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HT Starch Report - PDO Standard - 140C

The document details the testing procedures and results for drilling fluids conducted by M.B. Petroleum Services LLC. It includes specific measurements for moisture content, pH levels, API filtrate loss, and the performance of various chemical mixtures used in drilling operations. Additionally, it outlines the methodology for determining chloride content in the samples.

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Abderrazak Zouaghi
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21 views3 pages

HT Starch Report - PDO Standard - 140C

The document details the testing procedures and results for drilling fluids conducted by M.B. Petroleum Services LLC. It includes specific measurements for moisture content, pH levels, API filtrate loss, and the performance of various chemical mixtures used in drilling operations. Additionally, it outlines the methodology for determining chloride content in the samples.

Uploaded by

Abderrazak Zouaghi
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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(Testing: )

M. B. PETROLEUM SERVICES LLC.


DRILLING FLUIDS
LABORATORY

MBL: DATE:
BATCH No.: RPT#:
HT STARCH

Moisture = %
M = 100 x (W1 – W2) ÷ SAMPLE
Where:M is the percent moisture content, W1 is the mass of glass dish and sample before
drying;W2 is the mass of glass dish and sample after drying.

WSW SSW
D.W 930 ml +Salt 67.62 + D.W 864 ml+ NaCl 307g
CaCl2 20.58g+ MgCl 15.68g .

343 ml Water 343 ml


1.05g Sodium Bicarbonate 1.05g
17.5g API Base Clay 17.5g
(Mix for 10 mints)
6.3g H.T Starch 6.3g
(Mix for 20 mints)
0.35g Sodium Sulphite 0.35g

Hot Rolling for 16 hrs @ 284 ˚F /140 oC

pH

Reading @ 600 rpm @ambient

Reading @ 300 rpm

Fluid Loss
00:07:30 mints
V1
30:00:00 mints
V2

Filtrate volume: V2 – V1 = V3 X 2

(WSW) (SSW)

MBPS. DFL - POB 695, PC 111, CPO Seeb. OMAN. Tel: + 968 24580176 (North Athaibah).
MBLab Analysis Report/01/2020
Performance after hot-rolling Specifications Results
Wellsite water
Dial reading @ 600 rpm ≤ 18
pH 7-8
API filtrate loss ≤ 10 ml
Saturated salt water
Dial reading @ 600 rpm ≤ 20
pH 7-8
API filtrate loss ≤ 10 ml

Performance Test (MUD):

Mixing Concentration Mixing Time


Order
Chemical
for 500 ml Minutes
1 Tap Water 470 -
2 Sodium chloride 82.5 10
3 Sodium hydroxide 0.25 3
4 Xanthan (tech grade) 2.15 10
5 H.T Drilling starch 9 20
6 Calcium carbonate (WM or 50 MIC) 25 5
7 Sodium bisulphite 0.5 ml 1

Directly without hot rolling measure below properties & hot roll for 16 hrs @ 284 ˚F /140oC:

Parameters Result BHR Result AHR


pH = -
Rheology @ 50 oC:
600 / 300 rpm =
200 / 100 rpm =
6 / 3 rpm =
10" sec / 10' mints =
P. V = 600 rpm - 300 rpm
Y. P = 300 rpm - P. V =
Filtrate volume:
HTHP FL (cc/30min),
differential pressure 500 psi, -
@284 0F, F/L ≤ 6.0 ml

MBPS. DFL - POB 695, PC 111, CPO Seeb. OMAN. Tel: + 968 24580176 (North Athaibah).
MBLab Analysis Report/01/2020
Determination of Chloride (Cl-):

- 10g of starch sample 350 ml of D.W (mix for 30 mints).


- Transfer sample into a 500 ml volumetric flask.
- Keep on washing cup with D.W and fill up to the line.
- Take 20 ml of Sample using measuring cylinder + Potassium Chromate (10 – 20
drops) + titration against AgNo3 (0.1 N), end point reddish.

= = X2= %

- Take 20 ml of D.W using measuring cylinder + Potassium Chromate (10 – 20 drops)


+ titration against AgNo3 (0.1 N), end point reddish.

= = %

MBPS. DFL - POB 695, PC 111, CPO Seeb. OMAN. Tel: + 968 24580176 (North Athaibah).
MBLab Analysis Report/01/2020

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