Ademola Work Final
Ademola Work Final
BY
ENG1804914
A PROJECT SUBMITTED IN
OF ENGINEERING (B.ENG).
FACULTY OF ENGINEERING,
UNIVERSITY OF BENIN
TITLE PAGE
AUGUST, 2024.
CERTIFICATION
Campus in Edo State. This certification serves as a partial fulfillment of the requirements for
the awarding of the Bachelor of Engineering (B.Eng.) degree in Civil Engineering at the
PROJECT COORDINATOR
PROJECT SUPERVISOR
HEAD OF DEPARTMENT
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DEDICATION
Most significantly, I dedicate this project to Jehovah God for everything He has done for
me, particularly for His protection, direction, and provision during not just this project but
also my time at this esteemed university. Thank you also to Prince (Dr.) and Dr. (Mrs.)
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ACKNOWLEDGEMENT
I would like to take this opportunity to express my deepest gratitude and appreciation to God
and all those who have contributed to the successful completion of my final year project.
Their support, guidance, and encouragement have been invaluable throughout this journey.
First and foremost, I am immensely grateful to my supervisor: Engr. Dr. R. O. Ogirigbo, for
his unwavering support, expertise, and continuous guidance as well as the project
coordinator, Engr. Ehi Oria-Usifo, for his hard effort. His valuable insights, constructive
feedback, and patience have been instrumental in shaping this project and enhancing its
Benin, Department of Civil Engineering, for their dedication to imparting knowledge and
I am indebted to my family and friends for their unwavering support, understanding, and
encouragement throughout this demanding undertaking. Their constant motivation, love, and
Lastly, I would like to acknowledge the support and encouragement of my fellow classmates
and colleagues. Their camaraderie, intellectual discussions, and shared experiences have
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ABSTRACT
This research project, entitled "Experimental Study on the Effect of the Partial Replacement
of Cement with Marble Powder on the Compressive Strength and Sorptivity of Concrete"
aims to delve into the impact of partially replacing conventional cement with marble powder
(MBP) on concrete's compressive strength and sorptivity. As sustainability becomes a
paramount concern in the construction industry, exploring alternatives and incorporating
waste materials is of increasing importance. The study involves the preparation and testing
of various concrete mixtures with varying percentages of marble powder (MBP)
replacement for cement. The outcomes are expected to shed light on the feasibility and
potential advantages of using marble powder (MBP) as a partial substitute for cement in
concrete.
This study directly addresses this imperative by investigating the practicality of integrating
marble powder (MBP) as a partial replacement for cement in concrete. Marble powder
(MBP), a byproduct of the stone industry, not only contributes to waste reduction but also
presents economic and environmental benefits. Through a series of experiments involving
different percentages of marble powder (MBP) replacement (0%, 2%, 4%, 6%, 8%, and
10%), we evaluated the compressive strength and sorptivity of the resulting concrete
specimens to understand how marble powder (MBP) content influences these crucial
properties.
According to this research, the results showed that as the percentage of marble powder
concrete increases, the compressive strength decreases alongside its cost and the weight of
concrete. At around 10% partial replacement of coarse aggregate with marble powder in
concrete gives a significant decrease in cost and weight of the concrete without much
affecting the compressive strength of concrete.
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TABLE OF CONTENT
Title Page
Certification i
Dedication ii
Acknowledgement iii
Abstract iv
Table Of Content v
List Of Tables xi
v
2.1 Concrete 8
2.2.1 Cement 9
2.2.2 Aggregate 9
2.2.3 Admixture 10
2.2.4 Water 10
2.8 How Does Marble Powder (Mbp) As Partial Replacement Of Cement Impact On
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3.1 Materials 27
3.1.5 Water 28
3.1.6 Oil/Grease 29
3.2.4 Curing 38
3.3.1.2 Apparatus 39
viii
3.3.2 Specific Gravity 40
3.3.2.1 Apparatus 40
3.3.2.2 Procedures 40
3.3.3.1 Apparatus 41
3.3.3.2 Procedures 41
3.3.4.1 Apparatus 42
3.3.4.2 Procedures 42
3.3.5.1 Apparatus 43
3.3.5.2 Procedures 43
3.3.6.1 Procedure 44
3.3.7.1 Apparatus 45
ix
CHAPTER FOUR: RESULTS AND DISCUSSION 46
5.1 Recommendations 60
REFERENCES 61
APPENDIX 62
x
LIST OF TABLES
Table3.2 Approximate compressive strengths (MPa) of concrete mixes w/c ratio of 0.5 32
Table 3.3: Approximate free-water contents to give various workability (El-Reedy, 2020) 34
Table 3.4: Mix Design Showing Different % Replacement of Cement with (MBP) 37
Table 4.8: Water absorption capacity of the cast concrete at varying replacement % 58
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LIST OF FIGURES
Figure 3.3: Relation between wet density of concrete and free-water content 35
xii
CHAPTER ONE
1.0 INTRODUCTION
development, prompting researchers and engineers to explore alternative materials that can
reduce environmental impact while maintaining structural integrity (Ahmed et al., 2021).
One promising avenue of investigation involves the integration of waste materials into
concrete production, with a specific focus on marble powder (MBP), a byproduct of the
This study aims to investigate the impact of partially replacing cement with marble powder
construction material, consists of cement, aggregates, water, and additives. Cement, as the
the identification of alternatives or supplements to cement is crucial for reducing the carbon
footprint of concrete. Marble powder (MBP), characterized by its finely ground nature,
in construction and architecture. However, the extraction and processing of marble result in
significant waste generation in the form of marble powder (MBP). Traditionally considered
a nuisance, researchers are now actively seeking ways to repurpose this waste product. The
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inclusion of marble powder (MBP) in concrete provides a dual advantage by addressing
The compressive strength and sorptivity of concrete are pivotal properties that determine its
investigating the effects of partially replacing cement with marble powder (MBP) on these
properties is of significant interest. This study aims to contribute to the dynamic field of
incorporating marble powder. The findings of this research are poised to guide the industry
2021).
