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50 views46 pages

017 DLT 5190.4-2004 The Code of Construction Part 4 Chemistry Fo

Uploaded by

Omar Adil
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© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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ICS 27.

100
P 61
Registration No.: 1349-2004

ELECTRIC POWER INDUSTRIAL STANDARD

OF THE PEOPLE'S REPUBLIC OF CHINA

P DL/T 5190.4-2004
Substitute DLJ 58-1981

The Code of Erecion and Acceptance of

Electric Power Construction

Part 4: Chemistry for Fossil fuel Power Plant

Et! n~ 1i:MB I& ij~~A~tt*~JU m


~4f$*: Et!rl-t~

Issued on: March 9,2004 Implememted on: June 1, 2004


Issued by: National Development and Reform Commission of the People's Republic of China
NOTICE

This code is written in Chinese and English. The Chinese text shall be taken as the ruling one
in the event of any inconsistency between the Chinese text and the English text.

~
I
-~-------- - -

Contents
Preface 11
I Scope I
2 Normative Cited Documents 2
3 General 3
4 Raw Water Pretreatment 6
5 Boiler Make-up Water Treatment 9
6 Membrane Treatment Facilities IJ
7 Condensation Water Treatment. 13
8 Sample and Dosing System 14
9 Circulated Cooling Water Treatment 15
10 Tank 17
11 Rotary Machine 18
12 Special Pipes and Valves 22
13 Anti-corrosion Construction Technologies 25
14 Startup and Adjustment of Water Treatment System 28
15 Hydrogen-producing Equipment 32
16 Chemical Cleaning of Heating Equipment and System 35
17 Chemical Supervision during Startup and Test Running of Heating Equipments 36
18 Acceptance of Work 40
Appendix A(Normative AppendixtFiltering Material 41
Preface

This code is revised and compiled on the basis of first edition DLJ 58-1981 according to
assignment of Item 74 in electricity [2000] No. 22 document "Notice on Confirming Standard
System of Electricity Industry in 1999 and Modifying Planning Project" issued by State Economic
and Trade Commission.
This code was firstly issued in October 91h of 1981, and this edition is its first revision.
More than 20 years has been passed since the first issue and implement of this code, and
during this period, Chinese electricity industry has been advancing rapidly: generating sets with
large capacity and high parameters have been placed in service one after another, chemical water
treatment for power plant and hydrogen-producing equipments have been significantly changed,
many new equipments and new processes have been adopted, and some traditional equipments
and processed have been improved and renovated. During this period, many achievements and
construction experiences have been obtained by electricity construction workers and researchers,
which provide important scientific foundations for the revision and compilation of this code.
Main revised contents are as follow:
Adding preface;
Adding range and normative cited documents;
Deleting Chapter 4 "Pretreatment of Condensation Water" in original edition;
Adding section "Condensation Water Treatment";
Adding section "Membrane Treatment Equipments";
Adding section "Sample and Dosing System";
Adding section "Heating Equipment and System Chemical Cleaning";
Adding contents of scale inhibition, corrosion mitigation and make-up water
treatment in section "Circulated Cooling Water";
Renovating contents of "Water and Steam Quality Standard for Newly-built Set
Test Run";
Deleting section "Leakage Test of Equipment System" in initial edition, and
merging its contents into "General";
Deleting most contents in Appendix of initial edition, and only holing the part of
filtration materials;
DLJ 58-1981 wi II be substituted by this code after its implement.
This code is advanced by China Electricity Council (CEC).
This code is administrated and explained by Standardization Technical Committee of Power
Plants Chemistry in Electricity Industry.
Chief drafting units: North China Electric Power Research Institute, Henan Electric Power
Construction and Debugging Institute and Henan NO.1 Electric Power Construction Company.
Major Drafter: Lao Qinan, Wei Zhaohui, Sun Zhaoyong, Mo Ni, Van Liubao

II
1 Scope

This code prescribes technical requirements of chemical supervision during storage,


construction, acceptance, startup and capital construction for water treatment and
hydrogen-producing equipments of thermal power plant.
This code applies to newly-built, expanded, and rebuilt thermal power plant with steam
turbo generator unit capacity equal to or more than 200MW. This code can also be employed as
reference code for newly-built, expanded, and rebuilt thermal power plant with steam turbo
generator unit capacity less than 200MW, as well as wastewater treatment facilities with similar
equipments in this code.
2 Normative Cited Documents

Clauses in the following documents have become clauses of this code through citation of
this code. For those cited documents with date, their following revised parts or revisions are all
unsuitable for this code. However, studies on the application of the latest editions of these
documents are encouraged by signatory parties to this code. The latest editions of those cited
documents without date are all suitable for this code.
GB 2894 Safety Signs
GB 4962 Technical Safety Regulation for Gaseous Hydrogen Use
GB 8978 Integrated Wastewater Discharge Standard
GB50177 Design Code for Hydrogen and Oxygen Station
GB/T 12145 Quality Criterion of Water and Steam for Generating Unit and Steam Power
Equipment
DL414 Technical Guidelines for Environmental Protection in Thermal Power Plant
OLiT 543 Quality Inspection Standard for Water Treatment Equipments Used in Power
Plant
DLlT665 Acceptance Standard of Water and Steam Integrated Sampling and On-line
Analyzing Unit
DLiT 794 Chemical Cleaning Guide for Steam Power Plant
DLiT 855 Code for Maintenance and Safekeeping of Thermal Power Equipment in
Electric Power Construction
OLiT 5007 Code of Erection and Acceptance of Electric Power Construction (welding
section)
DL 5009.1 Safety Operation in Power Engineering Construction (Thermal Power Plant
Part)
DLiT 50 I I Code of Erection and Acceptance of Electric Power Construction (Section of
steam turbine set)
OLiT 5031 Code of Erection and Acceptance of Electric Power Construction (pi ping section)
DLiT 5047 Code of Erection and Acceptance of Electric Power Construction (Section of
steam boiler set)
SO 233 Guideline for Lay-up of Thermal Power Equipment in Thermal Power Plants
SDJ69 The Code of Erection and Acceptance of Electric Power Construction (Section
of architectural engineering)
Workman Protection (87) No. 36 Electrical Safety Regulation for Explosion Hazard Area of
People's Republic of China (Trial)
Pressure Vessels Safety and Technical Supervision Regulation Issued by China State Bureau
of Quality and Technical Supervision (1999) Boiler No. 154

2
3 General

3.1 General Regulations


3.1.1 This code prescribes technical requirements of power plant chemistry for various
equipments during construction and acceptance. For those parts relevant to mechanical installation,
pipe construction, welding process, monitoring meters and procedure control, this code shall be
util izecl in cooperation with corresponding professional technical standards.
3.1.2 Manufacturers of chief equipments shall have manufacturing license issued by state,
province (municipality, or municipality directly under the Central Government]) or relevant
national administrative supervision and management department. Acceptance of equipment
manufacturing quality shall be executed according to currently related national regulations. For
those without regulations, their acceptance shall be carried out according to technical conditions
prescribed in contract.
3.1.3 Constructions of various equipments shall be carried out according to design drawings and
relevant technical documents of their manufactories. When design is required to modify, or
equipment (or material) is substituted, the modification or substitution shall be firstly approved by
design and construction units, then they must pass approval procedure. and design modification
bill or technical documents on substituted equipment or material shall be attached in acceptance
document.
3.1.4 Construction and acceptance of nonstandard equipments not listed in this code shall be
carried out according to contract or referring to relevant regulations, specifications, standards and
design prescriptions. Construction and acceptance technical standards for equipments imported
from abroad shall be fixed according to relevant technical clauses in contract.

3.2 Acceptance and Storage of Equipments and Materials


3.2.1 Supply sheet, specification, technical materials and drawings shall be checked by open
package inspection according to procurement contract. Quantities, specs, package and appearance
quality of equipments and materials shall be checked according to sheet, and open package record
shall be written. [f such problems as rust, frost crack, deterioration, damage or bug appear in
equipments or materials, then relevant units shall mutually analyze reasons, find out
responsibilities and dispose problems timely.
3.2.2 Equipments or materials shall be kept according to DUT 855 and technical documents of
manufactory.
3.2.3 Quality of anti-corrosive coating shall be chiefly inspected during acceptance after
anti-corrosive device is transported to construction site, and "exterior inspection" and "leakage
test" shall be carried out. Relevant parties shall mutually analyze reasons, find out responsibilities,
and dispose problems timely if bug appears.
3.2.4 Special materials and chemical agents used for water treatment and chemical cleaning shall
comply with relevant technical requirements in procurement contract and quality requirements
Iisted in relevant codes. After arrived at construction site, they shall be sampled for inspection, and
properly kept by classification according to requirements.

3
3.3 Cooperation Requirements on Civil Project
3.3.1 Before installation and emplacement of equipments, construction unit shall be jointly with
other parties concerned, such as installation, civil construction and supervision, to check the
following items:
a) Geometrical dimensions, corresponding positions and heights of equipment foundation
shall comply with design requirements;
b) Dimensions and positions of reinforced concrete beam and column, as well as built-in
fitting and reserved holes on equipments foundation shall comply with design requirements;
c) Underlayer shall be set for the foundation of flat bottom water tank, the center of which
shall lean out and be 15mm~20mm higher than the edge.
3.3.2 Reinforced concrete structures related to water treatment shall be checked and accepted
based on regulations of design drawings. Reinforced concrete structures and buildings with
anti-corrosive requirements shall be checked and accepted according to regulations on
anti-corrosive project issued by construction department.
3.3.3 Anti-corrosive coating made in construction site shall be checked by construction unit
layer by later; such bugs as crack, blowups and holes must be eliminated immediately.
Anti-corrosive coating shall be checked and accepted according to regulations on anti-corrosive
project issued by construction department after its construction is finished.
3.3.4 Water filling test shall be carried out for reinforced concrete containers.
3.3.5 Before adjustment and trial running of water treatment equipments, the following work
shall be finished by civil construction:
a) Constructions of indoor and outdoor anti-corrosive floor and channels for water treatment
room as well as neutralization tank shall be finished and passed acceptance. Channels for drainage
and deslagging shall be unblocked with all-ready cover boards, the surface of which shall be flush
with floor;
b) Indoor painting and coating for water treatment room, as well as constructions of floor,
platform, ladder, doors and windows shall be finished according to design requirements;
c) Constructions for facilities in laboratory, such as water supply, drainage, heating,
ventilation, air-conditioning, illumination, electric source and test-bed shall be finished according
to design requirements;
d) Constructions for structures of acid and alkali storage as well as anti-corrosive and
ventilation facilities shall be finished and passed acceptance.
3.3.6 Before adjustment and trial running of hydrogen-producing equipments, the following
work shall be finished by civil construction:
a) Constructions for wan, lightning rod and earth mat shall be finished according to design
requirements and passed acceptance.
b) Constructions for facilities in hydrogen-producing station, such as water supply, drainage,
heating, ventilation, illumination and electric source shall be finished according to design
requirements and passed acceptance.

