.0011 300.68 0.0386 425.46 0.1590

164.92 0.0019 305.23 0.0420 429.79 0.1651
171.17 0.0021 310.63 0.0467 441.10 0.1832
183.88 0.0027 318.15 0.0528 445.55 0.1926
212.61 0.0042 343.22 0.0750 447.79 0.1962
228.63 0.0049 353.13 0.0838 450.39 0.2017
237.41 0.0057 358.48 0.0887 452.39 0.2057
241.90 0.0066 364.49 0.0942 454.68 0.2100
245.26 0.0072 373.56 0.0998 458.35 0.2196
247.63 0.0082 379.16 0.1047 468.65 0.2491
250.89 0.0092 383.98 0.1103 470.46 0.2544
269.81 0.0176 386.76 0.1132 471.52 0.2588
272.29 0.0191 406.62 0.1355 472.54 0.2637
274.96 0.0208 409.80 0.1389 473.75 0.2683
278.12 0.0226 412.29 0.1418 475.31 0.2727
280.74 0.0243 414.92 0.1455 475.15 0.2776
284.99 0.0270 420.54 0.1523

A–1 1 0
Table 227. Test data for specimen 68–120

Test Number : 077 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 193.9 MPa Ultimate Stress : 484.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

159.5000 0.0019 328.6900 0.0532 441.4700 0.1506

170.9400 0.0024 335.1200 0.0583 444.3000 0.1544
184.2900 0.0030 340.7600 0.0628 446.9200 0.1575
196.4600 0.0037 347.3400 0.0678 449.5000 0.1611
211.0100 0.0044 351.5400 0.0707 454.1700 0.1679
244.7000 0.0069 356.3400 0.0743 456.3100 0.1711
249.3900 0.0079 377.4600 0.0898 461.4800 0.1796
253.9800 0.0094 383.3000 0.0947 464.0600 0.1838
260.6400 0.0116 389.3400 0.0972 465.8000 0.1872
264.7900 0.0132 395.5800 0.1024 469.8900 0.1956
268.4900 0.0149 400.4300 0.1063 477.4800 0.2170
272.1000 0.0166 403.7500 0.1096 478.8400 0.2212
276.5000 0.0187 407.4600 0.1127 480.1400 0.2260
279.4100 0.0202 410.4800 0.1153 481.0000 0.2300
287.7600 0.0249 413.3500 0.1179 482.7700 0.2389
296.3100 0.0302 415.9300 0.1204 483.3800 0.2432
303.0300 0.0350 422.1200 0.1258 484.0900 0.2479
323.0100 0.0488 427.5200 0.1313 484.2600 0.2515

Table 228. Test data for specimen 681–06

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 169.7 MPa Ultimate Stress : 486.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

42.27 0.0002 238.56 0.0108 400.72 0.1097

66.60 0.0002 242.83 0.0120 408.24 0.1165
89.70 0.0004 246.00 0.0131 414.37 0.1233
111.70 0.0006 263.93 0.0193 423.41 0.1301
132.17 0.0011 278.13 0.0265 430.09 0.1368
147.75 0.0017 292.61 0.0338 436.23 0.1436
162.10 0.0023 304.54 0.0409 449.19 0.1569
175.26 0.0031 317.71 0.0478 451.88 0.1635
188.09 0.0039 326.40 0.0549 458.64 0.1701
199.05 0.0047 337.71 0.0619 463.12 0.1768
208.70 0.0057 349.15 0.0690 467.88 0.1832
215.87 0.0066 357.29 0.0758 471.81 0.1898
222.49 0.0077 365.70 0.0827 475.05 0.1961
227.66 0.0086 384.31 0.0962 479.53 0.2024
233.18 0.0098 394.31 0.1030 482.36 0.2078

A–1 1 1
Table 229. Test data for specimen 682–09

Test Number : MEA Test Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 191.6 MPa Ultimate Stress : 503.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

21.24 0.0002 230.91 0.0075 417.82 0.1099

38.68 0.0003 238.21 0.0083 428.58 0.1199
59.36 0.0005 242.76 0.0094 436.51 0.1302
80.88 0.0006 248.56 0.0104 446.57 0.1404
104.32 0.0008 253.04 0.0115 452.78 0.1508
122.24 0.0011 279.79 0.0203 459.81 0.1614
143.34 0.0015 302.27 0.0303 466.57 0.1721
156.99 0.0020 320.95 0.0403 472.64 0.1829
171.96 0.0025 336.74 0.0503 479.12 0.1939
185.06 0.0032 352.60 0.0603 481.32 0.2052
196.36 0.0039 369.77 0.0704 488.08 0.2167
206.70 0.0048 381.42 0.0802 490.84 0.2277
217.46 0.0056 393.97 0.0900 493.60 0.2409
224.91 0.0065 404.31 0.0998 498.28 0.2515

Table 230. Test data for specimen 733–40

Test Number : 016 Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 254.3 MPa Ultimate Stress : 557.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

63.5814 0.0003 262.4600 0.0084 462.4630 0.2270

84.9001 0.0005 268.5910 0.0105 476.4350 0.2399
106.8720 0.0009 275.6970 0.0138 480.1400 0.2456
124.6350 0.0013 281.1460 0.0173 484.6510 0.2495
152.2530 0.0018 287.8630 0.0215 492.9110 0.2665
166.9750 0.0023 295.3100 0.0271 501.5690 0.2853
185.7380 0.0028 308.0140 0.0382 506.0760 0.2975
202.8910 0.0032 325.7820 0.0544 515.0850 0.3156
209.3630 0.0033 342.4300 0.0703 520.9320 0.3343
221.3840 0.0035 360.2990 0.0893 529.8790 0.3558
229.2450 0.0036 380.5990 0.1106 537.4600 0.3760
240.0750 0.0043 398.3240 0.1313 543.7160 0.3972
248.1560 0.0050 417.7070 0.1569 550.2940 0.4162
253.6530 0.0059 436.4070 0.1842 554.0220 0.4328
257.4490 0.0069 452.0410 0.2093 556.9630 0.4463

A–1 1 2
Table 231. Test data for specimen 733–41

Test Number : 017 Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 249.5 MPa Ultimate Stress : 530.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

57.54 0.0003 315.80 0.0467 481.10 0.2757

103.56 0.0011 333.74 0.0648 489.91 0.2954
147.78 0.0021 351.77 0.0837 503.35 0.3317
194.54 0.0038 368.00 0.1007 509.95 0.3536
205.22 0.0039 383.59 0.1184 514.83 0.3748
229.48 0.0045 399.42 0.1376 520.18 0.3932
248.07 0.0055 402.92 0.1403 523.68 0.4139
255.24 0.0063 426.19 0.1725 527.32 0.4321
262.66 0.0075 447.50 0.2064 528.83 0.4459
267.73 0.0090 437.57 0.1907 530.67 0.4654
275.69 0.0125 461.90 0.2318 530.78 0.4808
287.00 0.0201 472.78 0.2550 530.79 0.5001
297.14 0.0284

Table 232. Test data for specimen 734–23

Test Number : 218 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 221.9 MPa Ultimate Stress : 475.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

35.201 0.0002 316.982 0.0882 415.842 0.2432

50.230 0.0004 318.460 0.0900 424.156 0.2605
109.948 0.0011 327.099 0.1011 436.441 0.2900
171.163 0.0019 344.669 0.1252 443.083 0.3083
231.938 0.0065 352.387 0.1363 450.399 0.3307
261.579 0.0293 357.424 0.1437 454.902 0.3459
263.135 0.0311 371.837 0.1662 457.632 0.3558
264.870 0.0328 377.470 0.1756 465.020 0.3876
291.185 0.0584 378.464 0.1775 467.415 0.3998
292.756 0.0600 401.099 0.2160 472.976 0.4350
300.484 0.0681 405.002 0.2226 475.332 0.4714

A–1 1 3
Table 233. Test data for specimen 734–24

Test Number : 219 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 228.2 MPa Ultimate Stress : 521.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

21.163 0.0001 373.504 0.1373 473.833 0.3118

92.275 0.0006 374.976 0.1393 478.661 0.3253
164.513 0.0011 376.803 0.1413 494.476 0.3783
176.243 0.0012 410.308 0.1858 498.945 0.3933
226.308 0.0032 411.421 0.1879 503.802 0.4166
257.628 0.0160 418.736 0.1988 508.854 0.4450
260.197 0.0182 438.544 0.2322 512.788 0.4711
274.920 0.0315 445.014 0.2446 516.091 0.4978
320.321 0.0777 453.704 0.2621 518.131 0.5150
322.313 0.0799 462.894 0.2834 519.151 0.5309
324.377 0.0820 473.060 0.3095 521.240 0.5848

Table 234. Test data for specimen 732–25

Test Number : 014 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 244.0 MPa Ultimate Stress : 526.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

36.15 0.0001 288.81 0.0229 483.08 0.2457

60.31 0.0003 302.72 0.0340 486.34 0.2590
84.51 0.0006 323.55 0.0524 490.23 0.2692
108.59 0.0011 342.47 0.0694 494.65 0.2836
132.31 0.0016 358.96 0.0860 500.81 0.3004
156.59 0.0021 375.53 0.1021 504.35 0.3079
180.62 0.0028 391.90 0.1188 507.79 0.3226
203.99 0.0034 407.09 0.1365 513.05 0.3378
221.44 0.0038 421.20 0.1537 515.33 0.3490
240.27 0.0047 432.99 0.1692 518.65 0.3610
243.07 0.0049 445.48 0.1872 519.90 0.3632
253.14 0.0063 457.09 0.2055 522.92 0.3819
260.80 0.0082 466.51 0.2220 524.52 0.4021
268.76 0.0111 476.07 0.2395 526.23 0.4151
275.87 0.0145 478.09 0.2429 526.46 0.4309

A–1 1 4
Table 235. Test data for specimen 732–26

Test Number : 015 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 244.4 MPa Ultimate Stress : 528.4 MPa
Engr. Engr. Engr.
Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

33.1610 0.0001 286.5200 0.0188 470.6100 0.2373

58.0510 0.0003 292.8000 0.0228 479.3800 0.2556
82.5420 0.0006 300.7600 0.0282 481.5200 0.2604
106.4300 0.0011 307.1600 0.0331 486.1000 0.2614
129.9400 0.0016 324.4700 0.0480 487.8900 0.2723
154.9900 0.0022 341.3800 0.0640 494.8400 0.2897
178.0200 0.0028 358.3900 0.0813 501.2900 0.3075
206.4600 0.0037 374.8500 0.0982 508.0900 0.3266
209.3700 0.0037 389.7700 0.1143 514.6400 0.3459
223.7100 0.0041 403.2300 0.1309 518.8800 0.3648
237.0900 0.0045 414.9900 0.1455 519.5500 0.3694
244.5600 0.0052 425.4800 0.1603 522.3200 0.3719
251.4300 0.0060 435.6200 0.1751 525.2200 0.3906
257.1300 0.0070 445.9400 0.1919 526.4100 0.4006
261.7100 0.0082 455.4300 0.2085 527.8400 0.4115
267.7700 0.0100 462.6900 0.2210 528.4200 0.4296
275.7600 0.0135

Table 236. Test data for specimen 734–06

Test Number : 220 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 228.0 MPa Ultimate Stress : 536.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

18.238 0.0001 318.152 0.0474 451.977 0.1875

42.648 0.0004 346.750 0.0746 472.198 0.2156
53.881 0.0005 348.942 0.0768 480.488 0.2285
179.881 0.0022 376.168 0.1078 495.178 0.2547
190.256 0.0024 378.054 0.1101 503.226 0.2711
199.656 0.0028 380.449 0.1123 514.473 0.2981
250.900 0.0076 410.366 0.1407 515.879 0.3023
257.241 0.0091 412.257 0.1427 524.799 0.3300
280.837 0.0188 422.414 0.1531 526.932 0.3386
303.807 0.0353 448.831 0.1834 533.283 0.3696
306.289 0.0373 450.275 0.1854 536.822 0.4116

A–1 1 5
Table 237. Test data for specimen 734–07

Test Number : 221 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 219.1 MPa Ultimate Stress : 529.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

39.655 0.0002 332.413 0.0708 490.091 0.3044

55.337 0.0003 373.667 0.1109 502.862 0.3496
67.588 0.0004 383.268 0.1215 503.489 0.3519
123.036 0.0007 416.276 0.1618 513.658 0.4004
133.957 0.0007 419.481 0.1660 514.574 0.4050
146.791 0.0008 443.578 0.2024 518.959 0.4332
210.418 0.0024 452.379 0.2175 521.610 0.4522
217.917 0.0031 465.184 0.2424 526.237 0.4960
256.709 0.0134 470.317 0.2534 527.056 0.5068
274.839 0.0246 473.247 0.2600 527.249 0.5092
317.530 0.0577 486.091 0.2932 533.659 0.4116

Table 238. Test data for specimen 73–119

Test Number : 222 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 212.8 MPa Ultimate Stress : 488.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

81.198 0.0005 317.202 0.0694 428.975 0.1950

160.878 0.0012 319.709 0.0717 430.599 0.1973
198.210 0.0023 337.189 0.0889 443.887 0.2178
206.442 0.0029 347.960 0.0999 459.285 0.2402
245.229 0.0116 350.139 0.1022 465.825 0.2586
249.388 0.0138 369.571 0.1225 472.187 0.2741
253.026 0.0160 379.942 0.1339 483.440 0.3045
277.109 0.0338 382.053 0.1363 485.320 0.3168
279.943 0.0361 397.620 0.1544 488.115 0.3497

A–1 1 6
Table 239. Test data for specimen 732–16

Test Number : 012 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 240.8 MPa Ultimate Stress : 541.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

30.76 0.0000 333.00 0.0585 491.68 0.2327

51.55 0.0002 340.74 0.0655 494.49 0.2408
82.38 0.0006 349.35 0.0726 500.65 0.2515
119.05 0.0013 363.37 0.0864 509.64 0.2700
151.04 0.0020 376.95 0.0984 517.34 0.2907
176.61 0.0027 386.90 0.1080 521.02 0.2948
193.73 0.0033 399.61 0.1203 524.73 0.3088
211.94 0.0036 413.26 0.1342 528.09 0.3203
240.09 0.0049 424.21 0.1462 532.52 0.3385
257.88 0.0071 433.32 0.1567 533.30 0.3501
269.13 0.0098 445.81 0.1677 536.02 0.3669
277.83 0.0138 459.01 0.1844 537.79 0.3805
285.55 0.0181 474.02 0.2054 540.14 0.3980
291.91 0.0223 481.76 0.2167 540.42 0.4137
302.71 0.0311 485.41 0.2212 540.81 0.4314
314.19 0.0413 489.04 0.2305 541.81 0.4492

Table 240. Test data for specimen 732–17

Test Number : 013 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 252.6 MPa Ultimate Stress : 555.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

20.02 0.0000 315.60 0.0374 506.90 0.2655

42.34 0.0001 333.72 0.0542 522.51 0.2973
87.99 0.0008 349.17 0.0684 530.96 0.3220
125.42 0.0016 366.36 0.0851 534.58 0.3360
159.13 0.0025 383.00 0.0995 538.98 0.3462
181.55 0.0031 397.17 0.1132 540.32 0.3555
208.85 0.0041 410.44 0.1262 543.40 0.3729
238.65 0.0050 426.68 0.1429 546.91 0.3854
251.97 0.0059 437.78 0.1552 548.39 0.3946
256.64 0.0065 450.76 0.1706 549.97 0.4048
264.81 0.0080 458.38 0.1802 551.73 0.4110
270.67 0.0094 466.46 0.1907 552.43 0.4234
281.79 0.0113 465.84 0.1959 554.68 0.4394
292.09 0.0171 476.96 0.2130 554.91 0.4499
303.46 0.0264 491.28 0.2365 555.72 0.4638

A–1 1 7
Table 241. Test data for specimen 732–15

Test Number : 226 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 235.3 MPa Ultimate Stress : 563.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

29.582 0.0001 379.611 0.0953 515.150 0.2914

56.208 0.0003 395.718 0.1109 525.892 0.3231
79.423 0.0004 397.992 0.1131 530.537 0.3389
161.338 0.0009 428.919 0.1465 531.311 0.3411
172.776 0.0010 445.501 0.1663 538.423 0.3695
236.484 0.0034 447.199 0.1684 542.004 0.3849
275.366 0.0136 482.960 0.2218 548.632 0.4181
301.010 0.0291 493.861 0.2420 551.826 0.4360
337.284 0.0572 495.071 0.2443 556.858 0.4692
340.018 0.0596 509.925 0.2780 558.600 0.4821
360.175 0.0774 514.328 0.2891 563.196 0.5341

Table 242. Test data for specimen 732–22

Test Number : 227 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 215.8 MPa Ultimate Stress : 530.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

