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Powdered Metal Design Solutions

Powder metallurgy

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Powdered Metal Design Solutions

Powder metallurgy

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subbu
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POWDER METALLURGY Benefits of P/M How P/M Parts are Made Secondary Operations a Choosing the Right Materials TO sessstnteteenenesenenne swuEngineering Properties 19s srrccrccenreserstn ae Designing P/M Parts TB ssssssatcsenicon Near-Fully Dense P/M Products D2 ecnerseunssittctiil Applications of P/M Parts BB: csresenneenneneniitl How to Specify P/M Parts DA cesestnssnee The Internet for Design Solutions 2 ossseenBibliography and More Information aOR a Vi) WHAT IS P/M? Powder metollurgy—or P/M is « highly developed method of manufacturing precision metal parts. Made by mixing elemental or alloy powders and compacting the mixture in @ die, the resultant shopes are then sin- tered or heated in « controlled-otmosphere furnace to bond the particles metalurgicaly. Basicaly a “chipless metalworking process, PIM typically uses more than 97% of the starting raw material in the finished part Because of this, P/M conserves energy and materials. The PIM process is cost effective in producing simple cor complex parts at, or very close to, final dimensions in production rales which con range from a few hundred to several thousand ports per hour As a result, oly minor. if any. machining is required, PIM parts also may be sized for closer dimensional control and for repressed for both higher density and strength In addition, both ferrous and non-ferrous P/M ports can be oil impregnated to function as self-ubricating bearings. Ferrous P/M ports can be resin impregnated to seal interconnected porosity and then plated with nother metal if so required: infiltrated with « lower melting point metal for greater strength and impact resistance; ond heat treated to o higher strength and hardness ‘Most P/M parts weigh less than 5 pounds {2.27 kal although parts weighing as much as 35 pounds |15.89 kal can be fabricated in conventional P/M equipment ‘Many of the early PIM parts, such as bushings ond bearings. were very simple shopes, as contrasted with the complex contours and multiple levels which are: economically produced today. a 8 8 Taal Sangh 0%! 5 Figure 1- Comparison of material srenaths P/M SAVES STEPS Since the PIM process is not shope-sensitive ond nor mally does not require drafl, ports like coms, gears, sprockets and levers ore very economically produced. Previously, designs had offen required that ports such as «com and a gear, or @ spur gear and pinion gear be joined together by a secondary assembly method These additional ossembly steps quite frequently can be eliminated with multiple level designs which combine the separate shopes into © one-piece P/M port. In ‘other instances, two PIM paris may be assembled afer pressing. and then bonded into a one-piece part during sintering, P/M IS VERSATILE The bosic versatility of P/M is applied in numerous industries, including cutemotive, business machines, cerospace, electrical and electronic equipment, small ‘and major oppliances, agricultural and garden machi: ery, off-highway equipment, sporting goods, hand and: power tools. Thousands of different cost-saving reliable PIM designs now serve these industries ina wide range of engineering applications which fal into two main groups. In one group ore pars which are very aif ficult to make by any other production method, For exemple, paris of dificul-to-fabricate materials such os tungsten and molybdenum, or tungsten carbide, cannot bbe made efficiently by any other process. Also, porous borings. ters ond many hard and soft mognetic parts cre exclisvely products of the PIMA process. Another ond larger application group consists of com ponents where P/M is an effective alternative to machined parts, castings ond forgings (Figure 1). P/M. technology hes also expended into precision hot forging from sintered preforms, thus extending its capabilties to providing P/M ports with inereosed strength, toughness cond fatigue lif. The following sections describe the PIM process, materials, perlormance properties and design porame- fers thot define the technology's capabilities and pro- vide guidelines for development of a relicble, efficiently produced port ADVANTAGES OF THE P/M PROCESS Eliminates or minimizes machining Eliminates or minimizes scrap, ‘Maintains close dimensional tolerances. Permits a wide voriety of alloy systems Produces good surface finishes. Provides materials which may be heaMreated for increased strength or increased weor resistance * Provides controlled porosity for self-lubrication or filtration, Fociltates manufacture of complex or unique shopes which would be impractical or impossible with other metalworking processes Provides excellent port-to-part reproducibility and repeatability Suited to moderate-to high volume component production requirements, Offers long-term performance rebcbilty in eritical cepplications. + Cost eflective. + Energy or environmental efficient FOR THE LATEST AND MOST COMPLETE INFORMATION how p/m parts are ma 8 Typical parts can be produced at rotes of several hun: dred to thousonds per hour with the P/M process Although normally associated with high volume proce tion, P/M is also feasible for economic part production in lower volumes. Also, extending tooling use to produce more than one part, such as in varying thicknesses or a common part with different size holes, will enhance the low volume economic rattanale for PIM. Another con- sideration is that the port design should take edvantage of the ability of the PIM process to minimize secondary processing operations in comparison with these require iments if the part were to be produced by competitive methods. When these factors are considered, P/M parts can often offer cost and performance edvantages in short pradkction runs. BASIC P/M STEPS The three basic steps for producing conventional parts by the powder metcllurgy process are mixng, compoc!