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net

ICS 75.160.20
E 31

National Standard of the People’s Republic of China

GB 19147-2016
Replaces GB 19147-2013

Automobile Diesel Fuels

车用柴油

(English Translation)

Issue date: 2016-12-23 Implementation date: 2016-12-23

Issued by the General Administration of Quality Supervision,
Inspection and Quarantine of the People’s Republic of China
the Standardization Administration of the People’s Republic
of China

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Contents

Foreword ............................................................................................................................ i
1 Scope .......................................................................................................................... 1
2 Normative References ................................................................................................. 1
3 Terms and Definitions .................................................................................................. 3
4 Product Classification .................................................................................................. 4
5 Technical Requirements and Test Methods ................................................................. 4
6 Sampling ..................................................................................................................... 9
7 Marking, Packaging Transportation and Storage ......................................................... 9
8 Safety .......................................................................................................................... 9
9 Standard Implementation ............................................................................................. 9
Annex A (Informative) Minimum Temperatures of Regions with the Hazard Rate of 10%
........................................................................................................................................ 11
Annex B (Normative) Inspection of Nitrate Type Cetane Number Improver in Diesel
Fuels ............................................................................................................................... 13

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Foreword

ChinaStandards.net is in charge of this English translation. In case of any doubt about the
English translation, the Chinese original shall be considered authoritative.

All the technical contents of this standard are compulsory.

This standard is developed in accordance with the rules given in GB/T 1.1-2009

This standard replaces GB 19147-2013 Automobile Diesel Fuels (V ).

In addition to a number of editorial changes, the following technical changes have been
made with respect to GB 19147-2013.

——"It is forbidden to add methanol in automobile diesel fuels manually" is added (see 5.1;
5.1 of 2013 edition);

——The technical requirements and test methods for automobile diesel fuels (III) (see
Table 1 of 2013 edition) are deleted and technical requirements and test method for
automobile diesel fuels (VI) (see Table 3) are added;

——The flash point of 5#, 0# and -10# automobile diesel fuels is improved to 60℃ at
least (see Tables 1 and 2; Tables 2 and 3 of 2013 edition);

——The arbitration test method for 10% carbon residue on residuum is modified to that
specified in GB/T 17144;

——The arbitration test method for polycyclic

aromatic hydrocarbon contents is modified to that specified in SH/T 0806;

——The determination method as specified in NB/SH/T 0916 for fatty acid methyl ester
contents are added and adopted as arbitration test methods;

Chapter 9 "Standard Implementation" is modified (see Chapter 9; Chapter 9 of 2013

edition).

This standard was proposed by the National Energy Administration.

This standard is under the jurisdiction of the Subcommittee on Petroleum Fuels and
Lubricants of National Technical Committee on Petroleum Products and Lubricants of
Standardization Administration of China (SAC/TC 280/SC 1).

The previous editions of standards replaced by this standard are as follows:

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——GB/T 19147-2003, GB/T 19147-2009, GB 19147-2013 Automobile Diesel Fuels (IV)

and GB 19147-2013 Automobile Diesel Fuels (V).

ii

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Automobile Diesel Fuels

Warning——If suitable precautionary measures are not taken, the products in this
standard may be at risk in the process of producing, transportation, loading and
unloading, storage and application, etc. This standard does not purport to address
all the safety concerns associated with the product. It is the responsibility of the
user to adopt appropriate safety and preventive measures and determine the
conditions specified in relevant national laws and regulations.

1 Scope

This standard specifies the terms and definitions, product classification, technical
requirements, test methods, sampling, marking, packaging, transportation and storage as
well as safety of automobile diesel fuels and the standard implementation.

This standard is applicable to the automobile diesel fuels used for compression ignition
engine automobile, made from petroleum or added with additive which can improve the
service performance. This standard is not applicable to the automobile diesel fuels with
biodiesel fuel as the blending component.

2 Normative References

The following referenced documents are indispensable for the application of this
document. For dated references, only the edition cited applies. For undated references,
the latest edition of the referenced document (including any amendments) applies.

GB 190 Packing Symbol of Dangerous Goods

GB/T 258 Standard Test Method for Determination of Acidity of Light Petroleum
Products

GB/T 260 Determination of Water Content in Petroleum Products

GB/T 261 Determination of Flash Point - Pensky-Martens Closed Cup Method

GB/T 265 Petroleum Products - Determination of Kinematic Viscosity and

Calculation of Dynamic Viscosity

GB/T 268 Petroleum Products - Determination of Carbon Residue (Conradson

Method)

GB/T 386 Standard Test Method for Cetane Number of Diesel Fuel Oil

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GB/T 508 Petroleum Products - Determination of Ash

