Macro Porosity Formation A Study in High Pressure Die Casting D Blondheim
Macro Porosity Formation A Study in High Pressure Die Casting D Blondheim
Alex Monroe
Michigan Technological University, Houghton, MI, USA
Abstract
Porosity formation in high pressure die casting (HPDC) The general region where macro porosity forms is pre-
impacts mechanical properties and casting quality. Much dictable with simulation, but its actual size and distribution
is published regarding micro porosity and its impact on of the voids are random. These results challenge the
mechanical properties, but there is limited research on the industry accepted practices for inspections and process
actual formation of macro porosity. In production appli- controls. This also underscores the importance of up-front
cations, macro porosity plays a critically important role in design for manufacturability to avoid macro porosity-re-
casting quality and acceptance by the customer. This paper lated quality issues.
argues that the most useful definition of macro porosity is
the limits of visual detectability. With this definition, it will Keywords: high pressure die casting, porosity, casting
be shown macro porosity presents stochastically within a defects, defect classification, macro porosity, micro
controlled HPDC process. This means macro porosity has porosity
a random probability distribution or pattern that should be
analyzed statistically and cannot be predicted precisely.
Introduction macro porosity.6,7 The cause and size provide one high-
level classification system for porosity, although more
Porosity is considered a defect, and it is inherent to alu- detailed defect classification systems exist.2,8,9
minum high pressure die casting (HPDC) due to the nature
of metal solidification.1 Research completed by the North Porosity is well documented within the HPDC indus-
American Die Casting Association (NADCA) shows that try.1,2,6,10,11 Shrink porosity is caused by volumetric con-
porosity concerns are one of the leading contributors to traction of metals during solidification. Shrink porosity is
scrap costs and the biggest problem within die casting.2 often irregular, with ragged shapes. Gas porosity occurs
Approximately 30% of the industry has identified when a gas concentration within the liquid metal is higher
addressing porosity as a top concern.3 There is high than the solubility of the metal. Gas porosity is typically
motivation to improve porosity scrap given the die casting spherical in shape. The mechanisms causing these two
industry has $8 billion annual sales in North America4 and types of internal voids can also interact during the solidi-
suffers from an 8% median scrap rate.5 Porosity defects can fication of a casting. This interaction is termed gas assisted
be described by the primary cause: shrink porosity and gas shrink. This porosity has shape characteristics of both
porosity and classified by the size: micro porosity and shrink and gas porosity.
Castings are typically inspected in a raw state with X-ray or Experimental Study
computed tomography (CT) equipment or by visual
inspection after secondary machining. From an X-ray or A small housing casting, produced on a 900-ton die cast
CT image standpoint, production intent equipment has a machine out of A362.0 aluminum alloy, as seen in Table 2,
pixel size resolution of 100 lm on castings that can fit up
to 400 mm 9 400 mm image windows.29,30 Specialized Table 1. Equivalent Visual Angle for Different Defect
micro-CT research equipment exists to capture micro Sizes and Distances
porosity resolution of 10–50 lm on parts typically less than
50 mm cube.14,31 This type of equipment has significant Equivalent visual angle (minutes of an Arc)
limitations in a production castings environment based on Casting defect size (mm) Distance from defect (mm)
size and time needed to perform analysis. Therefore, the
150 250 500 600
capable range of micro-CT equipment should not be con-
sidered in defining an industrial application of macro 0.1 2.29 1.38 0.69 0.57
porosity. The focus should be given to capabilities of
0.25 5.73 3.44 1.72 1.43
industrial, production intent X-ray equipment.
0.5 11.46 6.88 3.44 2.86
Visual inspection of castings is the next challenge. Visual 0.75 17.19 10.31 5.16 4.30
acuity defines what the human eye is capable of detecting. 1 22.92 13.75 6.88 5.73
Snellen eye charts, as typically found at optometrists’
offices, were developed based on the studies showing
Si Fe Cu Mn Ni Zn Ti Sr
was selected for this experiment. Previous X-ray audits X-ray images were reviewed following ASTM E505
showed varying levels of porosity within this casting even standard36 to determine porosity cause. Shrink porosity
when process parameters remained consistent. The porosity (ASTM Category C) and gas porosity (ASTM Category A)
was located near a semi-circular feature on the side were seen within the castings. The castings were graded
opposite the gating. The porosity level found in this loca- with a 1 (best), 2 (moderate), and 3 (worst) score. Figure 2
tion of the casting does not impact overall part quality provides examples of all three gradings.
based on product testing.
