Quick Start Guide

00825-0100-3492, Rev AB
November 2019

Rosemount™ 499AOZ

Dissolved Ozone Sensor

Quick Start Guide November 2019

Safety information

CAUTION
Sensor/process application compatibility
The wetted sensor materials may not be compatible with process composition and operating
conditions.
Application compatibility is entirely the operator's responsibility.

CAUTION
Equipment damage
Do not exceed pressure and temperature specifications
Pressure: 65 psig (549 kPa abs) max.
Temperature: 32 to 122 °F (0 to 50 °C)

WARNING
Physical access
Unauthorized personnel may potentially cause significant damage to and/or misconfiguration of end
users’ equipment. This could be intentional or unintentional and needs to be protected against.
Physical security is an important part of any security program and fundamental to protecting your
system. Restrict physical access by unauthorized personnel to protect end users’ assets. This is true for
all systems used within the facility.

Contents
First steps..................................................................................................................................... 3
Install........................................................................................................................................... 6
Wire........................................................................................................................................... 10
Calibrate.................................................................................................................................... 15
Maintenance.............................................................................................................................. 17
Accessories................................................................................................................................ 20

2 Emerson.com/Rosemount
November 2019 Quick Start Guide

1 First steps
1.1 Unpack and inspect
Procedure
1. Inspect the shipping container. If it is damaged, contact the shipper
immediately for instructions.
2. If there is no apparent damage, unpack the container. Be sure all
items shown on the packing list are present. If items are missing,
notify Emerson immediately.

1.2 Product description

Figure 1-1: Rosemount 499AOZ Sensor Parts

A. Membrane retainer
B. Membrane assembly
C. O-ring
D. Cathode
E. Electrolyte fill plug (wrap with pipe tape)
F. Pressure equalizing port
G. Sensor cable (integral cable shown)

1.3 Specifications
Table 1-1: Sensor Specifications

Physical characteristics Specifications

Range 0 to 3 ppm (mg/L) as O3

Pressure 0 to 65 psig (101 to 549 kPa abs)

Temperature (operating) 32 to 122 °F (0 to 50 °C)

Process connection 1-in. male national pipe thread (MNPT)

Quick Start Guide 3

Quick Start Guide November 2019

Table 1-1: Sensor Specifications (continued)

Physical characteristics Specifications

Wetted parts Polysulfone, Viton®, Teflon®, and silicone

Cathode Gold (not normally wetted)

Accuracy Accuracy depends on the accuracy of the chemical test used to

calibrate the sensor.

Linearity ±5% of reading or ±3 ppb (whichever is greater) at 77 °F (25 °C)

Repeatability ±2% of reading at constant temperature

Response time 30< 20 sec to 90% of final reading at 77 °F (25 °C)

Membrane permeability Defined between 32 and 122 °F (0 and 50 °C)

connection

Electrolyte volume 0.8 oz. (25 mL), approximately

Electrolyte life 3 months (approximately); for best results, replace electrolyte

monthly.

Cable length See Ordering information table in the Product Data Sheet for cable
length options.

Cable length (maximum) 300 ft. (91 m), up to 100 ft. (30.5 m) is standard.

Sample flow Flow through: 1 to 5 gpm (3.8 to 19 L/min)

Open channel: 1 ft./sec (0.3 m/sec)
Low flow cell: 2 to 5 gph (7.6 to 19 L/hr)

Weight/shipping 1 lb./3 lb. (0.5 kg/1.5 kg)

weight(1)

(1) Weights and shipping weights are rounded up to the nearest whole pound or 0.5 kg.

Table 1-2: Other Specifications

Type PN Wetted Process Maximum Maximum

materials connection temperature pressure

2-in. tee 915240-03 PVC and Buna ¾-in. NFPT 120 °F (49 °C) 60 psig (515
N; body is kPa abs)
915240-04 schedule 80 1-in. NFPT

915240-05 PVC 1½-in. NFPT

Low flow 24091-00 and Polycarbon- Compression 158 °F (70 °C) 90 psig
cell (1) 24091-01 ate/ fitting for (722 kPa abs)
polyester, ¼-in. O.D.
316 stainless tubing or
steel, and ¼-in. female
silicone national pipe
thread (FNPT)

4 Emerson.com/Rosemount
November 2019 Quick Start Guide

Table 1-2: Other Specifications (continued)

Type PN Wetted Process Maximum Maximum
materials connection temperature pressure

Valved 9390004 for Acrylic, 316 ¼-in. NFPT 150 °F (65 °C) 100 psig (858
rotameter use with low stainless (316 stainless kPa abs)
flow cell steel, and steel)
Flow: 0.5 to 5 Viton
gph (1.4 to 19
L/hr)

(1) Temperature and pressure specifications for the low flow cell exceed the temperature and
pressure specifications for the sensor.

