Static and Fatigue Tests of A Woven Glass Fabric Composite Under Biaxial Tension-Torsion Loading
Static and Fatigue Tests of A Woven Glass Fabric Composite Under Biaxial Tension-Torsion Loading
A preliminary study of the static and fatigue behaviour of a plain woven glass
fabric-reinforced laminate under uniaxial and biaxial loading is presented,
using newly developed thin-walled tubular specimens. Problems associated
with fabrication of the tubular specimen were investigated. Both the Tsai-Wu
and the Tsai-Hill strength criteria seem to be applicable to the static strength
data of the glass fabric composite under combined tension/compression-
torsion loading. Some biaxial fatigue test results are also given.
The fatigue failure process of fibre-reinforced compos- posites 3"4. A biaxiai stress state combining axial and
ites must be more complicated under biaxial loading shear stresses can be attained when the tubular
than under uniaxial loading. Fibre composites inher- specimen is simultaneously twisted along its longitudi-
ently have a heterogeneous microstructure. It can be nal axis while it is subject to axial loading 5.
inferred that fatigue degradation would be accelerated Today, fabrics such as plain woven glass cloth are also
due to the stress coupling effect on material damage widely used as reinforcement for composite materials in
when biaxial stresses, for instance axial and shear addition to unidirectional fibres. Thus knowledge of
stresses along fibres, are applied to composites. There- the fatigue properties of fibre composites using such
fore, material evaluation for fibre composites under reinforcement is required. Filament winding is a typical
biaxial stress states is required not only for static method used to fabricate thin-walled tubular speci-
loading but also for cyclic loading in many applications. mens. Alternatively, tubular specimens may also be
Various test methods have been employed to obtain fabricated by winding unidirectional prepreg tape on a
directly both static and fatigue properties of composite mandrel 6. A mould is used to control the dimensions of
materials under biaxial loading. The uniaxial test using the specimen, or the mould can be replaced by heat-
off-axis specimens is one of the simplest and cheapest shrinkage film. No fabrics were used in such cases.
methods although only a limited range of axial and
shear stress combinations can be used. The method Owen and Griffiths 7 successfully developed the wet
using fiat cruciform specimens in conjunction with a winding technique for resin-impregnated glass fabric to
special testing machine is a more advanced technique. fabricate thin-walled tubular specimens in order to
The use of flat plates enables specimens to be subjected conduct static and fatigue tests. Discontinuity at both
to arbitrary combinations of three stress components, ends of the fabric must exist when fabric is used as
but the disadvantage of this technique is that stress reinforcement for tubular specimens. There are other
concentrations at the corners of the specimens are problems accompanied with fabrication; for example,
unavoidable. Therefore, the test method employing how to eliminate voids and how to control the glass
thin tubular specimens has been widely used, where an content. The effects of these problems on fatigue test
internal pressure and/or a torsional moment along the results have not been revealed. In addition, the
longitudinal axis of the specimen is simultaneously problem of how to grip the specimen in the testing
applied in addition to the axial loading ~'2. However, a machine has still to be resolved.
wide range of stress combinations cannot be covered if
only the internal pressure is superimposed on the axial This paper deals with problems associated with the
loading. Among multi-stress states, the existence of fabrication of tubular specimens of a plain woven glass
shear stress parallel to the fibres is important since the fabric-reinforced composite, which are used for static
shear stress strongly affects the strength of fibre corn- and fatigue tests. Some results are reported for static
0010-4361/91/040281-09 (~) 1991 Butterworth-Heinemann Ltd
COMPOSITES. VOLUME 22. NUMBER 4. JULY 1991 281
and fatigue tests conducted on the tubular specimens was rotated at 5 rpm for 24 h at room temperature to
under biaxial tension/compression and torsion loading. prevent resin dropping. After solidification, the tube,
about 4 mm thick, was pulled off the mandrel and then
cured at 353 K for 4 h in an oven.
EXPERIMENTAL DETAILS
Fabrication Biaxial testing
Table 1 gives details of the plain woven glass cloth Tubular specimens fabricated as described above were
reinforcement and the unsaturated polyester resin mechanically ground to the configuration shown in Fig.
matrix used in the present study. Tubular specimens 2. Initially, relatively short specimens (type A, L --
were fabricated using the wet winding machine shown 230 mm) having a gauge length of 100 mm were used,
in Fig. 1, according to the following procedure. but this was later changed so that the specimen length
Fluorocarbon release agent was sprayed onto the was L -- 300 mm (type B) with the gauge length kept
chromium-plated mandrel (50 mm in diameter), and a the same.
