Experiment - 01 (Bim B prpare 250 ml 20. sotubin of Maln’s Sat. Ling his —Solutian find aut the molarity and or y the a KMnDy Solufion i a | Ppparatu» Requived —__ | Bunette , Burctte Stand, Pipett Beoken , Canital flask, Mecuuni 9 Pak, | | Tie, Fuel. Gls te. it gauze, burner, watch f weight bo, fractional weight hoy 1 Moleclor Sayan 2KMnDy + 34,04 ——— K, 0, + 2MnS04-* 34,0 + y+ 34,04 5 [0] FeSD, (NAsj2 S0y- 60 ————> Fe, (50)), + 2INHy), S0y/x5 +H,Dy + [0] ie Sonia = ZKMn0y + 8HyS0y >, Sy + 2Nn SOy + JO Fe Sy (NHy), + SOy-64,0 +5 Fe, (504) Te Ta ic Roy Mn Oy + BHT + be eS I Wraes mae foo pee =] x5 _Maty + BHT 5 Re — Shee EWA Teacher's Signature MohanObservation Weight of Enpty watch qloas a 2,72 yom Weight 4 Watch gloss + MohvS Salt = 26.62 ghoun Weight Mohn's Salt = 4.9 quo Volume g Mehr's Salt solution prepared = 250 mb Molonity of Makn's Salt Solution = 0.05 M iy) \folume 4 Mohn's Salt solution taken fur each Titvotion = 20 ml i aaa Tnitial [Frat | hee a cara ti eS (20m | 0.0. |r. cee 14.9 mk 2} 20m} 8 | 29.4 3] 20m} zo4 | 44 yf} 2om} 44 | se.6 Me molarity g KMnOy Sol” M,= Molarity og Meshx's Salt Sal” ie Volume KMny Sol” = Was Volume Hhn's Saf SoPage No.2. _-_KMnOy ipa sal inca eee, | Lid = Ge do ptt oo hay) | 3 ay Aen Are ws. . ts 7 l fee a ee | Mobw’s Salt = Fe SOy. (My), SOy. 6 HQ ______ ‘Maku, moss of Mobn’s lt = 392 g/mol —— by ion prponing 1000 mo 1M_Mohx’s Salt Solubon ___|_ ____, He _veguived mohars Salt 3492 g—_____ 4 |__2. fix_proparing 250_ Mo Mabr's Salt Sol | Ho Salt Aeguted “= 222 5 250% 4 249 yom a | 4. Prepare 250 ml of 0.05 M_ Maha’ ‘en dissolving 44 gras. of Mohs Salt in wnfey |_2. Rinse the pipette with the 0.05 M Mahs's Salt Solrbian | | __and_pipette out 20 ml of Jt ma_washed tidiabion flosk | 3, Add_ ane _deat- tue (~ 20.md) full of diluted sulphusic | | aud 2M) to Ae Solution in tthasen flak, | 4. Nate te initial fending of the burette. 5. Now add KMn0y solution from burette tilla pomnent sight pink Calaur id imparted to He Solution in the | —ditaation flosk an addition gf fost Single dnap af KMady l* i 6. Note the final Yeadiny of te puretio ——_— he co ee Steps 4-5 times to get 3 seb of ontordent ‘Teacher's Signature+ Glulabion @_Molonity of the _KMnOy Solution daom owrall blanced equation Ut ia Cleon thot Armoles of KMn Oy vequired 10 mates 4 Mohn's Solution JOMM = 2M, Ve My= Melnity af 2M nDy sl” MV, = aM, Vy We ion a M, x 14.6 = ch 0.05 x 20 M, = 0.2 146 M = 0.0136M L, The Malanity § KMny Sal” is 0.0136 M Strength q the KMnOy Sel" Strength = Melarity X Molar Mass Strength = 0.0136 x 158 Strayth = 2.164 pond LitorPage No._3 — Fi Nf AD = ik — Stag of keay = 2.164 gamit te Chan alt the” apparatia worth _dbisth Starbing fhe a then inte with th Satan | MohanPage No.4 Experiment - Cee Tig Fh detect the presente vceeciaate (Als eance ey) fiat ale ste ia = ___¥| | Bppasshus Requived. au ____| Beakon, "Tete, Teat-tube sland, Tat halen Tgp, — _ me | Chinadish_ Filter paper it a A ae ignition tubes —_— ess cae thew ait _Covalently ated in the Organic compound | |__dind_de nat_heponc to iwnic Aeaction Lie | Ihe Cononsion may be accamplished by several methods Organic Compaurd. Ls with_metabtic Sodium inn ignition tube, hiss ——— reac MohanDy Sodium Huss Extract (lossaigre 5 Extract) Take a small piece J Na alang with Grganic Compaurd in vqnition tube. Heat this ignitian dube upto ned hot ord pouk vit into @ china dish “having distilled 1,0. Repeat the Experiment 3-4 times. cf New Gait the content of China cish ond filter tt to get Laspaigne’s Extract 64 ° Sodium fusien extract Tpnition tke Organic. ition att A eo yap Buse De ais 0 Ching dish Step-t - Sodium and OrgonicCompod | Step - Red Host ignition is heated uptd ved hats atime tie ial distibfed Woter Gtep-3. - The Contents baited | Step-4- Filter to get clear fo 