3.4 Leakage Test for Equipment System


3.4.1 Hydraulic pressure test for system must be carried out to inspect tightness of connections
(welding line, flange or threaded connections) after installation of pipes and equipments are all
finished. Test pressure of steel pipe is 1.25 times of work pressure. Test methods and notice shall

4
be carried Ollt according to relevant regulations in DUT 503 I.
3.4.2 Pressure for hydraulic test of rubber-line, fiberglass reinforced plastic, plastic and other
nonmetal pipes are equal to their rated work pressure. For equipments and pipes with different
rated pressure installed in the same system, hydraulic pressure test for system shall be carried out
under the lowest rated pressure among equipments and pipes.
3.4.3 Desalting water shall be adopted for hydraulic pressure test of stain Jess steel pipe.
3.4.4 Element working pressure hydraulic test shall be carried out for ion exchanger and ion
regenerator in water treatment system to ensure tightness of valves connected to the ion exchanger
or generator after system installation is finished.
3.4.5 Hydraulic pressure test shall be carried out according to relevant regulations of Boiler No.
154 Documents issued by China State Bureau of Quality and Technical Supervision (1999) for
pressure equipments and containers. For those equipments and containers with certification to
prove them passing hydraulic pressure test before leaving factory, this test can be exempted.
Hydraulic pressure test for tightness on connected pipelines shall also be carried out for these
certificated equipments and containers.
3.4.6 Inleakage shall be ensured for open containers by water filling test and welding line by oil
penetration test.
3.4.7 Water filling test shall be carried out for equipment and pontoon in container to ensure
their inleakage.
3.4.8 Test for containers and equipments of cement structure shall be carried out according to
relevant regulations in SDJ69.
3.4.9 Water filling test, water penetration test, oil penetration test or hydraulic pressure test for
each equipment, container and system shall be carried out before painting and heat preservation.
Tests for equipments and containers with coating layer shall be carried out before construction of
anti-corrosive coating.

5
4 Raw Water Pretreatment

4.1 General Regulations


4.1.1 The installation of clarifier (clarification tank) shall comply with the following
requirements:
a) Central lines ofcollecting channel eyelets shall be located in the same horizontal line with
deviation not exceeding ±3mm.
b) Partition in collecting channels shall be welded tightly.
c) Sampling tube:
Sampling tube extending into containers shall be bent downwards with horizontal depth
1)
of 50mm~ IOOmm;
2) The elevation shall comply with design requirements;
3) The material shall comply with design requirements;
4) Sampling valve shall be located in position easy to operate and fixed firmly.
d) Additionally equipped honeycomb chute pipes or boards shall comply with design
requirements. They shall be arranged in order, and kept closely and tightly. Clearance between
modules mustn't be larger than bore.
e) Elevations of overflow pipe and outlet pipe shall comply with requirements with deviation
not exceeding ±5mm.
4.1.2 Ladders for clarifier (clarification tank), filter tank and containers shall be fully welded and
anti-corrosively treated.
4.1.3 Elevation deviations of adjacent weir crests in delivery boxes for clarification tank and
filter tank shall be no more than ±5mm.
4.1.4 For filter (tank) with cap, the integrality and crack of cap shall be inspected before
installation. The cap shall be fixed tightly and water spray test shall be carried out to check
whether desquamation or damage exists in the cap.
4.1.5 Physical and chemical properties, gradation, granularity and uniformity coefficient of filter
materials and supporting layer materials shall comply with design requirements.

4.2 Air Separator and Sludge Blanket Clarifier


4.2.1 The installation of air separator shall comply with the following requirements:
a) The elevation shall comply with design requirements with vertical errors of shell no
higher than 0.4% of its height.
b) The deviation between central line of raw water pipe extended into air separator and
central line of air separator shall not exceed 5mm, and top edge of distribution plate shall be
horizontal.
c) There shall be a clearance of 30mm~40mm between support ring and foundation. The
support ring shall be horizontal with errors less than 0.1 %.
4.2.2 The installation of sludge blanket clarifier shall comply with the following requirements:
a) Ovality and vertical errors of shell shall be less than 2% and 0.25%, respectively.
b) Deviations between central lines of upside collecting channel, inner tube and sludge
collecting tube and central line of clarifier shell shall not exceed 0.5% of its shell diameter.

6
c) Internal horizontal and vertical steady flow plates shall be welded firmly, pore size and
distance between pores shall comply with drawing regulations, and pore edge shall be smooth and
free of burr.
d) The cone of influent nozzle shall be processed strictly in accordance with design
requirements, inner surface of which shall be bright and clean. Nozzle and sleeve shall be installed
levelly. The two nozzles shall be paralleled to each other, and tangent to the cone of clarifier.
e) Link bearing of inner and outer tubes shall be welded firmly. Manhole of inner tube and
cone shall be watertight.
f) Upper and nether edges of sludge feeding hole in the same layer of inner lube shall be
positioned in the same level, and pore edge shall be smooth and free of bun'.
g) Water shall be filled into inner tube and then outer tube in water filling test for clarifier.

4.3 Clarification Tank


4.3.1 Hydraulic circulating clarification tank shall comply with the following requirements:
a) Deviations among central lines of collecting channel, nozzle and reaction chamber shall

not exceed 0.5% of collecting channel diameter, and ovality of collecting channel and hydraucone

in throat of reaction chamber shall not exceed 1%. Velticality and levelness of reaction chamber

shall comply with requirements of design drawings.


b) Nozzles shall be processed according to design drawings with smooth and clean inner
surface. Deviation between central line of nozzle and central line of throat shall not exceed 3mm.
c) Up-and-down sliding guide of throat shall be installed after emplacement of nozzle, throat
and raiser, and the installation shall guarantee freely movement of throat without obvious friction.
4.3.2 Mechanical mixing clarification tank shall comply with the following requirements:
a) Bias error among central lines of the first reaction chamber, the second reaction chamber
and clarification tank shall be no more than 0.25% of tank diameter.
b) The installation of bearing and driver of mechanical mixing devices shall be executed
according to relevant regulations of OUT 5047.
c) Bias error between central line of stirrer main shaft and central line of the second reaction
chamber shall be no more than 0.5% of diameter of the second reaction chamber.
d) Fabrication and installation of the following parts shall comply with design requirements:
1) Finish size and connecting angles of paddles.
2) Emplacement for bottom flushing device of impeller lifter and adjustment of nozzle
angle.
3) Inselt height of chemical inlet, sludge thickening cone, blowing pipe and bottom
blowing pipe of clarification tank.
4) Distance between cleaning shoe and tank bottom. The distance shall be no less than 5mm
with errors of +4mm when no design requirement is provided.
5) Levelness of umbrella plate shall comply with requirements of design drawings.

4.4 Pressure Filter Tank and Siphon Filter Tank


4.4.1 Elevations of siphon auxiliary pipe nozzle, outlet of filter tank, weir crest of influent
distribution box, the bottom of U-type elbow in influent pipe and weir crest of drainage well shall

7
be constructed according to design drawings, the deviation of which shall not exceed ± IOmm.
4.4.2 Breakwater below the cover of filter tank shall be kept horizontally, the deviation of which
shall not exceed ±2mm.
4.4.3 Quarter bend shall not be adopted for the installation of siphon auxiliary pipe. Pipe nozzle
shall not be extended into elbow pipe during welding. Orifice of gas suction pipe on the top of
siphon elbow pipe shall be inserted into siphon pipe for approximately 10mm-20mm.
4.4.4 Chute pipe of 15° used for pressure rinsing shall be constructed accord ing to design
drawings, with angle permissible variation of ±2°. Orifice of chute pipe shall be close to gas
suction pipe as much as possible; meanwhile, these two pipes shall be both installed in the same
side of siphon auxiliary pipe.
4.4.5 Siphon pipe and its jiquidometer, siphon auxiliary pipe, gas suction pipe, and siphon
breakage pipe shall all be watel1ight.

4.5 Filter
4.5.1 Mechanical filter shall comply with the following requirements:
a) Filter shall be installed verticaJly with shell with vertical errors of shell no higher than
0.25% of its height. After shell spotting, stabilizer, sizing blocks and foundation embedded parts
shall be welded firmly before back grouting.
b) Central lines of branch pipe and main pipe shall be mutually perpendicular for distribution
system, drainage system and air distribution system of fi Iter. The horizontal deviation of branch
pipe shall not exceed ±2mm.
c) Central line of release cap seat shall be perpendicular to branch pipe level. The height of
release cap seat shall be consistent with allowable deviations of ±3mm.
d) For filter with distribution system of branch-and-main-pipe type, distribution holes shall
be smooth and free of burr. Mesh used as branch pipe sleeve shall comply with design
requirements and be fastened firmly.
e) For filter with air scrubbing device, upper level of bottom blanket shall be flush with the
top of air-blowing hole or water cap.
t) For filter with anti-corrosive layer set in its shell, the quality of anti-corrosive layer shall
be inspected before materials filling.
g) For filter used in reverse osmosis system, if activated carbon or other brittle filter
materials is fi lied into fi Iter, its bottom blanket shall comply with requirements of Appendix A in this
code.
4.5.2 Fibrous filter shall comply with the following requirements:
a) All blowing pipes shall lead directly to blowing channel independently.
b) The installation of Roots blower shall be carried out according to relevant regulations in
DUT 5047.
c) Inverse U-type elbow and exhaust damper shall be set for blast pipe of Roots blower. The
apex of communicating pipe between inverse U-type elbow and fibrous fi Iter shall be higher than
the apex of fibrous filter.

8
5 Boiler Make-up Water Treatment

5.1 General Regulations


5.1.1 [on exchanger and carbon dioxide remover shall be installed vel1ically with shell with
vertical errors of shell no higher than 0.25% of its height. The height of reactor shall be more than
5.0m with maximum vertical error not exceeding 12mm. After shell spotting, stabilizer, sizing
blocks and foundation embedded parts shall be welded firmly before back grouting.
5.1.2 Before charging of ion exchanger, internal anti-corrosive layer shall be checked, and faults,
if any, shall be repaired according to relevant regulations in Chapter 13 and Clause 3.2.3 in this
code.
5.1.3 Synthetic fiber mesh used for exchanger shall be cut out by electric iron. Mesh sleeve of
branch pipe shall be oversewn by thread of the similar property of sleeve or acid (or alkali)
resistance during fabrication. If PVC (PolyvinyIChloride) mesh sleeve is adopted, shrinkage
length due to hot water fastening shall be left.
5.1.4 [nstallation quality of water cap shall be inspected according to regulations of Clause 4.1.4.
5.1.5 Before charged, resin and trademark shall be checked barrel for barrel to avoid mixed
loading. Resin shall be kept from label, pigtail or impurities during charging. Charging height of
resin shall comply with design regulations.
5.1.6 Water bedding shall be set in ion exchanger during resin charging, and it is better that its
height can protect bottom and middle drainage.
5.1.7 Quartz sand bedding must be made even by layer according to gradation of manufactory
when adopted for ion exchanger, the height of which shall comply with design requirements.
Silicon dioxide content shall be no less than 99% for purity requirements of quartz sand, which
shall also pass chemical stability test. Quartz sand shall be rinsed clean by clarified water before
charged.
5.1.8 Dehydration and frost crack shall be prevented during the storage of ion exchange basin.
Dehydrated basin, if found, shall be dipped in saturated saline solution for 24 hours firstly, and
then other operations can be carried out. Ambient temperature for winter storage shall be higher
than 5'C.
5.1.9 Wash tub pipe shall be equipped for resin trapper, if installed.
5.1.10 Equipments, such as ion exchanger, acid and alkali storage vessel, and batcher, shall be
checked and accepted according to relevant regulations in OUT 543.
5.1.11 Valve mounted in the system must pass hydraul ic pressure test before installation, control
gas of valve shall be purified with stable pressure to guarantee rei iabil ity of control operation.
5.1.12 Creepage performance test shall be carried out for anti-corrosive liner of equipment and
pipe, and those don't pass the test shall be returned to manufactory or repaired on site.
5.1.13 Rust, welding slag, mud and sand, and other impurities in equipment and pipe shall be
removed.

5.2 Ion Exchanger


5.2.1 Technical requirements for internal devices of ion exchanger shall comply with regulations
of design (or manufactory) drawings. Those without regulations of design (or manufactory) shall

9
be checked and calibrated according to the following clauses:
a) Assembling allowable deviations of catching devices and drainage (such as inlet damper,
quaquversal grid plate, pile-type water cap, etc.) are as follow: its deviation with central line of
tunnel body shall be lower than 5mm, and horizontal deviation shall not exceed ±4mm.
b) For catching devices and drainage of branch-and-main-pipe type, central line of branch
pipes shall be perpendicular to central line of main pipe. Their levelness and verticality shall be
lower than 4mm/m and 3mm/m, respectively. Distance deviations between two adjacent branch
pipes and any two branch pipes shall not exceed ±2mm and ±4mm, respectively.
c) Regeneration devices and medium drainage shall be installed horizontally. Eyelet
directions of regeneration pipe and medium drainage pipe shall be in accordance with
manufacturing drawings. Nozzle of actinoid regeneration pipe shall upright, and no blocking
phenomenon appears by water test.
5.2.2 Inert resin, plastic bailor resin of the same type can be adopted for resin compaction layer
of up-flow regeneration ion exchanger, the thickness of which shall comply with design
regulations. Charged thickness of those without design regulations shall be 200mm~250mm.

