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 .
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Volume 4
Nanoscience
 .
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP001 View Online
 View Online

A Specialist Periodical Report

Nanoscience
Volume 4
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP001

A Review of Recent Literature

Editors
P. John Thomas, Bangor University, UK
Neerish Revaprasadu, University of Zululand, South Africa

Authors
Mohammad Al Kobaisi, RMIT University, Australia
Anuradha, RMIT University, Australia
Ramjee Balasubramanian, Old Dominion University, USA
Sean N. Baxter, Bangor University, UK
Sheshanath V. Bhosale, RMIT University, Australia
Jack R. Brent, The University of Manchester, UK
Gilberto Casillas, University of Wollongong, Australia
Francis Leonard Deepak, International Iberian Nanotechnology
Laboratory, Portugal
R. Dunpall, University of Zululand, South Africa
Akhil Gupta, Deakin University, Australia
.

Duong Duc La, RMIT University, Australia

David J. Lewis, The University of Manchester, UK
Karthik Ramasamy, UbiQD, LLC, USA
Anushri Rananaware, RMIT University, Australia
N. Revaprasadu, University of Zululand, South Africa
Richard A. Taylor, The University of the West Indies, Trinidad and Tobago
Aleksander A. Tedstone, The University of Manchester, UK
P. John Thomas, Bangor University, UK
 View Online

ISBN: 978-1-78262-159-1
PDF eISBN: 978-1-78262-035-8
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP001

EPUB eISBN: 978-1-78801-249-2

DOI: 10.1039/9781782620358
ISSN: 2049-3541

A catalogue record for this book is available from the British Library

r The Royal Society of Chemistry 2017

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 Preface
DOI: 10.1039/9781782620358-FP005

Welcome to the fourth Royal Society of Chemistry SPR on Nanoscience.

Research in the area of Nanoscience continues to burgeon, attracting
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP005

interest from all areas of physical and medical sciences. The area is truly
at the forefront of worldwide research efforts. Concomitant with this
status, is an increase in the volume of outputs and scale of activity. In this
context, gaining a perspective of developments is challenging for both
new comers to the field and seasoned veterans. We have attempted to
address this challenge and provide an overview of the developments in
the area, focusing specifically on the past few years. Chapters in this
volume cover developments in 2D materials, transmission electron
microscopy, cancer treatment, ligand design and synthesis, quantum dot
solar cells, luminopphores as well as synthetic strategies for nanocrystals.
We very much hope you enjoy reading the book.

P. John Thomas (Bangor)

Neerish Revaprasadu (Zululand)
.

Nanoscience, 2017, 4, v–v | v

c The Royal Society of Chemistry 2017
 Author biographies
DOI: 10.1039/9781782620358-FP006

Dr Mohammad Al Kobaisi, born in 1971 in

Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP006

Iraq, awarded his MSc in Physical Chemistry

from Shahid Beheshti University in 1999,
and PhD under the supervision of A/Prof.
Colin Rix and Professor David Mainwaring
from RMIT University in 2007 investigating
the design of new selective adsorbent
polymers for sensing application. Since 2007
he continued his research career working
in Professor David Mainwaring team in
designing drug delivery and vaccine delivery
systems in collaboration with the pharma-
ceutical industry. His general research
interest remains in molecular design and in developing nano- and micro-
functional materials as vaccine delivery systems.

Anuradha obtained her Master’s degree in

chemistry at Jamia Hamdard University,
New Delhi, India. Now she is pursuing PhD
degree at RMIT University, Melbourne,
Australia with Dr Sheshanath Bhosale. Her
.

interest involves synthesis of Aggregation

Induced Emission molecules for application
in supramolecular chemistry mainly.

vi | Nanoscience, 2017, 4, vi–xii

c The Royal Society of Chemistry 2017
 View Online

Ramjee Balasubramanian graduated with a

B.Sc. (Chemistry) from Loyola College, Madras
and obtained his M.S. (Chemical Sciences)
and PhD (Organic Chemistry) from the Indian
Institute of Science, Bangalore, India. After
postdoctoral stints in the laboratories of Prof.
Alexander Wei (Department of Chemistry,
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP006

Purdue University, IN) and Prof. Royce W.