Quick Start Guide 5

Quick Start Guide November 2019

2 Install
Install the sensor in a flowing sample. Keep the sample flow as constant as
possible at a value within the following limits:

Sample flow unit Flow limits

Flow through 1 to 5 gpm (3.8 to 19 L/min)

Open channel 1 ft/sec (0.3 m/sec)

Low flow cell 2 to 5 gph (7.6 to 19 L/hr)

Figure 2-1: Sensor Orientation

Install sensor within 45 degrees of vertical.

6 Emerson.com/Rosemount
November 2019 Quick Start Guide

Figure 2-2: Flow Through 1½-in. Tee

A. Union coupler
B. 1-in. national pipe thread (NPT), two places
C. Sensor body: Rosemount 499A
D. 1-in. NPT flow cell adapter
E. O-ring 2-222
F. 1½-in. sched 80 CPVC tee body

Quick Start Guide 7

Quick Start Guide November 2019

Figure 2-3: Flow Through 2-in. Tee

A. Union coupler
B. Adapter
C. 1-in. NPT (two places)
D. Sensor body: Rosemount 499A
E. O-ring 2-222
F. 2-in. sched 80 PVC tee body

8 Emerson.com/Rosemount
November 2019 Quick Start Guide

Figure 2-4: Low Flow Cell (PN 24091-00)

A. Inches
B. Millimeters
C. Outlet
D. Inlet

Quick Start Guide 9

Quick Start Guide November 2019

3 Wire
NOTICE
For additional wiring information on this product, including sensor
combinations not shown here, please refer to the Liquid Transmitter Wiring
Diagrams.

Figure 3-1: Rosemount 499AOZ Sensor Wiring to Rosemount 1056 and

56 Transmitters

Table 3-1: Rosemount 499AOZ Sensor Wiring to Rosemount 1056 and 56

Transmitters

Terminal Letter Wire color Description

number

1 A White Resistance temperature

device (RTD) return

2 B White/red RTD sense

3 C Red RTD in

4 D Clear RTD shield

5 N/A N/A +5 V out

6 N/A N/A -4.5 V out

7 D Clear Anode shield

8 E Gray Anode

9 D Clear Cathode shield

10 Emerson.com/Rosemount
November 2019 Quick Start Guide

Table 3-1: Rosemount 499AOZ Sensor Wiring to Rosemount 1056 and 56

Transmitters (continued)
Terminal Letter Wire color Description
number

10 F Orange Cathode

Figure 3-2: Rosemount 499AOZ Sensor Wiring to Rosemount 5081

Transmitter

Table 3-2: Rosemount 499AOZ Sensor Wiring to Rosemount 5081 Transmitter

Terminal Letter Wire color Description

number

1 N/A N/A N/A

2 N/A N/A +0.8 V

3 A White RTD return

Quick Start Guide 11

Quick Start Guide November 2019

Table 3-2: Rosemount 499AOZ Sensor Wiring to Rosemount 5081 Transmitter

(continued)
Terminal Letter Wire color Description
number

4 B White/red RTD sense

5 C Red RTD in

6 N/A N/A Reference guard

7 N/A N/A Reference in

8 D Clear Solution ground

9 N/A N/A pH guard

10 N/A N/A pH in

11 N/A N/A -5 V

12 N/A N/A +5 V

13 E Gray Anode

14 F Orange Cathode

15 N/A N/A HART®/FOUNDATION™ Fieldbus

(-)

16 N/A N/A HART/FOUNDATION Fieldbus (+)

12 Emerson.com/Rosemount
November 2019 Quick Start Guide

Figure 3-3: Rosemount 499AOZ Sensor Wiring to Rosemount 1066

Transmitter

Note
Connect clear shield wires to solution ground terminal on TB 2. Use wire nut
and pigtail if necessary.