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1.2 STATEMENT OF THE PROBLEM
The incorporation of marble powder into concrete introduces a promising avenue for
sustainable construction practices, addressing waste management issues and reducing the
The central predicament lies in the absence of comprehensive studies that systematically
evaluate the impact of marble powder (MBP) at varying replacement percentages. While the
potential benefits are acknowledged, the lack of detailed investigations hinders the industry's
ability to optimize the use of this waste material. Determining the optimal percentage of
marble powder (MBP) replacement is crucial for striking a balance between sustainability
and maintaining structural integrity. Without this knowledge, the industry operates without
specific guidelines, potentially leading to suboptimal mix designs and missed opportunities
The study aims to address these problems by investigating how partially replacing cement
with marble powder (MBP) on the compressive strength and sorptivity of concrete. The
central problem is finding a sustainable solution while assessing full potential of marble
construction practices.
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1.3 AIM AND OBJECTIVE OF THE STUDY
The main aim of this study is to conduct a detailed experimental investigation into the effect
of the partial replacement of cement with marble powder (MBP) on the compressive
To achieve this aim, this research is guided by the following specific objectives:
1. To assess how the incorporation of marble powder (MBP) affects the sorptivity of
concrete.
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1.4 SCOPE OF STUDY
The scope of this research centers on the experimental investigation of concrete mixtures
featuring different proportions of marble powder (MBP) as a partial substitute for cement.
The primary focus is on assessing the influence of marble powder (MBP) on crucial
properties such as compressive strength and sorptivity. The study encompasses a diverse
understand the influence of marble powder (MBP) content on compressive strength and
sorptivity. These mixtures were subjected to an array of testing procedures to assess the
sorptivity provides valuable information about the material's durability and resistance to
knowledge to the construction industry. It seeks to address the existing gap in understanding
how marble powder (MBP) at various replacement percentages influences critical concrete
properties. The outcomes of this study are anticipated to guide industry professionals and
researchers in formulating concrete mix designs that balance sustainability objectives with
structural performance.
In conclusion, the scope of this research is expansive, offering a detailed exploration of the
designed to provide practical insights for industry practitioners and researchers seeking to
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1.5 JUSTIFICATION OF STUDY
The justification for this study lies in the imperative to address the construction industry's
powder (MBP), emerges as a crucial endeavor to align with eco-friendly practices and
offers a potential solution to waste management concerns but also has the prospect of
Additionally, this study aims to bridge existing research gaps by providing detailed insights
examining its effects on crucial parameters like compressive strength and sorptivity, the
research intends to offer valuable information to engineers and researchers. These insights
will empower them to make informed decisions about the integration of marble powder
(MBP) into concrete mix designs, promoting more sustainable practices in the construction
industry.
In essence, the justification for this study rests on its potential to contribute practical
knowledge and solutions to the challenges posed by traditional construction materials. The
fostering the adoption of more sustainable alternatives and, in turn, supporting global
sustainability objectives. The study's outcomes may influence the industry's trajectory
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CHAPTER TWO
LITERATURE REVIEW
The increasing demand for sustainable practices in the construction industry has prompted a
shift towards exploring alternative materials, particularly those derived from waste products.
Marble powder, generated as a byproduct during the processing of marble stone, has
This literature review aims to provide a comprehensive overview of the current state of
research pertaining to the partial replacement of cement with marble powder in concrete.
The focus is specifically on two crucial properties: compressive strength and sorptivity. By
understanding the implications of incorporating marble powder into concrete mixes, this
review aims to contribute valuable insights into the broader discourse on eco-friendly
construction materials.
The use of waste materials in concrete aligns with the principles of sustainable construction,
utility, is being reevaluated for its potential contributions to the improvement of concrete
properties. This literature review synthesizes findings from various studies, shedding light
on the effects of incorporating marble powder on compressive strength and sorptivity, both
of which are pivotal factors in assessing the suitability and durability of concrete structures.
As the construction industry continues to grow, the environmental footprint associated with
byproduct of another industry, offers a dual benefit by reducing waste and potentially
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review aims to provide a foundation for researchers, engineers, and industry professionals to
make informed decisions about the use of marble powder in concrete mixes. The subsequent
sections will delve into key findings, challenges, and opportunities identified in the current
body of research related to the partial replacement of cement with marble powder.
2.1 CONCRETE
The origins of concrete-like materials can be traced back to around 6500 BC in Syria and
Jordan, where a primitive mixture of lime, volcanic ash, and stones was used (Aspris, 2018).
Notably, the Great Pyramid of Giza in Egypt, constructed around 2550 BC, showcases the
particularly skilled in concrete use, employed a mix of volcanic ash, lime, and rubble. This
innovation is evident in iconic structures such as the Pantheon and the Colosseum (Landolfo
Concrete's versatility allowed the creation of intricate architectural designs, including arches
Concrete's durability, strength, and resistance to fire and weathering make it a crucial
construction material (Mindess, Young, & Darwin, 2003). Its moldable properties have
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enabled the realization of various architectural designs, emphasizing its indispensable role in
construction.
While concrete offers numerous advantages, challenges exist, including cracking due to
production (Scrivener & Crumbie, 2018). Addressing these challenges is crucial for
2.2.1 CEMENT
components. The most common type is Portland cement, produced by grinding clinker with
a small amount of gypsum (Kosmatka, Kerkhoff, & Panarese, 2002). The chemical reaction
between cement and water forms a paste, initiating the hardening and setting processes in
concrete.