Once the die was brought up to temperature with the typ- Results and Analysis
ical start-up process, 100 castings were produced at iden-
tical process settings. These settings matched the Critical process parameters were collected for all sample
production settings and had no adjustments made for the castings (n = 99) during the experiment. The data were
entire sample run. The castings were pin-stamped with a within typical production variation for the casting. Mean
serial number in the robot extraction cell. With this serial and 95% confidence intervals for these parameters are seen
number, all process data are traced to the X-ray images. in Table 3. Based on the grading samples on the images,
The castings were completed in just under two hours. there were 9 samples each identified as Grade 1 (good) and
Grade 3 (worst). These parts that represented the extremes
Castings were sawed so the area of interest could be easily of the macro porosity found within the casting were
X-rayed to provide repeatable images and remove back- reviewed in detail.
ground features non-critical to this study. A sample of the
sawed casting is seen in Figure 1. One casting was dam- The best castings showed scattered shrink porosity typi-
aged during the sawing process used to prepare it for the cally 0.2 mm to 0.4 mm thick and up to 1.0 mm long. This
X-ray (sample number 76). Its process information was porosity was scattered throughout the section in review,
removed from all analysis. This sample showed no sig- with a tendency for it to form furthest way from the gating
nificant difference in process values. (part is gated from the left side of the X-ray images). The
nine Grade 1 (best) castings can be seen in Figure 3.
The X-ray equipment used was a Bosello SRE Max with a
225 max KV power rating. Images were registered using The worst castings showed a gas assisted shrink with
open source Fiji imaging software34 and the selective plane rounder, but irregular shaped voids, consistent of gas
illumination microscopy (SPIM) registration plug-in.35 The feeding into a shrink porosity. Gas porosity within the
worst castings grade was typically 3.0 mm to 4.0 mm in accepted analysis and quality implications of porosity in
diameter. For shrink porosity, the worst castings had HPDC.
0.4–0.6 mm thick and 5.0–10.0 mm long porosity voids.
Overall, the worst of the worst (WOW sample—#43) had This experiment could did not determine if the Grade 1
an approximate 8.0-mm-diameter void in the casting. The castings were more dense (less porous) than the Grade 3
nine worst castings (Grade 3) can be seen in Figure 4. castings. It simply observes that the levels of macro
porosity are higher while no process parameters varied
Shapiro-Wilk normality tests37 showed the process significantly. This leaves open the question of whether the
parameters to be non-normal in the 99 samples. As a result, Grade 1 castings traded macro porosity for micro porosity
the Wilcoxon Signed Rank test38 was performed to com- that could not be detected by X-ray. Further study is
pare the samples between the best and worst groupings. merited and ongoing.
Table 4 contains all the individual recorded data for the
samples. Table 5 shows the p-values calculated with the
Wilcoxon test. None of the critical process parameters Part Geometry Impact on Stochastic Macro
showed to be significant. Porosity Formation
The results of the experiment have shown that macro Predicting the morphology of macro porosity is not a useful
porosity formation is random when industry accepted exercise. Macro porosity is easy to detect with visual
control parameters are held constant in a production envi- inspection on machined surfaces or X-rays. Feeding-based
ronment. The size and distribution of the voids varied rules have been successfully developed to manage porosity in
significantly throughout the casting run, even though no sand and permanent mold castings. Macro porosity is reduced
process settings were changed. When comparing the best when an adequately large volume of liquid metal is available
and worst samples, the process parameters showed no to replenish the volumetric contraction of the solidifying
statistical difference. These parameters remain important to metal. The feeding volume must be connected by a liquid path
the process, but they do not fully explain the randomness throughout the solidification of the casting’s cross sections
associated with the porosity formation. As will be dis- being fed. From Chorvinov’s rule, it can be surmised that
cussed in the next section, the general location of the thicker sections require more solidification time.25
porosity formation remained predictable, but the actual
macro porosity formation was random. Production con- Computer simulations of these feeding rules are effective
trolled processes produce randomly formed porosity. This for identifying where porosity can form, but they fail to
random macro porosity should challenge many of the properly predict the morphology of the macro porosity.