53.560 0.0005 325.970 0.0621 455.794 0.2132

77.759 0.0006 336.761 0.0723 478.769 0.2544
155.999 0.0012 355.620 0.0910 485.473 0.2687
176.921 0.0015 357.644 0.0930 496.895 0.2963
205.216 0.0026 359.630 0.0950 500.654 0.3067
221.357 0.0041 383.033 0.1196 504.896 0.3192
251.508 0.0088 395.834 0.1338 515.499 0.3572
297.723 0.0366 416.534 0.1584 518.969 0.3723
300.224 0.0388 424.443 0.1684 524.848 0.4059
302.653 0.0409 435.186 0.1829 530.343 0.4710

A–1 1 8
Table 243. Test data for specimen 73–109

Test Number : 228 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 222.2 MPa Ultimate Stress : 534.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

32.850 0.0001 336.327 0.0891 468.932 0.2571

59.574 0.0003 337.961 0.0911 482.822 0.2865
104.921 0.0006 350.675 0.1055 489.521 0.3036
127.785 0.0008 377.216 0.1322 500.221 0.3337
191.731 0.0016 390.451 0.1468 502.823 0.3424
199.177 0.0019 392.393 0.1489 510.534 0.3706
205.563 0.0020 429.614 0.1941 512.655 0.3793
241.531 0.0071 431.108 0.1962 513.667 0.3837
275.601 0.0261 432.646 0.1982 526.150 0.4512
293.674 0.0435 459.852 0.2403 530.439 0.4881
306.523 0.0566 461.086 0.2424 534.006 0.5508

Table 244. Test data for specimen 731–04

Test Number : 010 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 256.5 MPa Ultimate Stress : 493.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

8.29 0.0001 272.92 0.0172 435.18 0.1900

22.58 0.0007 283.53 0.0235 445.30 0.2054
35.00 0.0011 289.53 0.0277 450.97 0.2155
53.14 0.0016 296.27 0.0325 458.77 0.2295
82.16 0.0024 299.32 0.0357 465.85 0.2439
95.14 0.0028 311.78 0.0465 473.01 0.2584
119.59 0.0035 320.91 0.0554 475.11 0.2631
159.98 0.0048 334.02 0.0679 477.20 0.2672
174.77 0.0054 347.89 0.0828 478.09 0.2679
187.55 0.0060 361.71 0.0964 478.90 0.2758
203.69 0.0064 375.19 0.1112 482.31 0.2831
240.20 0.0077 387.00 0.1248 483.18 0.2866
251.80 0.0113 398.53 0.1388 488.03 0.2992
260.52 0.0134 406.89 0.1494 492.21 0.3149
266.20 0.0148 416.00 0.1617 493.08 0.3271
271.89 0.0167 425.66 0.1752

A–1 1 9
Table 245. Test data for specimen 731–05

Test Number : 011 Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 234.0 MPa Ultimate Stress : 570.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

39.16 0.0001 319.71 0.0487 512.44 0.3145

74.25 0.0005 335.35 0.0634 523.58 0.3431
107.29 0.0011 345.23 0.0725 530.14 0.3669
151.01 0.0022 362.62 0.0908 536.91 0.3889
187.59 0.0034 379.33 0.1076 542.07 0.4098
201.62 0.0039 393.56 0.1227 547.56 0.4384
213.94 0.0042 406.91 0.1385 553.22 0.4654
233.52 0.0048 418.10 0.1514 555.89 0.4896
244.49 0.0060 428.97 0.1654 561.52 0.5219
253.92 0.0074 439.08 0.1790 564.74 0.5496
262.56 0.0091 447.35 0.1907 567.28 0.5770
270.46 0.0116 457.55 0.2041 569.40 0.6049
278.53 0.0153 464.72 0.2167 568.50 0.6194
283.34 0.0181 479.35 0.2410 569.29 0.6316
294.38 0.0260 490.43 0.2626 570.00 0.6451
309.61 0.0396 503.95 0.2905 570.41 0.6604

Table 246. Test data for specimen 733–42

Test Number : 053 Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 138.9 MPa Ultimate Stress : 366.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

36.89 0.0001 212.64 0.0724 363.51 0.3141

81.24 0.0006 224.78 0.0881 366.21 0.3275
109.37 0.0012 234.48 0.0987 365.23 0.3426
119.43 0.0015 244.10 0.1098 361.24 0.3507
126.92 0.0019 256.89 0.1250 356.19 0.3575
130.73 0.0021 269.42 0.1402 348.37 0.3646
136.31 0.0025 282.96 0.1576 339.58 0.3712
140.16 0.0029 295.72 0.1751 328.57 0.3781
145.85 0.0037 307.50 0.1927 311.87 0.3865
151.22 0.0054 317.37 0.2092 297.48 0.3923
162.25 0.0128 328.94 0.2295 281.67 0.3979
174.94 0.0265 338.01 0.2474 269.39 0.4014
191.15 0.0478 345.53 0.2629 253.78 0.4040
201.33 0.0605 356.49 0.2925 234.47 0.4047

A–1 2 0
Table 247. Test data for specimen 734–40

Test Number : 038 Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 133.9 MPa Ultimate Stress : 365.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

29.51 0.0001 143.94 0.0052 263.42 0.1246

45.17 0.0003 146.52 0.0059 276.04 0.1384
55.34 0.0004 147.73 0.0063 287.41 0.1516
66.93 0.0006 149.18 0.0069 300.80 0.1673
80.09 0.0008 151.89 0.0082 309.67 0.1788
91.18 0.0011 156.16 0.0109 317.74 0.1894
102.23 0.0014 163.03 0.0162 321.70 0.1945
109.98 0.0017 169.47 0.0225 328.21 0.2046
116.46 0.0019 175.20 0.0282 333.18 0.2119
120.34 0.0021 183.59 0.0377 340.54 0.2247
123.08 0.0023 193.33 0.0489 349.87 0.2417
127.10 0.0026 200.62 0.0567 357.93 0.2578
130.18 0.0029 206.60 0.0636 361.61 0.2689
133.99 0.0033 214.43 0.0721 362.49 0.2742
137.27 0.0037 226.27 0.0856 364.09 0.2765
139.41 0.0041 241.51 0.1016 364.97 0.2775
141.80 0.0046 251.03 0.1112

Table 248. Test data for specimen 734–19

Test Number : 338 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 130.4 MPa Ultimate Stress : 354.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.3600 0.0001 183.1900 0.0425 299.4700 0.1677

69.6300 0.0003 185.4900 0.0447 302.7600 0.1720
104.8700 0.0007 194.5700 0.0535 307.6400 0.1787
110.7800 0.0010 199.0200 0.0580 310.7900 0.1831
127.6700 0.0022 205.7200 0.0646 318.4200 0.1942
132.8700 0.0032 207.9000 0.0668 321.8800 0.2013
138.5800 0.0051 214.4600 0.0733 327.5000 0.2104
142.7900 0.0071 225.2300 0.0842 332.8600 0.2210
155.3400 0.0164 235.9500 0.0952 339.4200 0.2327
157.4800 0.0184 240.1900 0.0996 342.1600 0.2417
164.7700 0.0248 248.4200 0.1082 343.9100 0.2441
167.1800 0.0272 258.5700 0.1192 346.2900 0.2511
169.5200 0.0294 268.5200 0.1302 350.5000 0.2631
171.5200 0.0314 278.0600 0.1412 352.3400 0.2722
173.8500 0.0337 285.5100 0.1500 353.9600 0.2833
180.8700 0.0403 292.5200 0.1588

A–1 2 1
Table 249. Test data for specimen 734–22

Test Number : 339 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 131.3 MPa Ultimate Stress : 365.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

25.2600 0.0001 186.8700 0.0573 294.7900 0.2073

74.7300 0.0002 188.6900 0.0595 298.8700 0.2118
116.3100 0.0008 190.5500 0.0617 304.4800 0.2211
122.9900 0.0012 197.7900 0.0707 311.3200 0.2363
138.9000 0.0053 201.4500 0.0750 317.7300 0.2477
142.2500 0.0075 208.6400 0.0840 321.0300 0.2518
145.0700 0.0096 212.1700 0.0884 323.9500 0.2606
154.4700 0.0190 219.2000 0.0971 329.1500 0.2736
156.1900 0.0210 222.6800 0.1016 334.0800 0.2822
158.3200 0.0233 227.6500 0.1080 338.1800 0.2961
160.2700 0.0257 229.3300 0.1100 342.3000 0.3068
162.3500 0.0280 239.5200 0.1233 346.3900 0.3221
164.2800 0.0304 255.9800 0.1453 349.3300 0.3283
171.9400 0.0394 265.4000 0.1586 356.7800 0.3503
173.8900 0.0418 275.3500 0.1723 360.9500 0.3657
175.7700 0.0440 284.1800 0.1855 360.1700 0.3720
177.5900 0.0462 289.4300 0.1940 365.2000 0.3851

Table 250. Test data for specimen 732-27

Test Number : 043 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 2570 h
Yield Stress : 139.6 MPa Ultimate Stress : 419.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

54.670 0.004 150.050 0.014 276.170 0.152

62.100 0.004 155.060 0.016 344.910 0.255
102.100 0.007 161.050 0.018 356.690 0.276
113.460 0.008 165.610 0.021 392.930 0.360
122.810 0.009 171.140 0.025 407.250 0.407
128.860 0.010 197.890 0.053 416.120 0.446
140.410 0.012 205.220 0.062 418.900 0.460
145.130 0.013 260.650 0.131 419.840 0.505

A–1 2 2
Table 251. Test data for specimen 734-08

Test Number : 333 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 127.7 MPa Ultimate Stress : 377.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.990 0.000 201.880 0.054 300.510 0.159

53.340 0.000 220.140 0.072 307.360 0.168
81.630 0.001 222.370 0.074 320.220 0.186
109.700 0.001 231.220 0.083 326.300 0.195
122.980 0.002 248.340 0.100 340.890 0.220
139.960 0.006 250.480 0.102 342.320 0.222
162.010 0.019 256.640 0.109 355.150 0.248
169.910 0.025 272.720 0.126 356.480 0.251
172.570 0.028 274.650 0.128 366.090 0.278
192.480 0.045 280.390 0.135 374.820 0.304
194.840 0.048 293.380 0.150 377.640 0.329

Table 252. Test data for specimen 734–09

Test Number : 334 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 139.6 MPa Ultimate Stress : 419.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

69.570 0.000 227.650 0.035 326.370 0.107

91.750 0.000 230.960 0.037 331.810 0.111
123.330 0.000 249.940 0.051 352.110 0.128
131.620 0.000 253.160 0.053 356.880 0.132
143.360 0.001 262.310 0.059 372.750 0.148
150.760 0.001 274.630 0.068 379.020 0.154
156.890 0.001 277.660 0.070 390.760 0.167
188.280 0.010 280.660 0.072 392.550 0.170
192.590 0.013 298.340 0.085 406.350 0.190
196.580 0.015 301.230 0.087 414.750 0.206
217.920 0.029 309.760 0.094 417.400 0.221

Table 253. Test data for specimen 73-120

Test Number : 335 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 136.7 MPa Ultimate Stress : 386.4 MPa

Experimental Data Not Available.

A–1 2 3
Table 254. Test data for specimen 732–18

Test Number : 040 Test Temp. : 290°C

Material Type : CF–8M Heat Number : 73
Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 140.0 MPa Ultimate Stress : 444.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

32.15 0.0001 189.17 0.0034 365.51 0.1686

47.62 0.0001 189.26 0.0037 378.04 0.1841
64.14 0.0003 189.77 0.0042 390.04 0.2007
85.81 0.0005 203.66 0.0128 400.67 0.2173
109.85 0.0008 216.66 0.0234 411.57 0.2361
137.33 0.0013 233.49 0.0387 420.82 0.2548
160.82 0.0018 254.17 0.0579 428.34 0.2732
176.05 0.0022 270.95 0.0727 433.46 0.2884
189.27 0.0026 288.48 0.0899 435.29 0.2929
189.36 0.0028 308.44 0.1079 436.81 0.2991
189.25 0.0029 322.78 0.1219 439.73 0.3110
189.19 0.0031 337.39 0.1368 441.12 0.3270
189.23 0.0032 352.49 0.1533

Table 255. Test data for specimen 732-23

Test Number : 238 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 138.5 MPa Ultimate Stress : 408.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

39.952 0.0002 224.072 0.0589 319.338 0.1596

41.205 0.0002 225.843 0.0609 324.781 0.1661
76.550 0.0003 241.520 0.0761 337.125 0.1817
105.553 0.0006 248.507 0.0830 345.640 0.1930
133.524 0.0020 250.679 0.0851 365.740 0.2249
138.580 0.0027 265.926 0.1006 371.130 0.2342
161.457 0.0080 276.716 0.1120 387.910 0.2681
184.842 0.0236 278.772 0.1142 388.747 0.2702
195.375 0.0325 294.879 0.1318 399.140 0.2986
197.891 0.0349 304.673 0.1424 403.988 0.3157
214.836 0.0502 317.504 0.1575 408.483 0.3442

A–1 2 4
Table 256. Test data for specimen 732-24

Test Number : 237 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 143.0 MPa Ultimate Stress : 424.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.738 0.0001 220.316 0.0438 335.441 0.1485

19.668 0.0001 245.902 0.0653 337.508 0.1506
32.646 0.0001 248.408 0.0673 359.185 0.1740
76.517 0.0002 255.811 0.0737 362.906 0.1783
85.673 0.0002 279.768 0.0951 379.586 0.1998
95.129 0.0003 282.158 0.0972 382.738 0.2043
163.380 0.0064 284.418 0.0993 394.791 0.2226
168.990 0.0085 305.165 0.1185 402.656 0.2361
185.270 0.0175 307.421 0.1207 414.950 0.2609
206.716 0.0330 309.681 0.1226 419.258 0.2723
217.661 0.0417 324.872 0.1377 424.116 0.2952

Table 257. Test data for specimen 73-110

Test Number : 239 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 138.5 MPa Ultimate Stress : 395.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

42.550 0.0002 238.341 0.0716 331.449 0.1747

59.248 0.0002 256.103 0.0890 332.988 0.1769
71.576 0.0002 268.974 0.1021 349.763 0.2022
153.928 0.0059 271.016 0.1045 351.137 0.2047
159.463 0.0078 289.712 0.1244 364.327 0.2276
164.147 0.0101 291.676 0.1265 365.565 0.2299
202.531 0.0389 293.907 0.1290 371.159 0.2410
205.178 0.0412 314.548 0.1532 378.871 0.2583
207.679 0.0435 316.387 0.1554 388.790 0.2863
226.980 0.0609 318.104 0.1577 390.460 0.2910
236.091 0.0696 329.683 0.1726 395.782 0.3195

A–1 2 5
Table 258. Test data for specimen 731–06

Test Number : 046 Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 144.1 MPa Ultimate Stress : 411.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

29.02 0.0001 186.38 0.0130 332.89 0.1288

65.85 0.0004 190.12 0.0151 350.86 0.1449
105.44 0.0010 195.94 0.0187 361.90 0.1562
119.94 0.0013 200.74 0.0219 372.27 0.1668
132.67 0.0018 205.77 0.0259 384.53 0.1808
141.35 0.0024 215.21 0.0333 390.69 0.1887
149.35 0.0031 226.34 0.0425 394.06 0.1937
157.58 0.0041 239.92 0.0534 396.56 0.1981
162.67 0.0050 254.04 0.0643 400.20 0.2041
167.37 0.0061 268.83 0.0754 405.92 0.2139
171.76 0.0073 280.80 0.0860 409.11 0.2204
174.93 0.0083 292.82 0.0954 410.07 0.2234
177.95 0.0094 305.56 0.1056 411.19 0.2260
181.65 0.0109 319.21 0.1168

Table 259. Test data for specimen 732–09

Test Number : 041 Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 136.2 MPa Ultimate Stress : 436.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

37.5850 0.0001 171.4200 0.0100 381.2500 0.2277

69.3680 0.0003 176.4600 0.0126 391.7700 0.2460
102.0400 0.0008 186.5000 0.0189 396.7800 0.2542
114.3600 0.0011 197.4700 0.0279 405.0100 0.2717
124.7100 0.0014 211.5200 0.0413 410.7000 0.2872
129.8600 0.0017 229.1000 0.0578 417.4200 0.3029
134.2700 0.0020 246.5600 0.0739 423.5200 0.3173
137.9400 0.0023 267.6000 0.0945 427.7300 0.3357
141.2700 0.0027 288.8900 0.1150 429.2200 0.3470
145.0300 0.0032 309.2100 0.1353 431.7900 0.3501
147.6700 0.0035 330.8000 0.1595 433.2200 0.3636
150.5000 0.0039 344.6900 0.1765 432.2100 0.3687
154.3100 0.0046 357.7500 0.1931 435.9300 0.3796
160.1600 0.0059 369.5400 0.2100 436.0800 0.3807
166.7300 0.0079

A–1 2 6
Table 260. Test data for specimen 205–26

Test Number : 097 Test Temp. : 25°C

Material Type : CF–8M Heat Number : 205
Aging Temp. : 400°C Aging Time : 18,000 h
Yield Stress : 248.5 MPa Ultimate Stress : 670.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