Upper limit shall be taken for ion exchanger with diameter bigger than 2500mm.
5.2.3 For ion exchanger with air scrubbing device, bottom blanket level shall be flush with the
top of air-blowing hole or water cap.
5.2.4 Large shim shall be adopted for ion exchanger with bolt-fastening fittings to prevent the
damage of anti-corrosive layer.
5.2.5 Water quality for charged resin: clarified tiltering water used for cation bed, effluent of
cation bed used for anion bed, and desalting water used for mixed ion.
5.2.6 Trademark, physical chemical propelties and the proportion between anion and cation
exchanger resin of the resin charged in mixed bed shall comply with design requirements.

5.3 Blast Carbon Dioxide Remover


5.3.1 Connections bet\;veen any two members in the remover shall be tight. Internal
anti-corrosive layer shall comply with design requirements.
5.3.2 Influent distribution device upside and internal perforated plate (or grid) shall be horizontal,
with deviation not exceeding ±8mm.
5.3.3 Corrosion-resistant material shall be adopted for influent valve, which mustn't be
substituted by other kind of valve. Switch of valve flash board shall be correctly corresponding to
pontoon movement.
5.3.4 Blower fan and blast pipe shall be arranged to prevent water from pouring into blower fan.
5.3.5 Vent pipe of carbon dioxide remover arranged indoor shall be extended to outside.

10
6 Membrane Treatment Facilities

6.1 Electrodialysis Plant


6.1.1 General Regulations
6.1.1.1 Ion exchange membrane shall be kept away from oil, organic solvents (liquor), boric acid,
bleaching powder and other oxidants.
6.1.1.2 Direct voltage mustn't be applied on electrodialysis plant before it is filled with water.
6.1.1.3 Water shall be periodically fed during storage, assembly and idling to keep ion exchange
membrane wet and to prevent it from dehydrating and going moldy.
6.1.2 For the installation of ion exchange membrane stack provided in the form of subassembly,
attention should be paid to the following items:
a) It shall be protected by wet method, and anti-freezing measures shall be taken in winter.
b) Inversion and collision are forbidden during hoisting and conveying to prevent membrane
from displacement or deformation, and wrappage for protection shall not be damaged.
e) If ion exchange membranes stack don't put into operation immediately, external packing
and enclosed flange shall be temporarily reserved until membrane put into operation.
d) Ion exchange membrane stack shall be emplaced according to equipment arrangement
drawing, and leveled by its own tai Is or plastic plate.
e) After connected into system, ion membrane stack shall be kept in the condition full of
water.
6.1.3 For the ion exchange membrane stack provided by bulk cargo and assembled on site,
attention should be paid to the following items:
a) Ion exchange membrane shall be inspected before assembly, and no damage shall be
found.
b) Before cutting, ion exchanger membrane shall be dipped in raw water for operation for
more than 48 hours.
e) [on exchange membrane shall be stored in clean water or plastic package; membrane sheet
shall be kept from folding, and cut and punched by drawings.
d) Clapboard shall be selected and cleaned before assembly, and distribution channel of
clapboard with even thickness shall be straightway.
e) Assembly shall be checked at any moment of the process to guarantee the correctness;
membrane sheet and clapboard shall be mounted straight; influent and effluent holes shall be
aimed at each other.
f) Distances between tetragonal bed plate of membrane stack and ejector plate shall be
measured firstly during fastening screw cap to make measured values equal, and then the force
shall be evenly and stably applied from middle bolt of the long side to two sides to ensure each
screw cap fastened synchronously.
g) Water filling test shall be carried out following requirements of manufactory after the
assembly of ion exchange membrane stack.

6.2 Reverse Osmosis Equipment


6.2.1 Membrane element for reverse osmosis shall be stored following requirements of

II
manufactory before installed into system.
6.2.2 Pressure vessel shell shall be stored indoor and positioned horizontally, and meddle
hang-up is forbidden. Impact damage shall be prevented during construction.
6.2.3 Soundness of parts, such as fresh water pipe, membrane sheet, baffle and brine seal ring,
shall be inspected before the assembly of membrane module. Pressure vessel shell shall be
installed in prescribed order of manufactory after vessel soundness and installation direction of
brine seal ring are confirmed. Assembly environment shall satisfy requirements of manufactory,
and no leakage shall be found after installed module filled with water.
6.2.4 For multicell reverse osmosis equipments, allowable deviations of geometrical dimensions
for membrane module frame on foundation and membrane module on frame shall be ±5mm and
±3mm, respectively.
6.2.5 Polytetrafiuoroethylene shim shall be applied for fiange between high-pressure pump and
membrane module.
6.2.6 Internal wall of pipe between security filter and membrane module shall be kept clean, and
chemical cleaning can be adopted if necessary.
6.2.7 Temperature and pressure protective devices for water supply system shall be sensitive and
reliable.
6.2.8 Chemical feeder and on-line chemical meters in reverse osmosis system shall be installed
and inspected before trial running, which shall be able to put into operation at any moment.
6.2.9 Infiuent water quality shall comply with regulations of manufactory for reverse osmosis
equipments.

12
7 Condensation Water Treatment

7.1 General Regulations


7.1.1 Gradient of resin delivery pipe shall comply with design requirements; ups and downs are
forbidden. Large curvature radius shall be chosen for elbow, and prevention of resin blocking shall
be considered for the installation of valve type and flange shim.
7.1.2 Insulating shim shall be adopted for connections between stainless steel pipe and common
carbon steel pipe.
7.1.3 Control valve and isolating valve shall be installed on compressed air pipe to prevent air
entering into condensation water system.
7.1.4 Element working pressure hydraulic test shall be carried out for ion exchanger after
hydraulic pressure test for condensation treatment system to ensure tightness of valves connected
to the ion exchanger.
7.1.5 Except for Clause 5.1.7, other clauses in Section 5.1 in this code are all suitable for Section
7.1.
7.1.6 Differential pressure and temperature protective devices for condensation water treatment
system shall be sensitive and reliable.

7.2 Ion Exchanger


7.2.1 Ion exchanger (prepositive hydrogen and high-speed mixing bed) shall be installed
according to relevant regulations of Section 5.2 in this code.
7.2.2 Assembling allowable deviations of influent baffle or distribution funnel are as follow: its
deviation with central line of ion exchanger body shall be lower than 5mm, and horizontal
deviation shall not exceed 2mm.
7.2.3 lCrl8Ni9Ti stainless steel or similar materials shall be adopted for filter element of ion
exchanger and catcher as well as elements such as bolt, nut and clip in internal equipments of
fixed ion exchanger.

7.3 Electromagnetic Iron-removal Filter


7.3.1 Electromagnetic iron-removal filter shall be installed vertically with shell with vertical
errors of shell no higher than 0.25% of its height.
7.3.2 Filler height in electromagnetic iron-removal filter shall comply with design requirements,
and impurities mustn't be interfused during charging.
7.3.3 Distances between electromagnetic iron-removal filter and installation position of various
electric, thermal and chemical meters shall be larger than 1m

7.4 Pipe Precision Filter


7.4.1 Pipe precision filter shall be installed vertically with shell with vertical errors of shell no
higher than 0.25% of its height.
7.4.2 Filter elements in pipe precision filter shall be intact, firmly mounted and tight.

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8 Sample and Dosing System

8.1 The installation of water and steam analysis and sampling device shall comply with the
following requirements:
a) Installation position of sampling device, valve, materials of connecting pipe and
drainage system shall comply with design requirements.
b) Secondary valve installation shall be firm and easy to operate and maintain; pressure,
temperature and flow of measured medium entering into water and steam analysis and sampling
device shall comply with manufactory regulations.
e) Allowable deviation range for hole diameter at sampling point and sample pipe diameter
shall be in the range of +0.5mm~+ 1.0mm, and hole edge shall be smooth and free of burr. Weld
junction shall comply with regulations in OUT 5007. Insert depth of sample pipe shall be 1/2 of
pipe diameter with sample connection back to medium flow direction.
d) Sampling pipe line, cooling system, depressurized system and sampling valve shall all
be watertight and able to put into operation normally.
e) Sampling and analysis device shall be checked and accepted according to DUT 665.
8.2 The location of sampling point shall comply with design requirements. Sample point for
low-pressure water supply before dosing, if not prescribed, shall be located at the position about
Im below outlet of deaerator. [nlet pipe of dosing point shall be 0.5m lower than the sample point.
8.3 Specs and materials of sample pipe shall comply with design requirements, the inside of
which shall be clean and straightway. Proper minimum distance shall be chosen for pipe and cable
laying with arrangement like smooth vertical and horizontal strokes. Mechanical damage shall be
avoided for pipe processing. Pipe arrangement shall be kept away from place with severe shake,
moisture or corrosive medium. Rigid bracket shall be set in the front of door firstly. Radian of pipe
and cable laying in row shall be consistent, the outer surface of which shall be no crack, sagging
and overroasting phenomenon after bent. There shall be obvious deviation of pipe in the same
diameter. Weld junction shall comply with regulations in DUT 5007. Unblockage and tightness
test shall be carried out after pipe construction.
8.4 The installation of dosing system shall comply with the following requirements:
a) Manufacturing quality of box and channel shall comply with requirements of Clause 10.1
in this code.
b) Materials of dosing pipe shall comply with design requirements, the inside of which shall
be clean and straightway. Outer surface of the pipe shall be no crack, sagging and overroasting
phenomenon after bent. There shall be obvious deviation of pipe in the same diameter. Weld
junction shall comply with regulations in OUT 5007. Tightness hydraulic pressure test shall be
carried out after construction is finished. Test method and notice shall be executed according to
regulations in OUT 503 1.
e) Installation and maintenance of feeding pump shall comply with requirements of Clause
11.2.3.
d) Liquidometer of box or channel shall be installed vertically in the position easy to observe,
with clear indication and solid protection cover.

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9 Circulated Cooling Water Treatment

9.1 Algae and Bacteria Killing System


9.1.1 Vacuum chlorine liquid
9.1.1.1 Ventilation and automatic alarm leak detector shall be mounted in chlorine cylinder room
and chlorine control room equipped with gas mask.
9.1.1.2 Chlorination device and pipe shall comply with the following requirements:
a) Constructed according to design requirements.
b) Anti-corrosive materials shall be adopted.
c) After installing all the chlorine pipes, leak detection with nitrogen or vacuum negative
pressure leak detection shall be done under the pressure of work. Be sure it is seal and free of
leakage.
d) Chlorine pipes shall be installed fastness. Copper pipe or silver plated copper pipe shall be
adopted between the exit of chlorine bottle and the main chlorine pipe. Flexible joint shall be
processed in order to removable easily. The exit pipe of chlorination machine is laid with a slope
and engineering plastics tubes and pipes shall be adopted. All joints shall use adhesive and try to
reduce joints.
9.1.1.3 Polytetranuoroethylene, copper or lead packing pieces shall be adopted for all packing
pieces of valves, flange and lock nut in the chlorine system. Rubber packing piece is forbidden.
9.1.1.4 Chlorine bottle shall be kept cool and dry. Spray pipe shall be set on the upside and the
temperature of water shall be controlled under 40·C. Weighbridge shall be checked and
cel1ificated by measurement department. Certificate of quality is required.
9.1.1.5 Minimum work pressure shall be not below 0.1 MPa (or according to minimum limit
residual quantity prescribed by the manufacturer) when using ch lorine, whi Ie it mustn't be
connected directly with injector.
9.1.1.6 Chlorine point shall be set under the lowest operation level (about 150mm). While
chlorization under negative pressure is adopted, hydraulic pressure of injector shall be kept stable.
The injector shall be adjusted to optimum work condition.
9.1.2 Sodium hypochlorite [while electrolyzing saline solution (seawater) to prepare sodium
hypochlorite) shall comply with requirements as follow:
a) Saline solution (seawater) shall be filtrated before fed into the electrolysis bath;
b) Hydrogen gas which amasses in the sodium hypochlorite trough shall be drawn by
explosion proof type fan timely. The thickness of hydrogen gas shall be controlled below 0.4%
(v/v);
c) ElectrolyzeI' shall be isolated; connecting pipe shall be anti-corrosion; system shall be
watertight; pipe laying shall not be out of level in order to prevent gas accumulation.
9.1.3 Chlorine dioxide
9.1.3.1 Feeding Tube of chlorine dioxide system shall comply with design requirements.
Leakage test shall be carried out after installation to ensure tightness.
9.1.3.2 Storage raw material of chlorine dioxide (e.g. hydrochloric acid, sodium chlorite etc.)
shall be separated. Liquid-phase sodium chlorite shall be adopted.
9.1.3.3 Cutoff protection shall be set in automatic feeding chlorine dioxide equipment for
automatic stoppage and alarm.