- Ing ond sintering IFigure 2 ing-Elemental, portilly alloyed or preolloyed metal powders are first mixed with lubricants or other allay addtions to produce a homogeneous mixture of Ingredients. These additives may help impart machin- ‘bility. wear resistance or lubricity 10 the base alloy ‘composition. The mixing may be done by either the ‘metal powder producer or the P/M parts manufacturer Compacting-A coniroled amount of med powder is automaticaly gravily-fed Into a precision die and is compacted, usually at room temperature. af pressures as low as 10 tons per sq. in. or as high os 60 or more fons pet 5q, In. (13B to 827 MPal depending on the density requirements of the part and the powder being pressed. Normally, compacting pressures in the range of 25-50 tons per sq, in. (345 to 690 MPa! are used, Higher pressures limit tool life, especialy with thin or fragile tool components Compacting the loose powder produces a ‘green compact” which, with conventional pressing techniques, has the size and shape of the finished port when eject ced from the die, ond sufficient strength for in-process handling and transport fo a sintering furnace. Typical compacting techniques use rigid dies set into special mechanical or hydroulc presses. Tool sets ate made of either hardened steel ondfor corbides, and consist at least of a die body or mold, an upper and lower punch and, in some cases, one or ‘more core rods, Die materials are selected to withstand the high compaction pressures and abrasive character istics of the metal powders, The pressing cycle for producing a simple partis shown in Figure 3. The die receives @ charge of mixed powder, delivered to the cavity by o feeder shoe. The Upper and lower punches compress the powder. The volume of powder fed into the die is controlled by the relotive postion of the lower punch in the dhe. After fille ing, the feed shoe is withdrawn ond the upper and lower punches compress the powder. When compaction is completed the upper punch is withdrawn, relative motion between the lower punch and die ejects the pressed compact and the feeder shoe sides the piece ‘away from the die covily. The feeder shoe continues forward ond refill the cavity with another charge of powder ond the cycle automaticaly repeats. This compacting cycle is typical. When more then one pressing level is needed, however, os for excmple in Figure 2 « The PIM Process making flanged shapes or cluster gears, multiple punch: es with separote actions may be needed [Figure 4). Holes in the direction of pressing can be molded by Using additional core rods. Figure 5 shows o multilevel PIN\ port and compacting press in the background, ‘More specialized compaction and alternate forming methods are sometimes used, such as isostatic pressing, extrusion and injection molding, Warm compaction of ferrous powders, ot temperatures of 200-300 |95- ISOC! is used to achieve higher densities and create on iton-plostic composite with unique mognetic properties. Sintering-h the typical sintering step. the green com- pact, placed on a mesh belt, slowly moves through @ controlled-cimosphere fumace [Figure 61 The parts are heated below the melting point of the bose metal, held ot the sintering temperature, end then cooled. Bosicolly «solid stale process, sintering transforms compacted 1 Oycle 2 charging ting) die with powdery ‘3Compaction begins Acompucron 4 si #4 TT Figure 3 - Pressing cycle for 9 single level port PIM Cluster Gear (Dual Level) uch Core Rod. Die. =f he. Figure 4 - P/tA tooling for 2 tworlevel port Figure 6 - Sintering Ports entering furnace. mechanical bonds between the powder particles into metallurgical bonds. This provides the P/M pats xia: 1y functional properties. Typical sintering temperature ranges are 1450-1550F (790-845'C) for bronze and 2050-2100F (1120-1150°C) for Ferrous alloys. Belt fur nace cycles average 1-15 houts for small bronze bush ings and 2-3 hours for average size ferrous ports. Throughput vories with port size, belt width and speed, reaching ¢s high as 1000 pound/hour (450 ke/howr) in lorge furnaces. Enhanced sintering of ferrous P/M is done at higher femperaiures. on average 300 higher than conven tional belt sintering, to provide increased mechonical properties, superior soft magnetic parts and improved stainless sige! materiols The sinfer-hardening process sing @ controlled cooling rate in the cooling section of the belt-sintering furnace, transforms the steel matrix of «ferrous part to martensite, thereby eliminating the need for 2 secondary hardening step. PIMA ports ore generally ready for use afler sintering. However. fo provide special properties, the parts can be repressed, impregnated, machined, tumbled. ploted or heat-trected. Rae M ACN C CONICS Secondory Operation Typical Pars (Objectives Repressing Caring Al Dersiicoten, modfy surface shape (coming). dimensional conral Sting Al Dimensional centro Impregnation oi Bearings ‘Moke bearings selflubricating Resin Shuto! Inprove machinabily, Prepare surface fr plating wth ether matols ‘Seo pes gos er kqud tght. Provide lubrication, Infiteation Ferrous lnprove strength seal ports gos or lui igh Siucturl Prepare arface fr alarng wih ther metals Inprve duchy and rmochinebiy Heat Treating Quench and Temper Fertous Shucturol Improve srength and hordes. Steom ect Ferrous Icke srice herd ond wear resston!Inprve coroson resisonce cand seal porosity Mochining Dill ond Top all To instal st screws or assembly fosters Tring al NMochine to exact tolerances Feem undercuts or features not possible wih compaction tootng Mliog Al Form underuts oss Grinding al Remove stock: make faces fat ond parca improve sure fish and dinersiona oleronces, Finishing Debuting Al Remove shorp edges reloted to punch and de foaing Burishing Ferrous Stucke Bal io roller bush for size contol and surface fish Coating OI Dp Ferrous Corrosion resistence Cooper, Nickel, Feros Corson resistence; oppecrence Coctium, Zin Chromium Plating Weldng Ferrous Make esses from two or more pats. (68 olem? min density Block Ove Ferrous Corrosion resistonce, point bose rea impregnoted Mechanical Surface al Cleanlinprove srfoces Treiman Gloss Beading Wire Brash Sanding. Turdling! Veotry Finishing ‘Shot Peering Ferrous Sct Improve surface fotgue He Forgings Folrone Powe Motlinay Deen Maal ‘SECONDARY OPERATIONS The controlled porosity in P/M parts permits their impregnation with ol or @ resin, [igure 7) Also, with suitable compaction techniques, porosity con vary in dif- ferent areas of the P/M part Ollsinpregnoted P/M beorings have been used in ‘automobiles since the late 1920s. Conventional P/M, becrings con absorb from 12 to 30% by volume of generally, addiive-fee, non-cutomotive engines oil lnjoregnation is achieved by sooking the parts in heat ced oil, or by vacuum techniques. When friction heats the por, the oil expands and flows to the beoring sur face On cooling, he oil returns into the metal pores by copillary action The some porosity, however which is so beneticial for cil mpregnation con be quite detrimental to @ port undergoing some secondary operations. Molten sats, cutting fluids, cleaning and plating solutions can be tropped in the pores, hereby leading to later corrosion or unsightly “bleed-out’. Farts ore typically pre-imprege noted with @ resin prior to ony such exposure to fluids ‘r solutions. Immersion in molten salts is discouraged altogether Burr relief slots, [Figure 8), are practical modifications to inside diameters of parts with hubs being drilled anc! topped to receive set screws, Use of such a slot or recess provides room for the machining burr while stil keeping it away from the shaft on which the port is mounted. Ferrous P/M ports con be succassllly welded or brazed. Most conventional welding methods (TIG, MIG, electron beom. resistance, friction, laser or copacitve discharge] are applicable. Welding perfor- mance is determined mainly by part densty,olloy com postion, proper joint design ond elimination of contami rants (oils, Iericonts, coolants, elc |. Furnace brazing, Using