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Salt Analysis Microbit

The document provides a detailed guide for the analysis of anions and cations in chemistry practicals, including identification and confirmation tests for various ions. It outlines specific reagents and observations for identifying ions such as Carbonate, Acetate, Chloride, Nitrate, Sulphate, and several cations including Ammonium, Lead, Copper, Aluminium, Zinc, Barium, Calcium, and Magnesium. Additionally, it includes promotional information for a booster batch course in Kerala.

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deepakkmanoj69
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127 views5 pages

Salt Analysis Microbit

The document provides a detailed guide for the analysis of anions and cations in chemistry practicals, including identification and confirmation tests for various ions. It outlines specific reagents and observations for identifying ions such as Carbonate, Acetate, Chloride, Nitrate, Sulphate, and several cations including Ammonium, Lead, Copper, Aluminium, Zinc, Barium, Calcium, and Magnesium. Additionally, it includes promotional information for a booster batch course in Kerala.

Uploaded by

deepakkmanoj69
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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dafsg

icro
M Bi t
+ 2 chemistry
Practicals
salt analysis

കേരളം
പഠിക്ക ട്ടെ

കൂടുതൽ ലാബ് നോട്ടുകൾ ലഭിക്കാനായി ക്ലിക്ക് ചെയ്യൂ


MicBroi t
dafsg

Analysis of Anions

(Identification)

Step v
Obser ation Anion

Carbonate
Dil. HCl Bubbles
(CO₃²⁻ )

Dil. H₂SO₄ rub with Acetate


Vinegar smell
watch glass (CH₃COO⁻ )

Colourless gas,
Conc. H₂SO₄ & Warm with NH₄OH give Chloride (Cl⁻ )
white fumes

Conc. H₂SO₄, heat,


Brown gas Nitrate (NO₃⁻ )
add paper ball

White ppt,
Sulphate
BaCl₂ Solution insoluble in
(SO₄²⁻ )
dil. HCl

Analysis of Anions

(Confirmation)

Step v
Obser ation Anion

White ppt, Carbonate


BaCl₂ Solution
soluble in dil. HCl (CO₃²⁻ )

Neutral Ferric Acetate


Deep Red
chloride solution (CH₃COO⁻ )

Dil. HNO₃ + AgNO₃


White ppt Chloride (Cl⁻ )
solution

Freshly prepared Brown ring


Nitrate (NO₃⁻ )
Ferrous sulphate + between
Conc. H₂SO₄ solution

Lead acetate Sulphate


White ppt
solution (SO₄²⁻ )
MicBroi t
dafsg

Analysis of Cations

(Group Test)
Step Observation Cation
Ammonium
Na₂CO₃ solution No ppt. (NH₄⁺ )

group zero

Lead (Pb²⁺ )
Dil. HCl White ppt group one

Copper (Cu²⁺ )
Dil. HCl + h2S Black ppt group two

White
Excess NH₄Cl + gelatinous Aluminium (Al³⁺ )
NH₄OH ppt group three

Excess NH₄Cl + White ppt Zinc (Zn²⁺ )

NH₄OH add h2S group four

Excess NH₄Cl + White Barium (Ba²⁺ ),


NH₄OH add NH₄₂CO₃ crystalline Calcium (Ca²⁺ )

ppt group Five

White Magnesium

Excess NH₄Cl + crystalline (Mg²⁺ )

NH₄OH add ppt group six

കൂടുതൽ ലാബ് നോട്ടുകൾ ലഭിക്കാനായി ക്ലിക്ക് ചെയ്യൂ


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da

ro
MicBi t
Analysis of Cations

(Identification & Confirmation)


tep
S Obser ation
v Cation
Ammonia Ammonium
NaOH solution, smell, white (NH₄⁺ ) identified
heat fumes with
HCl

Ammonium
Nessler’s reagent Brown ppt. (NH₄⁺ )
confirmed

Dil. Acetic acid + Lead (Pb²⁺ )


potassium Yellow ppt. identified
chromate

Lead (Pb²⁺ )
Potassium iodide Yellow ppt. confirmed

Copper (Cu²⁺ )
NH₄OH dropwise Pale blue identified

lame est paste Copper (Cu²⁺ )


F t

with Conc. HCl


:
Blue flame confirmed

NaOH solution White Aluminium (Al³⁺ )


dropwise gelatinous identified
ppt

Ash est Conc.


t :
Aluminium (Al³⁺ )
HNO , boil, cobalt
₃ Blue ash confirmed
n itrate solution
MicBroi t
dafsg

NaOH solution Zinc (Zn²⁺ )


White ppt identified
dropwise

Ash test: Conc. Zinc (Zn²⁺ )


HNO₃, boil, cobalt Green ash confirmed
nitrate solution

Dil. Acetic acid + Barium (Ba²⁺ )


potassium Yellow ppt. identified
chromate

Flame test: paste Barium (Ba²⁺ )


with Conc. HCl Pale green confirmed

NH₄Cl + NH₄OH + Calcium (Ca²⁺ )


ammonium oxalate White ppt identified

Flame test: paste Calcium (Ca²⁺ )


with Conc. HCl Brick red confirmed

Mangeson reagent Magnesium


+ NaOH solution Blue ppt (Mg²⁺ ) identified

Ash test: Conc. Magnesium


HNO₃, boil, cobalt Pink ash (Mg²⁺ )
nitrate solution confirmed

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