Table 3-3: Rosemount 499AOZ Wiring to Rosemount 1066 Transmitter

Letter Color Terminal description

A Orange Cathode

B Gray Anode

C White Return

D White/red Sense

E Red RTD in

Quick Start Guide 13

Quick Start Guide November 2019

Figure 3-4: Rosemount 499AOZ Sensor Pin-out Diagram

Table 3-4: Pin-out Diagram

Terminal number Description

1 Cathode

2 N/A

3 RTD sense

4 Anode

5 RTD return

6 RTD in

When making a connection through a junction box (PN 23550-00), wire

point-to-point.

NOTICE
Use a wire nut and pigtail (included) when connecting several wires to the
same terminal.

14 Emerson.com/Rosemount
November 2019 Quick Start Guide

4 Calibrate
4.1 Zero point calibration
Even in the absence of ozone, the sensor generates a small signal called the
zero current. Failing to correct for the zero current can introduce a bias,
particularly if the ozone concentration is small (<0.4 ppm). Zero the sensor
when it is first placed in service and every time the fill solution is changed.
To zero the sensor:

Procedure
1. Pour a cup of deionized or bottled water.
2. Place the sensor in the water.
3. Wait until the sensor current has reached a stable low value (at least
two hours).
4. Follow the transmitter prompts for zeroing the sensor.
Note
Refer to the manual for the transmitter you are using (Rosemount
56, 1056, 5081, or 1066).

The zero current should be between -10 and +10 nA.

4.2 Full scale calibration
Because stable dilute ozone standards are not available, the sensor must be
calibrated against the results of a laboratory test run on a grab sample of the
process liquid.

Procedure
1. Place the sensor in the flow cell.
2. Start the sample and reagent flow.
3. Adjust the sample flow to the correct range.
4. Adjust the concentration so that it is near the upper end of the
operating range.
5. Wait for the readings to stabilize.
6. Follow the transmitter prompts to complete the calibration.
Note
Refer to the manual for the transmitter you are using (Rosemount
56, 1056, 5081, or 1066).

7. After calibration, go to the Diagnostics menu and check the

sensitivity.

Quick Start Guide 15

Quick Start Guide November 2019

The sensitivity should be between 250 and 450 nA/ppm. For more
information, refer to the transmitter manual.

16 Emerson.com/Rosemount
November 2019 Quick Start Guide

5 Maintenance
Periodic maintenance and cleaning are required for best performance of the
sensor. Generally, the membrane and fill solution should be replaced every
four to six months. Sensors installed in harsh or dirty environments require
more frequent maintenance. The optimum maintenance frequency is best
determined by experience.

WARNING
Pressurized spray injury
Before removing the sensor, be absolutely certain that the process pressure
is reduced to 0 psig and the process temperature is lowered to a safe level!

5.1 Cleaning the membrane

Keep the membrane and sensor tip clean and free from dirt. Clean the
membrane with water sprayed from a wash bottle. Use a soft tissue to
gently wipe the membrane.

5.2 Replacing the electrolyte solution and membrane

WARNING
Harmful substance
Fill solution may cause irritation. May be harmful if swallowed.
Read and follow the instructions.

Procedure
1. Unscrew the membrane retainer.
2. Remove the membrane assembly and O-ring.
See Figure 1-1.
3. Hold the sensor over a container with the cathode pointing down.
4. Remove the fill plug.
5. Allow the electrolyte solution to drain out.
6. Inspect the cathode.
a) If it is tarnished, clean it by gently rubbing in the direction of
the existing scratches (do not use a circular motion) with
400-600 grit silicon carbide finishing paper.
b) Rinse thoroughly with water.

Quick Start Guide 17

Quick Start Guide November 2019

7. Remove the old pipe tape from the plug.

8. Wrap the plug with one or two turns of pipe tape..
9. Prepare a new membrane.
a) Hold the membrane assembly with the cup formed by the
membrane and membrane holder pointing up.
b) Fill the cup with electrolyte solution.
c) Leave the membrane assembly filled with electrolyte solution
and set it aside.

10. Hold the sensor at about a 45 degree angle with the cathode end
pointing up.
11. Add electrolyte solution through the fill hole until the liquid
overflows.
12. Tap the sensor near the threads to release trapped air bubbles.
13. Add more electrolyte solution if necessary.
14. Place the fill plug in the electrolyte port and begin screwing it in.
15. After several threads have engaged, rotate the sensor so that the
cathode is pointing up and continue tightening the fill plug.
Do not overtighten.
16. Place a new O-ring in the groove around the cathode post.
17. Cover the holes at the base of the cathode stem with several drops of
electrolyte solution.
18. Insert a small blunt probe, like a toothpick with the end cut off,
through the pressure equalizing port.
See Figure 1-1.