layer of resin applied to the mandrel. Glass cloth, The specimens used by Krempi and Niu had tapered
350 mm wide, was then placed in contact with the tabs in both ends of the tube 5. Another specimen
mandrel and wound onto it by slow rotation of the requires metal flanges to be bonded to both ends of the
mandrel as resin was applied with a brush. Initial tube for fixing the specimen to the testing machine 8.
tension was given to the warp of the cloth by a dead These precautions, necessary for avoiding stress
weight. Care was taken to prevent the introduction of concentrations and to support both ends of the
voids between the glass cloth layers because it was specimen, and fixing the specimen to the machine rods
impossible to remove them later. After 12 layers of are time-consuming processes. Therefore, a chuck was
glass cloth were wound onto the mandrel, the mandrel developed for clamping the specimens in this study.
The tubular specimen was held tightly by tapered
Table 1. Composition of specimen collets as bolts were turned (see Fig. 3).
A servo-controlled fatigue testing machine
Matrix Polyester resin m Polylite
(SHIMAZU EHF-EB 10/TQ 1, of dynamic loading
FG-284 from Dai-Nihon Ink
capacities + 10 tonf (axial force) and + 100 kgf.m
Chemical Industries
(twisting moment) ) was used (see Fig. 4). This
Reinforcement Plain woven glass cloth - -
machine, which can apply axial and torsion loads
MG-252 from Asahi Glass
simultaneously, was operated by a mini-computer using
Works
a programme developed by the authors. A computer-
Catalyst Methyl ethyl ketone peroxide
controlled data acquisition system was also employed.
Accelerator Cobalt naphthenate 0.6%
solution Preliminary experiments were conducted under several
conditions in order to confirm the test procedure
Brush
l/i
Plain woven glass cloth
o__/MandreGea
Belt
, ~r_ . . . . . . . ~ Moor /
L
Fig. 2 Dimensions of tubular specimen (in mm)
Fig. 5 Magnified cross-sections of tubular specimens parallel Static strength under biaxial loading
to the longitudinal axis: (a) fabricated with initial tension; (b)
fabricated without initial tension Static and subsequent fatigue tests were conducted
54
,i
a,
I
t
114
Q1 84
ilil
4x~13
;kll
rll
,llll 60 10~
I 100
:1111
I : ill i
ii
/72 "
a b
Fig. 7 Anti-buckling fixture for compression testing of tubular specimens: (a) inner piece; (b) outer piece. Dimensions in m m
using specimens having lower nominal glass contents fully in an electric furnace. Fig. 9 shows glass cloth
(Vf about 27_+3%) than former ones. Fig. 8 shows the obtained from the gauge section after burning the
strength under uniaxial and biaxial loading. In this specimen. It is found that some pieces of glass cloth
figure the symbols denote the experimental results were removed irregularly near the end. Therefore, the
while the dotted lines denote the loading path (straight glass content in the gauge section is not expected to be
lines due to proportional loading). It can be seen from uniform. In order to check this, the gauge length of a
Fig. 8 that there is considerable scatter in the strength specimen was cut into pieces and their glass contents
values observed. measured. Large scatter (about 24 to 30%) was
Fabrication of the test specimen requires grinding the observed, with low glass content corresponding to the
outer surface of the specimen, resulting in damage to damage zone. Usually the mean glass content is used as
the glass fibres in the outer lamina. To examine the the nominal glass content and the data are mutually
degree of fibre damage, a specimen was burned care- compared. It is proposed that the large scatter of glass
100
_Tsai-Wu theo~
~ 50
ii//
0 Tsai-Hill th7
O9
¢.-
//i /
/t.
Transverse surface
I I I I I I
-300 -200 -100 0 100 200 300
Normal stress,o 1(MPa)
Fig. 8 Ultimate static strength under uniaxial and biaxial J
loading (open circles denote experimental results) a 1
•~ 6
'ongitodina,su,ace I
Failure
R
305 -
t~
170 E
I1)
}-- 301
Fig. 11 D i m e n s i o n s of d u m b - b e l l t y p e s p e c i m e n (in m m )
180
150 297 I I I I
•
0 1500 3000 4500 5100
ro 100 ~- Time (s)
Q. • Fig. 13 Temperature increase inside the tubular specimen
during zero-torsion fatigue test at a speed of 10 Hz
C O M P O S I T E S . J U L Y 1991 287
1.0 -- If the shear or axial stress has a linear effect on the
o Biaxial(ix=4:9) fatigue failure process under biaxial stress, then the
0.8 • Biaxial (¢t=1:1)
[] Tension higher degradation in the case of 0¢= 1:1 (in which the
.9 0.6 • Torsion specimen is subjected to a higher shear stress compo-
nent) would be expected. Therefore, the failure surface
09 in the multi-axial stress state at a given cycle is not
09
0.4- proportional to the static one. It is apparent that the
fatigue life of woven glass fabric composites is affected
0 by many factors.