191.30 0.0016 431.56 0.0324 600.09 0.1400

216.73 0.0018 445.23 0.0383 607.97 0.1484
234.10 0.0020 458.65 0.0452 621.82 0.1670
254.13 0.0026 474.03 0.0537 624.86 0.1723
276.36 0.0037 482.16 0.0583 628.61 0.1762
297.46 0.0048 501.75 0.0695 630.48 0.1811
308.01 0.0055 513.98 0.0769 636.90 0.1895
321.36 0.0066 528.91 0.0863 640.61 0.1953
332.49 0.0079 535.40 0.0904 642.88 0.1995
344.52 0.0094 546.34 0.0979 643.48 0.2041
356.19 0.0111 556.40 0.1026 645.47 0.2076
365.26 0.0126 564.22 0.1085 647.37 0.2111
374.73 0.0144 568.76 0.1122 648.22 0.2179
382.19 0.0161 573.68 0.1160 651.78 0.2214
389.35 0.0179 578.41 0.1201 659.84 0.2267
397.58 0.0202 586.31 0.1274 659.19 0.2298
410.97 0.0244 590.64 0.1318 660.80 0.2337
424.59 0.0293 596.05 0.1360 663.88 0.2517

Table 261. Test data for specimen 205–27

Test Number : 189 Test Temp. : 25°C

Material Type : CF–8M Heat Number : 205
Aging Temp. : 400°C Aging Time : 18,000 h
Yield Stress : 254.0 MPa Ultimate Stress : 642.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

17.540 0.0001 368.255 0.0196 572.446 0.1578

30.976 0.0002 410.249 0.0349 590.300 0.1827
41.902 0.0002 427.740 0.0433 592.913 0.1868
53.175 0.0003 457.991 0.0600 607.912 0.2140
122.255 0.0006 461.189 0.0621 614.783 0.2288
134.240 0.0007 489.417 0.0807 620.492 0.2434
193.178 0.0011 492.320 0.0827 625.766 0.2584
269.980 0.0044 513.803 0.0992 628.863 0.2691
278.196 0.0051 542.786 0.1251 635.540 0.2974
285.976 0.0058 544.818 0.1271 637.911 0.3108
362.193 0.0180 570.946 0.1557 642.363 0.3658

A–1 2 7
Table 262. Test data for specimen 205–30

Test Number : 098 Test Temp. : 25°C

Material Type : CF–8M Heat Number : 205
Aging Temp. : 400°C Aging Time : 18,000 h
Yield Stress : 248.7 MPa Ultimate Stress : 646.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

206.46 0.0017 300.74 0.0206 589.99 0.1599

232.03 0.0019 425.81 0.0304 596.92 0.1690
241.03 0.0022 439.16 0.0364 600.23 0.1746
265.57 0.0029 454.41 0.0444 608.70 0.1898
273.64 0.0034 467.23 0.0515 610.94 0.1934
294.30 0.0046 473.59 0.0623 616.00 0.2039
305.86 0.0052 485.56 0.0715 618.42 0.2101
316.30 0.0061 514.52 0.0911 623.86 0.2235
326.24 0.0070 533.89 0.1031 627.25 0.2341
335.74 0.0082 539.57 0.1075 630.15 0.2444
344.85 0.0094 552.28 0.1185 632.95 0.2549
351.41 0.0104 557.75 0.1240 633.81 0.2596
360.08 0.0118 562.05 0.1280 634.96 0.2659
368.89 0.0132 567.33 0.1334 636.11 0.2725
376.70 0.0154 572.12 0.1384 637.06 0.2802
384.83 0.0172 575.73 0.1421 638.20 0.2865
390.75 0.0186 582.66 0.1506 639.67 0.3103

Table 263. Test data for specimen 205–25

Test Number : 061 Test Temp. : 290°C

Material Type : CF–8M Heat Number : 205
Aging Temp. : 400°C Aging Time : 18,000 h
Yield Stress : 179.4 MPa Ultimate Stress : 505.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

73.83 0.0002 263.54 0.0096 427.35 0.0939

105.52 0.0006 274.92 0.0124 446.96 0.1061
127.98 0.0009 285.57 0.0155 462.80 0.1199
141.76 0.0012 294.26 0.0185 473.64 0.1309
156.10 0.0016 301.80 0.0212 482.97 0.1419
167.01 0.0020 317.07 0.0277 483.46 0.1437
176.70 0.0024 343.30 0.0410 485.46 0.1484
191.30 0.0033 363.02 0.0523 494.14 0.1610
202.85 0.0039 379.90 0.0624 500.51 0.1719
226.10 0.0048 395.39 0.0723 504.16 0.1812
240.81 0.0057 414.01 0.0844 505.94 0.1900
251.80 0.0072 432.47 0.0972

A–1 2 8
Table 264. Test data for specimen 205–28

Test Number : 062 Test Temp. : 290°C

Material Type : CF–8M Heat Number : 205
Aging Temp. : 400°C Aging Time : 18,000 h
Yield Stress : 177.3 MPa Ultimate Stress : 507.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

58.95 0.0001 249.60 0.0078 437.50 0.1023

97.97 0.0005 272.90 0.0135 445.27 0.1084
127.29 0.0009 282.70 0.0168 456.48 0.1183
150.45 0.0014 296.26 0.0216 464.98 0.1266
161.64 0.0018 302.94 0.0243 473.76 0.1359
175.49 0.0024 313.87 0.0292 480.32 0.1442
183.44 0.0029 324.21 0.0344 488.44 0.1558
191.23 0.0035 334.40 0.0395 488.76 0.1597
198.38 0.0041 345.57 0.0459 492.46 0.1664
204.58 0.0044 357.23 0.0525 495.10 0.1720
207.90 0.0045 376.94 0.0642 499.73 0.1812
212.41 0.0048 388.54 0.0713 503.65 0.1911
217.47 0.0050 402.99 0.0806 506.79 0.2007
224.91 0.0052 414.19 0.0880 507.79 0.2125
231.66 0.0055 426.47 0.0961

Table 265. Test data for specimen 205–29

Test Number : 063 Test Temp. : 290°C

Material Type : CF–8M Heat Number : 205
Aging Temp. : 400°C Aging Time : 18,000 h
Yield Stress : 168.2 MPa Ultimate Stress : 495.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.298 0.000 273.080 0.013 405.300 0.082

52.043 0.000 277.910 0.015 431.860 0.098
84.180 0.000 292.950 0.020 438.340 0.103
114.680 0.001 299.220 0.022 458.180 0.121
142.790 0.001 317.940 0.031 463.760 0.128
159.560 0.002 322.480 0.033 477.880 0.145
171.100 0.002 343.290 0.044 480.320 0.149
208.420 0.004 349.020 0.047 482.720 0.153
222.010 0.005 369.930 0.059 489.350 0.169
244.360 0.007 376.410 0.063 493.280 0.182
255.660 0.009 398.280 0.077 495.090 0.207

A–1 2 9
Table 266. Test data for specimen 743–40

Test Number : 018 Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 273.5 MPa Ultimate Stress : 542.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

64.02 0.0001 242.65 0.0024 305.32 0.0073

79.92 0.0002 251.00 0.0026 307.13 0.0079
102.27 0.0004 262.07 0.0030 311.09 0.0090
134.03 0.0007 271.34 0.0035 319.74 0.0129
163.90 0.0013 279.30 0.0040 329.32 0.0187
201.03 0.0019 289.45 0.0049 333.38 0.0216
222.64 0.0020 293.02 0.0053 336.51 0.0241
233.57 0.0021 300.97 0.0064 337.73 0.0248

Table 267. Test data for specimen 743–41

Test Number : 019 Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 273.0 MPa Ultimate Stress : 531.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

61.35 0.0001 332.46 0.0220 492.73 0.2468

99.28 0.0004 351.27 0.0381 500.24 0.2679
147.04 0.0009 366.49 0.0532 505.80 0.2888
194.95 0.0017 383.14 0.0703 511.08 0.3097
216.27 0.0020 396.74 0.0853 516.24 0.3324
230.83 0.0021 411.77 0.0990 520.44 0.3547
248.01 0.0026 426.53 0.1172 523.26 0.3782
267.12 0.0036 437.88 0.1324 525.92 0.3995
275.88 0.0041 451.84 0.1530 528.28 0.4215
286.63 0.0051 461.57 0.1698 529.56 0.4442
293.24 0.0060 471.00 0.1881 529.97 0.4676
299.88 0.0074 478.94 0.2046 530.62 0.4873
305.46 0.0087 478.90 0.2059 531.29 0.5134
313.12 0.0111 480.54 0.2136
323.90 0.0167 485.31 0.2275

A–1 3 0
Table 268. Test data for specimen 743–36

Test Number : 209 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 282.2 MPa Ultimate Stress : 555.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.597 0.0001 355.981 0.0222 497.284 0.1267

60.766 0.0005 369.842 0.0290 502.649 0.1330
71.086 0.0006 401.412 0.0474 517.135 0.1519
150.844 0.0012 405.065 0.0497 521.329 0.1579
162.520 0.0013 415.478 0.0566 531.181 0.1744
219.047 0.0019 441.064 0.0751 534.400 0.1804
246.267 0.0025 443.932 0.0774 535.376 0.1825
278.189 0.0039 452.506 0.0844 542.887 0.1990
299.878 0.0059 473.669 0.1029 546.057 0.2074
305.062 0.0066 476.161 0.1052 553.665 0.2382
351.221 0.0199 491.090 0.1201 555.519 0.2562

Table 269. Test data for specimen 744–34

Test Number : 210 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 292.9 MPa Ultimate Stress : 601.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

31.273 0.0002 371.929 0.0256 537.570 0.1376

63.195 0.0005 406.314 0.0433 557.323 0.1615
73.871 0.0005 418.093 0.0500 561.810 0.1681
171.674 0.0012 421.946 0.0522 572.540 0.1859
209.941 0.0015 452.155 0.0706 577.223 0.1950
221.739 0.0016 465.602 0.0795 588.099 0.2203
288.211 0.0037 496.211 0.1012 590.684 0.2279
305.594 0.0051 504.454 0.1077 596.293 0.2465
311.705 0.0058 507.234 0.1098 599.219 0.2609
357.263 0.0188 528.987 0.1290 601.267 0.2845

A–1 3 1
Table 270. Test data for specimen 74–135

Test Number : 211 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 259.0 MPa Ultimate Stress : 570.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.921 0.0000 370.692 0.0406 515.735 0.1776

27.968 0.0001 373.988 0.0428 521.325 0.1878
49.482 0.0002 414.154 0.0705 535.977 0.2189
59.892 0.0003 424.868 0.0788 540.700 0.2313
185.372 0.0012 427.547 0.0808 548.315 0.2547
196.019 0.0014 460.084 0.1089 550.821 0.2634
240.021 0.0025 462.277 0.1109 554.146 0.2764
284.784 0.0058 472.191 0.1208 561.279 0.3117
290.833 0.0066 495.011 0.1470 563.110 0.3231
319.094 0.0136 496.505 0.1490 567.207 0.3552
352.060 0.0295 497.999 0.1511 570.243 0.4211

Table 271. Test data for specimen 744–21

Test Number : 186 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 273.1 MPa Ultimate Stress : 551.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

27.489 0.0002 286.173 0.0058 364.179 0.0283

37.730 0.0003 293.457 0.0065 367.404 0.0303
47.986 0.0003 300.299 0.0073 373.795 0.0343
122.563 0.0009 306.491 0.0080 376.932 0.0364
237.999 0.0027 324.277 0.0106 382.669 0.0403
243.982 0.0030 335.371 0.0141 385.515 0.0423
249.457 0.0033 340.342 0.0160 390.936 0.0463
254.859 0.0035 345.598 0.0184 393.729 0.0483
260.129 0.0039 353.516 0.0223 398.627 0.0523
265.337 0.0042 357.381 0.0243 401.342 0.0543
270.191 0.0045 360.906 0.0263 406.283 0.0583

A–1 3 2
Table 272. Test data for specimen 744–25

Test Number : 188 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 270.5 MPa Ultimate Stress : 565.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.191 0.0001 427.065 0.0904 508.494 0.2718

29.109 0.0002 432.025 0.0968 519.386 0.3129
40.396 0.0002 450.401 0.1246 519.916 0.3151
147.623 0.0008 454.965 0.1332 520.301 0.3174
160.206 0.0009 469.091 0.1610 536.446 0.3909
206.921 0.0013 470.001 0.1631 537.121 0.3931
216.853 0.0015 484.397 0.1973 544.109 0.4321
284.604 0.0045 485.264 0.1995 545.700 0.4408
368.997 0.0329 496.156 0.2309 546.181 0.4429
377.315 0.0393 505.506 0.2610 553.266 0.4910
379.985 0.0414 506.084 0.2632 561.941 0.5884

Table 273. Test data for specimen 742–42

Test Number : 166 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 312.7 MPa Ultimate Stress : 589.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 370.90 0.0137 488.09 0.0889

253.26 0.0028 387.53 0.0193 510.31 0.1124
305.40 0.0048 401.24 0.0261 544.67 0.1599
323.58 0.0059 418.04 0.0357 564.75 0.2042
340.03 0.0075 437.59 0.0489 589.10 0.3110
353.80 0.0096 467.62 0.0714 589.93 0.3449

Table 274. Test data for specimen 744–39

Test Number : 163 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 326.4 MPa Ultimate Stress : 663.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 407.90 0.0153 560.82 0.0989

299.42 0.0040 423.94 0.0196 602.75 0.1356
341.87 0.0062 437.85 0.0246 640.72 0.1874
363.93 0.0082 455.83 0.0321 666.18 0.2490
380.44 0.0101 495.61 0.0539 674.39 0.2943
393.51 0.0123

A–1 3 3
Table 275. Test data for specimen 74–245

Test Number : 159 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 278.8 MPa Ultimate Stress : 617.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.000 0.0000 376.120 0.0179 514.960 0.1082

234.550 0.0022 389.090 0.0231 539.480 0.1312
290.390 0.0044 408.500 0.0333 559.900 0.1572
309.100 0.0055 430.310 0.0458 578.040 0.1860
330.350 0.0075 452.460 0.0606 602.140 0.2383
343.310 0.0094 469.450 0.0731 615.080 0.2834
355.420 0.0117 488.080 0.0873 613.660 0.2839
365.500 0.0144 489.760 0.0890 616.980 0.3221

Table 276. Test data for specimen 741–28

Test Number : 293 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 309.1 MPa Ultimate Stress : 668.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

12.454 0.0001 443.067 0.0303 609.894 0.1800

16.807 0.0000 448.216 0.0325 618.831 0.1961
64.526 0.0003 493.025 0.0574 624.126 0.2062
86.700 0.0004 504.731 0.0654 628.109 0.2143
254.804 0.0017 507.986 0.0677 638.893 0.2393
263.999 0.0018 537.567 0.0915 641.953 0.2475
272.616 0.0021 548.302 0.1016 646.470 0.2599
359.680 0.0076 550.488 0.1036 655.942 0.2910
365.363 0.0083 582.547 0.1399 659.682 0.3056
370.541 0.0090 590.173 0.1499 665.317 0.3351
437.782 0.0280 602.414 0.1679 668.037 0.3674

A–1 3 4
Table 277. Test data for specimen 741–29

Test Number : 294 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 304.5 MPa Ultimate Stress : 638.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

20.328 0.0001 459.563 0.0498 583.828 0.1908

39.274 0.0001 479.887 0.0646 589.322 0.2019
96.456 0.0003 482.716 0.0667 601.708 0.2302
230.596 0.0011 485.319 0.0688 602.576 0.2323
241.127 0.0012 522.525 0.1029 605.901 0.2408
250.722 0.0014 524.501 0.1051 617.661 0.2756
346.080 0.0063 536.260 0.1184 620.793 0.2869
351.940 0.0070 554.767 0.1425 626.818 0.3111
390.453 0.0150 556.261 0.1447 630.480 0.3286
428.097 0.0310 564.984 0.1579 633.469 0.3461
431.982 0.0330 582.575 0.1886 637.902 0.4001

Table 278. Test data for specimen 74–230

Test Number : 295 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 299.4 MPa Ultimate Stress : 631.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

17.452 0.0001 394.430 0.0148 548.051 0.1129

58.657 0.0002 400.309 0.0165 572.727 0.1417
69.006 0.0002 422.208 0.0246 574.421 0.1439
90.537 0.0004 460.964 0.0447 586.662 0.1619
102.198 0.0004 478.615 0.0559 594.791 0.1756
196.364 0.0010 481.876 0.0581 600.694 0.1871
207.686 0.0011 509.102 0.0779 609.064 0.2057
257.914 0.0020 511.908 0.0801 612.741 0.2150
315.230 0.0043 514.521 0.0823 619.612 0.2365
320.857 0.0047 543.842 0.1085 622.709 0.2484
354.954 0.0076 545.922 0.1107 631.611 0.3220

A–1 3 5
Table 279. Test data for specimen 742–25

Test Number : 024 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 269.0 MPa Ultimate Stress : 575.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