special copper brazing alloys designed for PIMA parts, con be completed during the sintering process Fgxe 9. Figure 7 - O11 impregnetion Figure 8 - Gur colt slot Figure 9 - Furnace AAs precision engineered materials « diverse group of metal powders is avalable for « wide range of PIN products, Generally, powder mixes for compacting are prepared from three powder types, The fist is admixed where elemental alloying powders such as copper nick- el, graphite and tin ore added to base element pow- ders such os iron or copper Partially alloyed powder is composed of two or more elements where the alloying tadatives ore diffusion bonded to the base powder dur- ing the powder monufacturing process. These powers Ose nmr ane Cee cxeduce @ helerogencous micrastructure with good dimensional control and excellent as-sintered mechani cal properties. Preclloyed powders, on the other hand ore stomized from alloyed furnace melts: each powder particle has the some nominal composition throughout Prealloyed powders yield homogeneous phase con: stituents in the microstructure. For a brief overview showing the scope of conven: tional P/M metericls, four tables are given FERROUS STRUCTURAL PARTS Material Density glem? Tensile Strength? ‘Comments 10°psi (MPa) Carbon Steel (-0008 69 540970 « ‘Chen con ele OBkce *+* ANNE 25 5501 + Copper Steel- £C-0208 7 solaioe Good stored strancth ZAC. 08%ce mE Sn 85 [5901 = Nickel Steel-FX.0205 69 soca Good Keo rected FANOStce mE SAAR 120 18201 + strength poet ene Infitrated Steel - Fx-1008 73 87 woos Good srenath 105C0 08%ee Ram ERRORS |20 (230) ++ closed flora poresy Low Alloy Steel, Fl-aé05 695 5 4ool* Good horde, prealloyed O54 cc eonRscresrer m= 1301900 conssency net Nie" recent, Low alloy steel, Fin-4205 705 731800) ocd ser Ni'Mo= 1SEN, O58 ce aa SRNR 150110301 ¥# bah sere and bot treted Diffusion Fo.040s, 7.05 10317101 Very geod Aleyed sete 05% ANNE 140970) $¢ —critore skonghh iC Mo Sinter Fic-4608 700 \o0(690) High hardness ond stenath Hardened Steel 2% Cu 08% ce frm stering Ni Me prealoy - Sloinloss steels - 55-434 N2 ELON 60 (410) Good emen restnes, 234 sonss sppecronce SS.316N2 6s souioie 316 sans SS-410%T ES NNN 10 1720)» 410torles + Relerence: MPF Standard 35, Material Stondords For PIM Stet » Aesntered ‘Host Weoted ‘6 Combined carbon tol Pols. Srenath and denay are owen os typical vals, SOFT MAGNETIC PARTS Material Dens ‘Mag. Induction Coercive Force = kor T Oe. Alm ron, lower density 66 100 10 2000 20 160 Iron, high densty| 72 130 3 3500 7 136 Phosphorous iron O458P 7.1 120 12 3500 15 120 Phosphorous iron O.ASRP 72 130 13 000 12 % Silicon ron 3% Si 72 130 13 6000 10 80 Nickel iron 5O% Ni 74 120 12 20000 0.25 2 410 Stainless Steel 71 105 os 1750 20 140. "Magione Feld 15 cero NONFERROUS PARTS Material Usage and Characteristics Copper Electrical parts Bross Electrical ports. Applications requiring goed corrosion resistance. appearance and ductility CZ-1000, 10% zine CZ-3000, 30% zine Nickel siver CNZ-1818, 18% nickel, 18% zine Aluminuen ello Ticniam tensile strength 34 x 10%) Improved corrosion resistance, toughness Good sirengthinass rato. cortasion resstonce: ‘SELF-LUBRICATING BEARINGS tensile strength 20 X 103 psi 140 MPa} MPo| ® 7.9 gfem*, tensle strength 34 x 1D%psi (230 MPa) Good corrosion resstonce, lightweight, good electri ical and thermal conductivity Material Density, glem? Oil Content, % Vel. K Strength, psi (MPa) ~CT-1000 60-64 24 19000 {130) CIG-1001 64-68 7 2300001160) Diluted Bronze FCTG-3604 60-64 7 22000150) lron Graphite FG-0303 56-60 18 10.000 70) 10 engineering properties A wide range of powder metallurgy moterials, meet- ing the design requirements of particular applications ‘fe avalble. The following property descriptions include those related to density, mechanical characteris tics and physical properties, Density—Most properties of «PIM part are closely reloted to its final density. This densiy is the mass per Unit volume of the part expressed in grams per cubic centimeter {gfem']. Normally, the density of structural pats is reported on a dry unimpregnated basis, while the density of bearings is reported on « fully oil impreg- nated basis, Densiy is most commonly determined using the method given in ANPIF Standarel 42** Density is also expressed os relative density, which is defined os the ratio of a PIM par's density to thot of tts pore-free equivalent. In practice, P/M parts less than 75% of relative density are considered to be low dens ty: those above 9OR ore high density: and those in between these two ranges are considered as medium densiy. In general, sruclural ports have relative densi- ties ranging from 80% to cbove 95%. Forgings and HP products often exceed 99% Many sell-lubricating bear- ings have relative densities of the order of 75% and fi ter parts usualy have relative densities of SO% Porosity—Porost isthe percentage of void volume in © part. Iris the converse of densily. A part which has 85% relative density will hove 15% porosity. Porosity in PIM ports can be present asa nelwork of infercon- nected pores that extend fo the surface like @ sponge oF a5 a number of closed holes within the part Interconnected poresly is important to the performance of self-kbricating bearings and is port of the specifica tion for these types of materials Porosity is @ controllable function of the raw material cond processing techniques. Parts can be procuced either with uniform porosity or with variations in porosity land density] from one section to another to provide dierent properties. For exomple, porls con be made self-lubricating in one aree and dense and strong in other areas. Permeability—The obiliy to poss fluids oF gas os, for example, in filers is cnother unique property thal can be designed ino P/M products. Depending on the forming and sintering techniques, PIM part can pro- ‘valable Fam the Nica Pow nas FadoraionPIRCSoN New lore, CB540-6002 (rel 09-452.7700 fox 609-987-8523 espns! Ema lamers vide permedbilty canging from highly restricted fo open flow. The port can be produced with permeabilties which will separate materials selectively; cffuse the flow of gases or lquids: regulate flow or pressure drop in supply lines: or act os flame arrestors by cooling goses below combustion temperatures. iters can be produced in olmost any configuration, including sheets nd tubes MECHANICAL PROPERTIES As with wrought and cost metals, chemical compost tion of PIM\ parts srongly influences the mechanical properties In P/M parts, however, properties ore dependent on additional factors, such as: density; part- cle size: pore size, shape and distribution; and extent of sintering For this reason, mechanical property data are often given in graphs showing the relationship belween the property and the density or percent of relate clnsiy) The graphs or chorts shown, Figures 10, Tl & 12. repre- sent typical volues ond the rend of properties versus densily from test specimens confarming to chemical and density requirements found in MPIF Standard 35, ‘Materials Stondords for P/M Structural Parts [refer to this standard for a complete ising