15
9.1.3.4 Aerator and automatic alarm leakage detecting device shall be settled in the chlorine
dioxide feeding room. Anti-corrosion measures shall be taken for floor according to design
requirements.
9.1.3.5 A great variety of drug blowing pipe shall be jointed respectively. They mustn't be
arranged in the same pipe.
9.1.4 Corresponding anti-corrosion measures shall be taken for other feeding equipments and
pipes of chlorization chemicals.

9.2 Scale Inhabitation and Anti-corrosion Equipment


9.2.1 Concentrated sulfuric acid system shall comply with requirements as follows:
a) Base of concentrated sulfuric acid chest shall be welded firmly on the settled flat roof.
The bottom of chest shall be inclined to the blowdown side, and gradient shall be greater than
0.5%. Waterproof establishment and moisture absorption equipment shall be set on the top of chest
and vvash establishment shall be set nearby.
b) Seamless steel pipe shall be adopted for all pipes in the equipment.
c) Lead or polytetrafluoroethene shim shall be adopted for interface of valve and flange.
Rubber pad shall be forbidden.
d) Tightness test shall be carried out according to regulations in this code after system
installation.
e) Acid mixing tank shall be fabricated according design requirements. All welding lines
shall be checked by oi I penetration test.
f) Before preliminary storage in concentrated sulfuric acid equipment, water accumulated in
the equipment or system shall be drained away. Fire adjacent to equipment is forbidden after acid
storage.
9.2.2 When water quality stabilizer treatment method is adopted, chemical feeding equipment
shall be constructed, checked and accepted according to design requirements.
9.2.3 Treatment establishment of ferrous sulfate shall be checked and accepted according to
designed technical requirements.

9.3 Make-up Water Treatment


9.3.1 When acid basin treatment method is adopted, related equipment shall comply with
relevant regulations in Section 5.2.
9.3.2 When lime treatment method is adopted, it shall comply with relevant regulations in
Chapter 4 as well as Section 11.1 and 12.2.
9.3.3 When bypath filter treatment method is adopted, equipment shall comply with relevant
regulations in Section 4.4 and 4.5.

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10 Tank

10.1 Manufacturing quality of tank shall comply with the following requirements:
a) Tank shall be strictly processed and manufactured following design with level tank wall
(bottom);
b) Such reinforcement as ribbed bar shall be welded firmly;
c) For tank with anti-corrosive layer, the layer shall be intact and pass inspection;
d) Its accessories shall be all ready, and the quality of which shall comply with relevant
operation standards;
e) It shall be eligible in water filling test (concrete product shall be tested according to code
SDJ 69, and metal members shall be of no leakage in 24 hours after water filling).
10.2 Anti-corrosion layer for internal wall shall be constructed after electric welding of all pipes
and accessories (meter supports, water gage, fastening iron, etc.) is finished and accepted.
10.3 For flat bottom tank mounted on foundation, the contact between tank bottom and
foundation shall be even and tight. Antirust painting shall be brushed on outer surface of tank
bottom before tank emplacement. Bedding shall be laid on foundation according to design
requirements. Water filling test shall be carried out after water tank emplacement, and relevant
pipes shall be connected after the stability of foundation settlement.
10.4 Arc of horizontal tank or abutment shall be identical and evenly contact with tank wall, and
there shall be no obvious gap between them.
10.5 Enough flow area shall be left for breathing pipe of water tank, and the end of overflow
pipe shall not be extended under water surface of drain.
10.6 Floating roof tanks shall comply with the following requirements:
a) Floating roof can only be mounted after internal anti-corrosion layer construction is
finished. 24-hour leakage test shall be carried out for floating roof.
b) Tightness of rubber bladder shall be inspected before installation for soft floating roof
tank. The connection between upper port of floating roof and mounting ring shall be watertight,
and these two parts shall be kept in the same level with deviation not exceeding ±O.2% of water
tank diameter.
c) Ovality of tunnel body and floating roof shall be ±O.J% for hard floating roof tank, and
concentricity between guide tube of floating roof and water tank shall not exceed ± IOmm.
Verticality between tunnel body and guide tube shall be lower than 0 15% of tank height. Top
circle bearing seal of floating roof shall be watertight and able to freely up-and-dovvn fluctuate in
the tank.
10.7 Mesh of proper materials shall be set in outlet and blowing outlet for tank sealed with
plastic covered ball
10.8 Water gage shall be installed vertically in the position easy to observe with clear indication,
and solid protection cover shall be mounted. Glass tube water meter mustn't be adopted for
outdoor water tank in extremely cold areas.

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11 Rotary Machine

11.1 Slaked Lime Machine and Lime Crane


11.1.1 Slaked lime machine shall comply with the following requirements:
a) Rotary drum shall be exactly and evenly mounted on roller, which shall be turned
limberly and freely. Levelness of drum body, axial dimensions of roller abutment and axial
drunkenness value of rotary drum shall all comply with technical requirements of manufactory.
b) Transmission gear shall be meshed well. Tooth flanks shall contact with each other evenly,
and bottom and side clearances shall both comply with drawings requirements.
c) Connecting tube seat at throat of lime feeding pipe shall be connected with raw water.
Mud hole with thread bulkhead at throat shall be only used for slag drainage and not connected
with raw water.
d) Vent pipe shall be extended to outdoor.
11.1.2 Monorail of lime crane shall be mounted horizontally, height difference in full running
distance of which shall be lower than 10mm. Welding line shall be rubbed down, and wheel
movement shall be flexible, stable and free.

11.2 Special Pump for \Vater Treatment


11.2.1 Installation and acceptance of general centrifugal pump shall be executed according to
relevant regulations in OUT 501].
11.2.2 Anti-corrosion pump manufactured by nonmetal materials or with liner shall comply with
the following requirements:
a) Impaction and press shall be avoided during disassembly and cleaning, and the pump shall
not be contacted with organic solvents and stored under high-temperature environment.
b) Before installation, the following items shall be inspected:
1) Binding impeller shall be clean and free of damage and crack.
2) Axle head nut, bearing seal and axle sleeve shall be free of deformation, burr and crack.
Axle head screw thread shall be intact.
3) There shall be no obvious stratification and deformation in hot-pressed pump shall, end
cover and other parts.
4) Anti-corrosion materials shall be adopted for shaft packing and mechanical seal.
5) Anti-corrosion layer for lining shall be intact and free of damage.
c) Attention shall be paid to the following problems during construction:
1) Shim used for junction plane of pump shell shall be of special anti-corrosion material,
the same as the material of shim used for flange of the system.
2) Sealed water source and water seal pressure of pump shall comply with design
requirements. In general, water seal pressure shall be slightly higher than the pressure of working
medium in pump.
3) Cooling water pipe of submerged drainage pump shall comply with manufactory
requirements.
11.2.3 Reciprocating pump shall comply with the following requirements:
a) Slide way of pump body, bearing bracket, exposed parts of axle or other finish machining

18
surface shall be applied as measurement benchmark for centering of pump body.
b) Safety valve in fluids conveyance system shall be checked by disassembly, and operating
pressure shall be adjusted according to design regulations. Operating pressure, if not prescribed,
shall be adjusted to 1.25 times of working pressure.
c) For reciprocating pump with working medium directly contacting with piston (plunger),
quick detachable sieve shall be mounted at entry according to design drawings. Sieve of 50 Mesh
-100 Mesh can be mounted, if no design requirement refers to sieve. Effective area of sieve shall
be no less than three times of sectional area of entry pump. Materials resistant to working medium
corrosion shall be adopted.
d) The following clearance value shall be measured and recorded during installation:
1) Drunkenness clearance between worm wheel and worm in gear box.
2) Clearance between plunger and lining of plunger.
e) Installation requirements for cylinder body of diaphragm pump are as follow:
1) All bolts in front and back cylinder ends shall be screwed down evenly. Diaphragm shall
not be deformed owing to extrusion after installation.
2) Capping for filling materials shall not be over-tight or loose.
3) Anti-corrosion materials shall be wrapped around connections of all screw threads of
feeding valve and drainage valve for seal during installation.
4) Hydraulic fluid shall be injected according to regulations of equipment technical
document, and there shall be no vapor in hydraulic cavity.
f) Test running of reciprocating pump:
1) It shall be carried out in the following order: no-load running shall be no less than 15
minutes; after functioning, the pump shall be operated under pressure in the order of 1/4, 1/2,3/4
of working pressure for at least 0.5 hours, and continuous operation shall be no less than 4 hours.
Record flow changes under each pressure.
2) After test running, reciprocating pump shall comply with the following requirements:
suction valve and drainage valve shall be available for use; safety valve, oil make-up valve and
exhaust valve of diaphragm pump shall be functioning, sensitive and reliable.
3) Diaphragm with crack shall be exchanged during test running, and diaphragm made of
butadiene-acrylonitrile rubber shall be adopted for concentrated acid medium.
4) Parts of safety valve, oil make-up valve and exhaust valve shall be manufactured by
anti-corrosion materials.
11.2.4 Self-priming pump shall comply with the following requirements:
a) Quick detachable sieve shall be mounted at entry according to design drawings. Sieve
without design requirement shall be selected and installed according to relevant regulations of
Clause 11.2.3.
b) Pump installation shall be carried out according to relevant regulations of Clause 11.2.1
and Clause 11.2.2.
c) There shall be some water sources near to self-priming pump, which is convenient for
water fi 11 ing of pump startup.
d) Pressure gauge shall be checked before startup. The function of inlet valve and outlet
valve shall also be inspected.
e) fnlet and outlet valve shall be opened before startup, and J min-2min is required for pump
startup when pump body is filled with water. Then gradually increase pressure indicated by

19
pressure gauge, and check operation conditions of pump.

