INTERNATIONAL ISO
STANDARD 2920
IDF
58
Second edition
2004-10-15
Whey cheese — Determination of dry
matter (Reference method)
Fromage de sérum — Détermination de la matière sèche (Méthode de
référence)
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Reference numbers
ISO 2920:2004(E)
IDF 58:2004(E)
© ISO and IDF 2004
ISO 2920:2004(E)
IDF 58:2004(E)
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ISO 2920:2004(E)
IDF 58:2004(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out through
ISO technical committees. Each member body interested in a subject for which a technical committee has
been established has the right to be represented on that committee. International organizations, governmental
and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the
International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 2920IDF 58 was prepared by Technical Committee ISO/TC 34, Food products, Subcommittee SC 5,
Milk and milk products, and the International Dairy Federation (IDF), in collaboration with AOAC International.
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It is being published jointly by ISO and IDF and separately by AOAC International.
(standards.iteh.ai)
This edition of ISO 2920IDF 58 cancels and replaces ISO 2920:1974, of which it constitutes a minor revision.
ISO 2920:2004
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© ISO and IDF 2004 – All rights reserved iii
ISO 2920:2004(E)
IDF 58:2004(E)
Foreword
IDF (the International Dairy Federation) is a worldwide federation of the dairy sector with a National
Committee in every member country. Every National Committee has the right to be represented on the IDF
Standing Committees carrying out the technical work. IDF collaborates with ISO and AOAC International in
the development of standard methods of analysis and sampling for milk and milk products.
Draft International Standards adopted by the Action Teams and Standing Committees are circulated to the
National Committees for voting. Publication as an International Standard requires approval by at least 50 % of
the National Committees casting a vote.
ISO 2920IDF 58 was prepared by Technical Committee ISO/TC 34, Food products, Subcommittee SC 5,
Milk and milk products, and the International Dairy Federation (IDF), in collaboration with AOAC International.
It is being published jointly by ISO and IDF and separately by AOAC International.
This edition of ISO 2920IDF 58 cancels and replaces IDF 58:1970, of which it constitutes a minor revision.
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iv © ISO and IDF 2004 – All rights reserved
ISO 2920:2004(E)
INTERNATIONAL STANDARD
IDF 58:2004(E)
Whey cheese — Determination of dry matter (Reference
method)
1 Scope
This International Standard specifies a reference method for the determination of the dry matter of whey
cheese.
2 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
2.1
dry matter of whey cheese
iTeh STANDARD PREVIEW
residue obtained by application of the procedure specified in this International Standard and including the
water of crystallization of lactose
NOTE
(standards.iteh.ai)
It is expressed as a mass fraction in percent.
ISO 2920:2004
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3 Principle 9b88c500b5f6/iso-2920-2004
A sample of whey cheese is desiccated in a ventilated oven set at a temperature of 88 °C.
4 Apparatus and materials
4.1 Grinding mill or other appropriate device.
4.2 Analytical balance, capable of weighing to the nearest 0,000 5 g.
4.3 Desiccator, provided with an efficient drying agent (e.g. silica gel with hygrometric indicator).
4.4 Drying oven, well ventilated and thermostatically controlled, capable of being maintained at
88 °C ± 2 °C.
4.5 Dishes, of stainless steel, nickel or aluminium, with height about 20 mm and diameter 60 mm to 80 mm.
4.6 Quartz sand or sea sand, which passes through a sieve with 10 openings per centimetre but not
through a sieve with 40 openings per centimetre.
For example, use woven wire cloth test sieves with nominal size of aperture of 500 µm and 180 µm
respectively (for details, see ISO 565).
If necessary, the sand shall be washed with hot concentrated hydrochloric acid and water, then dried and
ignited.
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ISO 2920:2004(E)
IDF 58:2004(E)
4.7 Glass stirrers, flat ended.
5 Sampling
A representative sample should have been sent to the laboratory. It should not have been damaged or
changed during transport or storage.
Sampling is not part of the method specified in this International Standard. A recommended sampling method
is given in ISO 707.
6 Preparation of test sample
Grind the representative sample of the cheese by means of the grinding mill (4.1). If the soft consistency of
the cheese makes the use of a grinding mill impossible, mix the sample thoroughly by means of another
appropriate device (e.g. a glass stirrer or spatula). Avoid losses by evaporation.
Keep the prepared sample in a suitable airtight container until analysis. Start the analysis within 1 h.
7 Procedure
7.1 iTeh STANDARD PREVIEW
Number of determinations
Carry out two determinations of the same (standards.iteh.ai)
test sample.
7.2 Determination ISO 2920:2004
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7.2.1 Weigh about 20 g of sand (4.6) in a9b88c500b5f6/iso-2920-2004
dish (4.5) together with a glass stirrer (4.7). With hard and
semi-hard whey cheeses, which can be adequately ground by means of the grinding mill, the use of sand may
be omitted.
7.2.2 Moisten the sand with water and dry the dish to constant mass in the oven (4.4) set at 88 °C.
7.2.3 Allow the dish to cool in the desiccator (4.3) and weigh to the nearest 0,000 5 g.
7.2.4 Quickly weigh, to the nearest 0,000 5 g, about 3 g of the test sample in the dish.
7.2.5 Thoroughly mix the test portion with the sand by means of the stirrer.
7.2.6 Dry the dish and contents in the oven (4.4) set at 88 °C for 4 h.
7.2.7 Allow to cool in the desiccator (4.3) and weigh to the nearest 0,000 5 g.
7.2.8 Dry in the oven (4.4) again for 1 h. Cool in the desiccator and weigh to the nearest 0,000 5 g.
7.2.9 Repeat the operations of drying and cooling until the difference in mass between two successive
weighings is not more than 0,001 g
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ISO 2920:2004(E)
IDF 58:2004(E)
8 Calculation and expression of results
8.1 Calculation
The mass fraction of dry matter, w, expressed in percent, is given by the formula:
m2 − m0
w= × 100 %
m1 − m 0
where
m0 is the mass, in grams, of the dish containing the sand and stirrer (7.2.3);
m1 is the mass, in grams, of the dish and contents before drying (7.2.4);
m2 is the mass, in grams, of the dish and contents after drying (7.2.9).
8.2 Expression of results
Take as the result the arithmetic mean of the two determinations, if the requirement of repeatability
(see Clause 9) is satisfied.
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9 Repeatability
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The absolute difference between two independent single test results, obtained using the same method on
identical test material in the same laboratoryISO by 2920:2004
the same operator using the same equipment within a short
interval of time, will inhttps://standards.iteh.ai/catalog/standards/sist/a9956d07-4abb-4249-af48-
not more than 5 % of cases be greater 0,2 % of dry matter per 100 g of the product.
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10 Test report
The test report shall specify:
a) all information necessary for the complete identification of the sample;
b) the sampling method used, if known;
c) the test method used, with reference to this International Standard;
d) all operating details not specified in this International Standard, or regarded as optional, together with
details of any incidents which may have influenced the test results;
e) the test results obtained, clearly mentioning the method of expression used.
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ISO 2920:2004(E)
IDF 58:2004(E)
Bibliography
[1] ISO 565, Test sieves — Metal wire cloth, perforated metal plate and electroformed sheet — Nominal
sizes of openings
[2] ISO 707, Milk and milk products — Guidance on sampling1)
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1) Equivalent to IDF 50.
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