103.90 0.0003 337.39 0.0109 517.03 0.1733

147.70 0.0009 348.85 0.0146 533.05 0.2090
192.53 0.0017 368.48 0.0230 545.09 0.2437
223.79 0.0019 392.33 0.0380 552.02 0.2650
235.31 0.0021 415.14 0.0562 555.85 0.2854
258.16 0.0028 438.00 0.0767 564.23 0.3238
273.43 0.0034 456.49 0.0934 567.11 0.3468
283.93 0.0041 471.29 0.1059 571.27 0.3814
294.13 0.0048 478.28 0.1134 573.37 0.4057
304.25 0.0055 478.15 0.1162 573.85 0.4243
310.71 0.0062 493.35 0.1355 574.58 0.4486
322.71 0.0079 506.11 0.1544 575.08 0.4701
329.47 0.0091

Table 280. Test data for specimen 742–26

Test Number : 025 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 261.0 MPa Ultimate Stress : 536.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

47.90 0.0000 293.22 0.0064 465.58 0.1573

93.90 0.0003 299.93 0.0074 464.49 0.1640
139.66 0.0009 310.53 0.0106 481.61 0.1941
173.46 0.0014 319.42 0.0144 498.93 0.2307
209.25 0.0020 332.15 0.0219 511.09 0.2647
222.43 0.0021 346.29 0.0334 514.61 0.2804
239.01 0.0024 367.51 0.0524 523.32 0.3161
251.46 0.0029 386.79 0.0705 530.14 0.3543
270.91 0.0041 405.10 0.0885 532.31 0.3751
281.95 0.0050 427.53 0.1091 535.15 0.4148
285.06 0.0053 451.26 0.1376 536.71 0.4528
289.33 0.0058 461.36 0.1511 536.81 0.4799

A–1 3 6
Table 281. Test data for specimen 744–07

Test Number : 187 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 281.7 MPa Ultimate Stress : 606.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

33.818 0.0003 408.357 0.0401 527.097 0.1875

44.883 0.0004 411.123 0.0421 540.350 0.2185
55.857 0.0004 437.230 0.0635 541.314 0.2207
77.949 0.0006 464.449 0.0909 547.194 0.2363
89.356 0.0006 473.573 0.1014 561.218 0.2788
232.092 0.0020 480.546 0.1100 566.519 0.2966
249.235 0.0024 489.602 0.1222 581.893 0.3571
298.291 0.0048 490.999 0.1244 585.170 0.3727
303.130 0.0051 515.096 0.1633 595.580 0.4292
311.135 0.0057 516.205 0.1655 602.809 0.4833
405.306 0.0380 517.265 0.1677 605.942 0.5303

Table 282. Test data for specimen 744–08

Test Number : 185 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 278.2 MPa Ultimate Stress : 619.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

21.425 0.0001 402.243 0.0303 565.723 0.1827

34.320 0.0002 406.424 0.0325 578.255 0.2080
87.225 0.0005 475.349 0.0774 579.174 0.2103
98.087 0.0006 488.694 0.0883 580.142 0.2125
109.579 0.0006 491.016 0.0905 596.206 0.2543
204.584 0.0013 493.774 0.0927 599.787 0.2654
268.360 0.0031 533.692 0.1349 602.932 0.2763
274.404 0.0034 535.579 0.1371 603.609 0.2784
326.839 0.0073 537.418 0.1394 610.577 0.3059
331.895 0.0080 562.965 0.1781 614.786 0.3266
383.160 0.0217 564.465 0.1804 619.238 0.3648

A–1 3 7
Table 283. Test data for specimen 74–119

Test Number : 190 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 267.5 MPa Ultimate Stress : 587.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

13.981 0.0001 326.357 0.0097 499.928 0.1205

26.410 0.0002 369.254 0.0227 501.758 0.1225
78.205 0.0006 373.821 0.0247 520.740 0.1453
88.876 0.0006 390.471 0.0329 522.426 0.1473
99.701 0.0007 394.411 0.0350 525.365 0.1516
111.803 0.0008 420.986 0.0516 545.743 0.1826
123.221 0.0009 432.745 0.0599 564.725 0.2208
212.906 0.0020 437.534 0.0635 572.192 0.2407
244.838 0.0029 440.256 0.0656 578.166 0.2603
295.288 0.0058 467.669 0.0886 584.815 0.2938
302.346 0.0064 472.477 0.0927 587.561 0.3302

Table 284. Test data for specimen 743–13

Test Number : 197 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 265.8 MPa Ultimate Stress : 647.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

12.849 0.0001 428.458 0.0438 589.825 0.2019

66.522 0.0006 482.969 0.0799 594.161 0.2105
77.323 0.0006 500.361 0.0936 606.349 0.2378
229.079 0.0023 502.914 0.0959 610.204 0.2479
236.103 0.0026 537.746 0.1288 621.525 0.2825
242.964 0.0028 539.673 0.1311 624.416 0.2929
325.196 0.0084 541.889 0.1335 631.498 0.3242
331.050 0.0091 568.627 0.1671 633.810 0.3369
366.093 0.0159 570.313 0.1694 639.350 0.3694
402.582 0.0300 577.395 0.1804 642.675 0.4003
424.396 0.0414 588.813 0.1999 646.866 0.4810

A–1 3 8
Table 285. Test data for specimen 743–14

Test Number : 198 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 260.3 MPa Ultimate Stress : 613.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

9.666 0.0000 391.837 0.0241 545.340 0.1374

21.484 0.0001 396.762 0.0261 547.040 0.1394
61.626 0.0004 444.860 0.0513 555.395 0.1498
83.460 0.0006 448.149 0.0534 565.741 0.1643
205.648 0.0018 451.252 0.0554 567.101 0.1664
214.581 0.0020 474.641 0.0716 572.639 0.1748
222.882 0.0022 487.732 0.0817 583.617 0.1943
291.051 0.0055 490.257 0.0837 588.911 0.2050
295.908 0.0058 517.896 0.1080 599.015 0.2288
304.272 0.0065 519.888 0.1101 603.435 0.2420
364.849 0.0154 530.574 0.1210 613.490 0.2991

Table 286. Test data for specimen 74–130

Test Number : 199 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 272.3 MPa Ultimate Stress : 624.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.372 0.0001 394.609 0.0265 559.656 0.1374

39.398 0.0003 413.752 0.0345 563.230 0.1416
93.048 0.0007 418.046 0.0365 581.786 0.1646
116.548 0.0009 462.364 0.0601 583.303 0.1667
163.079 0.0013 465.737 0.0621 592.900 0.1816
242.531 0.0026 469.022 0.0641 599.166 0.1923
249.728 0.0029 501.786 0.0862 603.279 0.2009
273.365 0.0041 507.025 0.0902 611.749 0.2207
325.777 0.0090 517.404 0.0983 615.519 0.2312
331.133 0.0098 541.198 0.1189 620.660 0.2517
355.240 0.0143 551.774 0.1291 624.674 0.2907

A–1 3 9
Table 287. Test data for specimen 742–16

Test Number : 022 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 268.6 MPa Ultimate Stress : 602.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

48.46 0.0000 328.25 0.0076 477.92 0.0846

92.80 0.0003 335.89 0.0085 498.19 0.0996
129.82 0.0008 342.28 0.0094 518.24 0.1178
162.57 0.0012 351.81 0.0111 536.80 0.1375
188.33 0.0018 360.03 0.0131 550.27 0.1560
215.98 0.0021 374.07 0.0178 563.34 0.1751
229.75 0.0022 385.15 0.0224 575.95 0.1972
253.17 0.0029 399.45 0.0299 584.19 0.2167
264.85 0.0033 416.92 0.0367 591.43 0.2375
285.26 0.0044 433.97 0.0488 597.46 0.2601
303.68 0.0054 450.14 0.0609 600.29 0.2797
311.15 0.0059 461.65 0.0695 602.13 0.2970
320.93 0.0068 476.65 0.0815 602.32 0.3098

Table 288. Test data for specimen 742–17

Test Number : 023 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 267.7 MPa Ultimate Stress : 579.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

43.97 0.0000 311.68 0.0075 456.70 0.0887

91.10 0.0004 320.87 0.0088 479.34 0.1045
141.86 0.0010 328.31 0.0101 501.87 0.1240
188.56 0.0019 339.56 0.0131 533.88 0.1580
222.89 0.0024 349.86 0.0168 548.18 0.1772
239.20 0.0027 358.75 0.0203 559.53 0.1963
248.53 0.0031 380.05 0.0313 572.39 0.2259
262.01 0.0036 403.69 0.0466 577.56 0.2451
277.78 0.0045 427.01 0.0628 579.42 0.2695
294.96 0.0057 446.97 0.0775 579.69 0.2911
305.05 0.0067 457.64 0.0851

A–1 4 0
Table 289. Test data for specimen 742–22

Test Number : 182 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 269.8 MPa Ultimate Stress : 626.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

29.307 0.0001 450.635 0.0601 555.718 0.1472

44.895 0.0002 453.035 0.0617 561.320 0.1533
151.596 0.0009 473.476 0.0760 571.992 0.1650
162.621 0.0010 475.586 0.0776 573.344 0.1664
184.346 0.0012 477.702 0.0792 588.411 0.1857
280.332 0.0042 496.322 0.0935 596.910 0.1974
285.417 0.0045 513.175 0.1071 601.111 0.2041
400.235 0.0334 515.010 0.1086 603.042 0.2075
423.110 0.0425 523.509 0.1155 608.403 0.2175
425.679 0.0441 526.841 0.1185 618.737 0.2431
448.433 0.0585 552.869 0.1441 626.125 0.3040

Table 290. Test data for specimen 742–23

Test Number : 183 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 267.7 MPa Ultimate Stress : 624.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

7.838 0.0001 452.588 0.0609 545.063 0.1425

18.933 0.0001 458.157 0.0646 566.546 0.1703
60.733 0.0005 461.162 0.0670 578.207 0.1885
160.862 0.0012 473.171 0.0759 593.351 0.2171
171.527 0.0013 475.804 0.0779 595.238 0.2212
256.719 0.0033 478.895 0.0802 599.835 0.2324
262.796 0.0036 527.837 0.1238 612.851 0.2728
331.949 0.0091 529.870 0.1261 615.947 0.2859
354.187 0.0131 532.289 0.1285 616.383 0.2881
359.040 0.0143 540.902 0.1378 621.270 0.3192
364.377 0.0158 542.934 0.1401 624.221 0.3676

A–1 4 1
Table 291. Test data for specimen 74–110

Test Number : 184 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 259.2 MPa Ultimate Stress : 607.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

27.251 0.0003 269.609 0.0045 417.156 0.0544

36.763 0.0003 299.651 0.0073 420.523 0.0568
95.948 0.0007 305.830 0.0080 505.387 0.1330
106.593 0.0008 311.627 0.0088 507.661 0.1354
129.649 0.0010 362.388 0.0226 515.644 0.1446
140.526 0.0011 367.439 0.0249 518.789 0.1486
183.265 0.0015 372.278 0.0271 525.515 0.1571
192.898 0.0016 388.531 0.0361 527.160 0.1592
201.932 0.0018 392.619 0.0384 541.579 0.1797
259.569 0.0039 396.330 0.0407 548.450 0.1900
264.765 0.0042 413.894 0.0521 554.159 0.1985

Table 292. Test data for specimen 741–04

Test Number : 020 Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 257.5 MPa Ultimate Stress : 620.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

57.76 0.0001 336.51 0.0097 505.01 0.0943

84.35 0.0003 349.61 0.0118 526.11 0.1091
108.16 0.0005 361.78 0.0143 544.66 0.1268
132.20 0.0008 375.38 0.0179 561.54 0.1466
156.26 0.0012 389.25 0.0226 575.34 0.1645
180.26 0.0016 400.36 0.0268 593.78 0.1967
199.16 0.0020 410.97 0.0316 605.06 0.2220
216.72 0.0021 425.03 0.0385 614.36 0.2574
226.06 0.0022 449.49 0.0533 617.97 0.2783
240.32 0.0026 464.93 0.0634 620.32 0.2996
328.50 0.0086 480.00 0.0742 620.54 0.3100
332.62 0.0092 481.96 0.0770 620.52 0.3306

A–1 4 2
Table 293. Test data for specimen 741–05

Test Number : 021 Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 259.1 MPa Ultimate Stress : 616.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.28 0.0000 348.16 0.0102 551.58 0.1684

65.38 0.0001 355.90 0.0114 560.05 0.1884
88.01 0.0003 366.76 0.0135 569.32 0.2109
107.09 0.0004 373.19 0.0152 576.12 0.2301
133.95 0.0008 385.18 0.0188 583.73 0.2527
165.32 0.0012 395.22 0.0225 593.51 0.2900
192.16 0.0017 409.99 0.0289 598.13 0.3141
209.14 0.0019 424.77 0.0375 601.79 0.3379
224.96 0.0020 443.70 0.0500 604.62 0.3558
239.70 0.0024 462.41 0.0649 607.18 0.3778
249.73 0.0027 478.24 0.0784 610.03 0.4046
264.87 0.0035 481.27 0.0823 614.29 0.4488
282.59 0.0043 497.88 0.0978 615.70 0.4714
301.23 0.0054 512.65 0.1115 616.36 0.4978
319.14 0.0069 526.86 0.1293 616.73 0.5243
328.20 0.0077 540.49 0.1494

Table 294. Test data for specimen 744–40

Test Number : 042 Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 171.8 MPa Ultimate Stress : 412.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

42.91 0.0000 170.80 0.0018 295.56 0.0639

51.82 0.0000 173.86 0.0019 312.41 0.0797
60.94 0.0001 176.18 0.0021 328.07 0.0942
76.80 0.0002 178.69 0.0023 343.16 0.1080
89.56 0.0002 181.06 0.0026 359.03 0.1244
103.75 0.0004 187.92 0.0036 373.28 0.1419
114.14 0.0005 192.66 0.0045 385.86 0.1599
127.29 0.0006 196.21 0.0054 396.80 0.1766
139.22 0.0008 202.49 0.0068 404.05 0.1924
148.28 0.0010 211.24 0.0080 409.30 0.2065
156.71 0.0012 221.04 0.0096 409.26 0.2067
160.85 0.0013 236.13 0.0154 407.78 0.2071
164.30 0.0015 256.44 0.0282 407.95 0.2098
167.80 0.0016 276.94 0.0463 412.30 0.2131

A–1 4 3
Table 295. Test data for specimen 743–42

Test Number : 039 Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 164.6 MPa Ultimate Stress : 442.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

57.58 0.0000 176.62 0.0027 358.71 0.1229

88.11 0.0002 179.68 0.0031 369.82 0.1363
123.54 0.0006 183.55 0.0038 380.25 0.1489
129.27 0.0007 190.19 0.0055 387.68 0.1592
144.82 0.0010 201.80 0.0095 398.32 0.1743
155.49 0.0013 216.24 0.0120 404.50 0.1845
161.27 0.0015 231.45 0.0149 414.05 0.2025
163.02 0.0016 243.78 0.0204 421.87 0.2191
165.82 0.0017 263.18 0.0361 428.54 0.2361
167.32 0.0018 280.88 0.0519 430.64 0.2405
168.82 0.0019 297.27 0.0669 432.81 0.2501
170.87 0.0021 313.32 0.0814 438.13 0.2694
172.67 0.0023 330.31 0.0967 441.81 0.2893
174.92 0.0024 342.43 0.1062 442.81 0.3044

Table 296. Test data for specimen 744-35

Test Number : 259 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 193.8 MPa Ultimate Stress : 424.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.281 0.0003 262.187 0.0618 364.863 0.1762

66.334 0.0002 264.606 0.0641 365.439 0.1783
76.556 0.0002 271.916 0.0708 367.945 0.1805
126.358 0.0005 290.609 0.0885 380.079 0.2008
147.294 0.0007 292.808 0.0906 386.896 0.2127
187.269 0.0068 299.241 0.0972 399.391 0.2392
192.034 0.0089 315.622 0.1147 404.331 0.2483
196.248 0.0110 318.192 0.1168 409.803 0.2664
224.796 0.0309 327.131 0.1259 413.412 0.2731
233.199 0.0378 338.928 0.1429 422.166 0.3093
241.553 0.0442 347.272 0.1512 424.697 0.3363

A–1 4 4
Table 297. Test data for specimen 744-36

Test Number : 258 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 165.2 MPa Ultimate Stress : 424.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.895 0.0003 259.236 0.0618 346.882 0.1505

52.240 0.0003 262.299 0.0644 357.597 0.1659
113.615 0.0004 270.063 0.0713 363.639 0.1726
134.258 0.0006 289.170 0.0885 377.679 0.1989
139.842 0.0008 291.882 0.0911 381.990 0.2011
187.211 0.0095 298.514 0.0973 394.875 0.2292
191.322 0.0117 315.744 0.1148 398.825 0.2378
205.060 0.0200 317.348 0.1172 407.730 0.2597
223.611 0.0333 323.405 0.1240 411.407 0.2684
234.886 0.0422 338.879 0.1410 417.099 0.2932
237.695 0.0442 341.474 0.1430 423.994 0.3209

Table 298. Test data for specimen 74-263

Test Number : 257 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 179.9 MPa Ultimate Stress : 436.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