2.2.2 AGGREGATE
Aggregates, comprising coarse and fine particles, occupy a significant portion of concrete.
Coarse aggregates, such as gravel or crushed stone, provide structural strength, while fine
aggregates, typically sand, contribute to workability (Neville, 2011). The proper distribution
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2.2.3 ADMIXTURE
mixing or placement. These can enhance workability, accelerate or delay setting time, or
improve durability. Common types include water reducers, accelerators, and air-entraining
agents (Malhotra & Mehta, 2006). Admixtures allow concrete to be tailored for specific
2.2.4 WATER
Water is a vital component that initiates the chemical reaction with cement, leading to the
hydration process. The quality of water used in concrete significantly impacts its final
properties. Excessive impurities or improper water-cement ratio can affect the strength and
Traditional aggregates like crushed stone and sand are commonly used in concrete, but
applications.
Recycled Concrete Aggregate involves crushing and reusing concrete from demolished
structures. This approach minimizes the environmental impact of concrete waste and
conserves natural aggregates (Sagoe-Crentsil et al., 2001). RCA has been successfully
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2.3.2 FLY ASH
Fly ash, a byproduct of coal combustion, can be used as a partial replacement for cement in
concrete. Its incorporation enhances workability, reduces heat generation during hydration,
and contributes to long-term strength development (Mindess, Young, & Darwin, 2003).
Several studies have demonstrated the positive effects of fly ash in improving the durability
Blast furnace slag, a byproduct of iron production, can be ground and used as a
permeability and improving resistance to aggressive environments (Neville, 2011). The use
of blast furnace slag as a replacement for traditional aggregates has been effective in various
construction applications.
Recycled rubber from tires can be processed into aggregates for specific applications.
Rubber aggregates are lightweight and offer benefits such as energy absorption, making
them suitable for use in sports surfaces and certain types of concrete (Buck, 1977). The
incorporation of rubber aggregates provides a sustainable solution for waste tire disposal.
Expanded glass beads are lightweight aggregates with insulating properties. When
incorporated into concrete, they reduce density while maintaining compressive strength
(Oikonomou, 2005). This makes them suitable for applications where weight reduction is
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2.4 EFFECT OF ALTERNATIVE AGGREGATES ON CONCRETE PROPERTIES
The use of alternative aggregates in concrete can significantly impact its compressive,
tensile, and flexural strengths. Previous studies have shown variations in strength based on
the type and proportion of alternative aggregates used (Fathifazl et al., 2009). For instance,
strength compared to traditional concrete, but this effect depends on factors like the source
and processing of the recycled material (Limbachiya et al., 2000). On the other hand,
supplementary cementitious materials like fly ash and blast furnace slag can enhance long-
negatively. For instance, recycled rubber aggregates have been found to enhance the
elasticity and energy absorption properties of concrete, making it more resistant to certain
impacts (B. Govinda Rajulu et al., 2017). On the contrary, the porosity of some alternative
aggregates, such as recycled concrete aggregate (RCA), might affect durability due to
increased water absorption (Katrina Mc Nei and Thomas H.K. Kang, 2013).
Numerous research studies have investigated the use of alternative aggregates in concrete
and their impact on various properties. Limbachiya et al. (2000) demonstrated that concrete
with up to 30% RCA exhibited comparable compressive strength for certain water-cement
ratios. Other studies, such as those by Exteberria et al. (2007) and Yang et al. (2008),
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observed that the percentage of replacement and water-cement ratio play crucial roles in
The exploration of the partial replacement of cement with marble powder in concrete has
garnered significant attention in recent years. Numerous studies have investigated the effects
on compressive strength and sorptivity, providing valuable insights into the potential
benefits and challenges associated with this innovative approach to sustainable concrete
Notable among these studies is the work by (Kumar, R., and Bhatty, J., 2018) through their
Their results emphasized the durability benefits, showcasing a reduced sorptivity that
deterioration.
nano silica and marble powder on the properties of concrete. Their study delved into the
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Researchers such as (Rashid, Z. A., and Razak, H. A., 2018) examined the effects of
incorporating marble powder on the water absorption characteristics of concrete. Their study
revealed a decrease in water absorption, suggesting that the addition of marble powder
enhancing durability.
Also, (Shetty, A. and Partheeban, P., 2018) investigated the influence of marble powder on
the mechanical and durability properties of concrete. Their study explored the optimum
strength and durability. Their findings contribute to the ongoing efforts to establish
Furthermore, researchers like (Rathod, V. T and Deshmukh, N. A., 2019) focused on the
sustainability aspects of using marble powder in concrete. Their research assessed not only
the mechanical properties but also the environmental benefits of incorporating marble
powder. This aligns with the broader industry trend towards sustainable concrete practices
Researchers such as (Zegardło, B. and Moczko, E., 2019) explored the rheological
properties of concrete mixtures incorporating marble powder. They investigated the flow
concrete mix design. This aspect is essential for ensuring that the addition of marble powder
Similarly, (Akbulut, H. and Gürer, C., 2018) also examined the performance of concrete
insights into the durability aspects, especially sulfate resistance, which is crucial for
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structures exposed to harsh environmental conditions. Understanding the behavior of marble
In further exploration, (Ahmad, S. and Mahmood, N., 2019) they conducted a study
investigating the impact of marble powder on the compressive strength of concrete. Their
findings indicated that the partial replacement of cement with marble powder led to
Also, (Rana, A. and Tariq, A., 2020) explored the sorptivity of concrete when incorporating
marble powder. Their results demonstrated that the addition of marble powder contributed to
In a study (Kumar, P. and Bhargava, P., 2018) pointed out the effect of varying percentages
of marble powder on the compressive strength of concrete was investigated. The research
strength.