11.3 Air Compressor and Its Accessories


11.3.1 Construction and acceptance of general air compressor shall be executed according to
relevant regulations in OUT 5047.
11.3.2 Lubricant-free air compressor shall comply with the following requirements.
a) Attention shall be paid for the following problems during installation:
1) Oil-removal cleaning shall be carried out for oil-seal parts before installation. There shall
be no iron stain on mirror face of cylinder and piston rod.
2) After assembly of cylinder filling materials, tightness hydraulic pressure test shall be
carried out for water pipe under pressure prescribed in equipment technical documents. Those
without prescribed pressure shall be carried out under pressure of 1.25 times of working pressure.
Leakage shall be treated until water pipe passing hydraulic test.
3) Blade direction shall be right during assembly of oil wiper. Oil baflle on piston rod shall
be assembled firmly.
4) Before piston assembly, molybdenum disulfide powder shall be coated on the surface of
piston rod and cylinder mirror face, and redundant molybdenum disulfide powder on surface shall
be removed. Operation shall be carried out according to document regulations if other prescribed
in equipment technical document.
5) If piston rob with internal cooling is adopted, cooling liquor inlet and outlet pipe shall be
clean and straightway, and pipe connections shall be watertight.
6) Lubricant and oil quality in crankcase shall comply with manufactory requirements,
usage method of which shall comply with relevant regulations.
b) During test running, except for procedures regulated in equipment technical document,
the following requirements shall also be complied with:
I) Pressure and flow of cooling liquor during operation must be stable.
2) During operation, oil scraping on piston rod surface shall be functioning, and lubricant in
crankcase and crosshead mustn't be carried into cylinder.
3) Pressure can't be gradually enhanced until temperature is stable, filling material seal is
finished and all parts are operated freely during operation.
4) Service test shall be carried out, and tightness of piston clearance, gas valves at inlet and
outlet as well as the whole system shall be inspected.
11.3.3 Before emplacement of accessories of air compressor (such as drier, gas container, filter
cleaner and blow tank), Pipe orifice position, the equality of anchor bolt hole and foundation
position, as well as pipe shall be checked by shop drawing.
11.3.4 Pressure vessel in compressed air system shall be carried out according to relevant
regulations of Boiler No. 154 Documents issued by China State Bureau of Quality and Technical
Supervision (1999).
11.3.5 Roots blower shall be installed and accepted according to technical documents of its
manufactory.

20
11.4 Agitator
ll.4.1 After the installation of agitator impeller, there shall not be obvious bend and deformation
for guide bar and impeller, respectively. ldle running of agitator shall be flexible and free. Intense
vibration is forbidden during loaded running.
11.4.2 Quality of hose for lime slurry agitator shall comply with design requirements. Suction
pipe port shall be 250mm~300mm higher than conical bottom of agitator when floating drum
located at the lowest level.
11.4.3 Floating drum shall be watertight in 24-hour water filling test. Floating drum shall have
enough weight to guarantee emersed part accounting for 50% of drum body after dipped in water.

21
12 Special Pipes and Valves

12.1 General Regulations


12.Ll Plastic, glass reinforced plastic and engineering plastic pipe fittings shall comply with the
following requirements:
a) Interface shall be polished and cleaned up during pipe fittings bonding, which shall be
carried out strictly according to bonding process. Protection measures shall be taken after bonding,
and pipe fittings can't be installed before completely solidification of binder.
b) Isolation measures shall be taken if electric welding is adopted. Welding slag and cut
leftover material shall be kept away from pipe.
c) Approved film pressure products produced by manufactory shall be adopted as much as
possible.
d) Plain washer shall be applied in both ends of flange connection bolts, and evenly forced to
symmetrically fasten them. 2-3 spiral cords of bolt shall be exposed.
e) Long-term exposure under the sun must be avoided to prevent aging and deterioration.
12.1.2 Distance between branch hangers of pipe shall comply with design regulations; for plastic
and glass reinforced plastic pipe, bolster (rubber cushion etc.) shall be mounted between metal
buckle and pipe.
12.1.3 When several pipes are laid parallel, construction shall be carried out in the following
order: metal pipe firstly, then glass reinforced plastic pipe, and finally plastic pipe.
12.1.4 Valves and water blaster with higher deadweight shall be hoisted separately to prevent
pipe from excessive load.
12.1.5 Complex pipe fittings lined with rubber, plastic or polytetrafluoroethylene, and flange
interface shall be specially protected during transportation and installation to prevent from
damaging.

12.2 Special Pipes


12.2.1 Installation requirements of pipe for lime slurry are as follow:
a) During pipe (including pipe for magnesia slurry) laying:
1) Gradient of pipe to drainage direction shall be larger than 1:20.
2) U-type tabulation and abrupt enlargement of pipe diameter are forbidden.
3) Welded elbow shall not be adopted.
4) Emptying conduit or bulkhead shall be mounted at low level point of pipe.
5) Flange connections shall be equipped for T-type pipe and cross joint, and straight pipe
length ofT-type pipe and cross joint shall be shortened as much as possible.
b) Plug valve shall be adopted, while cutoff valve and gate valve mustn't be employed. Dead
points shall be avoided for valve position. Valve type shall be inspect to ensure them comply with
design requirements.
c) Flange connections shall be employed in consideration of disassembly. A couple of
flanges shall be mounted for every 2m~3m in declining parts of pipe, and all elbows shall be
connected with flange.
12.2.2 Installation requirements of pipe for acid and alkali are as follow:

22
a) During pipe construction:
1) Pipe shall be welded by qualified welder to guarantee welding quality.
2) Flange connection shall be watertight, and protective cover or baffle shall be adopted for
valve and flange of pipe for concentrated acid or alkali adjacent to sidewalk.
3) Materials of flange shim shall be selected according to design regulations; rubber
asbestos plate and acid-resistant (alkali-resistant) rubber pad can be employed for dilute sulfuric
acid pipe and hydrochloric acid (alkali liquor) pipe, respectively.
b) Exhaust pipe of hydrochloric acid tank shall be extended to outdoor through acid mist
absorber. Outlets of discharging pipe and overflow pipe shall be sealed by water sealed packing,
and connected to underground drain with anti-corrosion treatment.
c) Repaired pipe fittings lined with rubber or plastic is forbidden for concentrated
hydrochloric acid system.
d) Long tabulation shall be adopted for concentrated sulfuric acid pipe to decrease
connections.
e) Brass or aluminum material mustn't be used for fittings or valve in alkali liquor pipe.
Paint is also forbidden for internal wall of alkali liquor container and pipe.
12.2.3 Installation of plastic pipe shall comply with the following regulations:
a) It shall be carried out according to material characters, technical regulations and welding
regulations.
b) Quality of plastic pipe shall comply with the following requirements:
1) Pipe wall shall be free of exfoliation, crack and obvious sags and crests.
2) Ovality of plastic pipe with internal diameter below 150mm shall not exceed 5%.
3) Thickness error of plastic pipe with wall thickness below 30mm shall not exceed - 15%.
c) Rubber lagging box or bayonet joint shall be adopted following design for permanent
connections of pipe. Aboral welding shall be employed for gravity flow pipe.
d) Quality requirements of plastic welding rod and quality inspection of welding line after
welding shall be executed according to relevant regulations in Section 13.3.
e) Expansion joint shall be mounted for each 30 meters in straight pipe section. Expansion
joint shall be straight and free of distortion, the surface of which shall be free of such faults as
crack, bubble and deterioration. Ovality of elbow part shall be below 6%.
l) When the method of bayonet joint with binder is employed for connection of ABS
engineering plastic pipe, the pipe shall be immediately insel1ed without holdup and torsion after
processed, chamfered, snagged and coated with binder according to process requirements, and
then it can be used after completely solidification with at least 24-hour standing.
12.2.4 Installation of glass reinforced plastic pipe shall comply with the following regulations:
a) Appearance inspection shall be carried out for each fitting before installation, and any
fault, such as exfoliation, uneven thickness or bubble, is forbidden.
b) Binder shall be prepared according to manufactory requirement or design requirement.
Lab-scale test shall be made according to local climate conditions and material characters before
binding, and construction can only be carried our when test results comply with relevant quality
requirements. Overdue or depleted chemicals mustn't be used.
c) Binder on connections shall be even and smooth with height flush with pipe wall after
binding. Binding shall be close-grained, and its surface shall be free of air hole and rugosity.
d) Sampling pipe or meter pipe shall not be directly connected with pipe; sampling (or meter)

23
pipe flange or seat shall be mounted at flange connections if sampling (or meter) pipe must be
connected.
12.2.5 Installation of lining pipe (pipe lined with rubber or plastic, etc.) shall comply with the
following regulations:
a) All tabulations and pipe fittings shall be inspected before assembly:
1) Appearance quality and metal binding conditions shall be judged by visual inspection or
tightly knocking by wood mallet with weight below O.25kg.
2) Its tightness shall be completely inspected by creepage monitor, and creepage must be
avoided. Voltage for creepage test shall be larger than ISkV with probe movement speed of
3m/min-6m/min. Long-term stay of probe in rubber layer shall be avoided, and it shall be broken
immediately when disusing to prevent sparking through rubber layer.
3) Flange interface shall be smooth with tight joint and no radial channel. Rough flanging
of large-diameter pipe flange shall be polished.
b) Solvent in which rubber can soluble shall not be applied for the treatment of stained pipe
and pipe fittings lined with rubber.
c) Electric welding or drilling is forbidden on installed pipe lined with rubber.
d) Equipments and pipe fittings lined with hard rubber shall be stored in environment with
temperature above 5'C and kept away from long-term exposure under the sun.

12.3 Special Valves


12.3.1 Before valve installation, the following preparations shall be finished.
a) Valve type and specs shall be inspected whether comply with design regulations.
b) Tightness hydraulic pressure test shall be carried out under test pressure of 1.25 times of
working pressure. It can only used after passing the test.
12.3.2 Rubber quality shall be checked by creepage test for valve lined with rubber. Interface
shall be smooth and free of damage. Liner surface shall be free of bubble.
12.3.3 No-load test and open-close test under working pressure shall be carried out before
pneumatic valve is put into operation. Valve movement must be llexible with emplaced switch.
Manual operation is unsuitable.
12.3.4 Butterfly valve movement shall be flexible, and its installation direction shall be correct.
Soft shim shall not be adopted for butterfly valve lined with rubber.

24
13 Anti-corrosion Construction Technologies

13.1 General Regulations


13.1.1 Strict safety measures for fire protection, explosion prevention, gas defense and electric
shock precaution shall be establ ished before the construction of anti-corrosion protective layer of
equipment and concrete members, and the following tasks shall also be finished.
a) Water filling test, oil penetration test or hydraulic pressure test of equipment body, as well
as welding and locksmith work for equipment body and accessories (such as connecting pipe seat,
meter pipe, sampling pipe and internal attached members).
b) Fabrication, preinstallation and emplacement of pipe, reservation of anti-corrosion
clearance, and printing steel seal of serial number.
13.1.2 Welding beading, salient blemish and iron stain on surface shall be removed and cleaned
up by polishing for anti-corrosion metal surface. Sand (quartz sand, diamond grain or iron sand)
shall be of enough hardness and dried for rust removal by sand blasting. Other methods can also
be employed on the promise of ensuring rust removal (even silver gray metal surface shall
appear).
13.1.3 Anti-corrosion construction site shall be clean, dry and drafty. Dryness measures shall be
taken for rust removal by sand blasting under damp environment to prevent secondary rust.
Ventilation devices shall be installed for construction in container to guarantee ventilation volume
per hour no less than 30 times of equipment volume.
13.1.4 Rust-removed metal surface shall also comply with the following requirements:
a) The surface shall be of even metal color with a bit roughness, and free of holes, cracks,
remnant rusts, and welding beadings. It shall be rewelded and planished for surface with depth of
concaved spot exceeding 3mm.
b) Arc at liner edge and corner shall be smooth, and its radius shall be bigger than 5mm.
c) Rust and dirties shall be removed and cleaned up by organic solvents.
13.1.5 Rust removal effects must be checked and accepted by relevant person after removal and
cleaning, and primer shall be coated as quickly as possible. Metal surface after rust removal shall
be kept dry and clean during storage. If secondary contamination or rust appears owing to storage
malfunction, metal surface shall be treated again until accepted by relevant person.
13.1.6 Before anti-corrosion layer coating or lining, the following items shall be checked:
a) Approved cel1ificate for product and operation instruction shall be provided for varnish,
paint, sizing materials, solvent and lining materials. Specs and trademark shall comply with design
requirements.
b) Materials lifetime shall not exceed prescribed term, and those without uncertain specs and
trademark shall be investigated and ascertained before usage. Those materials without trademark
or manufactory symbol or overdue materials are forbidden.

