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Salt Analysis Booklet

Salt analysis booklet

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0% found this document useful (0 votes)
26 views6 pages

Salt Analysis Booklet

Salt analysis booklet

Uploaded by

4784arnavgupta
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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test Toe sodium carbonate bead enti quantity of sodium carbonate on a opin the Bunsen Dar Srhite, opaque beads 20 ed sippedins nile NO, and on inane salt or example) an the sng fame, green bead of sodium 0, —PeNaMn0, + COs ino + Na008 * eth ehromium at due toformation of Ana £10, +403 ‘ Po, teat P ve HClis taken ito the lower NaPO, + si are ee ‘and colour impe to the flame by salts is C00 —, nacoPo, ws pela of AP yg" Cal”, 2") are eerie ame 8 marcel in Table cat ae ou (GF). T ‘Te yellow colouration hv stim mask at of peau. aes vio the fame wa glans. the yellow sodium colour i cand ehe potassium flame appears ceo Pe yow ew wen het, courts | Green when Chet nd a | Gm wenn te tn Salt misture is Separately and by observing the typee of | sue wan ae fests of anions are performed. ae +H0+6 Ds + C0, —+ Caco, 4 + ma oe 2NaNO, + 1.50, —, ‘Na,SO, +25 J Bs eno HNO, «N07 FH +10, +211N0, —. 1s0,"roney Wermund — (ie aut ss areas St3 re a sup ceHacOOnP” — ey Na [FCN NOS) pre(CNNO} gore nas eNalte terol site 80; wo sat A, Nag80, + Hx0 +893 +380) +0 () Acetate (CH,COO)I" + 2 a grat + 280 > FOF HEMT 7 : Mnecoo- +9F2* #20 —* MORES - 5 traiorncH,coon! +440 > 4+ 30H,COOH + H” {Fe(OH),CH,COO) ‘brownish-ted Pmt «s) Thiosuate “pp sant + 84+80,1 +P gga vues CyOP 1H ein r= sepia —> MBA NS Ags #110 TT AGH HAO. Nis XE) is decolourised by thiosulpate soluon i +280F —> 805 + 1, solution Gn scvenigo, 2 HS0, + HCL 4, axHts0, + 2010) + #0 “Ho ‘saNacl+ 280 cus *2H806 x0, +281 —+ COLL exo, NaOH —* Nae 7 s pucxO44 + 2C#,000N sucr0, (HCOOH — PEO (o Bromide te +H,80, + KHSO, + HBr A Peasletouk shi Scr | = ‘alae [inset gos SST foie h nape ba, 2 By +2807 MBB a Seton me pane havo eee: NO, ‘age + 2NHi(0g) —> (At TEE pera bie ‘Strate ame Seen ies Saeeeter Layer tat Se cee + cc, M5 yor eran ci 2 Sree oss CCl cn be taken intra of CHCA) abr + Ch —+ ANCL + Be aver, In can of Fit eur oi CHC Ie ANAC let a 0 — aso, Hels Stia9) —. wae, analy a pes MnO, "+ Mach, + Ct + 24,0 KOl* AgNO, —y pci + KNO, aNal+ Cy (i Toate xin g0, 2+ HBO, +H an + 80, —+ ned #294,0 450s Layer teat See Lager tnt ove (oy Nirate NaNO, +140, —+ Nall80, + 1NOy AaCts 2860p antec Oita +, £10 omy ae Sema rn ee eh ro apne {HCO yetow Formulas 517 chemistry Ky tanto Kol a OH jeMoO, +24HNO, > ura TCEINHLNO, + 3NANO, #1280 12MoO, NH POs wa om 0 tl fl woride ‘rod in contact feagthpeont Saree « ey de it on shows | renee NaHSO, + HF . NaF + HS0, — 2NaNO, + 241.80, on, Fi sm a i 10, + 6Feso, aH80, — 3FeyS0,), *2NOe é eee o Ww) Oo, FeO No} S92. Bo, vp r o N8L0,+ 150, —. Naso, ¢ CO burns with blue flame and CO, — HO+004, = a SCOP +20; + 16H", pie ole 10C0, icals have different basic radicale venta, THUS e basis