Similarly, (Siddique et al., 2018) conducted an extensive review of studies related to the use
compressive strength but also highlighted the potential for reducing the permeability of
concrete.
In a recent study (Singh, R. and Garg, M., 2022) examined thoroughly the compressive
insights into the optimum percentage of replacement for achieving optimal strength.
Researchers like (Alam, M. S. and Jha, K. N., 2018) delved into the influence of marble
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suggesting enhanced resistance to water penetration, which is crucial for the longevity of
concrete structures.
Also, (Aly, M. and Hashmi, M. S. J., 2019) focused on the mechanical properties of concrete
with marble powder as a partial replacement for cement. Their study indicated an
improvement in both compressive strength and durability, emphasizing the potential for
Researchers like Singh and collaborators (Singh, L. P. et al., 2019) investigated the effect of
compressive strength.
Additionally, (Rathaur, N. and Khan, R., 2021) explored the synergistic effects of marble
powder and other supplementary cementitious materials on the sorptivity of concrete. Their
findings emphasized the potential for creating high-performance and durable concrete
mixes.
Likewise, Yadav and Saini focused on the durability aspects of concrete with marble
powder, particularly its impact on sorptivity (Yadav and Saini, M., 2022). Their study
increased durability.
Malik and Singh explored the long-term performance of concrete incorporating marble
powder (Malik, A. and Singh, M., 2020). Their findings suggested that the concrete
exhibited sustained compressive strength over time, indicating the durability benefits of
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In a study by Biswas and co-authors, the focus was on the optimization of the particle size of
marble powder for improved compatibility with cement (Biswas, S. et al., 2019). Their
findings suggested that a specific particle size range positively influenced both compressive
containing marble powder (Srivastava, V. and Mishra, A., 2018). Their research indicated
that the self-compacting concrete with marble powder achieved comparable or improved
concrete applications.
Rathore and collaborators investigated the impact of curing conditions on concrete with
marble powder (Rathore, D. et al., 2022). Their study demonstrated that appropriate curing
regimes enhanced the compressive strength and durability of concrete, further emphasizing
Gupta, N., Sharma, V., Bhandari, S., and Siddique, R. (2021) emphasized that sustainable
materials, like PKS, play a pivotal role in achieving sustainability in construction (Gupta et
al., 2021).
concrete with varying percentages of marble powder (Shukla, A., and Patidar, S., 2019).
Kumar and Sinha's research focused on the influence of marble powder on the
microstructural characteristics of concrete (Kumar, A., and Sinha, A., 2021). Their findings
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indicated a denser microstructure, leading to enhanced compressive strength and durability,
Ganesan and his team investigated the mechanical and durability properties of concrete
incorporating marble powder (Ganesan, K., et al., 2020). Their study highlighted
marble powder on the pore structure of concrete (Bhutta, A. R., et al., 2018). Their findings
suggested that the addition of marble powder led to a refined pore structure, contributing to
The exploration of incorporating waste materials into concrete dates back several decades,
byproduct from marble stone processing, has emerged as a promising candidate for partial
cement replacement.
Notable studies like ((Mehta and Siddique, 2016) pioneered investigations into the influence
of marble powder on concrete compressive strength. Their work laid the foundation for
subsequent studies, revealing a positive correlation between marble powder content and
compressive strength. Subsequent research by (Sarireh et al., 2017) and (Sachan et al., 2018)
expanded on these findings, delving into the effects of curing conditions on the compressive
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2.7.2.2 RECENT ADVANCES
Recent studies by (Ganesan et al., 2020; Shukla and Patidar, 2019; Malik and Singh, 2020)
further substantiate the positive impact of marble powder on compressive strength. Notably,
compressive strength. The works collectively underscore the evolving understanding of the
strength.
Researchers such as (Sarireh et al., 2017; Bhutta et al., 2018) ventured into studying the
sorptivity with increasing marble powder content, indicating potential benefits for enhancing
concrete durability. Bhutta and colleagues delved deeper into the pore structure, identifying
Recent studies by researchers like (Kumar and Sinha, 2021; Biswas et al., 2019; Verma et
aligning with reduced sorptivity. Additionally, Biswas and his colleagues emphasized the
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2.7.4 MULTIFACETED APPROACHES
The literature beyond 2018 reveals a trend towards multifaceted approaches. (Rathore et al.,
2022; Raj and Kumar, 2023) explored the combined effects of curing conditions, mineral
admixtures, and marble powder. These studies showcase a shift toward holistic concrete mix
designs, emphasizing not only the individual contributions of marble powder but also its
Research on marble powder highlights unique properties that influence its suitability as
Pozzolanic Activity: Marble powder has shown pozzolanic activity, which can contribute to
the strength and durability of concrete. Pozzolanic materials react with calcium hydroxide
to research by (Siddique and Noumowe, 2008), marble powder can exhibit pozzolanic
Particle Size Distribution: The particle size distribution of marble powder is crucial for its
finely ground marble powder for improving the performance of concrete. Smaller particle
sizes provide more surface area for pozzolanic reactions, leading to better strength and
durability.
workability. Research by (Shukla et al., 2015) suggests that the workability of concrete may
decrease with increasing marble powder content. Proper adjustments to the mix design, such
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Effect on Compressive Strength: Studies by (Işikdağ and Topçu, 2010) indicate that the
strength. The pozzolanic reaction and the filler effect of marble powder contribute to the
durability. Research by (Tawabini et al., 2019) suggests that incorporating marble powder
can reduce permeability and enhance the resistance of concrete to aggressive environmental
conditions.