13.2 Anti-corrosion Layer


13.2.1 Primer coat shall be even, complete, and free of missing spot, air bubble, flow-away,
folding or damage.
13.2.2 Putter, primer and enamel shall be matched referring to product indication and mustn't be

25
mixed optionally. Overdue materials mustn't be used.
13.2.3 Ambient temperature for construction and drying time of each layer shall be determined
according to different requirements of various paints and weather conditions.
13.2.4 During coating, water shall not be carried by painting tools, equipment surface and paints.
The layer shall be kept away from acid or alkali, dust and insolation, and smoking or lighting fires
shall be strictly forbidden. 1n addition,
13.2.5 The number and color of coatings shall be fixed according to design requirements.
Thickness of coating: primer shall be generally larger than SOlJ,m; final coating shall below 20lJ,m.
13.2.6 Thermal treatment shall be carried out according to design (or manufactory) regulations
after one coat of thermosetting resins paint to make it completely solidify.
13.2.7 Construction of glass fiber plastic.
a) For anti-corrosion layer manufactured by glass fiber plastic, such as anti-corrosion layer
for neutralization tank, ditch and floor contact with acid or alkali, its raw materials shall comply
with the following requirements:
1) Epoxy resin, furan resin, bisphenol A unsaturated polyesters resins and various curing
agents, diluting agents and filling materials shall comply with quality requirements in chemical
industry.
2) Shelf life of phenol-formaldehyde resin shall not exceed 3 months (calculated from
production date of product), and it mustn't be used when viscosity increases.
3) Acid fastness and grain size of filling materials shall be larger than 98% and less than
0.125mm, respectively.
4) Roving fillet cloth free of alkali, wax and twist, with thickness of 0.2mm~0.4mm

(0.3mm is proper in general), shall be adopted for glass cloth. Glass cloth shall be kept cool, dry,
clean and away from moisture and contamination.
b) Containers and tools for material preparation shall be anti-corrosion, clean, dry and free of
oil stain. Sizing material shall be prepared in prescribed order, which shall not be used if
gelatinization phenomenon appears during usage.
c) Manual pasting method, divided into continuous mode and intermittent mode, shall be
generally adopted for on-site lining of glass reinforced plastic. It shall be constructed according to
requirements of design indication. Those without design requirements shall be constructed
according to requirements in chemical industry.
d) Lining quality of glass reinforced plastic shall comply with the following requirements:
1) Lining layer and body surface shall be adhered tight, free of delimination, bubble, white
point, unsafe solidification and exposure of glass fiber. It can be checked by slightly knocking
with hand hammer with weight below 0.25kg, compact echo demonstrating firm coherence, and
bad binding in other conditions. Those lining layer with large-area air bubble or delimination shall
be completely removed and coated with cloth again after surface treatment. Repairing number in
the same position shall not exceed twice.
2) Glass reinforced plastic lining shall be smooth, sleek and with even color, and rubber
content mustn't be below 50% (w/w).
3) It shall pass creepage test under test voltage higher than 15kY.
4) The number of air bubble with diameter lower than 5mm shall not exceed 3 per square
meter.
5) It shall be dry, compact and smooth by solidification inspection. Complete solidification

26
can be inspected by the method below: wiping glass reinforced fiber surface with cotton dipped
with acetone, those without cotton sticking to them and cotton color not changing will be
qualified.

13.3 Construction of Plastic Products


13.3.1 Machine shaping temperature of rigid polyvinyl chloride shall be generally controlled at
13S"C±S'C, and work piece shall be evenly heated during heating up. Shaping product shall be
free of crack, deformation and charring.
13.3.2 There shall no oil and moisture contained in compressed air used for welding. Out blast
temperature of welding gun shall be generally controlled in the range of210°C~240°C.

13.3.3 Welding rod shall be soft, straight, of the same size, and free of impurity and aging rod.
Welding rod of different diameters shall be used for weldment of different thicknesses:
a) Welding rod with diameter of 2mm shall be chosen for weldment with thickness of
2mm~Smm.

b) Welding rod with diameter of 3mm shall be chosen for weldment with thickness of
Smm~ISmm.

c) Welding rod with diameter of 3mm-4mm shall be chosen for weldment with thickness of
~16mm.

13.3.4 Welding rod and the position of welding line shall be wiped by dichloroethane or alcohol
before welding to removal oil and grease as well as dirties on surface.
13.3.5 After welding, plastic product shall be free of crack, discolouration, charring,
delamination, bubble, and salient knurl. The surface of Welding line shall clean, and welding mark
shall be arranged evenly, closely and consistently with width.

27
14 Startup and Adjustment of Water Treatment System

14.1 Start-up Conditions of Water Treatment System


14.1.1 All items of construction work prescribed in Clause 3.3.5 in this code have been

completed.

14.1.2 Electric, hot working, on-line chemical meter, programmed control and automatic control

equipment related with water treatment system shall be fixed and debugged. It shall be showed

correctly, operated sensitively and functioning.

14.1.3 Before startup of water treatment system, approved adjustment technica I measures for

startup shall be prepared.

14.1.4 Lighting and communication facilities indoors shall meet requirements of test running.

14.1.5 Rotary machine shall be checked out by subsection test running.

14.1.6 When water treatment system is started under environmental temperature below 5·C,

reliable heating and anti-freezing measures shall be adopted.

14.1.7 All pipelines and equipments shall be color code all ready according to design regulations,

and flow direction of medium shall be marked clearly.

14.1.8 Before startup of water treatment system, all equipments and systems shall be checked

and accepted by debugging personnel. Construction corporation shall complete product

preparation; watchers or analysts shall be examined up to eligibility by training; serial number of

equipment shall be tagged; regulations about operating maintenance and weaving register report

forms have been pressed completely; analytical and assay instruments and appearances shall be all

ready.

14.2 Startup and Adjustment of Pretreatment Equipment of Raw Water


14.2.1 Adjustment of clarifier (tank)
a) According to water quality of raw water and chemicals type, lab-scale test shall be carried
through to determine dosage of chemicals.
b) Through adjustment test, reasonable control data and running mode of load, effluent water
quality, quantity of chemical feed and sludge discharge cycle shall be obtained.
c) Suitable sludge recycling ratio shall be obtained by running of mechanical accelerated
clarifier via adjusting unseal degree and rotation speed of mechanical stirrer.
d) After clarifier (tank) adjustment, effluent water quality and output pressure shall be up to

28
design regulations.
14.2.2 Adjustment of automatic valveless gravity filter
a) When watering into automatic valveless gravity filter, temporary water pipe shall be used
to reverse watering in order to soaked filter cake from bottom to top.
b) Rinsing strength, rinsing time, siphon formation time and filter operation period shall be
adjusted and measured via the adjustment of automatic valveless gravity filter. Effluent water
quality and equipment output pressure shall be up to design regulations.
14.2.3 Adjustment of mechanical filter:
a) Backflushing strength, backflushing time and operation period, misfunctioning pressure
difference between inlet and outlet, effluent water quality, and equipment output pressure of
mechanical equipment shall be adjusted and measured.
b) Backflushing strength, effluent water quality and equipment output pressure shall be up to
design requirements after adjustment test.
14.2.4 Adjustment of fine sand, activated carbon and security filter:
a) Turbidity of backflushing water for fine sand filter and activated carbon filter shall
comply with design requirements. And backflushing strength shall be controlled to prevent
carrying of filtering materials.
b) Product water of reverse osmosis shall be adopted for security filter, and backflushing
strength shall be controlled according to manufactory indication.
c) Misfunctioning pressure difference of fine sand, activated carbon and security filter shall
be controlled according to design regulations or manufactory indications. Those without concrete
regulations can refer to the following data: maximum pressure differences for fine sand, activated
carbon and security filter are 0.\ MPa, 0.042MPa and 0.176MPa, respectively. Controlling data can
al so be fixed by test running.
d) During stoppage, fine sand filter and activated carbon filter shall be operated for I h~2h
everyday and backflushed once a weak.
14.2.5 Adjustment of fibrous filter
a) Preliminary water filling startup of fibrous filter shall be carried out according to
regulations of manufactory documents.
b) Pressure difference between inlet and outlet shall be maintained at about 0.05MPa during
filter rinsing.
c) After operation adjustment, operation period shall be fixed, and effluent water quality as
well as equipment output pressure shall be up to design requirements.
14.2.6 Startup and adjustment of electrodialysis equipment.
a) Startup and adjustment of electrodialysis equipment can be carried out on the promise that
operation of raw water pretreatment equipment is stable and effluent water quality complies with
requirements.
b) Earthing of membrane stack, pipe frame, metal pipe and electrical cabinet shall be
checked and accepted. Voltage and frequency of electric source shall be fixed, and connections
between cable and polar plate bolt shall be inspected.
c) Inlet pipe and membrane stack shall be completely rinsed before startup of electrodialysis
equipment, and than direct current voltage can be applied. Electric source must be firstly shut
during stoppage, and then water can be stopped after membrane stack rinsing.
d) Influent and effluent water quality of electrodialysis equipment shall be periodically 01'

29
continuously measured.
e) Time intervals for electrode switching shall be determined according to water quality and
process operation cond itions.
t) Acid cleaning shall be used when desalting ratio decreases 5%, and disassembly cleaning
shall be employed if acid cleaning malfunctioning. Water quality and chemical impurity quality
for membrane stack rinsing shall be on the promise of not inducing ion exchanging membrane
pollution.
g) Membrane stack shall be kept wet during stoppage of electrodialysis equipment to prevent
dryness and deformation.
h) Items of adjustment test:
1) Detection of membrane stacks voltage.
2) Voltage value and effluent water quality corresponding to limited current.
3) Voltage value and effluent water quality corresponding to limited current under different
water quality conditions.
4) Desalting ratio.
S) Recovery ratio.
14.2.7 Startup and adjustment of reverse osmosis equipment.
a) All water equipments, tanks and pipes in system shall be rinsed by clean water; chemical
feeding and cleaning system shall be debugged and accepted.
b) Operation of high-pressure pump and membrane module can only be carried out on the
promise that operation of prepositive pretreatment equipment is stable and effluent water quality
complies with regulated indexes of reverse osmosis equipment manufactory.
c) When newly-mounted equipment is started, shell of pressure vessel, pipe and cleaning
system shall be cleaning up by clean water firstly, then membrane module can be installed, and
then low-pressure rinsing is adopted to make air out. High-pressure pump can only be stalted after
air is totally displaced and pipe system is free of leakage. When equipment is stopped, product
waler of reverse osmosis equipment shall be used to rinse membrane module for I Omin~20min
after the stoppage of high-pressure pump.
d) Protective measures shall be taken to prevent abrupt increasing of system internal pressure
damaging membrane module during high-pressure pump staltup and system switching. Inlet water
pressure of membrane module shall be adjusted to permissible range of design.
e) Membrane module shall be dipped in qualified water with temperature of 5·C~30·C

during short-term stoppage of reverse osmosis membrane, and it shall be operated for I h~2h
everyday and rinsed once a weak. For long-term stoppage, membrane module shall be rinsed, and
then membrane elements shall be fetched out of the shell of pressure vessel and placed into
double-layer plastic bag with protection liquor. Then fasten the plastic bags and place them in cool
room. Protection liquor concentration and conditions of membrane element shall be periodically
inspected.
t) Performance test with 48-hour continuous operation under different operation modes
(series or parallel connections) shall be carried out according to given pressure, flow rate and
temperature. Product water quality and quantity shall comply with design values. Desalting ratio
and recovery ratio shall also be calculated.