5-10 rninutes Sodium fusion extractPage No.5 T+ dasnigne’s extract ib ‘ppased for the eat of Nitacgen 2 __ Suphuwr ancl a ts Convent Organic _Compaund. into | inarganic_ compound (ionic. pe) Aya _| Ti Flemanth pion? in_tovalert Jorn _in_the @ygante Compound ane converted to icnic faoum by fusing ft with_Na_mefaf, eet we Diving the cameron of he Elements into itm josm the SES Sf. tectan fo8 an a Na tot Nt! NatN Nat + CN TNF 6 PS Na, Se HF tS Na + X HS Na x eels Rie Xe Na + C HN 6S Nacns Oe NRSC Teacher's Signatmre ——______— MohanFrys loss vane is fuse with Sodus metal Ly When the Orgone Cony! ; in ie Bee tube, Corban ad Nitnegen fram the ogonic Compound combine to jown Sodium cyanide. wee Ce NERS Nac SEE Nols OH" Selinm cyonnicle Exposinent 2Na0H + FeS0y ———> Fe(OH), + Na, S0y (cist gen!) Fe(OH), + 2NaCN———> Fe((N), + 2NROH Fe (CN), + 4NaCw——+ Nay [Fe Gn ] 5 Sedum ferrocyanicle 3Nhay f Fe (CN i He vf « ( J + 4Fed, a fey [Fen ],+ /2NaU. Fonic- fomocyanicle (Luussieon Blue Colous) © Feunation oy Prussian Blu 2 Or ish i Clean OHE toe pustince. y Neon a Noto :- The yole of HC i» to clissotve di nt, ferrous ide ushi ngenpe Modsks en ate Coke mete tos fe (0H), + HU —— Fell, + 2H,0 (clidy green pp)fee Soliton _audic |sUSRSSSSEACCL EAL ERA ERE a From Lassaigne’ ly When dhe Owanic Compauncl Js ject with Soctium metal in “te alien tube, then Sulphur present in She given GrqavieCempawna gets Corwertec! to farm Sodium Sulphide. 2h +5 —alohs Na,S ems ZN S™ Seclium sulphide Experiment iB Sodium Nitwpruaside teat Na,S + Na; [fe (cn), No] —> Na, [ Fe (Cn), Nos | Sodium thionityo prusicle | (Vialet Calewy) 4 en) Viele? (olawr indicate He presente of 2. Lead acctate teat NaS + (CH Coo), Pb ——> PbS] + 2CH,(00Na learct Sulphide ( Black ppt) ly fewaben of Blk pot incliate fh Sa ne gute ott Conon 9 TTay | — vadileal_ to ial 4 oe odivn fevion_exbrack. Ve Mohan————7=_ | From lassaigne’s Extract ty When the Qrgunic Compound 3 Jused wrth Sockum ! metal in the’ fisian tube, ¥ bath Sulphur and. Nitrogen are prsent. in the given Orgrwie Campawund, then they get Converted inte Seduun thiocynate. Na+ CHEN +5 —f28" > NacNS ———— NaM+CNS” Sectium thiocyaunate ~ Experiment 3NaCNS + Fell, ——— Fe((NS), + 3 NaCl fone +thiocynate, (Blood Red Colsux) 4 The appearance & Blood Red Gelour inclicate that = Bath Nibagen and Subphur are Present tapeten. in the given ryan Compound.te che GP Sulphur andl Nitrogen “hatha ee of oe ae Hau MohanFrom lassarqne's Extract Soclium metal by When the Byanic Conyound us fel with Secon me in the juin tube, Jf Palogens Qe prea idl Conypourd , ten tay get converted to Socliu halides Not x —faion, es Nat +X” Soclium halide [x= Un Ba r] Experiment: @. Silver Nitrate Teat @ Lf Chlorine is present AgNO; + NatL——> Agcl | + NaNo, (white ppt) Agu + 2NHy 0H eae fy Qu Hs), | +240 Diammine sibve, (I) chloudle Ag (NHS). + 4HNO, AgU J + 2 NH, NO, O Hf Bromine i» Present AgNO, + Nok ——> Ay Ba J + NaNO, (fa yul pp PT»Page New eee 2mal of Sodium Exboct | piled with toa HNOs Poets AgNO, is ddecl 4 it | Soluble in NAOH ©. Yellow precpitate is Formed ua is_inSoluble in NH, OHTodine i» B nt © mir ¥ Nae — AyI J + NaNO; WNOs [vee pp Ay + NHy0H ——— No Yeachian ©. Chlogun Tut ( dayex Tet) @ Y Bromine is Prevent 2Na Br + U, —— ZNall + By Pia (HU, oes O Toclin ent 2NoI + UO, —— 2No + TL. + CHU, ——> purple or vialet (olou * Note - The Bx ign ond I~ ians ao give He layer Test o | Claro Test bud Ch 1s rat ident: fect by thy Teed Reosan - Bromine and Jodine ane much selubb ry rganic Solvents than in water . Since ue ane wing Cluoine ob on oxidant, chleride igns are 1 ated hone. Chlorine id alaneat colgurteas be it wiLl hy na Hed here. He Chlorinated Solvents 0d it ib ‘site tnPage No.1 “Fede Sota ecback | @If Chief | — _axe Taps with | layer Tie thon add | pale Azouwn— Mohan