of mechanical properties). Test data obtained en standard specimens do not necessarily accurately represent the performance of an ccclucl port. Test specimen dato should be considered only as an approximate evaluation of part performance ‘More commonly, proof tests on actual parts are used in test configurations mutually agreed upon by users ond manufacturers Strength Properties-Figure 10 shows ultimate tensile ‘ond yield strengths of a 2% nickel and O.B% carbon, pressed and sintered P/M steel as a function of density Yield sirength, generally 62 to 98% of ultimate strength, is closer to the tensile strength than with wrought met- ols Also, the yield strength of many P/M materials, por- ticularly stainless steels, may be higher than the wrought forms. Figute TI shows impact eneray of two P/M nickel steels 18.0 function of density, with impact energy rising signif cantly at higher densities ond lower carbon contents Duetility-Ducilty, the amount af plastic deformation prior to tensile fracture, is relatively lowe in PIM materi- ‘ls, chiefly due to the presence of pores Duectilly as o function of densty is ilusrated in Figure 12. Elongation 6s 70 78 Density, gfem® strength and 0.2% yield point 0208 (2% Ni 0.8% C),as-Sintored Tensile and yield strength vs density. X-= FN-0205 (2% Ni, 0.5% C) ‘= EN.0208 (2% Ni 0.8% C) 40 35; 0 20 15 10 40 5 20| 40 7 30 20 es 70 74 Density, giem? Unnotched Charpy impact Energy as Sintored, Nick Stools Charpy impoct energy vs desnity Figure 11 | FN-0205, (2% Ni, 0.5% ) Figure 12 - Elongation vs density is generally less than 10% for ferrous materials. For ‘some P/M brasses and stainless steels, however, elon- gations range from 15 to 25%. Ductility of most P/M. moteriols can be increased considerably by hot or cold repressing followed by resintering. Hardness (Apparent)-Because of differences in structure, gross indentation hardness values of wrought metals and P/M ports cannat be compared directly. Hardness of o P/M part, when obtained using a stan- dard tester and scale, is referred to es “apparent hard- ness’, combination of the powder particle hardness ‘ond porosity [See MPIF Standard 43). Figure 13 shows how on indenter can compress the suface between por- ticles or displace powder particles in low-denstly parts Wrought Stee! PM Material Figure 13 - Hordness indenter penetrates deeper in P/M. material becouse of lawer densty Particle Hardness—Sometimes called metrix hardiness, It ts measured by a microhardness test, such as Knoop cor Vickers. Here, the purpose Is fo measure actual metal hardness, unaffected by any porosity. Microhardness tests and evaluation of heat treated cose depths ore discussed in detail in MPIF Standards 51 and 52. PHYSICAL PROPERTIES Corrosion Resistance-Porosty in PIN\ parts signi= contly affects corrosion resistance due to possible eeniropmen! of corrosive media. Higher density improves Corrosion resistance, as it does most other properties. Stainless steel PIM parts have relatively good corrosion resistence in the atmosphere and in weak acids Nonferrous P/M materials have corrosion-resistont properties similar to the wraught forms Surface FinishExcellent surface finish isan inherent feature of P/M parts. The overall smoothness and sur- face reflectivity depend on density, tool finish ond sec- ‘ondary operations. Conventional proflometer readings RMS) take info account the peoks and valleys of machined surfaces, while P/M\ parls have « series of very smooth surfaces which ore interrupted with cores of varying sizes, A chisel point stylus should be subsiut eed for the more typical radius stylus when mecsuring the surface finish of P/M parts with a profilometer Figure 14). Effective surface finish of PIM parts com pares favorably with ground or ground-and-polished Chisel Stylus For Surface Measurement ‘The stylus is chisel shaped and has {a standard radius onthe edge 1.27 mm (0.080 in) wige so that itwit not crop Inothe porosity of the PIM surface And give 8 false reading by mea- uring he eaves. a Sitee Etfect Of Chisel And Cone Styli On ‘An As-Sized P/M Surface, Figure 14 - Surface finish measurement using o chisel siyhis WL 12 surfaces of wrought and cost components. Surface smoothness con be further improved by secondary operations such as repressing, honing, burishing, or grinding Sound Damping-The porous nature of P/M ports provides good sound damping. Ringing. common with wrought steel gears and other parts. is reduced due to the controllable density in P/M products, This is on important benefit in business machines, air-conditioning blowers, and similar products where quiet operation is, highly desirable, Domping characteristics ean be further improved by inillrtion or impregnation with sound domping materials. The controllable density of P/M parts is also used to dissisate and muffle noise of air- driven tools Hardenability—The depth of hardening achievable in steel alloys is known as hardenablty. The higher the hardenabilty rating the more hordenoble the steel. Hardenabilty dota is provided in MPIF Standard 35 Material Stondards for PIM Structural Parts** * guolble Won fe Mol Powder dries Federaon rca Now Jey, OBS40-6682 ek 009-852-7700, fox 609-487-8529 vwinanatarg | Eel: fmt og SSC Im Nt The PIM process, smllr fo olher port fabrication methods, hes its own set of design guidelines for pro- ducing well engineered, economical products. The por Ticular ospects and requirements of P/M production should be considered. Design advantages then can be gained that ore unique to the P/M process, and is limi- fotions wil have been taken into account. Designing for powder metallurgy recuires close coop- eration between the port user. or buyer, ond the pro~ ducer especially in the initial design stoges. The P/M part should be designed in the context of the whale cssembly, with the porls manufacturer being informed throughout the entire process. An improved, lower-cost PIN\ pat often can be achieved through small changes in on assembly, Frequently, early designer-manufacturer inleraction results in an expansion of the PIM concept thot can simply the design and reduce cos. For greater depth and detail, designers are encour- ‘ged to sludy the MPIF Powder Metallurgy Design ‘Manual TOOLING CONSIDERATIONS The PIM part design and the complexity of tooling used to produce it are closely related Two major factors in the compacting operation infly- lence or control part design: the flow behavior of mets! powders and the pressing action, Metal powders do rot flow hydraulically becouse of friction between the particles and the dies. The design, therefore, should ensure adequate powder distribution within the die cavity to cllow satisfactory compaction. Because metal powders also have limited lateral flaw, there are some limitotions on the contours that con be produced, SIZES AND SHAPES Press Capacity Round Part, (tons) Max. Diameter (in) =30 15 [410 MPol compaction 25 103 (262 mm} 200 291739 mm) 500, 40111171 en Part Size- Wider parts cre possible if perpendiculor dimensions are reduced so that the moximum projected trea is not