Sustainability Benefits: The use of marble powder as a cement replacement aligns with
discusses the environmental benefits of incorporating waste materials like marble powder in
concrete.
Influence on Pore Structure: Incorporating marble powder could modify the pore structure
contribute to refined pore structures, reducing the size and connectivity of capillary pores.
powder particles may influence the water absorption properties of the concrete. A study by
(Celik et al., 2016) discusses the impact of mineral admixtures on the surface properties of
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2.7.6 SUSTAINABLE BENEFITS OF MARBLE POWDER IN CONCRETE:
The use of marble powder in concrete offers several sustainable benefits, aligning with
principles of environmental responsibility and resource efficiency. Here are some key
and minimizing environmental impact associated with quarrying (Topçu et al., 2013).
3. Energy Savings: The use of marble powder as a partial cement replacement can
material helps in decreasing overall carbon dioxide emissions associated with cement
2010).
durability of concrete structures, resulting in a longer service life and reduced need for
impact compressive strength and durability, leading to concrete structures with improved
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7. Economic Benefits for the Marble Industry: The utilization of marble powder in
byproduct into a valuable resource and fostering a circular economy (Celik et al., 2016).
applications, including pavements and precast elements, allows for sustainable practices
cement in concrete has garnered significant attention in recent literature, driven by the
literature.
1. Strength Enhancement:
Numerous studies indicate that incorporating marble powder in concrete can contribute to
cementitious hydration products, enhancing the overall strength of the concrete (Işikdağ
2. Durable Concrete:
Marble powder has been shown to enhance the durability of concrete. The reduction in
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against chemical attacks, thereby improving the durability of the concrete (Tawabini et
al., 2019).
3. Pozzolanic Reactivity:
Research suggests that marble powder exhibits pozzolanic reactivity when used in
concrete. This reactivity enhances the binding properties of the concrete and reduces the
presence of free lime, resulting in a denser and more durable material (Siddique and
Noumowe, 2008).
4. Workability Considerations:
The addition of marble powder may influence the workability of concrete. Studies
highlight that as the replacement level of cement with marble powder increases,
adjustments to the mix design, such as water-cement ratio, may be necessary to maintain
Marble powder incorporation can impact the setting time and hydration characteristics of
concrete. Studies have explored the influence of MBP on the early and later stages of
cement hydration, providing insights into the evolution of the concrete's properties over
The use of marble powder aligns with sustainable practices by repurposing a byproduct
of the marble industry. This not only provides economic benefits but also contributes to
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Literature reviews often discuss the optimal replacement levels of cement with marble
powder. Different studies have explored various replacement percentages, and finding the
right balance is crucial to maximizing the benefits of MBP without compromising the
pavements and precast elements. Studies have investigated its performance in various
contexts, providing insights into the suitability of MBP for different construction
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CHAPTER THREE
METHODOLOGY
This chapter describes the process used to evaluate the effects of replacing some of the
cement in concrete with marble powder. This study's main goal is to clarify the unique
characteristics that concrete displays when different amounts of marble powder are added in
place of regular cement. The experimental investigations were conducted at the University
The subsequent examinations will be carried out in compliance with pertinent guidelines and
For all formulations, the water-to-cement ratio (w/c) was kept constant at 0.5 to provide
uniform workability.
Marble powder was used to partially substitute cement in all tests at percentages of 0%, 2%,
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Table3.1: Showing the Ratios of Replacement
3.1 MATERIALS
The laboratory-produced concrete cubes were made using the following materials.
3) Cement (OPC)
5) Water
6) Oil
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3.1.1 ORDINARY PORTLAND CEMENT (OPC)
Ordinary Portland cement (OPC) of grade 42.5 (also known as Dangote cement) that
complied with applicable specifications was utilized in this investigation. This came from an
Edo State cement depot near the university of Benin, ugbowo campus. The cement was kept
airtight, only being opened to take a sample when required in order to avoid absorbing
moisture.
This was made with marble powder that was left over from an industrial rock crushing
The fine aggregate was purchased locally from Uselu market in Ovia North-East L.G.A. of
Edo State. The fine aggregate was air dried before casting to make sure that its natural
moisture content was reduced to the point where it could not have an impact on the test
results.
Crushed stone, gravel, or a mix of the two make up conventional coarse aggregate. The
crushed stone aggregate employed in this investigation was well-graded and locally supplied
from uselu market, with particle sizes ranging from 10 - 20 mm. It is bought from a nearby
supplier.
3.1.5 WATER
The study's water was pure, drinkable, and devoid of any pollutants or impurities. To ensure
uniformity in the mix design, the amount of water used in each mix was determined by
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calculating the desired water-to-cement ratio. The University of Benin's Civil/Structural
3.1.6 OIL/GREASE
Concrete molds, also known as concrete cube cavities, were lubricated with grease so that
the concrete could be readily removed from them once it had formed. In order to minimize
damage to the newly laid concrete specimen, it was also used to lubricate the cone during
Concrete specimens were formed for multiple testing using cubic molds with dimensions of
10 cm × 10 cm × 10 cm. In order to stop concrete from adhering to the mold surfaces, the
molds were cleaned and lubricated. The molds were subsequently put together, and the bolts
were tightened to stop cement paste leaks. Concrete was layered three times into the molds,
and each time, the concrete was fully compressed without segregation by vibrating the layer
to release any trapped air. Then, a trowel was used to complete surface polishing. After that,
the test specimen was sealed off from shock, vibration, and dehydration and left in molds for
a whole day.
Nine cubes were made for each blend in order to guarantee consistency and dependability of
the outcomes.