38.320 0.0002 198.728 0.0073 336.859 0.0937

40.152 0.0002 226.304 0.0196 358.528 0.1117
62.734 0.0003 230.316 0.0219 367.223 0.1200
72.026 0.0005 241.648 0.0284 386.259 0.1384
101.958 0.0007 262.365 0.0413 393.259 0.1455
112.620 0.0008 272.381 0.0478 405.966 0.1595
140.380 0.0014 275.514 0.0500 410.075 0.1671
148.405 0.0016 294.507 0.0628 423.768 0.1850
155.550 0.0019 304.683 0.0697 423.171 0.1873
181.372 0.0036 307.758 0.0718 430.695 0.2054
193.190 0.0056 326.420 0.0852 436.330 0.2253

A–1 4 5
Table 299. Test data for specimen 744–26

Test Number : 336 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 192.7 MPa Ultimate Stress : 440.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

106.11 0.0001 280.42 0.0515 375.61 0.1395

142.17 0.0003 289.10 0.0580 380.92 0.1462
171.87 0.0012 291.95 0.0603 384.35 0.1506
196.70 0.0039 294.72 0.0624 392.74 0.1617
201.56 0.0049 297.52 0.0646 398.63 0.1706
206.97 0.0065 305.61 0.0713 405.55 0.1817
212.68 0.0087 308.19 0.0735 410.35 0.1902
226.58 0.0154 310.94 0.0756 416.01 0.2021
230.71 0.0177 318.65 0.0822 417.15 0.2043
234.62 0.0201 326.10 0.0889 419.29 0.2110
238.39 0.0224 335.70 0.0976 425.77 0.2248
248.94 0.0292 342.64 0.1043 428.38 0.2313
252.34 0.0314 351.49 0.1130 431.64 0.2402
262.02 0.0381 357.75 0.1196 433.42 0.2488
265.25 0.0405 365.93 0.1285 435.67 0.2581
277.41 0.0493 371.80 0.1352 436.29 0.2603

Table 300. Test data for specimen 744–27

Test Number : 337 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 181.0 MPa Ultimate Stress : 420.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.87 0.0001 258.45 0.0532 376.49 0.1870

86.83 0.0003 268.36 0.0621 382.10 0.1956
140.52 0.0005 280.12 0.0731 387.60 0.2043
160.25 0.0010 291.47 0.0841 391.28 0.2136
172.60 0.0017 296.00 0.0885 393.48 0.2160
190.12 0.0046 304.61 0.0974 398.73 0.2277
195.82 0.0068 315.12 0.1084 404.59 0.2395
200.48 0.0089 321.17 0.1150 406.19 0.2485
210.77 0.0150 327.10 0.1216 411.17 0.2577
214.15 0.0173 331.05 0.1259 411.35 0.2601
216.89 0.0193 336.75 0.1326 414.90 0.2698
226.19 0.0262 338.58 0.1347 415.08 0.2720
232.02 0.0308 347.41 0.1456 416.85 0.2789
240.32 0.0376 355.92 0.1564 418.48 0.2880
245.63 0.0422 362.16 0.1650 419.34 0.2900
253.46 0.0488 369.80 0.1759 420.58 0.2969

A–1 4 6
Table 301. Test data for specimen 742–40

Test Number : 170 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 153.7 MPa Ultimate Stress : 452.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 286.83 0.0490

78.74 0.0002 347.63 0.0980
145.35 0.0010 392.11 0.1374
183.04 0.0027 426.74 0.1873
208.12 0.0055 447.13 0.2286
236.95 0.0154 452.68 0.2669
264.70 0.0321

Table 302. Test data for specimen 742–41

Test Number : 175 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 190.3 MPa Ultimate Stress : 483.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 236.23 0.0083 335.07 0.0561

43.48 0.0001 241.02 0.0093 346.32 0.0638
74.85 0.0004 246.71 0.0107 359.87 0.0727
111.79 0.0008 251.05 0.0119 368.82 0.0789
133.01 0.0012 254.74 0.0131 381.42 0.0877
146.65 0.0014 259.29 0.0147 394.19 0.0970
155.17 0.0017 263.38 0.0163 410.61 0.1074
162.99 0.0019 266.98 0.0178 422.27 0.1173
171.50 0.0022 271.22 0.0195 434.15 0.1290
180.07 0.0025 276.26 0.0218 445.44 0.1413
188.89 0.0030 280.21 0.0237 454.93 0.1531
195.31 0.0033 286.20 0.0270 461.77 0.1633
204.43 0.0039 293.15 0.0307 472.59 0.1816
210.66 0.0045 303.88 0.0366 481.07 0.2002
218.08 0.0053 314.33 0.0430 483.35 0.2125
221.83 0.0058 320.48 0.0468 483.13 0.2179
228.90 0.0068 327.32 0.0511

A–1 4 7
Table 303. Test data for specimen 74–246

Test Number : 174 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 184.4 MPa Ultimate Stress : 481.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.00 0.0000 232.55 0.0097 363.33 0.0877

39.37 0.0001 236.37 0.0108 383.42 0.1008
72.32 0.0003 241.09 0.0123 403.82 0.1187
106.72 0.0008 244.95 0.0138 415.39 0.1301
136.63 0.0014 249.46 0.0157 422.87 0.1381
145.89 0.0017 256.79 0.0187 430.44 0.1468
164.40 0.0023 264.17 0.0222 438.15 0.1570
175.54 0.0028 273.09 0.0270 444.12 0.1663
180.37 0.0031 280.12 0.0308 451.56 0.1776
193.85 0.0039 292.59 0.0389 458.30 0.1904
200.01 0.0045 299.76 0.0434 466.64 0.2072
204.99 0.0048 306.59 0.0478 466.05 0.2076
210.01 0.0054 314.15 0.0535 469.41 0.2174
215.08 0.0061 322.12 0.0588 473.03 0.2277
221.88 0.0072 331.36 0.0655 476.73 0.2426
225.01 0.0080 340.36 0.0714 480.22 0.2616
229.03 0.0088 350.68 0.0789 481.67 0.2752

Table 304. Test data for specimen 742–28

Test Number : 325 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 203.5 MPa Ultimate Stress : 473.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

17.080 0.0001 300.370 0.0347 406.440 0.1224

30.040 0.0002 310.690 0.0414 421.070 0.1400
50.360 0.0003 313.980 0.0436 426.140 0.1467
90.470 0.0006 338.650 0.0612 427.780 0.1489
100.950 0.0007 347.250 0.0678 439.520 0.1666
171.860 0.0018 350.000 0.0699 444.480 0.1755
190.750 0.0026 370.940 0.0875 452.860 0.1932
196.240 0.0029 378.240 0.0939 455.930 0.2025
245.040 0.0087 380.670 0.0961 462.940 0.2261
262.330 0.0145 398.320 0.1137 469.300 0.2473
267.560 0.0167 404.400 0.1202 473.290 0.2721

A–1 4 8
Table 305. Test data for specimen 742–29

Test Number : 326 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 215.2 MPa Ultimate Stress : 474.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

27.120 0.0002 268.040 0.0128 408.120 0.1026

44.370 0.0002 272.980 0.0146 410.450 0.1047
55.480 0.0002 309.550 0.0322 417.250 0.1114
86.410 0.0003 313.520 0.0345 429.960 0.1246
130.880 0.0005 324.890 0.0411 437.570 0.1335
140.790 0.0006 352.490 0.0588 450.860 0.1513
150.030 0.0007 355.710 0.0610 453.750 0.1559
192.710 0.0018 365.020 0.0675 461.870 0.1691
198.660 0.0020 382.350 0.0805 465.270 0.1759
214.220 0.0029 390.510 0.0871 470.750 0.1892
251.920 0.0080 393.070 0.0892 474.310 0.2089

Table 306. Test data for specimen 74–130

Test Number : 324 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 235.4 MPa Ultimate Stress : 517.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

21.010 0.0001 304.520 0.0274 436.450 0.1378

23.740 0.0001 308.170 0.0297 451.880 0.1554
96.150 0.0002 334.460 0.0476 456.960 0.1620
108.410 0.0003 343.580 0.0541 459.100 0.1643
160.820 0.0006 346.580 0.0564 477.670 0.1908
169.310 0.0006 368.940 0.0739 482.190 0.1984
192.110 0.0012 379.530 0.0827 492.940 0.2170
229.530 0.0026 401.270 0.1025 497.070 0.2283
248.700 0.0042 408.440 0.1091 505.340 0.2467
253.750 0.0050 411.000 0.1114 508.980 0.2537
293.090 0.0205 428.040 0.1289 517.560 0.2835

A–1 4 9
Table 307. Test data for specimen 742–27

Test Number : 052 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 174.9 MPa Ultimate Stress : 454.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.34 0.0000 236.55 0.0078 423.15 0.1632

83.52 0.0002 247.28 0.0121 428.95 0.1728
109.38 0.0005 259.81 0.0193 434.04 0.1824
131.30 0.0008 275.30 0.0296 438.59 0.1926
148.35 0.0011 292.41 0.0421 441.87 0.2008
163.85 0.0016 308.93 0.0550 445.91 0.2120
171.51 0.0020 326.09 0.0691 448.80 0.2181
179.31 0.0024 342.45 0.0820 448.87 0.2225
186.66 0.0029 358.21 0.0947 449.19 0.2264
192.52 0.0034 371.39 0.1038 451.04 0.2320
199.12 0.0042 385.51 0.1169 452.69 0.2384
208.25 0.0049 396.91 0.1286 454.29 0.2435
218.27 0.0057 405.83 0.1390 454.13 0.2457
222.08 0.0061 412.48 0.1477 454.26 0.2553
228.37 0.0067 417.64 0.1549

Table 308. Test data for specimen 744-06

Test Number : 330 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 185.4 MPa Ultimate Stress : 448.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.800 0.0001 267.360 0.0351 371.110 0.1235

30.150 0.0002 270.580 0.0374 373.180 0.1257
41.190 0.0002 294.990 0.0551 385.350 0.1391
62.670 0.0003 297.820 0.0573 389.150 0.1435
149.200 0.0010 300.720 0.0596 391.090 0.1457
155.050 0.0012 322.170 0.0772 406.950 0.1657
160.640 0.0014 324.720 0.0794 413.350 0.1745
211.060 0.0067 327.270 0.0816 426.950 0.1964
215.910 0.0080 349.090 0.1013 430.730 0.2034
232.460 0.0143 351.270 0.1036 442.920 0.2301
257.030 0.0283 368.970 0.1212 447.860 0.2504

A–1 5 0
Table 309. Test data for specimen 744-09

Test Number : 331 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 197.8 MPa Ultimate Stress : 507.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

13.390 0.0001 282.940 0.0302 414.890 0.1218

39.590 0.0001 287.000 0.0325 428.640 0.1349
72.350 0.0002 298.920 0.0391 430.800 0.1371
116.650 0.0003 321.040 0.0521 448.850 0.1570
135.280 0.0004 324.530 0.0544 450.790 0.1591
173.970 0.0015 334.960 0.0608 456.070 0.1657
179.350 0.0017 354.370 0.0738 472.140 0.1880
200.100 0.0030 357.470 0.0761 476.340 0.1956
233.810 0.0087 366.680 0.0825 484.930 0.2117
239.340 0.0104 383.880 0.0956 496.410 0.2385
244.390 0.0122 394.820 0.1042 507.070 0.2726

Table 310. Test data for specimen 74-120

Test Number : 332 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 176.6 MPa Ultimate Stress : 453.8 MPa

Experimental Data Not Available.

Table 311. Test data for specimen 744-18

Test Number : 233a Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 228.5 MPa Ultimate Stress : 510.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

8.442 0.0001 230.833 0.0083 350.463 0.0605

20.800 0.0001 239.849 0.0102 370.195 0.0727
41.886 0.0002 253.007 0.0138 379.351 0.0787
53.131 0.0002 254.654 0.0143 413.145 0.1031
129.137 0.0006 256.199 0.0148 428.086 0.1154
137.525 0.0007 281.982 0.0247 431.846 0.1185
144.719 0.0008 284.363 0.0258 457.804 0.1431
199.449 0.0040 286.699 0.0268 469.929 0.1570
203.403 0.0044 308.091 0.0372 490.996 0.1861
207.119 0.0047 327.487 0.0474 493.424 0.1901
228.390 0.0079 331.087 0.0493 510.474 0.2396

A–1 5 1
Table 312. Test data for specimen 743-15

Test Number : 262 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 180.0 MPa Ultimate Stress : 503.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

40.729 0.0002 259.018 0.0213 423.949 0.1307

60.887 0.0002 264.040 0.0234 426.338 0.1329
79.952 0.0003 294.467 0.0387 428.087 0.1351
90.021 0.0004 306.148 0.0451 449.406 0.1571
121.225 0.0005 309.889 0.0474 454.807 0.1638
129.808 0.0006 349.228 0.0715 465.867 0.1780
137.497 0.0007 364.990 0.0822 474.926 0.1915
196.295 0.0043 368.007 0.0845 484.068 0.2092
201.881 0.0050 384.862 0.0980 488.503 0.2187
207.112 0.0058 398.452 0.1086 497.634 0.2428
242.294 0.0146 401.080 0.1108 503.755 0.2803

Table 313. Test data for specimen 74-270

Test Number : 246 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 182.2 MPa Ultimate Stress : 495.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

41.840 0.0002 295.090 0.0383 412.530 0.1235

57.710 0.0002 306.420 0.0447 429.420 0.1407
78.370 0.0002 310.070 0.0469 435.740 0.1475
117.510 0.0004 340.570 0.0664 437.600 0.1496
139.570 0.0006 343.810 0.0685 454.760 0.1712
192.540 0.0037 353.080 0.0749 459.890 0.1780
198.850 0.0044 376.600 0.0924 472.920 0.2007
216.710 0.0069 379.270 0.0945 481.740 0.2187
249.270 0.0161 387.770 0.1013 484.770 0.2257
265.150 0.0228 403.140 0.1149 491.050 0.2437
269.810 0.0251 410.190 0.1213 495.010 0.2637

A–1 5 2
Table 314. Test data for specimen 742–18

Test Number : 051 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 166.2 MPa Ultimate Stress : 485.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.986 0.0000 183.780 0.0024 254.680 0.0105

69.838 0.0001 187.960 0.0027 261.500 0.0132
86.240 0.0002 194.900 0.0032 270.170 0.0171
100.320 0.0003 196.620 0.0033 328.240 0.0545
130.710 0.0007 197.700 0.0034 340.230 0.0635
137.260 0.0008 205.710 0.0038 356.170 0.0754
141.250 0.0009 209.150 0.0039 411.380 0.1169
157.350 0.0013 212.740 0.0040 424.790 0.1300
161.240 0.0015 226.360 0.0046 458.500 0.1721
165.070 0.0016 229.900 0.0048 464.560 0.1816
179.840 0.0022 233.920 0.0051 485.050 0.2446

Table 315. Test data for specimen 742–15

Test Number : 241 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 178.9 MPa Ultimate Stress : 516.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

42.830 0.0002 298.520 0.0375 433.390 0.1405

63.120 0.0002 326.950 0.0553 435.520 0.1427
102.860 0.0006 336.860 0.0618 452.420 0.1611
142.950 0.0013 340.150 0.0638 459.900 0.1700
163.120 0.0020 364.040 0.0814 476.920 0.1929
168.930 0.0024 373.410 0.0880 481.150 0.2003
220.410 0.0068 376.230 0.0902 492.650 0.2206
238.050 0.0101 397.550 0.1076 501.160 0.2393
243.040 0.0116 405.280 0.1142 504.160 0.2465
282.680 0.0285 407.810 0.1163 512.700 0.2740
294.720 0.0355 426.540 0.1338 515.990 0.3002

A–1 5 3
Table 316. Test data for specimen 742–24

Test Number : 240 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 184.2 MPa Ultimate Stress : 509.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

40.328 0.0002 285.582 0.0325 402.677 0.1060

73.263 0.0003 289.792 0.0347 421.982 0.1212
97.634 0.0004 301.985 0.0412 424.537 0.1233
130.710 0.0006 324.783 0.0540 439.691 0.1364
145.143 0.0010 328.407 0.0562 442.124 0.1386
172.470 0.0020 339.095 0.0627 444.447 0.1409
194.911 0.0038 359.479 0.0757 466.379 0.1628
201.229 0.0045 369.238 0.0821 472.485 0.1697
235.006 0.0111 372.374 0.0843 489.163 0.1910
240.667 0.0127 391.548 0.0976 498.985 0.2086
257.307 0.0189 394.408 0.0996 508.323 0.2346

Table 317. Test data for specimen 74-109

Test Number : 242 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10000 h
Yield Stress : 172.0 MPa Ultimate Stress : 476.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

41.960 0.0002 278.190 0.0388 401.560 0.1428

45.770 0.0002 302.930 0.0558 416.700 0.1600
61.070 0.0001 312.370 0.0626 422.110 0.1665
101.970 0.0004 315.120 0.0648 423.850 0.1688
125.570 0.0008 336.710 0.0817 436.970 0.1866
147.750 0.0015 344.530 0.0880 441.460 0.1932
204.990 0.0065 346.960 0.0904 452.320 0.2130
222.950 0.0107 366.630 0.1077 460.950 0.2303
228.350 0.0123 373.610 0.1143 464.570 0.2390
264.110 0.0298 375.920 0.1164 471.980 0.2601
274.860 0.0365 393.400 0.1339 476.750 0.2852

