HELLENIC GAS TECHNICAL JOB
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415 25 ATHENS, GREECE
Tels 210 sooo "REVISION
Fax : 210 6501551 |
DATE 05/04/2011
TRANSMISSION SPECIFICATION
HIGH PRESSURE (HP) TRANSMISSION
SYSTEMS
PLANT — APPLIED EXTERNAL 3-LAYER
POLYETHYLENE LINE PIPE COATING
This document isthe property of DESFA SA andi shall not be reproduced copied o7 used for ans purpose ater than that for
hich is specially furnishedODESF, HELLENIC GAS TRANSMISSION SYSTEM OPERATOR
inc tntoxaninngore
Job Spec.No 834/1
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QUALITY ASSURANCE PAGE
CHANGES LOG
REVISIONS LOG.
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CONTENTS
REFERENCE DOCUMENTS
1.0 SCOPE
20 GENERAL REQUIREMENTS
% SURFACE PREPARATION
40 MATERIALS
5.0 COATING APPLICATION
6.0 INSPECTION AND TESTING
7.0 REPAIRS
8.0 = MARKING
9.0 HANDLING, STORAGE AND TRANSPORT
10.0 TECHNICAL DOCUMENTATION
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REFERENCE DOCUMENTS
Job Spec. No. 171/1
[Steel Pipe]
ELOT EN ISO 8501-14
[Preparation of steel substrates before application of paints and related products - Visual
assessment of surface cleanliness - Part 1: Rust grades and preparation grades of
uncoated steel substrates and of steel substrates after overall removal of previous
coatings]
EN ISO 21809-1
[Petroleum and natural gas industries - External coatings for buried and submerged
pipelines used in pipeline transportation systems - Part 1: Polyolefin coatings (3-layer PE
and 3-layer PP)]
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SCOPE
ITEM
This specification defines the minimum requirements for the surface preparation,
coating application, inspection and handling of plant-applied three layer
polyethylene (PE) coating of pipes; the minimum requirements for the epoxy
primer, extruded adhesive, extruded polyethylene outer layer and the applied
coating; and the minimum requirements for repair of pipe coating.
SERVICE TEMPERATURE
The service temperature of the pipeline will be from -5° C to +50" C. However,
coated pipes may be stored at ambient temperatures down to -20° C and with a
surface temperature up to 80° C under the sun,
GENERAL REQUIREMENTS
GENERAL
A record of pipe serial numbers shall be kept for Owner's information. This
record shall contain all information on the delivered pipes, ic. lengths, damages,
cuts, repairs, transfer of serial numbers, coated stock, bare stock, scrap.
These records shall be available at all times for review of the Owner. Upon
completion of coating operations the Contractor shall satisfactorily account for all
materials or shall reimburse the Owner for the full cost of any materials not
balanced.
All coating materials, production and repair procedures as well as test methods
shall be approved by the Owner before coating starts.
Coating application procedures shall be documented and monitored by the
Contractor. Written records shall be maintained by qualified personnel.
‘The procedures shall include:
- Surface preparation, including number, type and size of cleaning machines,
grades and types of abrasive, removal of steel defects, cleanliness, surface
profile and methods of measurement.
- Complete details of the coating materials, together with quality control and
manufacturer's certification sheets and of materiais storage, which shall be in
accordance with the manufacturer's recommendations.
~ Application of coating, including details of application temperatures, curing
times and methods, cutback and beveling methods and acceptable prevailing
working conditions (humidity, dust and temperature),
- Inspection and testing, including instrument and equipment types, makes and
uses.
= Details of instrument and equipment calibration methods, including relevant
standards and examples of calibration certificates.
= Coating defect repair methods and materials.
- Storage, handling and transport procedures for both bare pipes and coated
pipes.
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STANDARDS
Coating shall conform to the requirements of EN ISO 21809-1 and the requirements
specified herein.
The coating shall fulfill the requirements given for coating class A, LDPE as per
EN ISO 21809-1
COATING THICKNESS CLASS
The coating thickness class, according to EN ISO 21809-1, shall be AZ (for moderate
duty). The minimum coating thickness shall he a8 per Table 2, EN ISO21809-1 for
class A2.
SURFACE PREPARATION
INITIAL CLEANING
All weld spatter, grease, oil, etc, shall be removed prior to biasting.
In case of presence of chlorides the pipes must be washed prior to preheating for
biasting.
Ita chemical cleaner is used, subsequent washing with potable water is required,
BLAST CLEANING
The pipe surface shall be preheated dried before blast cleaning
The ends of the pipe shall be protected with plugs so as to prevent entry of
abrasive into the pipe during the biast cleaning
Alternatively the Contractor may propose to link the pipes together to prevent entry
of abrasive.