GB/T 510 Petroleum Products - Determination of Solidification Point

GB/T 511 Petroleum Products and Additives - Method for Determination of

Mechanical Admixtures

GB/T 1884 Crude Petroleum and Liquid Petroleum Products - Laboratory

Determination of Density - Hydrometer Method

GB/T 1885 Petroleum Measurement Tables

GB/T 4756 Petroleum Liquids - Manual Sampling

GB/T 5096 Petroleum Products - Corrosiveness to Copper - Copper Strip Test

GB/T 6536 Standard Test Method for Distillation of Petroleum Products at

Atmospheric Pressure

GB/T 11133 Standard Test Method for Determination of Water in Petroleum

Products, Lubricating Oils, and Additives - Coulometric Karl Fischer
Titration Method

GB/T 11139 Distillate Fuels - Calculation of Cetane Index

GB/T 11140 Standard Test Method for Sulfur in Petroleum Products by

Wavelength Dispersive X - Ray Fluorescence Spectrometry

GB/T 17144 Petroleum Products - Determination of Carbon Residue - Micro

Method

GB/T 20828 Biodiesel Blend Stock (BD100) for Diesel Engine Fuels

GB/T 23801 Determination of Fatty Acid Methyl Esters (FAME) in Middle

Distillates by Infrared Spectroscopy Method

GB 30000.7-2013 Rules for Classification and Labelling of Chemicals - Part 7:

Flammable Liquids

GB/T 30515 Petroleum Products - Transparent and Opaque Liquids -

Determination of Kinematic Viscosity and Calculation of Dynamic
Viscosity

GB/T 33400 Determination of Total Pollutants in Middle Distillate Oil, Diesel Oil

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and Fatty Acid Methyl Ester

SH 0164 Petroleum Products - Rules in Packaging, Handling, Delivery and

Acceptance

SH/T 0175 Standard Test Method for Oxidation Stability of Distillate Fuel Oil
(Accelerated Method)

SH/T 0246 Determination of Water Content in Light Petroleum Products

(Coulometric Method)

SH/T 0248 Diesel and Domestic Heating Fuels - Determination of Cold Filter
Plugging Point

SH/T 0604 Crude Petroleum and Petroleum Products - Determination of Density

- Oscillating U-tube Method

SH/T 0606 Standard Test Method for Hydrocarbon Types in Middle Distillates by
Mass Spectrometry

SH/T 0689 Standard Test Method for Determination of Total Sulfur in Light
Hydrocarbons Motor Fuels and Oils by Ultraviolet Fluorescence

SH/T 0694 Calculation of Cetane Index of Middle-distillate Fuels by the

Four-Variable Equation

SH/T 0765 Diesel Fuel - Assessment of Lubricity Using the High-frequency

Reciprocating Rig (HFRR)

SH/T 0806 Determination of Aromatic Hydrocarbon Types in Middle Distillates -

High Performance Liquid Chromatography Method with Refractive
Index Detection

NB/SH/T 0916 Determination of Biodiesel Fuel (Fatty Acid Methyl Ester) in Diesel
Oil Fuel by Infrared Spectroscopy Method

ASTM D7039 Standard Test Method for Sulfur in Gasoline，Diesel Fuel，Jet Fuel，
Kerosine，Biodiesel，Biodiesel Blends，and Gasoline-Ethanol Blends
by Monochromatic Wave-length Dispersive X-ray Fluorescence
Spectrometry

3 Terms and Definitions

For the purposes of this document, the following term and definition apply.

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3.1

content of polycyclic aromatic hydrocarbons

the content of total aromatic hydrocarbon deducted by that of simple aromatic

hydrocarbon.

4 Product Classification

Automobile diesel fuels are classified into six designations according to solidification point:

5# automobile diesel fuels: applicable to be used in the regions with the hazard rate of
10% and the minimum temperature above 8℃;

0# automobile diesel fuels: applicable to be used in the regions with the hazard rate of
10% and the minimum temperature above 4℃;

-10# automobile diesel fuels: applicable to be used in the regions with the hazard rate of
10% and the minimum temperature above -5℃;

-20# automobile diesel fuels: applicable to be used in the regions with the hazard rate of
10% and the minimum temperature above -14℃;

-35# automobile diesel fuels: applicable to be used in the regions with the hazard rate of
10% and the minimum temperature above -29℃;

-50# automobile diesel fuels: applicable to be used in the regions with the hazard rate of
10% and the minimum temperature above -44℃;

Note: See Annex A to select automobile diesel fuels of different designations.

5 Technical Requirements and Test Methods

5.1 The additives used in automobile diesel fuels shall be free from recognized adverse
effects and shall be used according to the recommended suitable dosage. Automobile
diesel fuels shall not contain any additives and pollutants that may lead to automobile’s
failing of normal operation. It is forbidden to add methanol in automobile diesel fuels
manually.

5.2 The technical requirements and test methods for automobile diesel fuels (IV),
automobile diesel fuels (V) and automobile diesel fuels (VI) are detailed in Table 1, Table 2
and Table 3 respectively.