A–1 5 4
Table 318. Test data for specimen 741–06

Test Number : 048 Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 172.0 MPa Ultimate Stress : 500.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

43.97 0.0000 206.82 0.0035 446.50 0.1035

66.29 0.0001 215.45 0.0037 455.21 0.1108
83.95 0.0002 220.15 0.0039 465.41 0.1194
99.14 0.0003 229.32 0.0041 472.49 0.1267
107.85 0.0004 237.45 0.0044 478.40 0.1338
120.05 0.0006 249.54 0.0058 482.94 0.1390
127.18 0.0007 254.97 0.0067 483.13 0.1428
136.08 0.0008 263.92 0.0084 483.42 0.1449
149.54 0.0011 326.74 0.0309 485.26 0.1473
155.78 0.0013 344.39 0.0399 487.52 0.1511
174.93 0.0020 367.85 0.0534 490.45 0.1554
185.04 0.0025 392.09 0.0683 493.15 0.1603
196.53 0.0031 419.63 0.0864 495.99 0.1664
202.46 0.0033 434.98 0.0972

Table 319. Test data for specimen 742–09

Test Number : 047 Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 170.3 MPa Ultimate Stress : 485.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

45.5000 0.0000 209.8600 0.0038 361.8700 0.0570

87.0190 0.0003 213.2400 0.0039 374.6400 0.0656
113.9700 0.0005 220.2400 0.0042 387.9400 0.0744
129.9500 0.0008 226.1700 0.0043 399.1400 0.0823
138.3100 0.0009 234.0500 0.0046 410.2100 0.0908
148.3300 0.0012 243.7800 0.0056 418.6900 0.0972
153.3400 0.0013 256.2800 0.0078 439.2100 0.1128
160.6600 0.0015 270.6000 0.0112 453.8700 0.1281
168.4700 0.0019 284.8100 0.0157 465.9400 0.1432
173.2300 0.0020 291.2200 0.0181 475.7700 0.1594
181.0000 0.0024 299.0400 0.0211 482.4100 0.1741
185.1700 0.0026 311.2500 0.0270 484.5700 0.1784
194.0500 0.0031 322.6900 0.0327 485.1600 0.1813
199.9300 0.0035 337.8300 0.0416 484.9300 0.1905
205.9000 0.0037 349.0300 0.0487 485.1000 0.1967

A–1 5 5
Table 320. Test data for specimen 753–40

Test Number : 032 Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 313.5 MPa Ultimate Stress : 610.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

77.16 0.0001 365.32 0.0062 489.21 0.0761

118.01 0.0003 371.61 0.0069 507.80 0.0934
160.83 0.0007 381.23 0.0083 527.54 0.1132
197.95 0.0012 388.16 0.0099 548.51 0.1418
209.02 0.0014 394.15 0.0114 559.04 0.1605
227.05 0.0016 400.38 0.0133 574.58 0.1971
235.44 0.0016 412.09 0.0179 587.16 0.2345
243.44 0.0017 423.05 0.0231 594.90 0.2637
279.36 0.0023 440.90 0.0341 601.22 0.2945
306.14 0.0029 464.33 0.0519 606.19 0.3291
328.63 0.0037 480.06 0.0650 609.41 0.3687
343.73 0.0045 487.62 0.0719 610.35 0.4031
357.23 0.0054

Table 321. Test data for specimen 753–41

Test Number : 033 Test Temp. : 25°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 330.5 MPa Ultimate Stress : 589.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

68.82 0.0001 353.02 0.0056 503.22 0.0919

111.68 0.0004 362.44 0.0067 512.45 0.0990
156.27 0.0008 370.87 0.0080 525.70 0.1146
189.39 0.0013 379.64 0.0096 536.89 0.1304
204.14 0.0015 395.01 0.0135 553.88 0.1595
213.28 0.0016 406.69 0.0182 566.90 0.1937
226.29 0.0017 422.55 0.0259 576.29 0.2257
243.89 0.0019 441.60 0.0382 583.13 0.2586
288.66 0.0027 463.10 0.0548 587.81 0.2923
312.30 0.0035 479.22 0.0683 589.38 0.3107
327.04 0.0040 482.62 0.0712 589.78 0.3362
338.88 0.0047 484.99 0.0744 589.79 0.3585
344.82 0.0051

A–1 5 6
Table 322. Test data for specimen 753–30

Test Number : 203 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000h
Yield Stress : 315.6 MPa Ultimate Stress : 609.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

18.907 0.0002 395.921 0.0176 562.345 0.1509

42.475 0.0005 440.565 0.0385 571.550 0.1668
96.150 0.0008 459.322 0.0498 572.611 0.1688
192.666 0.0014 462.817 0.0520 583.648 0.1931
204.985 0.0015 499.739 0.0794 584.419 0.1951
249.778 0.0020 502.294 0.0817 590.347 0.2114
306.663 0.0036 505.185 0.0840 594.202 0.2237
323.363 0.0045 533.090 0.1115 598.685 0.2400
331.797 0.0051 535.115 0.1138 602.637 0.2583
368.503 0.0099 544.947 0.1256 607.022 0.2849
390.731 0.0157 557.140 0.1425 609.047 0.3146

Table 323. Test data for specimen 754-28

Test Number : 204 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000h
Yield Stress : 321.7 MPa Ultimate Stress : 619.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

12.251 0.0001 419.960 0.0218 568.133 0.1450

34.804 0.0002 465.888 0.0456 569.396 0.1471
88.596 0.0006 469.108 0.0476 583.531 0.1745
99.875 0.0006 472.698 0.0499 584.552 0.1766
174.477 0.0011 510.280 0.0778 585.426 0.1787
186.781 0.0012 512.563 0.0798 598.930 0.2154
264.141 0.0022 517.081 0.0838 602.573 0.2285
298.523 0.0031 539.085 0.1060 609.762 0.2594
306.052 0.0033 541.028 0.1081 613.162 0.2794
368.704 0.0080 544.623 0.1121 615.300 0.2953
393.258 0.0128 560.021 0.1325 619.088 0.3533

A–1 5 7
Table 324. Test data for specimen 75-135

Test Number : 205 Test Temp. : 25°C

Aging Temp. : 290°C Aging Time : 30,000h
Yield Stress : 310.6 MPa Ultimate Stress : 630.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

16.131 0.0001 424.177 0.0274 572.696 0.1450

39.509 0.0003 460.190 0.0458 574.110 0.1473
81.564 0.0006 464.179 0.0481 589.813 0.1742
140.433 0.0011 478.702 0.0572 593.763 0.1823
260.844 0.0026 505.059 0.0754 606.978 0.2168
269.748 0.0029 507.839 0.0776 616.731 0.2518
313.876 0.0044 510.862 0.0799 617.365 0.2539
338.668 0.0060 538.951 0.1047 622.388 0.2787
346.046 0.0067 541.292 0.1070 622.680 0.2808
397.464 0.0171 551.045 0.1176 628.922 0.3303
418.774 0.0251 571.038 0.1426 630.288 0.3659

Table 325. Test data for specimen 754–21

Test Number : 136 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000h
Yield Stress : 355.9 MPa Ultimate Stress : 693.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.000 0.0000 436.450 0.0171 593.610 0.1044

48.641 0.0002 459.850 0.0241 592.740 0.1047
208.470 0.0026 471.710 0.0283 634.930 0.1531
343.960 0.0061 486.140 0.0365 663.180 0.2118
388.060 0.0092 524.430 0.0578 685.700 0.2947
413.870 0.0123 560.710 0.0819 693.660 0.3958

Table 326. Test data for specimen 754-25

Test Number : 139 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 10,000h
Yield Stress : 406.3MPa Ultimate Stress : 706.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.000 0.0000 451.910 0.0129 637.060 0.1280

34.659 0.0001 473.520 0.0182 665.550 0.1697
206.780 0.0022 488.760 0.0244 678.530 0.1957
353.210 0.0040 537.850 0.0511 688.120 0.2220
392.300 0.0058 570.150 0.0733 703.330 0.2905
427.650 0.0089 603.730 0.0980 705.940 0.3728

A–1 5 8
Table 327. Test data for specimen 752–41

Test Number : 161 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000h
Yield Stress : 357.9 MPa Ultimate Stress : 726.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

68.878 0.0001 433.740 0.0099 641.470 0.1087

104.730 0.0003 455.510 0.0132 653.230 0.1205
148.220 0.0008 469.720 0.0158 668.750 0.1401
177.710 0.0010 486.150 0.0202 678.970 0.1539
196.030 0.0012 487.380 0.0217 689.900 0.1705
219.070 0.0016 524.100 0.0358 699.930 0.1906
254.830 0.0022 551.170 0.0499 709.200 0.2176
287.150 0.0029 574.600 0.0646 717.080 0.2421
308.750 0.0034 595.730 0.0779 718.110 0.2454
354.750 0.0049 610.280 0.0877 726.010 0.2752
400.620 0.0073 622.420 0.0961 726.850 0.3031

Table 328. Test data for specimen 754-39

Test Number : 162 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000h
Yield Stress : 395.1 MPa Ultimate Stress : 722.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.000 0.0000 487.210 0.0239 668.850 0.1412

361.240 0.0060 509.070 0.0321 692.810 0.1789
396.640 0.0083 539.540 0.0467 710.940 0.2040
423.810 0.0109 579.740 0.0698 720.130 0.2679
442.600 0.0133 617.330 0.0945 722.540 0.2900
467.520 0.0184 652.490 0.1225

Table 329. Test data for specimen 75-245

Test Number : 167 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 30,000h
Yield Stress : 323.1 MPa Ultimate Stress : 691.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

0.0000 0.0000 441.7100 0.0176 630.8700 0.1369

250.0600 0.0023 463.3100 0.0247 661.2200 0.1873
337.1400 0.0052 475.7100 0.0293 683.6300 0.2586
388.7400 0.0087 485.2900 0.0331 691.2700 0.3612
405.0500 0.0106 535.5200 0.0616
422.8200 0.0134 582.0500 0.0937

A–1 5 9
Table 330. Test data for specimen 751-28

Test Number : 033 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000h
Yield Stress : 334.7 MPa Ultimate Stress : 689.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

68.817 0.000 338.880 0.005 479.220 0.068

111.680 0.000 344.820 0.005 484.990 0.074
156.270 0.001 353.020 0.006 503.220 0.092
189.390 0.001 362.440 0.007 512.450 0.099
204.140 0.002 370.870 0.008 525.700 0.115
213.280 0.002 379.640 0.010 536.890 0.130
226.290 0.002 395.010 0.014 553.880 0.160
243.890 0.002 406.690 0.018 566.900 0.194
288.660 0.003 422.550 0.026 576.290 0.226
312.300 0.003 441.600 0.038 583.130 0.259
327.040 0.004 463.100 0.055 589.790 0.359

Table 331. Test data for specimen 751-29

Test Number : 297 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000h
Yield Stress : 352.0 MPa Ultimate Stress : 729.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

54.600 0.0000 445.340 0.0093 660.670 0.1059

102.720 0.0002 451.700 0.0101 677.290 0.1230
152.200 0.0005 511.560 0.0228 686.150 0.1336
190.280 0.0007 527.310 0.0279 690.990 0.1401
239.960 0.0010 544.120 0.0342 698.550 0.1508
251.660 0.0012 568.390 0.0448 702.650 0.1573
283.680 0.0017 585.260 0.0533 708.900 0.1682
353.810 0.0035 603.970 0.0638 717.000 0.1856
361.280 0.0038 614.160 0.0701 723.610 0.2034
382.340 0.0047 638.240 0.0870 725.590 0.2101
417.260 0.0068 651.250 0.0975 729.710 0.2397

A–1 6 0
Table 332 Test data for specimen 75-230

Test Number : 298 Test Temp. : 25°C

Aging Temp. : 320°C Aging Time : 50,000h
Yield Stress : 378.4 MPa Ultimate Stress : 759.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.710 0.0001 508.940 0.0237 714.680 0.1461

28.190 0.0001 567.950 0.0329 722.910 0.1596
43.390 0.0002 587.160 0.0413 726.700 0.1664
77.140 0.0003 619.600 0.0584 731.290 0.1755
135.460 0.0005 636.700 0.0692 737.430 0.1891
148.340 0.0006 639.880 0.0713 738.490 0.1914
238.630 0.0012 662.680 0.0885 742.130 0.2006
307.310 0.0020 665.240 0.0907 748.060 0.2190
364.410 0.0033 692.360 0.1171 751.520 0.2313
429.700 0.0060 698.030 0.1237 754.230 0.2429
505.220 0.0142 708.340 0.1371 759.480 0.2856

Table 333. Test data for specimen 752–25

Test Number : 036 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 346,5 MPa Ultimate Stress : 667.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

73.49 0.0001 381.17 0.0061 543.88 0.0696

119.13 0.0004 397.04 0.0075 566.03 0.0871
154.98 0.0007 407.83 0.0088 588.31 0.1036
188.94 0.0011 419.41 0.0104 606.86 0.1220
199.93 0.0013 425.20 0.0112 623.27 0.1447
205.64 0.0013 433.30 0.0130 639.85 0.1730
227.79 0.0015 442.18 0.0152 649.10 0.1938
239.21 0.0017 457.15 0.0196 657.41 0.2192
263.77 0.0020 471.75 0.0253 661.75 0.2383
297.97 0.0027 484.27 0.0310 666.43 0.2619
325.15 0.0035 488.93 0.0350 667.26 0.2736
346.41 0.0043 515.86 0.0508 667.75 0.2930
364.99 0.0052

A–1 6 1
Table 334. Test data for specimen 752–26

Test Number : 037 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 346.5 MPa Ultimate Stress : 688.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

59.65 0.0000 404.74 0.0071 570.33 0.0760

93.85 0.0002 415.16 0.0081 592.85 0.0929
130.88 0.0005 420.91 0.0086 611.04 0.1059
168.71 0.0009 432.01 0.0100 625.94 0.1218
199.47 0.0013 441.47 0.0114 642.65 0.1434
207.97 0.0014 451.91 0.0133 651.15 0.1567
220.14 0.0015 461.64 0.0157 660.27 0.1739
234.09 0.0016 475.87 0.0199 668.44 0.1924
251.98 0.0019 486.96 0.0241 676.12 0.2154
277.03 0.0023 488.94 0.0264 680.67 0.2334
310.62 0.0030 510.17 0.0365 684.79 0.2525
334.08 0.0037 539.13 0.0540 688.70 0.2790
353.25 0.0043 548.02 0.0599 688.85 0.2967
386.38 0.0058

Table 335. Test data for specimen 754-06

Test Number : 140 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 332.7 MPa Ultimate Stress : 741.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

52.922 0.0003 454.660 0.0134 671.190 0.1332

204.610 0.0023 480.910 0.0183 670.790 0.1333
226.170 0.0025 495.550 0.0249 701.930 0.1747
346.910 0.0054 541.000 0.0434 725.090 0.2325
406.130 0.0081 596.460 0.0744 739.370 0.2914
434.270 0.0109 645.880 0.1070 741.080 0.3489

A–1 6 2
Table 336. Test data for specimen 754-07

Test Number : 141 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 352.5 MPa Ultimate Stress : 728.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

38.296 0.0001 454.290 0.0144 663.470 0.1291

205.090 0.0020 474.210 0.0182 681.580 0.1546
227.300 0.0022 488.150 0.0231 702.230 0.1908
343.640 0.0048 528.390 0.0389 719.020 0.2465
402.370 0.0085 564.520 0.0576 719.220 0.2463
430.080 0.0111 607.110 0.0840 727.900 0.2976
636.250 0.1036 728.490 0.2975

Table 337. Test data for specimen 754-08

Test Number : 225 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 308.6 MPa Ultimate Stress : 718.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

33.260 0.0002 396.930 0.0083 662.250 0.1479

45.180 0.0002 404.440 0.0090 672.080 0.1628
61.780 0.0003 429.060 0.0121 680.680 0.1779
110.540 0.0005 482.310 0.0246 686.900 0.1909
122.510 0.0006 577.070 0.0696 696.420 0.2154
134.590 0.0007 580.460 0.0716 706.660 0.2489
208.410 0.0013 603.710 0.0883 707.070 0.2511
279.680 0.0027 606.410 0.0904 710.910 0.2691
313.330 0.0037 621.680 0.1030 711.590 0.2736
320.770 0.0040 641.880 0.1236 715.230 0.2964
373.210 0.0065 651.140 0.1329 718.730 0.3560

A–1 6 3
Table 338. Test data for specimen 75-119

Test Number : 144 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 354.0 MPa Ultimate Stress : 742.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

57.819 0.0009 464.680 0.0168 647.710 0.1080

199.560 0.0034 479.370 0.0197 677.920 0.1408
218.060 0.0039 488.860 0.0235 703.990 0.1833
320.720 0.0063 513.370 0.0316 721.850 0.2267
407.600 0.0109 542.610 0.0440 735.150 0.2859
440.510 0.0136 581.790 0.0654 742.780 0.3565