MAGMA was used to compare with the experimental but gate locations are determined by die design and gate
results.39 Six warmup cycles and one production cycle removal considerations. A temperature gradient from the
were calculated. Figure 5 shows the predicted porosity thick sections of the casting to the gate cannot be ensured.
zone (a) and the pore volume fraction (b) for the studied Resulting unfed pockets of liquid create the macro porosity
casting in the area that was X-rayed. The porosity zone is common to HPDC. Randomly sized and shaped macro
the predicted hot spot that is the extent of the unfed liquid porosity voids should form in these trapped pockets, but
pocket. Porosity volume fraction is concentrated into two also the size and shape of the trapped pockets are random
voids that approximate the center of the porosity observed because the solidification during filling and time that
via X-ray. More porosity is predicted on the right-hand side pressure is applied to the liquid metal after filling is
of the image like the experimental results. uncertain. Small extension or reduction of feeding will
make significant changes to the total porosity due to the
Prediction of the macro pore morphology should be nearly rapid solidification from the HPDC process.
impossible. This is because the pressure drop required to
homogeneously nucleate porosity is in the giga-Pascal Figure 6 plots the liquid volume in the sample area, as seen
range. Instead, pores require a heterogenous nucleation site in Figures 1 and 5, over the entire solidification time of the
such as an oxide bifilm or pre-existing trapped gas pores.20 casting. Feeding is predicted to be cut off to the sample
Filtering, degassing, venting/vacuum, and good furnace area at 9 seconds after filling, leaving 18.4 cm3 of
maintenance practices can reduce the number of remaining liquid aluminum. 1.9% of the sample area will
heterogenous nucleation sites, but they cannot be elimi- contain pores with the assumption that the aluminum will
nated. Their occurrence will also be stochastic by nature. have approximately 6% shrinkage. Increasing or decreas-
Since the nucleation sites are random, the macro pores also ing the feeding time by 0.25 seconds changes the unfed
must occur randomly. The simulation software can predict liquid volume by ± 3.5%. These small variations in feed-
these porosity zones but is incapable of showing the ran- ing time can come from a host of uncertainties in the
domness of the size and shape of the macro porosity. process. For example, cold flakes blocking feeding through
the gate, spray variation, initial metal temperature, and
Additionally, HPDC feeds exclusively through the gating other variables can reasonably be assumed to affect the
system into the part. Pressure is applied to enhance feeding, feeding time by 0.25 seconds or more.
# Grade Cycle Average slow Calc start Average fast shot Intens rise Intens Intens squeeze Biscuit
time (s) shot velocity (in/s) fast shot (in) velocity (in/s) time (ms) pressure distance (in) size (in)
(psi)
Cycle Average slow shot Calc start Average fast shot Intens rise Intens Intens squeeze Biscuit
time velocity fast shot velocity time Pressure distance size
With an exception of some structural automotive parts, in- chance none of the castings contain that defect. If the
line X-ray equipment is not typically found in most defect rate and the process remain constant and the
industrial die casting foundries. The cost of equipment and inspection has experience seeing high probability of all
time to process when compared to the risks of porosity good castings, what happens once that inspector finds a
typically makes this an uneconomical process. Instead, defective part? It is slightly better than a coin flip to have a
audit X-rays are performed on randomly chosen samples defect occur every two production weeks, based on a three-
during the production run. The number of samples and a shift operation. The warning flags in the foundry are sent
defect rate caused by worst-case macro porosity can be out, and the troubleshooting begins. Another random
used to understand the probability of selecting a sample lot sample selected could then show all good parts, and the
and seeing no defects. The binomial probability function is investigation of ‘‘what changed in the process’’ may occur,
used to find this probability. Table 6 shows the probability wasting resources because the process has not changed, and
of finding no defects for different defect rates and sample the sampling was just poor.
sizes.