exceeded. At higher press tonnages, 40 tsi (560 MPa), for exomple, the projected diefpunch crea will shrink, ond a 200 ton press will have @ maximum round die diameter of 252 in (640 mm), + Since compaction occurs in the vertical direction using only top and bottom motions, part lengths in the pressing direction ore limited + Compression ratio, the ratlo of the height of the loose powder filling the die 4o that of the compact- ed port, also tends to limit vertical par! lengths Shapes + Shapes with uniform dimensions in the pressing direction are easiest to produce and eject from the press + Cams, gears and sprockels ore ready made. + Thin walls ond projections may require fragile tools: consider corefuly * Face forms on upper or lower punches can provide bosses, pads, lettering, countersinks, etc. Multi-level Shapes + More complex, multi-motion tooling is required to maintain consistent density throughout parts with more than one level. + Both mechanical and hydraulic presses are aveil- able for making pars with five or more levels + Ports weighing © few grams to 26 pounds |118 ka) or more ore possible [Figure 15) Figure 15 - Variety of P/M parts 7 avalale hon he Maal Powder Fis Federation, Wnevion Now Jersey 08540:6802/ fel: 609-4527700, for 609-987-8523 vwerapg Ema: Foon ong 13, 14 DESIGN DETAILS Holes + Holes in the pressing direction can be round D-shaped, include keyways, splines, etc. Tooling members which create holes are called core rods + The core rods must remain straight andl not buckle dining compaction, or ejection ond dimensional problems may result. * Lightening holes ore frequently added to large parts to reduce projected pressing oreo, thus making ports easier to press and lower in weight '* Blind holes, blind steps in holes and tapered holes core recdlly produced + Side holes have to be produced offer o sintering ‘operation, usually by machining. Wall Thickness + Die ils clkimportant; do not mke walls thinner than 0.060 inch |1.52 mm} as @ general rule. * Long, thin walls result in fragile tooling and parts with endencies loward variations in density ‘+ Where the ratio of length-to-wall thickness is as high os 8 to | or more, special precautions must be taken to achieve uniform fill, and variations in densi ty ae unavoidable. Flatness + Total measured flatness depends on port thickness cond surface area + Thin ports tend to distort more than thick parts cur- ing sintering or heat treatment + Repressing improves flatness. + Projection bosses are easier to bring to flat than entire face areas Tapers and Drafts—Draft is generally not required or desired on sides of parts. While draft on outer sections for ejection is sometimes helpful it demands careful tim- ing of the tools and slower production rates, Fillets and Radit~Generous fillet rad are most desirable: + Tooling with such fillets is more economical, longer sting + Ports mode with generous fllels are made more ceosily ond more quickly + Parts made with fillets have grecter structural integrity Figure 16) ‘Chamfers and Bevels—Chomfers rather thon rock. ‘ore necessary on part edges to prevent burring. For ‘example, on « bushing (Figure 17], 0 30-45) charnfer cond 0.005 to OOIS inch (0.13 to 0.38 mm} Flot to eliminate feather edges are the preferred procice. Feather Edges ++ Original Design GS ¢ Avoid narcow, deep spines on tne part. Proterred Design fr =0z0 ‘A oundes corner gives batter powder tow in die and gives part increased ‘strength anc eliminates stress ‘sors in tools ana pacts, lOlo Rounded corners permit uniform powder flow in the die. Figure 16 Figure 17 - Chomfers are preferred on port edges Figure 18 - Chomfers in clearance Figure 19 - Countersink in clecrance, Large ongle chamfers may be produced by bevels in dies or core rods (Figure 18). Production rates would be slowed with such looling because of the need for cou- tion in preventing dle-fil and between-tool powder wedging problems. Countersinks—A countersink is @ chomfer around hole far a screw or bolt head. When the countersink fs formed by @ punch, « 0010 inch (0.25 mim) nominal flat is essential for avoiding sharp, fragile edges on the punch Figure 19), Flanges—A comparatively small flange, step, or over- hang con often be produced by machining a shelf or step in the dia, Too large a flange causes ejection diffi- cules Bottom flange edge ond juncture radi should be generous Bosses~Boss forming cavities may be located in punch tools. Cowties may not be too deep in ration to pert height (5% less] and drat angles should be at least 12° per side to avoid sticking af the compacted boss to the punch. Hubs—Hubs, which are complementary part sections to gears, sprockets, or cams, can be readily produced by the PIM process. Remember to include © generous radius between hub and flange section, and fo moxi- mize space between hub O.D. and geor or sprocket root diameters Studs—While studs with dratted sides can be made lke bosses, sometimes no draft is alowed or stud heigh!-to-diometer ratio is relatively large. In that case. tooling with additional punches is required. Always consider the frogiliy of the green compact prior io sintering Slots and Grooves—Grooves can be pressed into etther end of o port from projections on the punch face ‘with the following general imitations [Figute 20 + Curved or semicircular grooves to @ maximum depth of 20% of overall port lenath. + Rectangular grooves to o maximum depth of 15% of ‘overall part length. provided thot surfaces parallel to the pressing direction have up to 12° draft ond al comers are radiused. Figure 20 - Semiciscular and rectangular grooves con be pressed from o projection on the punch faces into either tend of the component provided that the guidelines for raft; height and radtus are Followed. Deep. narrow slots and grooves require fragile tool members and should be avaided, Undercuts + Undercuts on the horizontal plane Iperpendicular to pressing direction! cannot be made since they pre- vvent part ejection from the die. + Annular grooves may be machined os @ secondory ‘operation (Figure 21) + On a part such as shown in Figure 22, where @ [uncture undercut is needed fo allow fi-up too dead comer, an aliemotive approach is shown in Figure 23. Tolerances The tolerances which can be held in the PIM pracess compare favorably with other parts fabricating process: 5, Economically, olerances no closer than necessary should be specified. The following table illistrates toler tance characteristics of competitive near-net-shope forming methods: (Die dimensions, unless stated! other wise) Figure 21- Anoular grooves cannot be molded. They can be machined. 