30
14.3 Adjustment of Desalting Equipment
14.3.1 Tank and pipe in regeneration system shall be flushed and qualified in tightness test.
14.3.2 Clean water suction test or flow adjustment test shall be carried out for injector or
metering pump in regeneration system, and regeneration liquor can't be fed into metering box
before qualified test.
14.3.3 Acid or alkali pretreatment of ion exchange basin before operation shall depend on
quality and manufactory of the basin.
14.3.4 Regeneration dosage shall be 1.5~2 times of designed regeneration dosage for the first
regeneration of ion exchange basin.
14.3.5 Automatic control system of desalting system shall be debugged before charging of ion
exchange basin into ion exchanger by thermal professionals accompanied with chemical
professionals.
14.3.6 After adjustment of desalting equipment, effluent water quality and output pressure of
each pressure shall be up to design requirements.

14.4 Adjustment of Condensation Water Treatment Equipment


14.4.1 Except for Clause 14.3.3, other clauses in Section 14.3 of this code are all su itable for this
section.
14.4.2 Water cap installation shall be inspected before charging of ion exchange basin into
condensation water treatment equipment or system. Water cap, if loosen, shall be screwed down
and cleaned stage by stage.
14.4.3 Ion exchange basin shall be pretreated before usage.
14.4.4 Feeding test shall be carried out for ion exchange basin in each ion exchanger before
usage.
14.4.5 Severe polluted condensation water shall be completely discharged in the initial phase of
test running of new machine set. Condensation water feeding into its treatment equipment shall
depend on make-up capacity of desalting water and quality of condensation water. In general, iron
content in condensation water shall not exceed 400flg/L.
14.4.6 Misfunctioning ion exchange resin in exchanger shall be loosened by compressed air
before transportation duo to serious compaction.
14.4.7 After adj L1stment of condensation water treatment equipment, effluent water qual ity and
output pressure shall be up to design requirements.

31
15 Hydrogen-producing Equipment

15.1 General Regulations


15.1.1 Fire fighting and explosion protection of hydrogen-producing room and adjacent area
shall comply with requirements ofGS 4962, GB50177 and DL5009.1.
15.1.2 Electrolysis room shall be isolated from open fire or electrical devices and monitoring
meters that may generate sparks. The type, wiring and grounding of electrical devices and thermal
meters shall comply with requirements of Workman Protection (87) No. 36 and GB50 177.
15.1.3 Striking fire-ban symbol shall be set adjacent to hydrogen-producing station according to
regulations of GB2894.
15.1.4 Special valve for gas shall be chosen for hydrogen-producing system to ensure gastight.
Cooper and aluminum materials are forbidden for valve and gasket of electrolyte system.
15.1.5 Hydrogen pipe and oxygen pipe shall be isolated by incombustibles when parallel laid, or
the distance between them shall be no less than 500mm. Minimum parallel clearance between
valves, flanges or other mechanical connections of these two pipes can be reduced to 250mm in
the condition of staggering for a certain distance, and hydrogen pipe shall be arranged in outside.
Hydrogen pipe shall be located above for layered laying.
15.1.6 Red lead and other anti-corrosion paint mustn't be brushed on internal surface of
equipment and pipe contact with electrolyte. They, if brushed, shall be completely removed before
assembly.
15.1.7 Purity of nitrogen and carbon dioxide used for exchange shall be higher than 98% and
95%, respectively.
15.1.8 Desalting water shall be adopted for electrolysis of hydrogen-producing equipment.
15.1.9 Concentration of electrolyte shall be maintained in the following range: potassium
hydroxide 300g/L~400g/L (specific gravity 1.20~ 1.25), or sodium hydroxide 200g/L~260g/L

(specific gravity 1.20-1.25). Potassium hydroxide or sodium hydroxide shall be chemical pure or
analytical pure. 2g potassium dichromate (analytical pure) shall be added per liter of electrolyte.
15.1.10 Insulations between electrobath and earth as well as between terminal polar plate and
tension screw shall be measured by tramegger of 500Y, and insulation resistance shall be higher
than 1MD.
15.1.11 Short circuit between adjacent modules of electrobath is forbidden.
15.1.12 Carbon tetrachloride Iiqllor shall be filled in insolating container.

15.2 Inspection and Installation of Hydrogen-producing Equipment


15.2.1 Equipment and parts shall be detailed checked before assembly, and their specs and
technical conditions shall comply with design requirements.
15.2.2 Safety valve shall be disassembled for oil stain removal, the tightness of which shall be
checked. Movement pressure of safety valve shall be 0.05MPa~0.1 OMPa higher than working
pressure.
15.2.3 Pressure gage of hydrogen-producing system shall be cleaned by alcohol or gasoline, and
calibrated by water or alcohol.
15.2.4 Guide in pressure adjuster shall be free of distortion and deformation. Hydraulic pressure

32
test shall be carried out for pontoon, and two nuts shall be mounted to fasten connections between
guide and pontoon. Distance between pontoon and needle valve shall be properly adjusted to
maintain water level of pressure adjuster adjacent to central line of nilometer.
15.2.5 Installation requirements of electrobath.
a) Inspection before assembly.
1) Nickel layer on anode side shall be contact and free of oil stain on its surface.
2) Nickel layer in insulating case and sealing waterline shall be contact. Gas-guide hole and
electrolyte flow hole shall be straightway, and asbestos cloth shall be tightened and qualified in
transmission test.
3) Two-electrode plate and main electrode plate shall be smooth, and those with roughness
can only be leveled up by wood hammer.
4) Asbestos rubber gasket or polytetrafluoroethylene gasket shall be smooth and free of
fold. These gaskets shall not be cut by joint method.
b) Thermal screwing requirements for electrobath.
1) Installation of temporary vapor source and pipe shall guarantee that electrobath can be
evenly heated and prescribed temperature can be reached.
2) Thermal screwing temperature for electrobath using asbestos rubber plate or
polytetrafluoroethylene plate as gasket shall be IJO"C and 95"C, respectively.
3) Thermal screwing time shall be J6h~48h. Spring leaf stress shall be in the prescribed
range of manufactory after thermal screwing. Lengths of four tension screws between two
terminal polar plates shall be equal, with permissible error of ± Imm.
4) Cold screwing shall be carried out when natural cooled below 50·C after thermal
screwing, and hydraulic pressure test shall be carried out by desalting water or condensation water
under 1.5 times of working pressure after cooling to room temperature. Electrobath shall be free of
leakage.
15.2.6 Pressure adjuster, separator, cooler and hydrogen tank shall be cleaned up until free of
such impurities as rust, welding slag and paint before installation. Nondestructive evaluation test
shall be carried out for welding crater of equipment before leaving factory according to
regulations of Boiler No. 154 Documents issued by China State Bureau of Quality and Technical
Supervision (1999).
15.2.7 Requirements for pipe installation.
a) Pipe, valve and pipe fittings shall be free of cracks, scale and residual slag. The surface
contact with gas shall be cleaned up.
b) Except for connections with equipment and valve flanged or threaded, other connections
shall all be welded. Argon-arc welding shall be adopted for primer of carbon steel pipe and
stainless steel pipe.
c) Both ends of long metal pipe or members shall be earthed, and flanged connections shall
be bridged by metal lead.
d) Smooth 1Cr 18Ni9Ti stainless steel pipe shall be chosen for hydrogen pipe with gradient
higher than 0.3%. Discharging gate shall be mounted in the lowest position of the pipe.
e) Anti-freezing measures shall be taken for hydrogen pipe in cold region.
l) Tightness test under 1.25 times of working pressure, or gas tightness test under 1.05 times
of working pressure shall be carried out by desalting water or nitrogen after installation. Qualified
installation in gastightness test shall meet the following requirements: test pressure will not
decrease for 10 minutes after gas make-up stopped, or average leakage rate is below 0.1 % per
hour after gas make-up stopped for 24 hours.
g) Cold screwing shall be carried out to make distance between the two terminal polar plates
comply with manufactory requirements after emplacement of medium-pressure electrobath.

15.3 Startup and Adjustment of Hydrogen-producing Equipments


15.3.1 Startup conditions of hydrogen-producing equipment.
a) Electrical devices, thermal meters, illumination and communication, ventilation devices
and firefighting facilities shall be provided, debugged and accepted by professionals.
b) Relevant safety regulations, operation regulations, chemicals, analyzers, records and
report forms and displacing gas shall all be available.
c) Preliminary adjustment of pressure adjuster shall be finished, and guide movement shall
be flexible and free. Microcomputer operation controlling system shall be debugged and accepted
for medium-pressure hydrogen-producing equipment.
d) Electrolyte shall be filled in electrobath and alkali liquor system after washed up by
desalting water (or condensation water).
e) Air in system shall be completely displaced by nitrogen. Water displacement or gas
displacement method shall be employed for gas tank, and anti-freezing measures shall be taken in
winter.
f) Oil-free compressed air system sl1all be swept up.
g) Electrodes of electrobath shall be activated.
15.3.2 Startup and operation of hydrogen-producing equipment
a) Load shall be slowly enhanced after electrification of electrobath, and pressure shall not
be increased until bath temperature reaching 50°C and the slowly increased. After system pressure
reaches rated value, the following inspection and test shall be carried out:
1) Tightness of system and equipment
2) Liquor level of pressure adjuster shall comply with requirements.
3) Automatic water makeup of make-up tank.
4) Operation parameters of electro bath shall all reach prescribed requirements on
nameplate.
b) Internal pressure of pressure adjuster shall be higher than internal pressure of gas tank for
gas feeding into gas tank from hydrogen-producing tank.
c) Maintenance of hydrogen-producing equipment, if necessary, shall be strictly in
accordance with fire management regulations and fire permit system established by electric power
plant. Hydrogen content in system and fire area must be lower than 0.4% for the prevention of fire
or explosion accident.

34
16 Chemical Cleaning of Heating Equipment and System

Chemical cleaning of heating equipment and system shall comply with regulations in DLiT
794.

35
17 Chemical Supervision during Startup and Test Running of

Heating Equipments

17.1 General Regulations


17.1.1 Quality standard for water used for hydraulic test of boiler entity.
a) Desalting water must be adopted for utility drum boiler and once-through boiler with
steam pressure equal to or higher than 13.7MPa.
b) Desalting water by mixed bed treatment following primary desalination shall be adopted
for boi IeI' of austenitic steel.
c) Hydrazine of 200mg/L-300mg/L shall be added into desalting water, pH value of which
shall be adjusted to I O~ 10.5 by ammonia later.
17.1.2 Chemical water treatment equipments shall be able to produce water before chemical
cleaning of heating system to guarantee provision of qualified water for chemical cleaning.
17.1.3 Chemical feeding and treatment equipment as well as chief chemical supervision meters
for water supply, fire, condensation water and cooling water in electric generator shall be put into
operation in the same time of machine set staItup. Chemical feeding equipment and rubber ball
cleaning device for circulating water shall be put into service during large-load test running.
17.1.4 Backflush shall be carried out for overheater of boiler with backflush device before
preliminary startup of chemical cleaning for the boiler. Ammonified desalting water with pH value
maintained in the range of9~ 10 shall be employed as backflush water, and backflush effluent shall
be clear and colorless.
17.1.5 Time interval between hydraulic pressure test and chemical cleaning for boiler shall be
shortened as much as possible. ln general, time interval between chemical cleaning completing
and boiler ignition shall not exceed 20d, and anti-corrosion protective measures shall be taken if
time interval exceeds this range.
17.1.6 Cold-state flushing and hot-state flushing shall be carried out for heating system before
the first startup of new mach ine set.
17.1.7 Sweeping and flushing for deaerator water tank and steam condenser bottom shall be
reinforced during test running of new machine set. Drainage or water exchange of the whole boiler
shall be enhanced until clarification of boiler fire, and chemical feeding treatment in boiler shall
also be strengthened.
17.1.8 Deaerator shall be put into operation during test running of new machine set, and it shall
be functioning in the stage of 72-hour or 168-hour test running.
17.1.9 Sampling of test running stage of new machine set.
a) For comprehensive sampling cabinet combined integrated water and vapor sampling
system with automatic monitoring, automatic thermostat of water and vapor sampling device shall
be qualified in sub-section test running before put into operation.
b) Sampling tube shall be washed out by rinsing pipe before secondary valve of sampling
device.
c) Opening of cooling water valve for each sampling tube shall be properly adjusted.
Qualified on-line analyzing meter can only be put into service after working condition of the

36
system is relatively stable.