I I I I I CONCLUSIONS
0.2
102 10 a 10 4 10 s 10 6 10r Problems associated with fabrication of tubular speci-
Number of cycles to failure, Nf mens of a plain woven glass cloth composite for biaxial
Fig. 14 N o r m a l i z e d f at i g u e lives u n d e r u n i a x i a l and biaxial static and fatigue tests have been discussed. Problems
loading with static and fatigue tests have also been examined,
and limited fatigue test results under biaxial loading
t~6 given. The following conclusions may be drawn from
this study.
Tsai-Wu crite~lien ~ Staticstrength 1) For static and fatigue tests under biaxial loading, a
new type of chuck having six tapered collets was
developed. A n appropriate tube configuration and
dimensions for biaxial loading tests on a glass fabric
composite were determined.
2) Initial tension applied to the glass cloth during
I/ / specimen fabrication reduces the axial tensile
strength of tubular specimens.
01 .max G1 3) A fixture designed to prevent compression buckling
of the tubular specimen was found to be effective
and useful for compression testing. A steel bar
inserter should be used to prevent shear buckling
when the tubular specimen is subjected to torsion
Fig. 15 Definition of stress ratio (stress state under biaxial moments.
loading)
4) Both Tsai-Wu and Tsai-Hill failure criteria can be
applied to predict the static strength of a plain
ing the multi-axial stress state in anisotropic fibre
woven glass cloth composite under biaxial loading.
composites, although Wang et al. t2 used the equivalent
Scatter of strength data is due to non-uniform and
stress for evaluating fatigue strength of their carbon
local damage produced by surface finishing of the
fibre-reinforced plastic under biaxial cyclic loading.
tube.
Here, every fatigue strength was normalized by the
mean static strength and plotted against the log-scaled
5) Little difference was found in the fatigue life
diagrams under .~ero-tension cyclic loading of
number of cycles to failure, i.e., a stress ratio was
tubular and dumb-bell type specimens. There is no
introduced for representing the normalized fatigue life
apparent effect of discontinuity and lap of the
under biaxial loading. The y-axis in Fig. 14 is the stress
reinforcement on the fatigue life of tubular speci-
ratio, defined as the ratio of the distances O B : O A on
mens.
the ot - o6 stress map (see Fig. 15). Point A on Fig. 15
represents the static strength (stress combination at
6) A temperature increase was experienced inside
tubular specimens at high cyclic speed under fatigue
failure); point B represents the maximum stress state
torsion loading. This temperature increase restricts
under cyclic biaxial loading.
the cyclic loading speed to below 2 Hz.
Although fatigue strength under uniaxial torsion 7) Fatigue life strongly depends on the biaxial stress
loading is always lower than that under uniaxial tensile ratio, and fatigue life degradation does not follow a
loading, fatigue life degradation under torsion loading simple relation with the biaxial stress ratio.
is less than that under tensile loading (here, the fatigue
life degradation is indicated by the slope of the S / N
REFERENCES
line). Two life degradations can be linearly extended to
the static strengths on Fig. 14. On the other hand, life 1 Owen,M.J. and Rice, D.J. 'Biaxialstrength behaviourof glass
degradations under biaxial loading cannot be extended. fabric-reinforcedpolyesterresins' Composites 12 No 1 (1981)
It is predicted that below 103 cycles rapid life degrada- p13
2 Francis, P.H., Walrath, D.E. and Weed, D.N. 'First ply failureof
tion occurs under biaxial stress. An interesting phe- G/E laminatesunder biaxial Ioadings'Fibre Sci and Techno112
nomenon found for the biaxiai fatigue lives is that the (1979) p 97
life degradation is lower in the case where biaxial stress 3 Puck,A. and Sehurm~mn,H. 'Die Zug/Druck-Torsionsprufung
ratio ix=4:9 (max. shear stress:max, normal stress) than an rohrformigenProbekorpern' Kunststoffe 72 (1982) p 9
4 Smith,E.W. and PsLseoe,KJ. "Therole of shear deformationin
that for 0c= 1:1. The cyclic shear stress component for the fatiguefailureof a glass fibre-reinforcedcomposite'Compos-
the former case (0t=4:9) is less than that for the latter. ites 8 No 4 (1977) p 237