Unless otherwise agreed, surfaces shall be cleaned by abrasive blasting to at least
degree SA 2 1/2 according to EN ISO 8501-1. Angular sharp grit or a mixture of
grt and shot shall De used. Shot applied alone is not accepted. Blast cleaning
abrasives shall be agreed with the Owner. The use of sand is not permitted.
After blast cleaning, the surface profile shall have an average peak to trough
height of 40 um and a maximum of 7 um. Dust on the pipe extesiar shall be
removed directly before coating by a method which is approved by the Owner, for
example compressed dry air assisted by vacuum cleaning
Blasting abrasives shall be kept dry, clean and free from contamination. Airlines
shall be filtered to remove oil and moisture. Blasting abrasive shall be cleaned by a
dust extraction system, which removes fine particles the size of which will be
determined after the initial site testing
When recovered metallic grit systems are used, a stabilized working mix of blast
cleaning material shall be established and maintained throughout the entire course
of the production by frequent small additions from fresh or cleaned stock at a rate
Sufficient to replenish consumption. Large additions of new material shall be
avoided. Report verifications of the mix quality shall be submitted to Owner by the
‘Contractor.
Blasting and other dust producing areas shall be kept separate from coating
application areas.
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The blast-cleaned surface shall not be contaminated with dirt, dust, metal particles,
hydrocarbons, water, or any other foreign matter, which is detrimental to the
coating
3.3 SURFACE INSPECTION
The metal surface shall be inspected after biast- cleaning under adequate lighting
from both ends and all slivers, scabs, burrs, gouges, sharp edges in welding area,
etc, made visible shall be removed by grinding. Grinding which reduces the pipe
wall thickness below the nominal wall thickness minus the permissible negative
pipe-manufacturing tolerance is not permitted.
Pipe ‘engths containing a dent shall be set-aside for the Owner's Representative
to determine its disposition. Gouges in a dent shall not be ground
The pipe surface shall be uniform throughout before coating,
Coating shall take place quickly after cleaning and before any contamination or
rust blooming appear. If the surface shows any contamination or rust blooming, the
surface shall be blast-cleaned again.
Pipes, which have not been coated within three hours, shall be reblasted
Blast cleaning shall be suspended if the pipe surface temperature falls 3° C
below the dew point
40 MATERIALS
44 GENERAL
The 3-layer polyethylene coating system shall consist of
- One fusion bonded epoxy powder primer coat
~ One adhesive coat,
~ One extruded polyethylene outer coat.
The manufacturer, trade name and data sheet for the coating materials proposed
by the Contractor shall be approved by the Owner prior to the placing of any order
for coating work.
The coating materials shall be handied, stored and applied in accordance with the
manufacturer's specifications, or as directed by an authorized representative of the
coating manufacturer.
Materials used are to be demonstrated either on independent test certificates (not
older than + year) or during the pilot production period of the plant,
The Contractor shall obtain from the manufacturer and submit to the Owner:
- The guarantee that the epoxy primer material, the adhesive material, the
polyethylene and the repair products delivered shall meet the coating
characteristics of this specification.
- Production test certificates each for the epoxy undercoat material, the adhesive
material and the poiyethylene.
- For epoxy powder, one test certificate shall be submitted per batch, including
results of the tests defined in this specification. The certificate shall be in
conformity with the specified methods and acceptance values.
+ Standard infrared scan of epoxy powder for each production batch and a
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certificate indicating that this complies with the normal scan for the product.
~ Major epoxy powder appiication data.
- Substrate temperature.
~The maximum time interval during which the adhesive has to be applied.
- Packaging and storage requirements of epoxy powder and repair products.
+ Details of marking on each package of powder and repair product including
+ Manufacturer's name,
+ Place of manufacture,
+ Complete identification of powder and repair product,
+ Production batch or cast number,
* Date of production,
+ Time limit for use,
+ Any special safety or storage instructions relevant to the batches,
+ Conditions of application of any repair products,
42 EPOXY PRIMER
Approved fusion bonded epoxy powder primer compatible with the adhesive shall
be used.
Epoxy Powder and Adhesive material shall be products of the same manufacturer.
Unless otherwise agreed, the selected epoxy powder shall meet the requirements
of paragraph 8.3, Table 3, EN ISO 21809-1, for Class A.