Murray (Department of Chemistry, University
of North Carolina, Chapel Hill, NC), he joined
Old Dominion University as an Assistant Pro-
fessor. Currently, he is an Associate Professor
and his research interests are in the general
areas of synthesis, functionalization and applications of polymeric nano-
capsules and inorganic nanoparticles.

Sean N. Baxter obtained his MChem from

the University of Wales, Bangor, in 2012.
He secured a PGCE and spent time teaching
before returning to Bangor University, where
he is currently a Senior Demonstrator,
pursuing his PhD. His research, under the
supervision of Dr P. John Thomas, is into the
synthesis and uses of thin film nanocrystals.
He is a member of the Royal Society of
Chemistry.
.

Sheshanath V. Bhosale (Shesh), born in 1976

in Indral Tq. Devoni, completed his M.Sc. in
chemistry from the Udgiri college Udgir
(S.R.T.M.U. Nanded) in 1999. He then
worked as a project assistant at NCL, Pune,
before moving to the Freie University Berlin,
Germany, where he received his PhD (Magna
Cum Lauda) in supramolecular chemistry
under the supervision of Prof. J. H. Fuhrhop
in 2004. Dr Bhosale pursued his post-
doctoral studies with Prof. S. Matile at
University of Geneva, Switzerland, under the
auspices of a Roche Foundation Fellowship.
This was followed by a stay at Monash University, Australia, for five years as
an ARC-APD Fellow. Shesh received a prestigious Future Fellowship (2011)
from the Australian Research Council and is now working at the School of
Science, RMIT University, Melbourne, Australia. Shesh is interested in
design and synthesis of p-functional materials, especially small molecules,
for sensing, biomaterials and supramolecular chemistry applications.

Nanoscience, 2017, 4, vi–xii | vii

 View Online

Jack R. Brent received his M.Chem. from the

University of Manchester in 2012 and has
recently completed his PhD under the
supervision of Paul O’Brien CBE FRS. His
doctoral studies focussed on the production
and examination of 2D materials, in par-
ticular, ultrasonically exfoliated phosphor-
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP006

ene and 2D tin(II) sulfide and the solventless

growth of MoS2 quantum dots. He is cur-
rently a Postdoctoral Research Associate at
the University of Manchester, working on
the production of 2D field effect transistors
with Professor Brian Derby.

Gilberto Casillas is currently a Transmission

Electron Microscopist at the Electron
Microscopy Centre at the University of
Wollongong, Australia. He received his PhD
in Physics from the University of Texas at
San Antonio, USA, in 2013. His main area of
research is focused in the implementation of
Aberration-Corrected S/TEM in combination
with Electron Energy Loss Spectroscopy in
the characterization of nanomaterials for a
wide range of applications, as well as in the
study of fundamental physical phenomena
at the atomic scale. He also focuses on in situ
.

TEM experimentation to explore the dynamics of deformation mech-

anisms at the nanoscale.

Francis Leonard Deepak is a group leader

in the Department of Advanced Electron
Microscopy, Imaging and Spectroscopy at
the International Iberian Nanotechnology
Laboratory (Braga, Portugal). He received his
PhD in 2005 from Jawaharlal Nehru Centre
for Advanced Scientific Research, Bangalore,
India. Subsequently, he was a postdoctoral
fellow (2006–2008) at the Weizmann Insti-
tute of Science, Israel. His broad area of
research is focused on the use of advanced
electron microscopic and spectroscopic
techniques for the study of materials/
nanomaterials for various applications, as well as in the study of
nanoscale phenomena. He also employs the Focused Ion Beam (FIB)
technique extensively towards the investigations of nanodevices.

viii | Nanoscience, 2017, 4, vi–xii

 View Online

Dr Rekha Dunpall obtained her PhD in

Biochemistry from the University of Zululand,
South Africa in 2016. Her research interest lies
in nanotoxicology, biosafety and the develop-
ment of biocompatible nanomaterials for
drug delivery and bio-imaging applications.
She has presented several scientific papers
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP006

at accredited conferences such as MAM-14,

NanoAfrica and BioNanoMed and has pub-
lished several articles in ISI journals. She
is currently involved in developing and opti-
mising in vivo animal models for anticancer
and drug delivery research.