Table 339. Test data for specimen 753-10

Test Number : 200 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 316.1 MPa Ultimate Stress : 766.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

15.470 0.0001 257.140 0.0021 685.390 0.1009

17.770 0.0001 340.180 0.0046 707.290 0.1215
30.840 0.0002 374.850 0.0060 722.630 0.1398
41.740 0.0002 387.210 0.0067 731.250 0.1521
63.970 0.0004 393.270 0.0070 753.540 0.1986
74.670 0.0004 415.140 0.0083 757.040 0.2095
85.580 0.0005 575.470 0.0389 757.370 0.2116
119.960 0.0007 580.430 0.0408 761.310 0.2277
131.950 0.0007 621.310 0.0591 763.880 0.2412
144.250 0.0008 642.270 0.0707 765.570 0.2594
181.040 0.0011 672.290 0.0906 766.280 0.2711

A–1 6 4
Table 340. Test data for specimen 753-11

Test Number : 201 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 344.3 MPa Ultimate Stress : 748.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

11.730 0.0001 251.070 0.0019 582.880 0.0449

17.140 0.0001 291.190 0.0026 611.890 0.0589
29.920 0.0002 300.100 0.0028 615.570 0.0609
40.310 0.0003 308.730 0.0031 636.160 0.0729
50.870 0.0004 341.120 0.0041 648.570 0.0810
61.090 0.0005 348.440 0.0043 689.120 0.1136
71.580 0.0005 376.080 0.0055 697.880 0.1223
82.390 0.0006 416.970 0.0077 710.000 0.1369
104.540 0.0007 446.100 0.0100 739.800 0.1898
228.180 0.0016 502.770 0.0185 746.470 0.2142
239.940 0.0017 526.130 0.0243 747.650 0.2233

Table 341. Test data for specimen 75-130

Test Number : 202 Test Temp. : 25°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 300.8 MPa Ultimate Stress : 711.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.680 0.0001 260.450 0.0025 562.070 0.0527

27.100 0.0001 268.520 0.0027 587.950 0.0680
57.420 0.0003 321.250 0.0044 602.990 0.0783
67.750 0.0004 328.040 0.0047 605.990 0.0803
112.940 0.0006 371.970 0.0066 635.380 0.1046
124.280 0.0007 406.490 0.0088 675.220 0.1519
182.390 0.0011 414.230 0.0094 686.970 0.1727
193.660 0.0012 439.280 0.0120 692.150 0.1833
204.490 0.0013 452.530 0.0140 695.610 0.1918
214.600 0.0015 486.850 0.0217 710.190 0.2560
251.850 0.0022 549.230 0.0461 710.880 0.2695

A–1 6 5
Table 342. Test data for specimen 752–16

Test Number : 034 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 326.7 MPa Ultimate Stress : 703.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

76.17 0.0001 396.10 0.0074 568.50 0.0724

116.51 0.0003 403.19 0.0080 591.38 0.0877
152.92 0.0007 415.13 0.0094 613.10 0.1019
195.20 0.0013 427.70 0.0111 631.87 0.1188
202.49 0.0014 438.06 0.0130 651.39 0.1405
217.08 0.0015 447.88 0.0148 663.74 0.1569
227.52 0.0016 464.22 0.0190 674.85 0.1763
254.96 0.0019 469.79 0.0207 686.51 0.2011
293.55 0.0027 469.75 0.0211 695.94 0.2289
318.58 0.0035 482.68 0.0255 702.18 0.2627
354.25 0.0049 487.15 0.0283 703.57 0.2788
374.46 0.0059 508.36 0.0376 703.58 0.3047
387.87 0.0068 538.21 0.0535

Table 343. Test data for specimen 752–17

Test Number : 035 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 353.1 MPa Ultimate Stress : 731.5 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

51.87 0.0000 415.15 0.0075 600.07 0.0693

92.12 0.0002 427.94 0.0085 617.69 0.0807
133.71 0.0006 438.10 0.0096 642.48 0.0970
169.18 0.0010 448.40 0.0107 662.79 0.1101
196.51 0.0013 456.96 0.0120 682.40 0.1292
206.15 0.0014 471.20 0.0143 696.62 0.1461
229.57 0.0016 479.11 0.0160 706.37 0.1602
241.54 0.0017 485.87 0.0177 715.42 0.1768
287.10 0.0025 490.84 0.0193 722.18 0.1928
311.74 0.0030 511.05 0.0257 726.45 0.2088
336.48 0.0038 531.56 0.0339 730.62 0.2269
366.47 0.0048 547.90 0.0411 731.50 0.2468
395.91 0.0062 578.07 0.0570

A–1 6 6
Table 344. Test data for specimen 752-15

Test Number : 142 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 405.3 MPa Ultimate Stress : 777.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

196.500 0.0023 476.870 0.0145 712.470 0.1307

234.030 0.0029 497.610 0.0192 736.930 0.1608
364.040 0.0064 542.590 0.0308 761.290 0.2061
416.570 0.0089 592.130 0.0526 774.830 0.2507
452.570 0.0120 636.250 0.0761 777.060 0.2910
683.480 0.1051 777.060 0.3241

Table 345. Test data for specimen 752-22

Test Number : 143 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 367.7 MPa Ultimate Stress : 749.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

48.437 0.0001 457.530 0.0062 673.900 0.0911

136.060 0.0010 476.050 0.0065 705.860 0.1202
170.050 0.0014 496.530 0.0081 726.020 0.1470
218.750 0.0022 527.000 0.0091 742.570 0.1859
218.750 0.0023 585.350 0.0315 748.660 0.2244
260.200 0.0025 634.610 0.0630 748.960 0.2250
749.070 0.2516

A–1 6 7
Table 346. Test data for specimen 752-23

Test Number : 231 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 338.9MPa Ultimate Stress : 726.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

22.240 0.0001 201.840 0.0011 407.290 0.0070

34.880 0.0002 214.420 0.0013 634.090 0.0772
51.080 0.0003 271.880 0.0020 646.910 0.0855
76.780 0.0004 291.410 0.0024 672.620 0.1043
88.920 0.0005 318.200 0.0031 682.600 0.1128
100.790 0.0005 334.380 0.0036 706.530 0.1391
112.790 0.0006 342.270 0.0039 708.140 0.1413
137.610 0.0007 349.800 0.0042 714.060 0.1505
150.940 0.0008 390.310 0.0060 722.490 0.1687
163.660 0.0009 396.200 0.0063 724.850 0.1775
176.280 0.0010 401.980 0.0067 725.730 0.1816

Table 347. Test data for specimen 75-109

Test Number : 145 Test Temp. : 25°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 359.0 MPa Ultimate Stress : 736.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

48.892 0.0012 472.220 0.0247 643.790 0.1140

199.300 0.0051 478.010 0.0261 676.920 0.1447
219.940 0.0054 489.830 0.0315 702.560 0.1779
348.950 0.0102 520.200 0.0433 719.440 0.2148
403.120 0.0139 551.920 0.0594 730.490 0.2542
428.950 0.0168 552.110 0.0591 736.790 0.2928
452.430 0.0204 600.380 0.0858 736.850 0.3318

A–1 6 8
Table 348. Test data for specimen 751–04

Test Number : 030 Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 311.7 MPa Ultimate Stress : 721.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

48.54 0.0000 408.53 0.0077 606.25 0.0714

90.43 0.0002 425.74 0.0089 630.29 0.0880
134.83 0.0005 443.64 0.0105 650.99 0.1013
179.28 0.0010 459.28 0.0123 666.13 0.1154
201.61 0.0014 473.69 0.0144 681.92 0.1326
218.76 0.0016 480.11 0.0155 695.37 0.1515
226.90 0.0017 489.23 0.0181 704.74 0.1687
262.63 0.0023 508.22 0.0229 712.42 0.1847
302.11 0.0032 537.36 0.0333 717.21 0.1999
341.04 0.0045 560.99 0.0451 720.61 0.2197
382.40 0.0063 582.85 0.0569 721.16 0.2289

Table 349. Test data for specimen 751–05

Test Number : 031 Test Temp. : 25°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 314.7 MPa Ultimate Stress : 746.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

69.62 0.0001 444.52 0.0099 618.84 0.0725

107.39 0.0003 461.24 0.0115 644.55 0.0900
147.01 0.0006 476.58 0.0133 665.59 0.1043
189.06 0.0012 485.24 0.0147 682.15 0.1204
205.23 0.0014 491.81 0.0160 707.31 0.1507
230.62 0.0017 505.54 0.0191 716.41 0.1659
253.21 0.0020 514.49 0.0214 728.36 0.1919
292.87 0.0027 525.23 0.0245 734.97 0.2082
338.76 0.0042 540.84 0.0298 739.68 0.2245
384.84 0.0059 560.52 0.0386 743.29 0.2445
393.36 0.0063 580.00 0.0488 745.32 0.2634
422.32 0.0080 598.87 0.0595 746.35 0.2819
433.57 0.0089

A–1 6 9
Table 350. Test data for specimen 754–40

Test Number : 05 4 Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 196.8 MPa Ultimate Stress : 470.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.18 0.0000 232.42 0.0037 321.07 0.0442

89.11 0.0003 235.69 0.0040 341.04 0.0590
123.96 0.0006 238.81 0.0045 358.98 0.0725
145.21 0.0010 241.44 0.0049 378.49 0.0875
168.03 0.0015 244.76 0.0056 388.33 0.0953
181.49 0.0018 248.03 0.0065 401.73 0.1046
186.97 0.0020 251.20 0.0074 416.71 0.1194
191.35 0.0022 255.12 0.0087 431.07 0.1357
194.07 0.0024 259.39 0.0103 440.38 0.1474
200.63 0.0026 267.13 0.0130 450.70 0.1642
209.03 0.0028 271.85 0.0150 458.00 0.1774
214.22 0.0030 277.26 0.0177 463.66 0.1900
220.40 0.0032 282.13 0.0203 468.28 0.1987
226.04 0.0034 293.96 0.0268 469.36 0.2018
228.27 0.0035 308.43 0.0357 470.76 0.2125

Table 351. Test data for specimen 753–42

Test Number : 050 Test Temp. : 290°C

Aging Temp. : Unaged Aging Time :–
Yield Stress : 191.5 MPa Ultimate Stress : 474.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

44.3440 0.00 222.08 0.0034 398.27 0.1090

83.0220 0.0002 230.60 0.0039 406.65 0.1179
116.82 0.0005 236.84 0.0045 412.76 0.1236
134.36 0.0007 241.51 0.0055 417.75 0.1304
149.20 0.0009 246.82 0.0071 429.08 0.1449
157.04 0.0011 257.83 0.0110 435.04 0.1534
167.23 0.0013 267.57 0.0153 448.85 0.1758
175.47 0.0015 275.63 0.0197 457.06 0.1903
181.93 0.0017 285.57 0.0256 461.73 0.2050
188.24 0.0019 303.24 0.0371 464.70 0.2151
191.40 0.0021 323.45 0.0513 469.08 0.2283
195.44 0.0023 339.98 0.0633 473.01 0.2433
200.38 0.0026 353.00 0.0738 474.09 0.2465
208.54 0.0029 363.78 0.0821 472.18 0.2507
217.28 0.0032 375.41 0.0914 472.42 0.2565

A–1 7 0
Table 352. Test data for specimen 754–29

Test Number : 252 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 193.3 MPa Ultimate Stress : 528.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

36.412 0.0002 179.423 0.0025 441.862 0.1347

41.148 0.0002 210.220 0.0040 451.291 0.1433
57.528 0.0002 249.736 0.0243 466.427 0.1593
70.250 0.0002 274.563 0.0351 468.035 0.1617
90.632 0.0004 300.745 0.0478 476.025 0.1705
100.911 0.0004 305.263 0.0503 489.641 0.1880
111.112 0.0005 337.575 0.0668 499.259 0.2017
121.536 0.0006 375.916 0.0883 505.088 0.2109
130.814 0.0007 379.132 0.0904 514.852 0.2408
148.456 0.0012 407.233 0.1086 521.458 0.2536
156.695 0.0013 421.315 0.1174 528.307 0.2792

Table 353. Test data for specimen 754–30

Test Number : 248 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 202.6 MPa Ultimate Stress : 495.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

45.680 0.0003 223.970 0.0065 437.350 0.1377

51.210 0.0003 239.970 0.0109 457.490 0.1616
77.100 0.0003 246.020 0.0132 469.940 0.1789
87.660 0.0003 266.990 0.0223 470.880 0.1812
131.440 0.0005 288.840 0.0333 478.480 0.1979
159.370 0.0008 317.470 0.0486 480.510 0.2001
167.100 0.0011 354.290 0.0707 483.830 0.2023
186.600 0.0017 381.810 0.0883 489.030 0.2185
191.790 0.0020 394.310 0.0971 490.780 0.2207
211.650 0.0039 404.210 0.1068 494.300 0.2384
218.380 0.0050 425.420 0.1247 495.230 0.2454

A–1 7 1
Table 354. Test data for specimen 75–236

Test Number : 253 Test Temp. : 290°C

Aging Temp. : 290°C Aging Time : 30,000 h
Yield Stress : 211.8 MPa Ultimate Stress : 486.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

36.892 0.0002 255.878 0.0141 361.326 0.0738

37.892 0.0002 261.540 0.0166 382.851 0.0889
94.768 0.0006 289.771 0.0303 404.074 0.1067
105.428 0.0007 294.023 0.0325 421.601 0.1244
166.972 0.0018 298.105 0.0347 424.542 0.1268
175.525 0.0020 317.777 0.0457 437.309 0.1402
183.733 0.0023 321.576 0.0480 450.461 0.1679
217.030 0.0043 335.938 0.0567 454.177 0.1704
223.160 0.0052 339.600 0.0588 467.364 0.1903
228.276 0.0061 343.106 0.0609 477.248 0.2153
251.084 0.0121 359.107 0.0716 484.505 0.2478

Table 355. Test data for specimen 754–26

Test Number : 095 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 205.6 MPa Ultimate Stress : 538.0 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

162.940 0.0011 288.440 0.0100 496.920 0.1370

170.480 0.0013 294.330 0.0114 499.300 0.1401
208.430 0.0024 323.730 0.0215 514.560 0.1594
213.960 0.0025 347.960 0.0328 519.350 0.1694
219.180 0.0026 366.250 0.0426 520.010 0.1712
225.250 0.0027 397.430 0.0605 524.370 0.1805
234.270 0.0028 411.880 0.0697 527.510 0.1911
265.920 0.0055 427.730 0.0796 531.100 0.1985
272.200 0.0065 431.270 0.0820 532.860 0.2008
278.730 0.0076 465.900 0.1042 533.870 0.2045
283.340 0.0087 482.360 0.1211 538.030 0.2252

A–1 7 2
Table 356. Test data for specimen 754–27

Test Number : 096 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 10,000 h
Yield Stress : 212.2 MPa Ultimate Stress : 534.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

177.540 0.0016 286.010 0.0088 424.200 0.0791

183.830 0.0018 321.270 0.0196 431.780 0.0848
188.850 0.0019 324.520 0.0210 444.420 0.0932
194.850 0.0021 337.700 0.0281 467.830 0.1091
200.550 0.0023 341.680 0.0300 471.420 0.1126
221.550 0.0027 356.970 0.0381 483.540 0.1269
226.910 0.0027 360.900 0.0402 492.980 0.1391
235.910 0.0029 364.890 0.0425 494.170 0.1410
245.150 0.0034 387.120 0.0555 502.840 0.1533
262.310 0.0047 409.150 0.0698 509.540 0.1658
266.490 0.0053 413.040 0.0723 521.010 0.1840

Table 357. Test data for specimen 752–40

Test Number : 172 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 231.7 MPa Ultimate Stress : 589.3 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

93.421 0.0002 326.590 0.0128 475.750 0.0805

166.240 0.0010 339.400 0.0162 492.070 0.0906
213.040 0.0021 352.160 0.0199 516.690 0.1042
245.550 0.0034 361.640 0.0232 543.400 0.1291
265.980 0.0046 371.940 0.0271 559.930 0.1493
284.890 0.0060 390.000 0.0347 574.500 0.1689
300.400 0.0081 408.280 0.0434 583.160 0.1895
313.740 0.0102 420.580 0.0495 588.990 0.2076

A–1 7 3
Table 358. Test data for specimen 752–42

Test Number : 171 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 268.5 MPa Ultimate Stress : 575.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

230.660 0.0030 369.990 0.0264 518.740 0.1080

265.350 0.0048 381.830 0.0310 532.150 0.1200
284.650 0.0062 404.550 0.0411 543.340 0.1316
297.110 0.0078 430.020 0.0540 552.940 0.1419
311.170 0.0098 459.230 0.0703 562.120 0.1553
322.820 0.0120 476.450 0.0810 569.480 0.1705
334.870 0.0150 494.220 0.0927 573.540 0.1820
348.320 0.0189 507.540 0.0988 575.810 0.1904