15 16 nn | Cannot Do Figure 22 - Undercuts conrot be formed except with secondary machining, Forming Typical Critical Method Dimensional Dimensional Tolerances (inJin)_ Tolerances (in.in) Pi 0002 70001 PIM (Secondary Forming) +0001 0.0005 Cold Formed 20010 0002 Hot Extrusion 20010 10003 Fine Blonking {Single Lovell 010005 20.0002 Die Casing ‘Mognesium, Aluminum «0002 200015 Zine 20.0025 20001 Hot Closed Die Forging Conventional 2002 10015 Pith, perpendiclor to press ons 200032 so0o2s" PIM, poral to press xis 10010 00005 Die patagine Wlaences wl be Fro fhe above * Future quenched fora. raha clang kr quenching ding he rear! reste ce hot engig con hold ean ihr toons Producer concemns in holding P/M tolerances: |. Whot is the relationship between sintering condi tions end the metal powder used? 2. What is the lorgest dimension that must be held? 3, What tool wear will this metal powder couse when compacting to the chosen green density? Thee hes een 4, Assuming symmetrical part shape around an ID. what run-out tolerance is required? 5. If ferrous parts, will hey be heat treated? © Ave tolerances demanding enough to requite sizing? Prototypes Three prototyping oplions are commonly used 1. Machine from a PIMA blank. PIMA blanks, 0s pressed and sinered or infitroted ore ovailable from PIM parts manufacturers. Machining and fin- Proterred Figure 23. Con be formed ducing compacting, ishing steps in fabricating the protatype part from the blonk should maintain the surface finish and porosity typical of the P/M part, The blank will be Uniform in density and may not cccurctely repro duce the density variation found in mult-level ports. Evaluating several density levels is suggested 2, Press from a set of tools that contain certain defined features (such as on ID spinel, sinter, and then machine the remaining features lsuch as gear teeth and a hub). 3. Press the entre part from a set of tools and sinter. This option is viable when the part configuration is relatively simple or where a large number of proto- types is required. This option is the most costly ond time consuming, but most reliable. DESIGN OF TYPICAL PARTS Gears are well sited to PIM production + Carbide dies provide long life and accuracy + Residual port porosity tends to dampen sound. + PIM gears can be made with blind comers, thus eliminating the need for undercut relief + PIM gears con be combined with other contigura- tions such os coms, ratchets, ether gears, and vari- ous components + Helical gears are possible: copper inlitration is sometimes used to improve teeth densities. + Since tooth shope is not © problem, true involule gecrt forms are easier to produce than by other fabrication methods When designing PM gears: + Note that the center hole location relative to the gear shape is affected by the running tolerances of the various tool members. This makes it more dificult to hold the close TI's obtainable with orbor cul gears, and hubs or pinions that increase the number of concenitic tool members increase the TIR toler- ‘once needed. TI's can be reduced by grinding sgecr [D's true to the gear pitch diometer. + Asthe AGMA closs of gear increases, s0 does the: cost of the gear because of the secondary operc: tions required to meet the tighter tolerances + To avoid having very thin teal members, gear hubs CF pinions should be located as far as possible from gear root diameters. See Figure 24 Coms are also well suited to P/M: + Process provides excellent surface finish ond port-to- part consistency. + The natural finish of self-lubricating P/M com will ‘often outwear a ground cam surface * For radial coms, the com shape fs formed in the die; for face cams the shape is formed in the punch foces. Assemblies + Two or more P/M parts offen can be joined to form © unit that is difficult, if not impossible, to make os @ single structure + Capitalizing on PIM flexblity, ts feosble to moke ossemblies of very different materials: a bronze bearing in o ferrous structural part, for example, or heat-treated part with « non-heot-treoted par. + PiMA ports can be joined by conventional methods such as staking, press-fiting, brazing, soldering, welding, epoxying. riveting, bolting, and olso by sin- tering together materials of appropriately different size chonge characteristics. + Copper infitration during sintering can be used to bond steel parts. Bearings + Bearings ore @ natural product for P/M because of its conttolled porosity and the resulting self-con tained lubrication Plain beorings, flanged bearings, soherical beorings ‘and thrust washers ore commonly produced, + The operating environment should be corefully con- sidered: external lubrication, cooling, hardened or chromium-ploted shafts fend fo increase permissible loads. Repeated stor-stop operation, oscilatory or reciprocating mation, high speeds, shock loads and temperature extremes tend to decrease permissible loads For detailed information on permissible loads, press fits ond tolerances, see the engineering section in PIF Stondard 35, Materials Standards for PIM SelF-Lubricating Bearings. No Figure 24 - Hubs should be locoted ax for as possible from gear’ reot diameter 17 18 The powder metallurgy process hos expanded into the production of near-fully dense materials and parts, wth residual porosity offen being less than 1%. These processes use diflerent compacting methods and may involve greater emphasis on high alloy materials and enhanced sintering techniques. Some of the specialized processes and alloys involved in this new and growing technology follow. POWDER FORGING Powder metaluray steel components with wrought properties are currently in moss production. One popu: lor material is type 4600 steel with varying carbon lev els and conventional heat-treatment when necessary. Several manufacturers within the PIN\ industry produce millions of powder forged [P/F) paris annually, primarily for automotive original equipment. The basic process common to most powder forged systems is to manufacture o “green” compact called o “preform, sinter and then resirike/forge the “preform” to the required final density Two PIF ports produced are shown in Figures 25 and 2; Figure 27 illustrates the strength and ductility advantages of powder forged 4640, ISOSTATIC PRESSING: isostatic pressing generally is used fo produce lorge PIN\ parts to near-net sizes and shapes of varied com plexi. Unike conventional press compaction, isostatic pressing Is performed in o pressurized fluid such as cl gos, or water. A flexible membrane or hermetic contain- ‘er surrounds the powder mass and provides a pressure differential between its contents and the pressurizing medium. The concept is shown schematically in Figure 28. A typical product made by this process is illustrated in Figure 29. Among the benefits of isostatic pressing are: + Complex shape capability. '* Minimized expensive powder input. + Applicability to dificul-lo-compact materials, + Uniform density and properties. Cold Isostatic Pressing (CIP)—Cold or room tempero~ ture compaction is carried out in liquid systems at pres- sure commonly reaching 60,000 psi (414 MPa). Metal powder is packed into complex-shaped rubber or elas- tomeric molds before compacting. Free of die frictional Figure 25 Powder forged (P/F) automotive connecting rods. Figure 26 - Ho! forged inner race, 40 Duet Figure 27 - Tensile properties vs relative densily Isostalic Pressure ‘Shape of Completed Part Figure 28 - \sestatic compacting. forces, the powder compact reaches a higher ond ‘mote uniform density than would