EPOXY POWDER RAW MATERIAL REQUIREMENTS
PARAMETER TEST METHODS _| UNITS | REQUIREMENTS
gfom? AS per
Density ELOTEN ISO 2811 manufacturer's spec.
| 40.05
Within 20% per
Gel ime Annex K, ENISO 218081 Sec | manufacturers spec
Moisture content (by mass)| EN ISO 21809-2 % $06
Gass transition temperature| Annex D, EN ISO 21809-1 °C 295
As per manufacturers
Residual het ‘Annex D, EN ISO 21809-1] Calg spec.
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43 AOHESIVE
Unless otherwise agreed, the adhesive shall meet the requirements of
paragraph 8.4, Table 4, EN ISO 21809-1, for Class A.
ADHESIVE RAW MATERIAL REQUIREMENTS
PARAMETER TEST METHODS | UNITS | REQUIREMENTS
Elongation at break at 23°C | ELOTENISO527 | % 2600
Strength at yield point at 23°C | ELOT ENISO 527 | MPa 26
Notch impact strength ELOT ENISO 179 | KJim?
VICAT Softening temperature | ELOTENISO.308 | °C 260
‘Water content ELOT EN ISO 19512) % <0.1
44 EXTRUDED POLYETHYLENE
The polyethylene material shall meet the requirements of paragraph 8.5, Table 5,
EN ISO 2809-1, for Class A.
POLYETHYLENE MATERIAL REQUIREMENTS
PARAMETER TEST METHODS | UNITS | REQUIREMENT
Density ELOT EN (SO 1183) glam? 20.920
Strength at yield point at 23°C | ELOT EN ISO 527) MPa 210
Elongation at break at 25°C | ELOTENISO 827, % 2600
Hardness Shore D ELOT EN ISO 868 | ~~ 2 100
VICAT Softening temperature | ELOT ENISO 306) °C 295
The Material shall, in addition to satisfying the production test requirements
covered by section 6.6, be suitably stabilized against thermal and UV effects as
per Annex G, EN ISO 21809-1 to withstand open air storage at the conditions
‘specified in section 4.0 for a periad of at least 1 year
45 REPAIR MATERIALS
The Contractor shall present details of proposed repair materials to the Owner for
approval. This information shall be submitted together with the relevant repair
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Job Spec.No 834/1
procedures.
The repair materials shall be such that the completed repair ensures a coating
Quality conforming to the requirements specified in this specific
6.0 COATING APPLICATION
5A GENERAL
Prior to the commencement of full production the Contractor shall carry out a
qualification test on lengths of line pipe to be coated 10 demonstrate that the
coating applied in accordance with the Contractors proposed procedures
complies with the requirements of this specification.
Production coating will commence only after all qualification tests including
Cathodie Disbonding tests have been approved by the Owner.
Long-term test results (thermal aging, electrical resistance, UV exposure etc) at
this stage can be covered by test results conducted by Independent Accredited
Laboratories taken from line pipe production (with same raw materials) from
previous arders of the Applicator
‘The pipes shall be coated on a continuous coating line without any risk of damage
to the pipe (external pipe wall, bevels, coating) during the heating, coating, curing
and quenching operations.
$2 HEATING
The heating equipment shall be suitably controlled to maintain uniform
temperatures and to achieve the required uniform temperatures along the total
length of the pipe and it shall be such that it will not result to any contamination of
the steel surface.
53 EPOXY PRIMER
The primer shall be applied immediately after the final preheating, including drying, is
terminated.
The pipes shall be heated to obtain a pipe temperature as recommended by the
powder manufacturer.
‘The epoxy powder shall be sprayed using electrostatic spray guns. The thickness of
the coat shall be a minimum of 60 jm, The coating fim shall be smooth, and uniform,
The pipe ends shall be left unprimed to a length of 50 mm,
54 ADHESIVE
The adhesive coat shall be applied by an extrusion process immediately after the
epoxy undercoat has been applied,
The thickness of the adhesive shall be a minimum of 250 um. The adhesive fim shall
cover the entire steel surface.
8.5 EXTRUOED POLYETHYLENE
The extruded polyethylene coat shall be apalied by extrusion process.
The temperature during extrusion shall be as recommended by the manufacture.
The number of wrap and the over-lapping shall be such that the polyethylene coat
thickness achieved shall meet the requirements of EN ISO 218091, for Class A.
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The coating shall be pressed by pressure rollers in order to avoid any air
inclusions.
‘When coating is completed, the pipe shall be cooled with water to such extend
where damage of the coating from further plant transportation and handling cannot
occur. During cooling, the pipe shall be handled so as to avoid damage to the
coating.
Overiap of the coatings shall be at least 50 mm.