CAUTION
Equipment damage
A sharp probe may puncture the bladder and destroy the sensor.
Do not use a sharp probe.

19. Gently press the probe against the bladder several times to force
liquid through the holes at the base of the cathode stem. Keep
pressing the bladder until no air bubbles can be seen leaving the
holes.
Be sure the holes remain covered with electrolyte solution.
20. Place a drop of electrolyte solution on the cathode; then place the
membrane assembly over the cathode.
21. Screw the membrane retainer in place.

18 Emerson.com/Rosemount
November 2019 Quick Start Guide

The sensor may require several hours operating at the polarizing

voltage to equilibrate after the electrolyte solution has been
replenished.

Quick Start Guide 19

Quick Start Guide November 2019

6 Accessories
Part number Description

23747-06 Interconnecting cable, Variopol (VP) 6, 2.5 ft. (0.8 m)

23747-04 Interconnecting cable, VP 6, 4 ft. (1.2 m)

23747-02 Interconnecting cable, VP 6, 10 ft. (3.0 m)

23747-07 Interconnecting cable, VP 6, 15 ft. (4.6 m)

23747-08 Interconnecting cable, VP 6, 20 ft. (6.1 m)

23747-09 Interconnecting cable, VP 6, 25 ft. (7.6 m)

23747-10 Interconnecting cable, VP 6, 30 ft. (9.1 m)

23747-03 Interconnecting cable, VP 6, 50 ft. (15.2 m)

23747-11 Interconnecting cable, VP 6, 100 ft. (30.5 m)

23567-00 1½-in. flow through tee with 1½-in. socket connections

915240-03 2-in. flow through tee with ¾-in. female national pipe
thread (FNPT) connections

915240-04 2-in. flow through tee with 1-in. FNPT connections

915240-05 2-in. flow through tee with 1½-in. FNPT connections

24091-00 Low flow cell with ¼-in. OD tubing compression fittings

9390004 Rotameter: 0.5 - 5.0 gph

22550-00 Junction box, 12 terminals

9200266 Extension cable for option -54, unterminated (specify

length)

9200275 Extension cable for optimum EMI/RFI cable,

unterminated (specify length)

23747-00 Extension cable for optimum EMI/RFI cable, terminated

(specify length)

2001492 Stainless steel tag

23501-11 Dissolved ozone membrane assembly; includes 1

membrane assembly and 1 O-ring

23502-11 Dissolved ozone membrane assembly; includes 3

membrane assemblies and 3 O-rings

9210299 #3 Dissolved ozone sensor fill solution, 4 oz (125 ml)

33521-02 Membrane retainer

33523-03 Fill plug

20 Emerson.com/Rosemount
November 2019 Quick Start Guide

Quick Start Guide 21

Quick Start Guide November 2019

22 Emerson.com/Rosemount
November 2019 Quick Start Guide

Quick Start Guide 23

 *00825-0100-3492*
Quick Start Guide
00825-0100-3492, Rev. AB
November 2019

EMERSON AUTOMATION SOLUTIONS

6021 Innovation Blvd.
Shakopee, MN 55379
+1 866 347 3427
+1 952 949 7001
[email protected]

NORTH AMERICA EUROPE

Emerson Automation Solutions Emerson Automation Solutions
8200 Market Blvd Neuhofstrasse 19a PO Box 1046
Chanhassen, MN 55317 CH-6340 Baar
Toll Free +1 800 999 9307 Switzerland
F +1 952 949 7001 +41 (0) 41 768 6111
[email protected] +41 (0) 41 768 6300
[email protected]

MIDDLE EAST AND AFRICA ASIA-PACIFIC

Emerson Automation Solutions Emerson Automation Solutions
Emerson FZE 1 Pandan Crescent
Jebel Ali Free Zone Singapore 128461
Dubai, United Arab Emirates, P.O. Box Republic of Singapore
17033 +65 6 777 8211
+971 4 811 8100 +65 6 777 0947
+971 4 886 5465 [email protected]
[email protected]

©2020 Emerson. All rights reserved.

Linkedin.com/company/Emerson-
Automation-Solutions The Emerson logo is a trademark and service
twitter.com/rosemount_news mark of Emerson Electric Co. Rosemount is a
mark of one of the Emerson family of companies.
Facebook.com/Rosemount
All other marks are the property of their
youtube.com/RosemountMeasurement respective owners.