17.2 Quality Standard of 'Vater and Vapor for Newly-built Machine Set during
Test Running
17.2.1 No quality standard for feed water, boiler water and steam is provided during boiler
ignition, main steam tube purging and relief door setting at present. Heating system shall be rinsed
until effluent is clear before boiler ignition.
17.2.2 Silicon dioxide content in superheated steam shall not exceed IOOf.lg/L during
rotation-impulsing for steam turbine.
17.2.3 During united startup of machine set, feed water quality shall be executed according to
Table I for the set with 1/2 rated load or above.
Table 1 Quality Standard for Feed Water

~)
Utility drum boiler Once-through boiler
Remarks
Item ::: 137 137-183 183-225 >22.5

Dissolved oxygen After 1/3 rated loading


<30 <20 <10 <10
flg/L of machine set
Iron
<80 <50 <30 <20
!lg/L
Hardness
::::0 ;::0 ::::0 ::::0
Il mol/L

pH 8.8-9.3 8.8-9.3 8.8-9.3 90-9.2

Hydrazine
10-50 10-50 10-50 20-50
~lg/L

Silicon dioxide
<60 <50 <30 <20
flg/L
Conductivity (25'C, after
hydrogen ion exchange) <04 <0.4 <0.3 <0.3

fl S/cm

17.2.4 Quality of boiler water shall be executed following Table 2 according to working pressure
of utility drum boiler during united startup of machine set.
Table 2 Quality standard for water in utility drum boiler
Drum pressure Salinity Sil icon dioxide Iron Phosphate
Treatment method pH
MPa mg/L mg/L Ilg/ L mglL
137-156 Phosphate treatment S50 :::;:150 _100 2-8 9-10
157-18.3 Phosphate treatment S20 so 25 - 300 05-3 9·-10
>18.3 Volatilization treatment gO SO.20 S300 90-9.5
17.2.5 During united startup of machine set, condensation water recovery shall be on the
promise of not influencing feed water quality for those sets without condensation water treatment
equipments. It shall be generally executed following Table 3.
Table 3 Quality standard for recovery condensation water and drainage water
Iron Dissolved oxygen Silicon dioxide Hardness
Appearance
flg/L flg/L flg /L flmol/L
o suspended substances S80 S30 :::;:80 :::;:10

37
17.2.6 Quality of internal cooling water of electric generator shall be executed according to
Table 4 during united stal1up of machine set.
Table 4 Quality standard for internal cooling water of electric generator
Conductivity (2S"C) Hardness Copper
pH (2S"C)
fl S/cm flmol/L flglL
~2.0 gO _40 ~6.8

17.2.7 Vapor and water quality shall be executed according to relevant regulations In GB/T
12145 after 72-hour or 168-hour test running of united operation of machine set.

17.3 Heating Equipment Protection during Layoff Period or Standby Period


17.3.1 The following anti-corrosion measures shall be taken for heating system before boiler
when once-through boiler and utility drum boiler with working pressure above 13.7MPa are
stopped.
a) For short-term stoppage (namely, in the range of J 5d~30d), ammonia - hydrazine method
can be taken for protection (isolated copper tube heat exchanger).
b) For long-term stoppage (namely, more than 30d), nitrogen or gas-phase corrosion
inhibitor filling method can be adopted for protection.
17.3.2 When boiler is interrupted during test running, the following method can be employed for
protection.
a) Methods for shol1-term stoppage.
1) Dry method for protection: remaining heat drying method by discharging water, hot wind
drying method, and dry wind drying method. Decompression rate, pressure and temperature for
discharging shall be fixed according to permissible temperature difference of boiler drum wall or
heating surface. Better drying effects can be achieved by hot wind drying or vacuumization
following water discharging.
2) Wet method for protection: ammonia - hydrazine method. Solution is prepared with
desalting water with hydrazine concentration of 200mg/L~300mg/L, then pH value of which is
adjusted to 10-10.5 by ammonia.
b) Method for Long-term stoppage.
1) Dry method for protection: Nitrogen purity for nitrogen filling method mustn't be lower
than 99.5%, and system pressure shall be maintained in the range of 0.02MPa-0.05MPa after
nitrogen filling. Gasified gas-phase corrosion inhibitor shall be filled into boiler after the drying of
boiler, and gas filling shall not be stopped until inhibitor contents in each part of boiler reaching
setting value. Then seal the boiler.
2) Wet method for protection: The same as regulations in 2) of Clause 17.3.2 a).
17.3.3 During test running of machine set, standby protection of heating equipment shall refer to
SD223 to select simple, convenient, reliable and effective protective method according to site
practical conditions.

17.4 Operational Requirement for Oil Equipment and Oil Quality


17.4.1 Checkup of oil equipment and system.
a) Rust, iron filings, sediment and other impurities accumulated in internal wall shall be
removed before assembly of oil system.
b) Chemical cleaning shall be carried out for oil system of steam turbine strictly according to

38
approved chemical cleaning measures.
c) Qualified steam turbine oil shall be coated for oil equipment and system unable to be
timely installed after cleaning or sweeping, and then they shall be temporarily sealed.
d) Steam turbine oil, fire-resistant oil, insulating oil and mechanical oil shall all comply with
relevant national quality standards.
e) Oil equipment and system shall be inspected before oil injection to make sure that they
meet oil injection conditions, and oil trademark and quality both comply with application
requirements. Equipment and system shall be washed by qualified oil firstly and then oil can be
injected.
f) Sizing test of oil shall be carried out before test running of machine set with load after oil
circulation rinsing, and granularity shall comply with requirements.
17.4.2 Acceptance, application and storage of oil.
a) Oil of different trademarks shall be stored in different storage tank. Oil mixing, if
necessary in special cases, can only be carried out after oil mixing test.
b) Oil shall be stored in by its sort, and kept away from heat source, inflammables, sunshine,
and rain to prevent oil from deterioration.
c) Oil tank and barrel shall be obviously labeled to give clear indication of oil category,
source, quantity and inspection certificates, and sealed tightly for storage. Oil without label or
unqualified mustn't be used. Mixing of oil barrel is forbidden.

17.5 Requirements for Environmental Protection


17.5.1 Drainage of various water treatment, wastewater treatment and chemical cleaning waste
liquor of heating system shall comply with GB 8978 and local pollutants drainage standard.
17.5.2 Toxic and harmful wastewater mustn't be drained by overflow, leaching well, seepage pit,
abandoned mine or dilution.
17.5.3 Waste liquor or sludge discharged from water or wastewater treatment shall be stored in
special stacking site and mustn't be dumped arbitrarily. Comprehensive utilization is favorable.
Measures to prevent flying ash and leakage shall be taken in special stacking site.
17.5.4 Discharged pollutants shall be monitored according to DL4J4 during pilot running.
17.5.5 Newly-built, enlarged and rebuilt project as well as construction project discharging
pollutants to waters directly or indirectly must observe national environmental protection and
management codes related to construction project. Environmental protection and controlling
facilities shall be put into operation in the same time of construction project put into production or
service.
17.5.6 Environmental protection facilities corresponding to project of stepped construction.
putting into production or service shall be checked and accepted accompanied with main work.

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18 Acceptance of WOI'k

18.1 The following materials, duplicates and fittings shall be handed over from supervision,
construction and troubleshooting unit.
a) Instructions and drawings of design modification.
b) Equipment installation record and acceptance certificate for subsection test running.
c) Adjusting test report of water treatment system and hydrogen-producing equipment.
d) Quality determination results of chemical cleaning for boiler body and heating system
before boiler.
e) Chemical supervision and adjusting test report during startup and test running of machine
set.
f) Supervision reports.
g) Extraworks acceptance cel1ificate and indications of equipments
h) Standby, fittings and special tools equipped with equipment by manufactory.
18.2 Water treatment equipment and hydrogen procuring equipment can be accepted and handed
over to production unit as unit project after installation and test running.

40
Appendix A(Normative Appendix)

Filtering Material
A.l Filtering material shall comply with design requirements. In the case without design
regulations, it shall be selected according to chemical stability and mechanical strength. General
requirements are as follow:
A.I.l Quartz sand can be adopted for water after agglomerate treatment.
A.I.2 Marble or anthracite coal can be adopted for water after lime treatment.
A.I.3 Dolomite or anthracite coal can be adopted for water after silicon removal by magnesia
mixture.
A.I.4 Anthracite coal can be adopted as filtering materials for phosphate or salt filter.
A.I.5 Quartz sand can be adopted as bedding in the bottom of ion exchanger and activated
carbon fi Iter.
A.2 Chemical stability test in acid, alkali and neutral solutions shall be carried out for quartz
sand and anthracite coal. Chemical stability test in alkali and neutral solutions shall be carried out
for marble and dolomite. After 24-hour dipping, filtering materials shall respectively comply with
the following requirements:
A.2.1 Increment of total solids shall not exceed 20mg/L.
A.2.2 Increment of silicon dioxide shall not exceed 2mg/L.
Note: Test method: Respectively add 500mL the following three kinds of solution into three conical beakers
(700mL-1 OOOmL): HCI of 400mglL (prepared by HCI with specific gravity a I' 1.19); NaOH of 400mg/L; NaCI of
500mg/L Then add 109 tiltering materials (with grain size in the range of 0.5mm-1 mm) to each beaker under
20'C. and shake the beaker for each 4 hours Take out filtrate after 24-hour dipping, and analyze total solids.
silicon dioxide and oxygen consumption.
A.3 Quartz sand in bedding of ion exchanger and activated carbon filter shall comply with the
following requirements: A.3.1
A.3.1 Purity: Silicon dioxide ~99%

A.3.2 Qualified in chemical stability test.


Note: Chemical stability test: Add 100g quartz sand (with grain size in the range of 0.5mm-lmm) and
100mL hydrochloric acid of 5% into beaker of 250mL. rinse them to neutrality after 4-hour dipping under 20·C.
and drain off Then add 400mL sodium hydroxide solution of 5%, rinse them out by water free of silicon after
4-hour dipping under 40'C. drain off. and bake to dry. Take 50g sample disposed by above procedures and place it
into plastic bottle of I OOOmL, then add 500mL water free of silicon, store under 20·C. and shake the blend for each
4 hours. Increment of silicon dioxide in the solution of qualified product shall not exceed 2011glL after dipping for
24 hours.
A.4 Constitutes of filtering materials shall comply with manufactory or design requirements.
Those without regulations shall comply with regulations in Appendix Table A.I.

41
Table A.I Granularity of Filtering Materials

Serial Grain size Nonuniformity coefficient
Category
number mm KRIJ
Quartz sand dm",=0.5 d","x=I.O
Monolayer filtering Marble d"",,=0.5 dnlnx=I.O
I 20
materials Dolomite d"",,=0.5 d",,,,.= 1.0
Anthracite coal dnlll,=0.5 d",nx= 1.5
Doublelayer filtering Anthracite coal dni l/l=0.8 dmnx= 1.8
2 2-3
materials Quartz sand d"III1=0.5 d",nx= 1.2
A.S Granularity uniformity test shall be carried out for filtering materials before charged into
filter, and test result shall comply with the following standard:

A.S.I Nonuniformity coefficient of filtering materials in unifJow type filter [d so : shall be


diD

below 2;

A.S.2 Nonuniform ity coefficient of fi Itering materials in bidirectional flow type fi Iter (d J80
diD

shall be 2~3;

Note: d so and diD are sieve pores that 80% and 10% tiltering materials can pass through. respectively.

A.6 Granularity of supporting layer shall comply with regulations in Appendix Table A.2 if
supporting layer structure is adopted for fi Iter (tank).
Table A.2
Layer Granularity Layer Granularity
(from above to below) mm (from above to below) mm
I 2-4 3 8-16
2 4-8 4 16-32

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