56 CUT-BACKS:
The coating shall be cutback immediately after cooling, and surplus material shall
be removed.
The epoxy, adhesive and polyethylene layers shall be totally removed, removed
length shall be 150 mm + 20 mm.
The remaining coating shall be beveled (o approx. 30° to ensure proper void-free
bonding of field-applied joint coating
The cutback prepared will be protected against ingress of moisture and rust by
application of a temporary protection system compatible to the welding (organic
phosphate or equivalent).
6.0 INSPECTION AND TESTING
64 GENERAL
An office and all necessary facilities required for the performance of his work shall be
made available to Owner's Representative by the Contractor.
Inspection and testing shall be carried out according to detailed Table 9, EN ISO
21809-1 by the Contractor and, unless otherwise agreed, in the presence of the
Owner's Representative.
It shall include the following operations:
~ Inspection of raw materials.
~ Systematic inspection of pipe surface preparation
- Inspection of application parameters,
- Systematic inspection of coated pipes.
+ Production testing
The Owner's Representative may check any pipe for conformity to any requirement
specified in this specification. He may take samples of the coating materials or repair
product and specimens of coated pipe(s) for testing in laboratories selected by the
Owner in order to check the quality of the testing products. He shall also have the
Tight to select the pipes to be tested.
The following properties will be checked according to detailed Table 9, EN ISO 21809-
1:
- Surface before blasting
+ Surface after blasting
- Environmental conditions
- Pipe temperature before blasting
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- Size, shape and properties of abrasive
- Water soluble contamination of abrasives
~ Surface roughness of blasted surface
- Visual inspection of blasted surface
- Presence of dust after dust removal
~ Elapsed time between blasting and coating
- Temperature of extruded adhesive
- Preheating temperature before coating
- Minimum epoxy thickness
- Minimum adhesive thickness
- Degree of cure
~ Appearance and continuity
- Total thickness of coating
~ Impact resistance
- Peel strength
- Indention
- Elongation at break
- Cathodic disbondment
- Flexibility
- Hot water soak test
- In process degradation of PE
- Pipe and preparation
~ Coating repairs
INSPECTION OF RAW MATERIALS
Upon delivery, the packaging and markings thereon shall be checked. Packaging
shall be in accordance with the manufacturer's instructions and marking shall be in
conformity with EN ISO 21809-1 requirements.
Non-conformity with any of the specified requirements shall cause the immediate
rejection of the delivery concemed.
Three 50 g samples of each coating material shall be taken for reference purposes
from the production batches. One shall be retained by the Contractor, one shall be
transmitted to the Owner and one shall be kept as a check sample in the
Contractor's laboratory for six months, away from humidity, at a temperature below
and close to 20°C.
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63 INSPECTION OF PIPE SURFACE PREPARATION
631 FINISH OF PREPARED SURFACE
6314 STANDARD
ELOT EN ISO 8501-1
6.312 METHOD
Visual comparison of prepared surface finishes with the illustration corresponding
to Sa 2 1/2 surface finish
6.3.1.3 INSPECTION
Each pipe.
63.1.4 ACCEPTANCE LEVEL
The inspection of each pipe shall be considered as accepted when the whole
prepared surface shows the same aspect as the relevant illustration.
63.1.5 CORRECTIVE ACTION
Rebiasting
632 EXTENT OF DUST ON PREPARED SURFACE
6321 EQUIPMENT
Adhesive tape.
632.2 METHOD
EN ISO 8502-3
‘Application of the adhesive tape on the prepared surface, removal, sticking of the
tape to white paper, and visual comparison to a reference sample.
63.23 INSPECTION FREQUENCY
Every 1 hour.
63.2.4 ACCEPTANCE LEVEL
Equal to or better than the reference sample.
The reference sample shall be considered as accepted when the proportion of
adhesive surface, showing dust particles is less than those for a test panel
approved by the Owner prior to production.
6325 CORRECTIVE ACTIONS
Recleaning
633 TOTAL ROUGHNESS OF PREPARED SURFACE
6331 EQUIPMENT
Electric micrometer equipment.
63.32 METHOD
Measure the profile height with an electronic micrometer.
6333 INSPECTION FREQUENCY
Every 1 hour.
6.334 ACCEPTANCE LEVEL
The condition of each pipe shall be considered as acceptable when 4 vaiues have
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64
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644.4
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an average of 50 im with a maximum of 100 jum. if any value(s) are outside the
above, an additional measurement shall be made around each point concerned.
The tota! roughness value obtained from the new measurements shall be as
specified above.
CORRECTIVE ACTIONS
Ifthe values measured are not as specified above reblast.