Table 359. Test data for specimen 75–246

Test Number : 177 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 30,000 h
Yield Stress : 213.0 MPa Ultimate Stress : 521.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

46.497 0.0000 258.800 0.0065 421.490 0.0760

77.711 0.0002 266.280 0.0075 427.680 0.0800
132.720 0.0009 285.060 0.0110 451.050 0.0965
155.130 0.0013 291.140 0.0126 460.800 0.1019
166.430 0.0015 313.720 0.0192 475.560 0.1176
189.580 0.0021 323.000 0.0225 479.520 0.1228
203.470 0.0027 337.710 0.0289 490.390 0.1379
212.740 0.0031 342.940 0.0302 495.670 0.1478
222.690 0.0036 377.670 0.0497 502.420 0.1582
229.870 0.0041 390.640 0.0570 511.320 0.1738
238.280 0.0046 402.720 0.0640 521.810 0.2189

A–1 7 4
Table 360. Test data for specimen 752–28

Test Number : 328 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 258.9 MPa Ultimate Stress : 587.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

25.970 0.0001 298.060 0.0063 508.970 0.0947

30.490 0.0001 314.610 0.0087 517.340 0.1013
45.790 0.0002 321.370 0.0100 532.600 0.1145
69.930 0.0002 348.700 0.0166 539.410 0.1211
94.410 0.0002 354.740 0.0184 555.440 0.1387
106.620 0.0003 371.160 0.0239 560.630 0.1453
119.350 0.0003 408.340 0.0382 569.760 0.1585
152.680 0.0005 413.440 0.0405 571.100 0.1608
172.700 0.0006 458.240 0.0624 579.490 0.1762
181.970 0.0007 487.300 0.0796 582.490 0.1829
243.170 0.0023 490.590 0.0818 587.910 0.2074

Table 361. Test data for specimen 752–29

Test Number : 329 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 264.1 MPa Ultimate Stress : 581.7 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

10.470 0.0001 198.390 0.0012 461.350 0.0630

15.080 0.0001 245.470 0.0025 486.660 0.0781
28.910 0.0002 264.430 0.0033 490.150 0.0803
40.310 0.0002 303.070 0.0064 517.200 0.0996
52.150 0.0002 314.860 0.0081 537.160 0.1170
86.080 0.0004 331.430 0.0111 543.650 0.1238
98.690 0.0005 359.010 0.0189 557.110 0.1391
123.080 0.0005 364.680 0.0209 562.080 0.1456
169.210 0.0008 402.960 0.0351 570.670 0.1588
179.540 0.0010 418.210 0.0416 574.430 0.1655
189.190 0.0011 449.620 0.0566 581.620 0.1876

A–1 7 5
Table 362. Test data for specimen 75–130

Test Number : 327 Test Temp. : 290°C

Aging Temp. : 320°C Aging Time : 50,000 h
Yield Stress : 239.6 MPa Ultimate Stress : 557.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

14.610 0.0001 250.740 0.0037 501.370 0.1157

15.780 0.0001 255.690 0.0041 508.070 0.1223
29.460 0.0002 277.600 0.0063 520.080 0.1354
63.210 0.0002 334.040 0.0190 525.390 0.1421
73.560 0.0002 339.410 0.0208 536.540 0.1575
107.350 0.0003 366.210 0.0312 540.710 0.1642
118.460 0.0005 390.590 0.0421 548.990 0.1796
167.810 0.0008 431.340 0.0637 551.730 0.1862
176.640 0.0010 455.150 0.0787 553.380 0.1906
200.580 0.0016 473.310 0.0918 556.490 0.2026
221.710 0.0023 484.180 0.1004 557.780 0.2119

Table 363. Test data for specimen 752–27

Test Number : 049 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 2,570 h
Yield Stress : 204.7 MPa Ultimate Stress : 528.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

64.52 0.0001 245.45 0.0031 396.80 0.0576

91.54 0.0002 249.86 0.0033 409.19 0.0657
122.15 0.0005 253.92 0.0035 423.78 0.0752
133.99 0.0006 257.98 0.0038 435.61 0.0833
145.78 0.0008 262.88 0.0042 443.82 0.0893
156.83 0.0010 269.37 0.0050 454.85 0.0971
164.93 0.0012 275.47 0.0058 464.08 0.1022
179.61 0.0015 279.51 0.0064 473.90 0.1108
183.09 0.0016 285.42 0.0074 484.10 0.1240
194.92 0.0019 289.31 0.0081 498.83 0.1407
198.02 0.0020 297.00 0.0098 506.89 0.1525
210.50 0.0022 341.65 0.0265 514.21 0.1641
217.85 0.0023 352.90 0.0323 520.25 0.1745
224.33 0.0024 363.57 0.0379 522.82 0.1817
232.13 0.0025 375.14 0.0446 527.72 0.1995
240.16 0.0028 387.46 0.0519 528.85 0.2102

A–1 7 6
Table 364. Test data for specimen 754–09

Test Number : 086 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 219.8 MPa Ultimate Stress : 614.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

170.910 0.0014 279.750 0.0047 482.940 0.0737

185.290 0.0017 284.780 0.0050 532.470 0.1042
192.190 0.0020 289.860 0.0055 546.750 0.1160
201.790 0.0021 295.770 0.0060 560.960 0.1292
208.390 0.0022 317.070 0.0085 563.880 0.1318
213.970 0.0023 324.180 0.0097 574.620 0.1440
219.980 0.0024 360.220 0.0183 590.390 0.1657
256.250 0.0034 376.650 0.0229 597.080 0.1776
261.960 0.0037 395.680 0.0301 598.230 0.1805
267.730 0.0040 414.460 0.0377 605.840 0.1992
271.970 0.0042 443.340 0.0512 607.370 0.2014

Table 365. Test data for specimen 75–120

Test Number : 087 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 10,000 h
Yield Stress : 209.9 MPa Ultimate Stress : 595.6 MPa

Experimental Data Not Available.

Table 366. Test data for specimen 753–12

Test Number : 260 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 264.4 MPa Ultimate Stress : 615.9 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

42.860 0.0002 242.480 0.0018 462.670 0.0549

46.130 0.0002 260.210 0.0026 477.470 0.0620
62.250 0.0002 265.620 0.0030 496.720 0.0730
73.840 0.0002 284.460 0.0040 511.520 0.0817
84.920 0.0002 292.560 0.0049 573.080 0.1317
96.220 0.0002 313.220 0.0069 587.290 0.1487
107.810 0.0002 342.890 0.0119 588.900 0.1509
155.230 0.0003 370.950 0.0193 599.960 0.1681
166.210 0.0004 387.840 0.0242 612.080 0.1955
176.320 0.0004 419.920 0.0358 615.790 0.2114
201.610 0.0007 445.240 0.0466

A–1 7 7
Table 367. Test data for specimen 754–12

Test Number : 247 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 227.2 MPa Ultimate Stress : 613.8 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

41.500 0.0002 240.490 0.0038 482.190 0.0713

48.630 0.0002 246.130 0.0041 533.550 0.1036
63.550 0.0002 261.530 0.0052 552.940 0.1191
73.690 0.0002 298.400 0.0089 560.220 0.1258
84.200 0.0003 315.180 0.0114 573.040 0.1390
94.900 0.0003 320.280 0.0122 578.930 0.1456
106.280 0.0004 339.060 0.0162 587.510 0.1566
117.700 0.0005 344.600 0.0174 592.150 0.1633
129.430 0.0006 436.660 0.0493 602.110 0.1809
158.620 0.0008 441.610 0.0513 609.860 0.2006
167.080 0.0011 478.120 0.0692 613.560 0.2163

Table 368. Test data for specimen 75–270

Test Number : 234 Test Temp. : 290°C

Aging Temp. : 350°C Aging Time : 30,000 h
Yield Stress : 209.0 MPa Ultimate Stress : 584.6 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

20.400 0.0001 178.270 0.0019 450.340 0.0725

25.300 0.0001 185.100 0.0021 472.740 0.0868
39.620 0.0002 210.620 0.0032 482.240 0.0933
51.040 0.0002 222.360 0.0038 496.940 0.1041
63.230 0.0003 243.480 0.0052 517.630 0.1218
74.150 0.0003 252.020 0.0060 520.020 0.1241
84.850 0.0003 291.630 0.0108 546.690 0.1528
95.840 0.0004 296.780 0.0117 553.470 0.1616
107.200 0.0005 303.530 0.0130 565.240 0.1790
118.220 0.0006 343.790 0.0238 579.400 0.2094
128.710 0.0007 431.440 0.0618 584.560 0.2344

A–1 7 8
Table 369. Test data for specimen 752-18

Test Number : 045 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 2,570 h
Yield Stress : 203.2 MPa Ultimate Stress : 591.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

53.16 0.0000 276.75 0.0050 472.83 0.0845

65.69 0.0001 290.82 0.0064 482.11 0.0904
83.84 0.0001 295.84 0.0071 486.77 0.0935
102.68 0.0003 303.20 0.0082 489.76 0.0966
129.64 0.0005 309.80 0.0094 509.96 0.1090
153.15 0.0009 316.91 0.0108 518.48 0.1156
167.42 0.0012 323.32 0.0121 536.20 0.1314
175.48 0.0013 335.40 0.0153 547.08 0.1430
188.90 0.0017 347.52 0.0193 556.17 0.1543
200.79 0.0020 361.98 0.0245 563.58 0.1645
205.86 0.0021 384.33 0.0342 572.07 0.1788
219.53 0.0024 403.70 0.0442 578.97 0.1907
230.76 0.0025 420.04 0.0531 584.98 0.2046
239.27 0.0027 434.94 0.0619 588.80 0.2162
249.21 0.0032 449.84 0.0707 591.03 0.2287
266.41 0.0042 460.81 0.0770 591.11 0.2332

Table 370. Test data for specimen 752–24

Test Number : 080 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 208.2 MPa Ultimate Stress : 630.4 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

166.180 0.0012 317.100 0.0073 530.080 0.0940

183.810 0.0016 334.120 0.0091 549.340 0.1040
192.600 0.0019 341.430 0.0100 562.550 0.1153
201.000 0.0020 358.330 0.0129 582.320 0.1326
208.500 0.0022 396.480 0.0230 596.330 0.1469
241.190 0.0028 425.890 0.0341 599.780 0.1520
249.440 0.0031 453.060 0.0473 615.390 0.1766
265.540 0.0038 459.790 0.0509 617.680 0.1813
275.700 0.0042 482.880 0.0638 624.620 0.1961
300.580 0.0059 493.570 0.0721 625.760 0.2001
309.110 0.0066 509.940 0.0813 629.660 0.2153

A–1 7 9
Table 371. Test data for specimen 75–110

Test Number : 081 Test Temp. : 290°C

Aging Temp. : 400°C Aging Time : 10,000 h
Yield Stress : 206.7 MPa Ultimate Stress : 593.1 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

160.190 0.0011 325.060 0.0108 486.950 0.0865

173.030 0.0014 335.670 0.0127 493.300 0.0904
181.380 0.0016 342.500 0.0142 518.010 0.1059
188.460 0.0018 350.450 0.0162 546.780 0.1307
195.140 0.0021 371.710 0.0223 555.630 0.1416
203.200 0.0022 376.380 0.0247 567.390 0.1564
226.540 0.0026 398.020 0.0338 569.820 0.1600
255.540 0.0036 430.060 0.0497 581.550 0.1792
263.500 0.0042 435.800 0.0533 584.070 0.1832
290.530 0.0063 455.870 0.0646 589.730 0.1987
315.580 0.0093 469.890 0.0733 592.600 0.2091

Table 372. Test data for specimen 751-06

Test Number : 044 Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 218.7 MPa Ultimate Stress : 598.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

54.2050 0.0000 288.9000 0.0049 469.3600 0.0611

70.7470 0.0001 301.3900 0.0056 483.4600 0.0707
92.5100 0.0003 315.0200 0.0067 486.9300 0.0751
121.7500 0.0006 326.3300 0.0079 506.9400 0.0898
144.3000 0.0009 338.3800 0.0095 523.5300 0.1002
167.9700 0.0013 348.9000 0.0111 539.3900 0.1154
184.1700 0.0017 360.4500 0.0132 554.2400 0.1320
196.9200 0.0021 370.0800 0.0154 564.6300 0.1454
207.1000 0.0022 379.1700 0.0177 575.8300 0.1627
213.9400 0.0023 389.4300 0.0208 583.6300 0.1782
223.4400 0.0024 401.6600 0.0252 589.8600 0.1940
232.1500 0.0025 421.1800 0.0336 593.0000 0.2000
241.6500 0.0028 434.8200 0.0404 593.9100 0.2096
256.4200 0.0033 441.9700 0.0442 597.6300 0.2170
274.6700 0.0041 459.1300 0.0546 598.2000 0.2181

A–1 8 0
Table 373. Test data for specimen 752–09

Test Number : 055 Test Temp. : 290°C

Aging Temp. : 450°C Aging Time : 2,570 h
Yield Stress : 197.7 MPa Ultimate Stress : 606.2 MPa

Engr. Engr. Engr.

Stress Engr. Stress Engr. Stress Engr.
(MPa) Strain (MPa) Strain (MPa) Strain

44.59 0.0000 243.86 0.0035 424.61 0.0403

90.76 0.0003 254.69 0.0039 438.26 0.0469
125.06 0.0006 264.50 0.0045 449.64 0.0527
147.87 0.0010 274.50 0.0052 463.48 0.0601
158.56 0.0012 291.16 0.0066 479.09 0.0689
170.34 0.0015 304.61 0.0079 487.00 0.0750
182.85 0.0018 318.99 0.0097 509.92 0.0899
185.86 0.0020 325.79 0.0106 526.84 0.0996
193.94 0.0022 330.57 0.0113 541.79 0.1111
198.67 0.0024 345.20 0.0142 559.48 0.1283
200.89 0.0025 353.23 0.0159 573.14 0.1451
209.16 0.0027 361.90 0.0180 582.87 0.1590
217.74 0.0028 379.79 0.0232 598.18 0.1875
233.70 0.0030 398.26 0.0293 603.47 0.2025
237.55 0.0032 411.17 0.0344 606.18 0.2268

A–1 8 1
A–1 8 2
 Distribution for NUREG/CR–6142 (ANL–93/35)

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NRC FORM 335 U. S. NUCLEAR REGULATORY COMMISSION 1. REPORT NUMBER
(2–89) (Assigned by NRC. Add Vol., Supp., Rev.,
NRCM 1102, and Addendum Numbers, if any.)
3201, 3202
BIBLIOGRAPHIC DATA SHEET NUREG/CR–6142
(See instructions on the reverse)
ANL–93/35
2. TITLE AND SUBTITLE
Tensile–Property Characterization of Thermally Aged
Cast Stainless Steels 3. DATE REPORT PUBLISHED
MONTH YEAR
January 1994
4. FIN OR GRANT NUMBER
A2243
5. AUTHOR(S) 6. TYPE OF REPORT

W. F. Michaud, P. T. Toben, Technical

7. PERIOD COVERED (Inclusive Dates)
W. K. Soppet, and O. K. Chopra

8. PERFORMING ORGANIZATION – NAME AND ADDRESS (If NRC, provide Division, Office or Region, U.S. Nuclear Regulatory Commission, and mailing address; if contractor, provide
name and mailing address.)

Argonne National Laboratory

9700 South Cass Avenue
Argonne, IL 60439

9. SPONSORING ORGANIZATION – NAME AND ADDRESS (If NRC, type “Same as above”: if contractor, provide NRC Division, Office or Region, U.S. Nuclear Regulatory Commission,
and mailing address.)
Division of Engineering
Office of Nuclear Regulatory Research
U. S. Nuclear Regulatory Commission
Washington, DC 20555
10. SUPPLEMENTARY NOTES

11. ABSTRACT (200 words or less)

The effect of thermal aging on tensile properties of cast stainless steels during service in light water
reactors has been evaluated. Tensile data for several experimental and commercial heats of c a s t
stainless steels are presented. Thermal aging increases the tensile strength of these steels. The
high–C Mo–bearing CF–8M steels are more susceptible to thermal aging than the Mo–free CF–3 o r
CF–8 steels. A procedure and correlations are presented for predicting the change in tensile flow and
yield stresses and engineering stress–vs.–strain curve of cast stainless steel as a function of time and
temperature of service. The tensile properties of aged cast stainless steel are estimated from known
material information, i.e., chemical composition and the initial tensile strength of the steel. The
correlations described in this report may be used for assessing thermal embrittlement of c a s t
stainless steel components.

12. KEY WORDS/DESCRIPTORS (List words or phrases that will assist researchers in locating this report.) 13. AVAILABILITY STATEMENT

Cast duplex stainless steel Unlimited

Cast stainless steel 14. SECURITY CLASSIFICATION

Thermal Embrittlement (This Page)

Tensile Properties Unclassified

Flow Stress (This Report)
Yield Stress Unclassified
Ramberg–Osgood Equation 15. NUMBER OF PAGES
Thermal Aging 254
16. PRICE

NRC FORM 335 (2–89)