of solubility asad into following Cath + NaC, —s cacyo, white C*C0, declourisesacidied KMng, Specific Tests in Solution © Sulphate To SE ada dil. ceases). Add BaCl, cone. HNO, Bac, ema, [ak +Na380, —+ BaS0,4 + 2Nact | sulpies, white ppt. ca 0a2*, |S gas inthe | sub Fon Han, |peeen oa (OS: MSS ae se, rr ethanol in a China-dish wit) Pee | ‘Mame of ethyl borate 2Na,BO, +3H,80, —s 24,80, + aNs,S0, 4 180, s2cHh0H 4, CHHo,n age Sia bre ari tame ra Gi) Phosphate SE + HNO, + am smonium molybdate solut Heat; yellow crystalline ppt confirms PO} + Ho y lo ea soe : (enc, (4:20, | cats | mie fer, | r Ma? | fa (EH Joe ce + Neato, Hb (®) Group I Ag’, Pb, Hai" sitatedl sie ee wet ritate, this group is absent. a Ag’ + Cr —+ Agel Po 6 2cr — Pc, Hey" + 2Cr — Hed Prana paris + POC, (is soluble in hot water and chus separated. * A8Cl is soluble in aqueous NH, as [Ag(NH,),JCl AgCl+2NH,—+ (AgtNH,), JO anne le ‘+ He,Cl, is blackened by NH, onan Mech, +28, —o HeNIL He NI ee a an Bane, eo) a 1 ad Se cp CTAB or NAOH ee gh DiS C38 MA Corer em) nwt dre puting, trite i= orange fry" confmed, Tuy ading i HCL as ogy ae sble in HNO, (1:1) whe HS + PS, aS Case gr eolbl in gu Tee om 0s lac) sll in HNO, =D) a HINO, —> APDINO,), # 2NO +38 +4140 sae OS + ae KL > ellow pet PL) "aero, 0%, tow ot PHC.) tw ca «+ 3CdS (yellow) + BHNO, ~*+ BCA(NO,), +2NO + 4H,0 +85 @) soluble in yellow are insoluble in +B +CH,COOH + K,(Fe(CN),] —> bluish white ppt Ca(NO,), + 2CH,COOH —+ (CH,COO),Ci + 2HNO, 24CH,COO),CA + K, [Fe(CN4] —+ Cda[Fe(CN] + 4CH,COOH ‘ish white pot MaS buf co addition of excess of bbrown/black by a Dissolve MnO, oF MaOH, ppt. in onidising agent KCI0, or PbO,sheattoboin No> a4 purl aa MnO, * 28ND, —s MnO, +0419, SPO, + 2M" «6H GPR S200, 0 Gi NAS SiS Gack ppd) ie soluble in cone, Hin sag Oidising agent like KCIO, cal Nis+2HcHO Nic soured ppt) are soluble in NaOH gives Ma(OH, pt whi b +HO+s soluble j fo | (O*NHOH + dimethy gyocine — chery rept Nich + 20H-—e—wou ‘ 9. — inNHOH CHy~C=NoH methyl elyime t Meta Hic_tmy 7 coed Od cherry red ppt (dimethyl pyoximate) {i9) Cob Like NiS, CoS (lack ppt) is alan soluble in cone Presence of oxidising agent KCIO, Cos +2nci+0-4s coc, +1,0+8 fone Oy sole + (D)* CH,COOH + KNO, —+ yellowish orang pot CoCt, + 2KNO, —+ 2KCI + CoNO,)s CH,COOH + KNO, —+ CH,COOK + HNO, o 6r0uP esate 523 sry xgremaoetetisaromae 5 cof nto + Kylcatoy)t age oso 4 280: poten alone xn ‘range 669 Ho +Not bolo HS white pot race of 7 VG NH,OH, HILO Brick red « Dial the peta CEHOOOHE (CH,CO0),Ba + K:Cr0,—> Mr __, “5x80,4.+20H,COONH, tie pet) — cap, | + 2CH,COONH. vier (cuc00),Se+ (NHS. {(cH,c00,Ca + NHCP Group Vi(Ma™) ue 0 ee yx nait0,—> «Sn eetaion io of the test tbe scratching the side of the yPO, 1 + 2NaCl+ HO o 1PO, —> MetNH IPO, MgCl, + NHOH +Na,HPO, 2 (@) Group Zero (NH.’) + Sat+ NaOH + en ving whit mes with HCL Hcl sow NH (g)* NACL HD +ucl—> NH. NH @) +H me sd Nesters AS brown ppt of brown Of um we) eae de ow ednuron eyiercr amon odie. Aiton’ eae (AA i lo eae asic mercury I)

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