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Table 1 Technical Requirements and Test Methods for Automobile Diesel Fuels (IV)
Quality index
Item Test method
5# 0# -10# -20# -35# -50#
Oxidation stability (calculated by total
insolubles)/(mg/100mL) SH/T 0175
≤ 2.5
a
Sulfur content /(mg/kg) ≤ 50 SH/T 0689
Acidity (calculated by KOH)/ (mg/100 mL) ≤ 7 GB/T 258
b
10% carbon residue on residuum (mass
GB/T 17144
fraction)/％ ≤ 0.3
Ash content (mass fraction)/% ≤ 0.01 GB/T 508
Copper strip corrosion (50℃, 3h)/grade ≤ 1 GB/T 5096
c
Water content (volume fraction)/％ ≤ Trace GB/T 260
d
Mechanical impurity None GB/T 511
Lubricity
SH/T 0765
Diameter of corrected wear scar (60℃)/μm ≤ 460
e
Content of polycyclic aromatic hydrocarbon
SH/T 0806
(mass fraction)/% ≤ 11
Kinematic viscosity f (20℃)/(mm2/s) 3.0~8.0 2.5~8.0 1.8~7.0 GB/T 265
Solidification point/℃ ≤ 5 0 -10 -20 -35 -50 GB/T 510
Cold filter plugging point/℃ ≤ 8 4 -5 -14 -29 -44 SH/T 0248
Flash point (enclosed)/℃ ≥ 60 50 45 GB/T 261
Cetane number ≥ 49 46 45 GB/T 386
g
Cetane index ≥ 46 46 43 SH/T 0694
Distillation range:
50% recovered temperature/℃ ≤ 300
GB/T 6536
90% recovered temperature/℃ ≤ 355
95% recovered temperature/℃ ≤ 365
GB/T 1884
Density h (20℃)/(kg/m3) 810~850 790~840
GB/T 1885
i
Content of fatty acid methyl ester
1.0 NB/SH/T 0916
(volume fraction)/% ≤
a
GB/T 11140 and ASTM D7039 may also be adopted for making determination. If any dispute, the method
specified in SH/T 0689 shall prevail.

b
GB/T 268 may also be adopted for making determination. If any dispute, the method specified in GB/T
17144 shall prevail. If the automobile diesel fuels contain nitrate type cetane number improver, 10% carbon
residue on residuum shall be determined with the base fuel without nitrate. See Annex B for the method to
inspect whether nitrate type cetane number improver is contained in automobile diesel fuels.

c
Visual observation may be used, namely, inject the sample into a 100mL glass measuring cylinder,
observe it at room temperature (20℃±5℃), the solution shall be transparent and free from suspension and
settled moisture.GB/T 11133 and SH/T 0246 may also be adopted for making determination. If any dispute,
the method specified in GB/T 260 shall prevail.
5

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Quality index
Item Test method
5# 0# -10# -20# -35# -50#
d
Visual observation may be used, namely, inject the sample into a 100mL glass measuring cylinder,
observe it at room temperature (20℃±5℃), the solution shall be transparent and free from suspension and
settled impurity. If any dispute, the method specified in GB/T 511 shall prevail.

e
SH/T 0606 may also be adopted for making determination. If any dispute, the method specified in SH/T
0806 shall prevail.

f
GB/T 30515 may also be adopted for making determination. If any dispute, the method specified in GB/T
265 shall prevail.

g
GB/T 11139 may also be adopted for the calculation of cetane index. If any dispute, the method in SH/T
0694 shall prevail.

h
SH/T 0604 may also be adopted for making determination. If any dispute, the method specified in GB/T
1884 and GB/T 1885 shall prevail.

i
Fatty acid methyl ester shall meet the requirements of GB/T 20828. GB/T 23801 may also be adopted for
making determination. If any dispute, the method specified in NB/SH/T 0916 shall prevail.

Table 2 Technical Requirements and Test Methods for Automobile Diesel Fuels (V)
Quality index
Item Test method
5# 0# -10# -20# -35# -50#
Oxidation stability (calculated by total
insolubles)/(mg/100mL) SH/T 0175
≤ 2.5
a
Sulfur content /(mg/kg) ≤ 10 SH/T 0689
Acidity (calculated by KOH)/ (mg/100 mL) ≤ 7 GB/T 258
b
10% carbon residue on residuum (mass
0.3 GB/T 17144
fraction)/％ ≤
Ash content (mass fraction)/% ≤ 0.01 GB/T 508
Copper strip corrosion (50℃, 3h)/grade ≤ 1 GB/T 5096
c
Water content (volume fraction)/％ ≤ Trace GB/T 260
d
Mechanical impurity None GB/T 511
Lubricity
SH/T 0765
Diameter of corrected wear scar (60℃)/μm ≤ 460
e
Content of polycyclic aromatic hydrocarbon
SH/T 0806
(mass fraction)/% ≤ 11
Kinematic viscosity f (20℃)/(mm2/s) 3.0~8.0 2.5~8.0 1.8~7.0 GB/T 265
Solidification point/℃ ≤ 5 0 -10 -20 -35 -50 GB/T 510
Cold filter plugging point/℃ ≤ 8 4 -5 -14 -29 -44 SH/T 0248
Flash point (enclosed)/℃ ≥ 60 50 45 GB/T 261
Cetane number ≥ 51 49 47 GB/T 386
6

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