INSPECTION OF APPLICATION PARAMETERS
PIPE TEMPERATURE AT START OF COATING
EQUIPMENT
Optical pyrometer, calibrates by “Tempil sticks" temperature recorder, or monitor.
METHOD
Specific to the instrument used which shall be calibrated at least twice per shift by
"Tempil Sticks’.
EXTENT OF INSPECTION
Continuous over total pipe length.
ACCEPTANCE LEVEL
Pipe temperature range as specified by epoxy and adhesive manufacturer.
CORRECTIVE ACTIONS
Rejection of pipes coated outside specified temperature range.
642 SPEED OF PIPE TRAVEL
6.4.2.1 EQUIPMENT
Contractor's choice
644.2 METHOD
‘Specific to the equipment used which shall be calibrated at least twice per shift
64.2.3 EXTENT OF INSPECTION
Continuous during pipe travel along the coating line.
64.2.4 ACCEPTANCE LEVEL
The inspection of pipe travel speed shall be considered as acceptable when the
measured speed conforms to the approved procedure.
64.25 CORRECTIVE ACTIONS
Intensified check of coating thicknesses. Correction of pipe travel
643 PLANT TEMPERATURE
6.4.3.1 EQUIPMENT AND RECORDER
Contractor's obligation
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METHOD
Specific to the instruments used, calibrated according to manufacturer's
instructions,
EXTENT OF INSPECTION
‘Once per 4 hours.
ACCEPTANCE LEVEL
As required in section 3 of this specification.
CORRECTIVE ACTIONS
Correction of variant parameter and, at the judgment of the Owner's
Representative, rejection of pipes coated since last acceptable test.
65 INSPECTION OF COATED PIPES
65.1 GENERAL
Equipment, methods, extent and acceptance criteria shall be as per EN ISO
21809-1, with the additional requirements outlined below.
If the results of one or more tests do not conform to the specified requirements,
additional tests shall be run at the rate of two per defective test, respectively on the
pipe coated immediately prior and after the pipe found to be defective.
if the additional tests are acceptable, the coating of the pipes shall be considered
to be in conformity with the specified requirements (except for the pipe where the
test failed which shall be rejected and recoated)
In case of unsatisfactory result of one of these additional tests, the Contractor shall
perform the test concemed on extra 10 pipes chosen at random and submit the
results obtained with notification of the values corresponding to a correct test.
The pipes with defective coating shall be rejected and recoated. Any further
action required shal! be based on the results of these tests.
65.2 VISUAL STANDARD:
65.21 METHOD
‘Visual.
65.2.2 INSPECTION
100% of the pipe coated surface.
6.5.23 ACCEPTANCE LEVEL
No disbonded areas, air pockets, groves, fissures, blisters, splits, scratches, or
other imperfections. The coating shall have a uniform colour and gloss.
653 THICKNESS
6.5.31 EQUIPMENT
Magnetic, electromagnetic or ultrasonic measuring instruments with « 10% accuracy.
6532 METHOD
Annex A, EN ISO 21803
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65.3.5
65.4
65.4.1
65.42
65.4.3
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EXTENT OF INSPECTION
Annex A, EN ISO 21809-1
On each pipe to be tested, the total of 12 measurements shall be carried out in
accordance with EN ISO 2608,
Initially one out often pipes shall be selected for checks.
If the required coating thickness is not met, each pipe shall be checked. The
frequency may subsequently be varied based on quality.
ACCEPTANCE LEVEL
EN ISO 21809-1, Table2 for Class A2.
CORRECTIVE ACTIONS
Revision of coating process and rejection of pipes with thickness below the
specified one.
CUT-BACK
EQUIPMENT
Rule or template.
METHOD
Specific to the material used.
SCOPE OF INSPECTION
At both ends of each coated pipe.
ACCEPTANCE LEVEL
The pipe shall be considered accepted when the cutback length is in
conformity with the requirements of section 5.6.
CORRECTIVE ACTIONS
AS required.
POROSITY (HOLIDAY TESTING)
EQUIPMENT
Adjustable holiday detector with voltage indicator, ard electrode consisting of:
= One circular metal searching coil,
~ One elastomer element for possible defect location
METHOD
EN ISO 21809-1, Annex B.
EXTENT OF INSPECTION
100% of coated surface
ACCEPTANCE LEVEL
As per EN ISO 21809-1. However, every coated pipe with more than two holidays
shall be rejected, Coated pipes with max. Two small holidays shall be repaired in
accordance with a procedure approved by the Owner. Any pipe subject to a
coating repair procedure shall be fully re-examined.
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