1) concrete mixer
3) Vibrating machine
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4) Weighing machine
5) Oven
6) Shovel
8) Head pans
9) Curing Tank
A key step in the production of concrete technology is mix design, which is figuring out how
much of each ingredient to add to get the right mix composition and performance. Its goal is
to produce a concrete mix that satisfies the needs for a particular building project, including
To determine the quantity of materials needed to cast each cube specimen, a mix design for
grade 25 concrete was completed. The materials obtained have a ratio of 1:1.6:4.4, with the
slump range chosen falling between 10 and 30 mm in accordance with BS 882 requirements.
The control mix was not made with marble powder (MBP) but additionally,2%, 4%, 6%,
8%, and 10% of the cement weight was replaced with marble powder (MBP) respectively.
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3.2.2.1 MIX DESIGN FOR C25 GRADE CONCRETE
5 % Defective
Figure 3.1: Relationship between standard deviation and characteristic strength (El-
Reedy, 2020)
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Target mean strength = 𝒇𝒎
𝒇𝒎 = 𝒇𝒄 + 𝒌. 𝒔
From Table 3 . 1 the compressive strength for w/c =0.50 is 42 MPa. From Figure 3 . 2
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Figure 3.2: Relation between compressive strength and free-water/cement ratio (El-
Reedy, 2020)
From Table 3.2, for 10-30 mm level of workability, crushed aggregates and maximum
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Table 3.3: Approximate free-water contents (kg/m3) required to give various levels of
From Figure 3.2 for free water content of 160 kg/m3, Specific gravity of uncrushed
aggregates =2.6(assumed), the wet density of concrete = 2400 Kg/m3. Therefore, the total
aggregate content is
Total aggregate content = Wet density of 1m3 concrete – water content – cement content =
34
Figure 3.3: Relation between wet density of concrete and free-water content (El-Reedy,
2020)
35
Fig 3.4: Proportions of fine aggregate determined from fineness modulus
36
Table 3.4: Mix Design Showing Different Percentage Replacement of Cement with
2. 2% (MBP)replacement
3. 4% (MBP)replacement
4. 6% (MBP) replacement
5. 8% (MBP) replacement
37
In order to provide an equitable comparison, the mix proportions were created to keep
the water-to-cement ratio at (0.5) for every combination. In accordance with ASTM
C192, the particular mix design was based on the absolute volume approach.
3.2.4 CURING
curing conditions were applied to the concrete specimens in order to guarantee uniform
curing for every sample. In order to achieve this, the specimens had to be placed in a
damp atmosphere with wet burlap and plastic sheeting to keep the humidity high, limit
moisture loss, and encourage the cement to hydrate as best it could. To rule out curing as
a factor influencing the outcomes, the curing time was the same for all specimen.
For the purpose of evaluating the growth of strength, concrete specimen will be cured for
varying amounts of time under specific circumstances (such as room temperature). Cubes
1. Fine aggregates were dry-mixed for two minutes with the necessary quantity of
cement.
2. After that, measured marble powder was added to the mixture, and it was dry-
3. To get a homogenous consistency, water was added gradually and the mixture
38
3.3 PARTICLE SIZE DISTRIBUTION
In this test, a substance is divided into many particle size classifications of decreasing
sizes using a succession of test sieves. The starting mass of the material is connected to
the mass of the particle retained on the different sieves. Both numerical and graphical
data are provided regarding the proportions of each sieve that pass through. The purpose
of the test was to ascertain the coarse aggregate's (granite) particle size distribution in
3.3.1.2 APPARATUS
iv. Scoop
v. Pan
3.3.1.3 PROCEDURE
1. If any particles get lodged in the holes of the sieves, clean them with a cleaning
brush.
4. Put the sieves in sequence such that the bigger openings go to the top and the
5. Store the specimen with the weight recorded on the upper sieve, and
39
subsequently place the entire sieve stack into the sieve shaker (remember to
6. Take note of the time and let the shaker run for 10 to 15 minutes.
7. After removing the sieve stack from the shaker, weigh each sieve and receiving pan
independently.
Specific gravity is defined as the ratio of the density of a substance to the density of
concrete mixes.
3.3.2.1 APPARATUS:
1. Weighing Balance
2. Wire Basket
3. Container
4. Wire Hanger
5. Brush
6. Oven
3.3.2.2 PROCEDURES:
4. Immerse the aggregates in water using the wire basket, ensuring complete
submersion.
40
6. Record the initial volume of water in the pycnometer.
7. Place the submerged aggregates in the pycnometer, ensuring the water level rises.
8. Record the final volume of water, considering the displaced water by the
aggregates.
W𝟏
G= (W𝟏−W𝟐)
(𝐖𝐞𝐢𝐠𝐡𝐭 𝐨𝐟 𝐖𝐚𝐭𝐞𝐫 𝐃𝐢𝐬𝐩𝐥𝐚𝐜𝐞𝐝)
AIV assesses the ability of aggregates to withstand abrupt shocks or impacts and
3.3.3.1 APPARATUS:
2. Cylindrical Steel Cup (diameter of at least 102 mm and a depth of at least 50 mm)
4. Tamping Rod
3.3.3.2 PROCEDURES:
4. Secure the cup tightly in the apparatus and deliver 15 consistent blows.
5. Expel the crushed material from the cup following the test.
41
6. Calculate the aggregate impact value (AIV) using the formula:
ACV evaluates aggregates' resistance to crushing under compressive loads and aids with
quality control in the concrete manufacturing process by confirming that the aggregates
3.3.4.1 APPARATUS:
1. A 150mm BS Sieve
3. Tamping Rod
4. Weighing Balance
3.3.4.2 PROCEDURES:
1. Get an aggregate sample that is retained on the 10 mm sieve after passing through the
12.5 mm sieve.
