INTERNATIONAL

STANDARD
INTERNATIONAL ORGANIZATION FOR STANDARDIZATION
ISO (the International Organization for Standardization) is a worldwide federation
of national Standards institutes (ISO Member Bodies). The work of developing
International Standards is carried out through ISO Technical Committees. Every
Member Body interested in a subject for which a Technical Committee has been set
up has the right to be represented on that Committee. International organizations,
governmental and nongovernmental, in liaison with ISO, also take part in the work.

Draft International Standards adopted by the Technical Committees are circulated

to the Member Bodies for approval before their acceptance as International
Standards by the ISO Council.

International Standard iTeh STANDARD PREVIEW

ISO 2517 was drawn up by Technical Committee
ISO/TC 47, Chemistry, and circulated to the Member Bodies in August 1971.
(standards.iteh.ai)
lt has been approved by the Member Bodies of the following countries :
ISO 2517:1974
Austria Ireland South Africa, Rep. of
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Belgium Israel Spain
c7982af8cb95/iso-2517-1974
Egypt, Arab Rep. of Netherlands Switzerland
France New Zealand” Thailand
Germany Poland United Kingdom
Hungary Portugal U.S.S.R.
I ndia Romania

* Disapproved clause 4.

No Member Body expressed disapproval of the document.

0 International Organkation for Standardkation, 1974 l

Printed in Switzerland
 INTERNATIONAL STANDARD ISO 25174974 (E)

Diacetone alcohol for industrial use - List of methods of test

1 SCOPE AND FIELD OF APPLICATION If it is necessary to seal this bottle, care shall be taken to
avoid the risk of contamination.
This International Standard specifies methods of test for
diacetone alcohol (4-hydroxy-4-methylpentan-2-one)
[ (CH&C(OH)CH2COCH3] for industrial use.
4 DETERMINATION OF DISTI LLATION CHARAC-
TERISTICS
2 REFERENCES
Use the method specified in lSO/R 918, subject to the
lSO/R 758,Method for the determination of density of
liquids at 20 “C. iTeh STANDARD PREVIEW following modif ications appropriate for diacetone alcohol.

lSO/R 759,
evapora tion
(standards.iteh.ai)
Method for the determination
on a wa ter bath.
of residue on 4.1 Thermometer (See 3.2 in lSO/R 918)

Use a thermometer conforming to the requirements of

lSO/R 760, Determination of water by the Karl ISO 2517:1974lSO/R
Fischer 198, with a scale including the range 125 to 175 “C
method. or any other suitable range.
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ISOIR 918, Test method for distiflation c7982af8cb95/iso-2517-1974
(distillation yield
4.2 Distillation (See 6.1 in ISO/R 918)
and dis tilla tion range).
The interval before the first drop of distillate falls from the
ISO 22 11, Liquid Chemical products for industrial use - end of the condenser shall be 5 to 10 min.
Measurement of colour in Hazen units (platinum-cobalt
scale). 4.3 Correction to be applied to the temperatures (See 7.2
in ISO/R 918)
ISO 2518, Diacetone alcohol and hexylene glycol for
industrial use - Test for miscibility with water. The correction is equal to

ISO 2887, secßutyl alcohol, methyl ethyl ketone, isobutyl

0,05 (760 -pl) “C
me thyl ke tone, i soamyl e thyl ke tone, diace tone alcohol and
or 0,04 (1 013 -p2) “C
hexylene glycol for industrial use - Determination of
acidity to phenolphthalein - Volumetric me thod.
where

pl is the barometric pressure in millimetres of mercury;

3 SAMPLING
p2 is the barometric pressure in kilopascals?
Follow the principles given in ISO . . .1). Attention is
drawn to the following recommendation : place the NOTE - It is essential that the distillation flask shall be clean and
laboratory Sample, representative of the material taken free from carbon deposits so as to minimize decomposition during
distillation. This tan be achieved by carrying out several
from the bulk, in a clean, dry, dark coloured, predistillations with the material before the test and by reserving
glass-stoppered bottle of such a size that it is nearly filled particular flasks for the purpose of the distillation test for diacetone
by the Sample. alcohol.

1) In preparation.

2) 1 kPa = 1 kN/m2.
ISO 2517-1974 (E)

5 DETERMINATION OF DENSITY AT 20 “C 10 DETERMINATION OF ACIDITY TO PHENOL-

PHTHALEIN
Use the method specified in ISO/R 758.
Use the method specified in ISO 2887.

6 DETERMINATION OF RESIDUE ON EVAPORATION

ON A WATER BATH

Use the method specified in ISO/R 759.

11 TEST REPORT
7 DETERMINATION OF WATER CONTENT
The test report shall include the following particulars in
Use the ketone modification of any of the methods relation to each test :
specified in ISO/R 760.
a) the reference of the method used;

b) the results and the method of expression used;

8 MEASUREMENT OF COLOUR
4 aw unusual features noted during the
Use the method specif ied in ISO 2211.
determination;

d) any Operation not included in this International

9 TEST FOR MISCIBILITY WITH WATER
Standard or the documents to which reference is made,
Use the method specified in ISO 2518. or regarded as optional.

iTeh STANDARD PREVIEW

(standards.iteh.ai)
ISO 2517:1974
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c7982af8cb95/iso-2517-1974