Worse yet, someone may take the failed inspection results
Understanding this probability should influence that how and change the process to try to ‘‘improve it.’’ Now the
troubleshooting is completed within the foundry. As an actual defect rate shifts from 2.5% to some other unknown
example, if a casting truly has a 2.5% scrap rate based on value. This can lead to a spiral of process changes over the
the random macro porosity and the X-ray technician ran- production life of a part, with limited knowledge of what
domly pulls 3 castings for inspection, there is 92.7% scrap rates are occurring.
40 4.0% rem can be used to help determine a lot size given the
historical defect rate and the confidence the manufacturing
30 desires.40
3.0%
20 2.0%
Casting Process Optimization
10 1.0% The randomness of the macro porosity should cause the
industry to review the techniques used for process opti-
0 0.0% mization. An appropriate sample size is needed for any
0 5 10 15 20 25 optimization process to ensure the worst-case scenarios are
Feeding Time aer Filling (s) detected in the macro porosity formation. Also, additional
process monitoring of the HPDC equipment, beyond the
Figure 6. Volume of liquid in the sample area as
injection system, is needed.
predicted by MAGMA.
Injection parameters and metal holding temperature are The next area to research is the density in the predicted
typically the focus of in optimization publications in porosity zones between castings. Research has shown that
HPDC.41–44 This approach is logical given the history and density is not a good predictor of mechanical proper-
commercially available products for the industry to capture ties.47,48 The difference levels of void space visible in the
this data. Questions should arise on the focus and priority Grade 1 versus Grade 3 X-rays lead to questions regarding
of these process inputs when significant macro porosity the density of the predicted porosity zones. Are the den-
variation occurs. It is clear from simulation that injection sities of these grade differences the same with different
parameters can influence predicted zones. This study shows distributions of size of the macro and micro porosity? This
the random formation of porosity in these zones. The is a useful question to have answered as its impact on
injection parameters should remain controlled and moni- quality inspection results (acceptable versus scrap casting)
tored; however, data collection on additional process and perceived mechanical properties could be misleading
monitoring systems should be prioritized45 to potentially to the industry.
further reduce this predicted porosity zone. These addi-
tional systems could include die temperature,46 vacuum,18 From this work, we know there is randomness in the size
and equipment cycle time and performance. Optimization and shape of macro porosity. This randomness influences
of these additional parameters could reduce the predicted classification of defects and process optimization decisions.
porosity zone. Therefore, the macro porosity that forms in Misclassification of macro porosity can lead to poor pre-
that zone will also be reduced. dictions of quality when supervised machine learning
algorithms are used. In this case, two significantly different
outputs on X-ray images are produced from nearly identi-
Conclusions cal inputs. It becomes impossible for machine learning to
find a pattern in what fundamentally becomes noise in the
High pressure die casting suffers from a porosity problem. ‘‘results’’ created by random macro porosity formation.
By better understanding how macro porosity forms, Furthermore, sample sizes for optimization studies must be
improvements can be made within the industry. Like micro carefully planned based on these random macro porosity
porosity, macro porosity is randomly formed in HPDC. formations. Small sample sizes will have a higher proba-
Casting design, inspection, and optimization processes are bility that the true worst-case macro porosity formation is
all affected by macro porosity. This random macro porosity not seen, thereby providing misleading optimization guid-
formation has been shown by an industrial case study and ance. These areas are worthy of additional research.
fundamental theory.
In conclusion, the stochastic nature of macro porosity
Simulation software uses casting geometry and tooling formation within the prediction porosity zone should
design to predict porosity zones but cannot predict the challenge the industry to further research HPDC process in
actual random size and distribution of those voids in the production environments. By researching these topics fur-
zone. Understanding this stochastic formation should ther, the industry will be better positioned to help improve
challenge previously accepted practices and improve the overall HPDC casting design and manufacturing of parts.
comprehension and classification of macro porosity defects
in die casting. Specifically, this provides the industry with
three areas of further study.
Funding
The first area of study is within the industry’s process
Research was sponsored by Mercury Marine – Mercury
control approach. Injection parameters are the main focus
Castings, a division of Brunswick, Inc.
within the industry and academic research for HPDC