2. Three layers of aggregate should be added to the cylindrical measure, with each layer
Weight of Fines
ACV= ×100
Weight of Aggregates
42
3.3.5 SLUMP TEST
The purpose of the concrete slump test is to evaluate the consistency or workability of
concrete mix that has been created in a laboratory using (BS 1881-102:1983).
3.3.5.1 APPARATUS
a. Slump cone: Shaped like the frustrum of a cone, with a height of 300 millimeters,
b. Base plate
c. Measuring tape
d. Tamping rod
3.3.5.2 PROCEDURES
1. Make sure that the interior surface of the slump cone is dry, clean, and clear of
2. lubricate its interior surface with oil/grease to stop the slump cone from sticking
3. Make sure the slump cone is securely positioned by placing it on a square metal
base plate.
4. Stabilize the cone by placing its metal arms on the base plate.
5. Place three layers of freshly mixed concrete within the slump cone, each about a
6. Make sure the strokes are uniformly distributed throughout the cross-section by
tamping the concrete 25 times with a tamping rod after each layer.
43
7. After the third layer has been compacted evenly, start filling the cone with new
8. Make sure the surplus concrete is removed by using a trowel to remove it.
9. While the cone is still being held in place, clean the base plate and the bottom of
10. Raise the slump cone vertically from the newly laid concrete and set it gently
11. For measuring and recording purposes, place the tamping rod atop the cone and
12. A measuring tape was used to determine the slump, which is the difference
between the cone's height and the height of the concrete specimen.
Compressive strength testing is a key test for determining how well concrete can support
loads. A compression testing apparatus was utilized in the process. Cubic samples were
examined after 3, 7,14, 21, and 28days of cure for every mixture. This made evaluating
the strength development over time and contrasting the concrete with the control mix that
3.3.6.1 PROCEDURE
(i) The cubes were taken out of the curing tank at various stages of curing.
(ii) The cubes were then left to dry for about an hour on a platform.
(iv) The cubes were placed so that the base plate of the compression machine was in
the center. The equipment is activated and measurements are obtained as soon as
44
𝐌𝐚𝐱𝐢𝐦𝐮𝐦 𝐋𝐨𝐚𝐝 (𝐊𝐍 )
Compressive Strength (N/ 𝒎𝒎²)=
𝐂𝐫𝐨𝐬𝐬 𝐒𝐞𝐜𝐭𝐢𝐨𝐧𝐚𝐥 𝐀𝐫𝐞𝐚 (𝐦𝐦² )
The water absorption test for marble-based concrete, also known as the sorptivity test, is
crucial for assessing the capillary absorption properties of the concrete. This test helps in
understanding how susceptible the concrete is to water penetration, which is vital for
evaluating its durability and performance in various environmental conditions. The test
was performed following the guidelines outlined in ASTM C64282 at the 28-day mark.
3.3.7.1 APPARATUS:
2. Dry Oven
3. Container
4. Brush
5. Measuring Cylinder
1. Weighing the concrete cubes that had been immersed for 28 days and then dried at
2. The cubes were allowed to completely soak in water after they had dried for at least
24 hours. To find just how much water the concrete had absorbed, they were weighed
again.
3. Record the water level at predetermined time intervals (e.g., every 5 minutes) until
45
CHAPTER FOUR
The standard sieve sizes that complied with the BS 1377-2-1990 specification for test
sieves were used for the sieve analysis. Grading curves were used to graphically depict
sieve analysis. According to the grading curves below, the fine and coarse aggregates
were within the BS 882: 1992 tolerances. When designing a concrete mix, grading plays
a crucial role in figuring out the fine aggregate content and, consequently, the quantity of
According to Table 4.1's sieve analysis, the fine aggregate is scattered throughout a
46
Table 4.1: Sieve analysis of fine aggregate
2 50
1½ 37.5
1 26.5
¾ 20
½ 14
⅜ 10
¼ 6.3
3/16 5
47
120
100
80
Percentage passing
60
40
20
0
0.01 0.1 1
Seive Sizes
19 1.603 5.397 23 77
48
120
100
80
Percentage mass passing (%)
60
40
20
0
0 5 10 15 20 25 30 35 40
Sieve size
49
120
100
Percentage mass passing (%)
80
60
40
20
0
75 150 212 300 425 600 1.18 200 2.36
Sieve size (mm)
TEST A
𝟗𝟏.𝟗𝟐
= × 𝟏𝟎𝟎
𝟑𝟑𝟎.𝟑𝟓
= 27.83
50
TEST B
𝟗𝟓.𝟒𝟑
= × 𝟏𝟎𝟎
𝟑𝟑𝟗.𝟐
= 28.13
𝐓𝐄𝐒𝐓 𝐀+𝐓𝐄𝐒𝐓 𝐁
Average AIV =
𝟐
𝟐𝟕.𝟖𝟑+𝟐𝟖.𝟏𝟑
=
𝟐
=27.98
INTERPRETATION OF RESULTS
AIV CLASSIFICATION
10 – 20% Strong
51
CHECK
𝟑𝟐𝟕.𝟓+𝟑𝟑𝟏.𝟑
Average Mass of aggregate used =
𝟐
=329.4
TEST A
𝟖𝟎𝟔.𝟗
= × 𝟏𝟎𝟎
𝟐𝟕𝟖𝟒
= 28.983
TEST B
52
𝐌𝐚𝐬𝐬 𝐨𝐟 𝐚𝐠𝐠𝐫𝐞𝐠𝐚𝐭𝐞 𝐩𝐚𝐬𝐬𝐢𝐧𝐠 𝟐.𝟑𝟔𝐦𝐦 𝐬𝐢𝐞𝐯𝐞
AIV = × 𝟏𝟎𝟎
𝐌𝐚𝐬𝐬 𝐨𝐟 𝐚𝐠𝐠𝐫𝐞𝐠𝐚𝐭𝐞 𝐫𝐞𝐭𝐚𝐢𝐧𝐞𝐝 𝐢𝐧 𝟐.𝟑𝟔𝐦𝐦 𝐬𝐢𝐞𝐯𝐞
𝟖𝟎𝟓.𝟓
= × 𝟏𝟎𝟎
𝟐𝟕𝟑𝟓
= 29.452
𝐓𝐄𝐒𝐓 𝐀+𝐓𝐄𝐒𝐓 𝐁
Average AIV =
𝟐
𝟐𝟖.𝟗𝟖𝟑+𝟐𝟗.𝟒𝟓𝟐
=
𝟐
=29.22
The slump test is prescribed by BS 1881: Part 102: 1983. The slump test result is shown
The slump value decreases as the amount of marble powder increases. The decrease is
caused by higher absorption of water by marble powder. This gives an idea of the water
Slump results for all the mixes were within the design limits (60-180mm), with an
53
Table 4.5: Slump for different types of mixes
M0 (control mix) 11
M1 (2% replacement) 11
M2 (4% replacement) 13
M3 (6% replacement) 15
M4 (8% replacement) 15
M5 (10% replacement) 16
18
16
14
12
10
SLUMP
0
M0 M1 M2 M3 M4 M5
54
4.4 Compressive strength
replacement of cement with marble powder in the concrete. There was a decrease in
compressive strength at 10% replacement and above compared with the control concrete.