be obtained using cold die compaction ot the some pressure. Powders with spherical or rounded particles ore not cold com- pacted becouse of their inabilly 10 form a sound or strong green body. Sintering con be performed by any of the conventional processes Hot Isostatic Pressing (HIP)—Hot isostatic processing is performed in a gaseous (inert argon or helium) ctmos- phere contained within the pressure vessel; usually, the goseous atmosphere os well as the part to be pressed are heated by 0 furnace within the vessel ‘Common pressure levels extend upward to 15,000 psi (100 Mo}, combined with temperatures to about 23007 (1250'C), Processing volumes currently reach to Sift (15 m) diameter by 10 ft. (3.0 ml long, Higher Figure 29 - Port made via cold isostatic compacting. pressures ond temperatures are in use but with consid erably reduced work volumes, The powder to be HiPed is hermetically sealed. usual- ly within a metal or gloss container or envelope which deforms plastically at elevated temperatures. Prior to seoling, the container Is evacuated fo eliminate residual ‘gases in the powder mass, In contrast to the cold isostatic pressing process, the hot process can readily employ powders with spherical ‘or non-interlocking particles, The powder is simply poured in and vibration packed into a container of desired shape, the powder mass is then simultaneously compacted and sintered during the HIP process. Denstication to near full densiy is achievable with most materials The resulting mechanical properties ore equivalent to wrought parts in a similar condition. In. some moterias, the properties of the HIP product are superior because of reduced anisotropy Depending on the material being compacted, removal of the HIP container is achieved by chemical leaching, machining or other mechanical methods. As with cold isostatic pressing. mandrels con form internal contours, swith porting agents generally used fo prevent bonding Dilferential thermal contraction eases mandrel removal for simple, regular shapes. Mandrels with locking-in features ore removable by methods used for confainer removal ‘METAL INJECTION MOLDING (MIM) ‘Metal injection molding offers ¢ manufacturing capa bilty for producing complex shaped parts in large quantities. The process utlizes fne metal powders, typi- cally less than 20 micrometers, which axe infimotely rmixed with various thermoplastics, waxes and other ingredients In contrast fo conventional powder metol lurgy. these polymeric binder materials may comprise os much os 40 volume percent of the mture. The resulting feedstock is granulated and can then be fed into a conventional injection molding machine. Multiple cavity tooling is commonly employed. Mest, but not cll, ofthe binder is then removed from the molded [green| com pponents by thermal or solvent processing, or a combi- raalion of both, The exact method chosen is dependent Upon the binders used for molaing and the cross sec- ions of the part. Following binder removal, parts ore sintered in ether olmasphere or vacuum, during which the remaining traces of binder are removed. Sintering temperatures are usually in excess of 2300 (126°C) Final relative densities are generally greater than 96% with inter-connected porosity less than 0.2% Parts weighing up to 250 grams are commonly pro= duced (Figures 30 ond 31}, Cross sections ore generally less than 0.250 inches 16.35 mm). However parts are not restricted fo this combination of massicross section 19 20 Figure 31 Pivotal laproscopic surgical scissors with heli cal gear ‘ond lorger parts are in production. Processing is nor- mally to « tolerance of #0.3-0.5%, although specific dimensions may be held as close os 201%, Due to the use of fine powders and! low porosity, MIM products have typical surfoce finishes of 32 RAAS (0.8 micro meters). Common secandry operations, such os plating oF hect irecting, are offen employed Since intercon nected porosty isso lew. parts do not have to be resin impregnated for plating and close contral over case depth is possible in carburizing The injection molding process eliminates the restriction of straight sided components required when parts are injected from o dle, ond offers opportinities for external undercuts end threads. A wide variety of alloys can be processed. including alloy steels, stainless steels soft mognetic clloys and tungsten carbide. Material stan- dards are avciloble in Stondord 35, Materials Standords for Metal Injection Molded Ports, published by MPIE Process details + Powder sizes are fine, usually less thon 20 micrometers + Low injection pressure, generally less than 10.000 psi [70 MP) + low mokling temperature, approxmotely 300 (47), + Shrinkage, molded part to finished size. is typically 20% + Final part densities are usually greater than 96% of the pore-fee densly + Ductlty is exceptionally high with elongation values of 30% o higher SPRAY FORMING Spray forming is © process used to produce semi-fin- ished mill products in the form of billets, tubes and sheet/plate. Unlike conventional PIM, MIM. or PIF pro cessing, spray forming is not used to fobricate individval net shape components. The process consists of sequen ficl stages of liguid metal atomization and droplet con- solidation to produce @ necr-net shape product. The os- sproyed material is close to full density with « fin, equiaxed grain structure. Mechanical properties mest or exceed those of ingot processed alloys. The process is known for its high rate of metal depostion, typically in the range 0.5-50 pound/second. Commercial pro= cessing includes alloy steels, stainless steels, tool steels, superalloys, aluminum and copper base olloys. An example of a superalloy spray formed tube is shown in Figure 32. Figure 32 - Spray tomized tubes of IN625, ‘SPECIALTY MATERIALS ‘SUPERALLOYS The use of high alloy P/M materials, notably superol loys, is most common in the production of near-net shapes ond forging preforms for aircraft lrbine engines Economic benefis have been the prime driving force in the use of PIMA for the manufacture of these high cost alloys. These superalloys are processed from highly-con- trolled. metalluraically clean powders produced by inert ‘905 otomization methods that minimize surface oxida tion during processing. After powder screening ond cleaning the powder is compacted using hot isostatic processing. Thermomechemical processing may be per formed to enhance mechanical properties or microstruc ture, Hol extrusion of the ctomized powder is an cller- rote consclidation method, PIN\ processing offers the advantages of « homoge- neous microsiucture and near-net shape configuration llower cost) As @ result ever 10,000,000 pounds of PIM\ superalloy components are new flying in both mile tory ond commercial aircraft engines. TOOL STEELS High performance tool steels and high speed steels are produced In mill shapes using P/M process tech- niques, Advantages for PIM tools steels + Finer grain structures + Improved homogeneity and distribution of sec: ondary and carbide phases + Elimination of secondary stringers. + Less distortion