compressive strength at 5% replacement with marble powder is the highest for all
percentage replacements with marble powder. The compressive strength of the sieved
marble powder at 15% replacement is higher than the compressive strength at 20%
replacement (69%) and higher than the compressive strength of the control concrete
(19%) at 7 days and those of the marble powder particles. At 28 days, 15% replacement
with sieved marble powder gave the highest compressive strength increase in the study
compared to the control concrete (16%) and hence for all replacements in the work. This
55
Table 4.6: compressive strength for 7 and 28 days
N/𝑚𝑚2 N/𝑚𝑚2
56
45
40
35
30
25
7 DAYS
20 28 DAYS
15
10
0
M0 M1 M2 M3 M4 M5 MSV1 MSV2
The movement of liquids through porous materials brought on by surface tension in the
capillaries is known as water absorption. The highest amount of water absorbed by the
marble powder, as determined by the given result, indicates that the material has a higher
57
Table 4.8: Water absorption capacity at of the casted concrete at varying
replacement percentage
58
CHAPTER FIVE
The research on the use of marble powder is vital because of the increment in the prices
of construction materials in Nigeria particularly cement which the marble powder has
successfully replaced up to 15% when sieved. Marble powder is one material that is
readily available in Nigeria particularly in Edo, Delta, Kogi and other states due to the
The following are conclusions deducted from the experimental investigation of the use of
marble powder in the mix increased, there was a noticeable reduction in the sorptivity
of concrete.
attributed to the dilution effect caused by the addition of inert marble powder
3. Based on the findings of the study, the optimal percentage of marble powder
59
marble powder, within the range of 0% to 10%, can yield concrete mixes that exhibit
cement with marble powder (MBP) on the compressive strength and sorptivity of
concrete has provided valuable insights. The findings support the potential of marble
5.1 RECOMMENDATIONS
1. In this experimental study, only the compression strength and workability of concrete
was checked, however, effect of marble powder on flexural and tensile strength of
3. Use of smaller aperture sieve sizes to sieve the marble powder and study for more
concrete.
5. Further study should be carried out on the durability of marble powder concrete to
60
REFERENCES
Ahmad, S., and Mahmood, N. (2019). Impact of marble powder on the compressive
strength of concrete. Construction and Building Materials, Vol. 203, pp. 224-236.
102-114.
Aly, M., and Hashmi, M. S. J. (2019). Mechanical properties of concrete with marble
Bhutta, A. R., et al. (2018). Effect of marble powder on the pore structure of
Biswas, S., et al. (2019). Optimization of particle size of marble powder for improved
compatibility with cement. Construction and Building Materials, Vol. 216, pp.
24-38.
incorporating marble powder. Construction and Building Materials, Vol. 258, pp.
120377.
Gupta, N., Sharma, V., Bhandari, S., and Siddique, R. (2021). Role of sustainable
61
Kumar, A., and Sinha, A. (2021). Influence of marble powder on the microstructural
122585.
Kumar, P., and Bhargava, P. (2018). Effect of varying percentages of marble powder
Malik, A., and Singh, M. (2020). Long-term performance of concrete with marble
Morsy, M. S., et al. (2020). Synergistic effects of incorporating nano silica and
Rathaur, N., and Khan, R. (2021). Synergistic effects of marble powder and
powder in concrete. Construction and Building Materials, Vol. 208, pp. 663-675.
Rathore, D., et al. (2022). Impact of curing conditions on concrete with marble
Rana, A., and Tariq, A. (2020). Sorptivity of concrete incorporating marble powder.
pp. 636-646.
Shukla, A., and Patidar, S. (2019). Experimental study on the mechanical properties
Siddique, et al. (2018). A review of studies on the use of marble powder in concrete.
Singh, L. P., et al. (2019). Effect of marble powder on the microstructure of concrete.
incorporating marble powder. Construction and Building Materials, Vol. 315, pp.
125385.
Yadav, M., and Saini, M. (2022). Durability aspects of concrete with marble powder:
Impact on sorptivity. Construction and Building Materials, Vol. 308, pp. 125022.
63
Zegardło, B., and Moczko, E. (2019). Rheological properties of concrete mixtures
incorporating marble powder. Construction and Building Materials, Vol. 212, pp.
373-381.
64
APPENDIX
65
66