in heot treatment. + Improved grindabitty. + Greater wear resistance + Improved toughness and fracture strength. Hot isostatic pressing (HIP) hos also been used in the commercial production of P/M tool steels to near-net tool shapes. such as hobs ond shoper cutters. Tool steel parts con olso be made by conventional cold compact- ing end high temperature sintering REFRACTORY METALS The refractory metals, alloys ond composites are pro- duced using non-fusion, powder metallurgy techniques. Products include tungsten lamp filaments, tantalum Capacitors, molybdenum heating elements, tungsten- copper composite heat sinks, ond tungsten-siver com- posite circuit breaker contacts. The tungsten-based “heavy alloys’ llungsten plus liquid phase sintering ids) cre used for radiation absorption, gyroscope weights ‘and kinetic energy penetrators. ‘BERYLLIUM The PIM processing of beryllium starts with cold iso- stotic pressing followed by hot pressing or a hot forging €or extrusion step. Sometimes hot isostatic pressing fs substituted for the hot pressing step. Ove to its light ‘weight beryllum is used mainly for cirraft and cero- space products, TITANIUM The use of P/M titanium metal and its alloys continues to inctease since P/M provides « near-net shape prod- ct os compared fo more expensive cast, forged ond machined processing, Depending on the application ‘and production quantities titanium P/M products are processed either by conventional press ond sinter tach: niques or hot isostatic pressing. The latier exceeds the minimum wrought alloy specifications, Product applica tions include aerospace/aircrafi components, sporting goods, chemical processing equipment and biomedical systems METAL MATRIX COMPOSITIONS (MMC) Powder metal processing has been successtully applied to a verity of metal matrix composites, the ‘most populer being cluminum-silicon corbide particulate reinforced materials. These composites offer high stif- ness (modulus), reduced thermal coeflicient of expansion with litle offect on thermal conductivity or density These Al-SiC composites are being used for their struc- tural sifness and strength in aircraft and sporting good products, os well os electronic thermal management applications as heat sinks. Manufacturing techniques. require cold isostatic pressing fo consolidate the pow- ders followed by hot extrusion or hot forging to full density 2 22 PIM parts are used in many products such as automo- biles and trucks, home eppliances. power tools ond hardware, riding lawn mowers and farmiof-rood equipment, business machines and sporting goods The overage North American passenger car contains ‘mote than 30 pounds (186 kgl of PIM, parts, which opercie in the engine, transmission, slgering, brake ond suspension systems. Automotive companies project P/M part usage to approach 50 pounds (227 kg in the near future Power transmissions of all types are “home” to P/M. Firearms have long been o fertile matket. not exclusively in the group of paris \sear notch, trigger hammer, etc which octualy tes the piece, Lock parts in both bross and stainless steel materials are popular. Pollution con- Figure 33 - Pi! gor's and products find mony uses EIEN TE TCS trol systems, exhaust systems andl ant-dock broking com ponents consume milions of parts annually Couplings, electrical relays with soft magnetic parts, speed controls, printing hardware for computer systems all contribute to the demand for P/M. Surgical implants cond sophisticated medicol instruments ore a growing ‘market. Tools of all kinds, including fooling stock for Compaction of P/M, continue to increase in use. Whenever machining makes up « large port of prod- Uct cost, P/M should be considered, within reasonable sizes, of course. For actual cose studies of successful applications of PIM, the reader is referred to the MPIF "Powder ‘Metallurgy Design Manual The importance of discussing the port application with con MPIF member P/M parts manulecturer can not be overstated. Its the best way to take advantage of the lotest techniques in ¢ ropidly growing industry, PIM is 0 high volume industry which can provide meaningful cost reductions combined with high quality. When requesting ¢ quotation, occurale part perfor mance specifications must be provided. Refer to the ‘Metal Powder Industries Federation Stondard 35, ‘Materials Standards for PIM Structural Pars, for prop- erties and specifications. In describing a part, stress function end enticl requirements for satisfactory ser- vice. For optimum results and efficiencies give the PIMA parts manufacturer the widest possbe latitude in speci fying material, design, physical charactoristics, dimen- sional tolerances, eic. Widely diflering costs may result from varying quality levels, change in tolerances or design, oF failure to specify minimum properties. There may be more than one MPIF material that can satisy’ the requirements Typical information needed includes the following: 1. Order quantities which include intial needs ond a future demand forecast, This enables the mos! eco- nomial approach to cos's, manufacturing integra- tion and delivery, 2. Detoiled crawings of the port and any assembly ckawings. Actual samples or prototypes would be helpful. Transmit any information such as knowledge (of materials that have worked well in the application. 3. Can port design be modified without affecting function? If so, where?’ 4, Wil the PIM port replace one currently in produc tion, oF is this & new application? Is the application miltory, aerospace, medical, ee? 5. Actual service conditions: heat, moisture, impact corrosiveness, el. 6, Necessary physical, mechanical, corrosion resis: tance or special properties (lensile, elongation, hardhess, flatness, conductivity, impact eneray, fatigue sirength, leak tightness, et] 7. The finish required {plating, oxide coating, surface fish). 8 If ony machining or secondary operations are ‘required, will they be performed by the PIM supplier? 9. For bearings: load, shalt material ond finish, speed, service conditions and diameter should be noted. For gears, specific dota ore required: a] number of teeth, b} diametral pitch, <) pressure angle, d) measure- how to specify p/m parts ment over wires | tooth thickness, fl toot and tip radius. g) helix angle and hand, h) AGMA quality class il mating geor dota and nominal center distonce, Inspection requirements-runout, pitch, protle and lead tolerance, or footh-to-teoth, lotal composite tolerance end testing radies. Tools for each PIM part are custom designed and developed speciically for that part, The expense of the fooling may justly the more economicol approach of initially testing prototypes. The quality level end inspection techniques required contribute fo the cost of @ P/M part, Programs such as SPC and ISO 9000, for example, should be thoroughly discussed and specified by the purchaser ond manulac- turer prior to submission of a quotation Fort producers are anxious fo keep current of potential PIM customers well informed obout their technology

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