Akhil Gupta completed his PhD in 2014 from

the Department of Materials Engineering,
Monash University, Clayton, Victoria,
Australia. He is currently employed as a
Research Fellow at Deakin University,
Waurn Ponds, Victoria Australia. He is also
a visiting Research Fellow at the CSIRO
Manufacturing, Clayton, Victoria Australia.
He is involved in fundamental and applied
research in the areas of organic electronics,
solar cells in particular, photonics and drug
discovery. He has additional research activ-
ities in the areas of supramolecular assem-
.

bly for light harvesting, device fabrication, and molecular gels for sensing
and photovoltaic applications.

Duong Duc La obtained his MSc degree in

Nanotechnology of hybrid materials for
superhydrophobic surface and hydrogen
sensing at HanYang University (Korea) in
2010. Now he is pursuing his PhD degree at
RMIT University (Australia) in the group of
Dr Sheshanath Bhosale. In his study,
he mainly focuses on fabricating hybrid
materials of inorganic and organic (supra-
molecules) compounds via novel approach of
self-assembly for photocatalysis, sensing and
electronics devices. He is also working on the
fabrication of graphene-based materials for
photovoltaic and adsorption applications.

Nanoscience, 2017, 4, vi–xii | ix

 View Online

David J. Lewis (ORCID iD: 0000-0001-5950)

is a Lecturer in Functional Ceramic and
Inorganic Materials at the University of
Manchester, U.K. He received M.Sci. and PhD
degrees at the University of Birmingham,
U.K. in 2002 and 2006 respectively.
Throughout his career DJL has developed
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP006

interests in nanomaterials of all dimensions

for a range of applications. He is a member of
both the Royal Society of Chemistry (MRSC)
and the American Chemical Society (ACS). In
March 2016 DJL was named by the Royal
Society of Chemistry as being in the top 10%
of highly cited authors in their ‘General
Chemistry’ portfolio of journals.

Dr Karthik Ramasamy is Director of

Chemistry at UbiQD LLC, and leads research
and development on synthetic methods and
scale-up. He received his BSc and MSc in
Chemistry from Bharathidasan University,
Tiruchirappalli, India. Dr Ramasamy received
his PhD in Chemistry under the supervision
of Professor Paul O’Brien FRS (founder of
Nanoco) at the University of Manchester, UK
for a thesis titled ‘‘New Molecular Precursors
for Metal Sulfides’’ in 2010. Before joining
.

UbiQD in 2016, Dr Ramasamy held post-

doctoral positions at the University of
Alabama and Los Alamos National Laboratory. Over the past eight years,
his research has mainly focused on developing new synthetic methods for
metal chalcogenide nanocrystals. He has more than 50 publications and
over 1000 citations relating to quantum dots and is an expert at optimizing
and scaling up the synthesis alloyed metal sulfides quantum dots.

Anushri Rananaware received her M.Sc.

degree in Organic Chemistry from Fergusson
College, Pune, India in 2007. Then she star-
ted working in R & D department of Sai Life
Sciences Pvt. Ltd, India for 6 years until 2014.
Now she is carrying her PhD degree under
the guidance of Dr Sheshanath Bhosale at
RMIT University, Melbourne, Australia. Her
research is mainly focusing on the synthesis
of novel AIE materials for various supra-
molecular applications.

x | Nanoscience, 2017, 4, vi–xii

 View Online

Neerish Revaprasadu is a professor of

Chemistry and SARChI Chair holder in
Nanotechnology. He obtained his
BSC(Hons.) from University of Natal in 1993
and PhD from Imperial college, London in
2000. He started as a Senior Lecturer at
Unizulu 2000, Associate Professor in 2004
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP006

and full professor in 2008. His research

interest is in the synthesis of semiconductor
nanomaterials. He has worked extensively
on cadmium, lead, copper, iron and bis-
muth chalcogenide materials. He also has
worked on applications of gold core shell
nanoparticles for drug delivery applications. He has co-authored 150
articles in peer reviewed journals and supervised more than 25 post-
graduate (M.Sc and PhD) students. In 2014 he was elected as member to
the South African Academy of Science (ASSAF).

Richard A. Taylor holds a PhD in Chemistry

and a BSc in Pure and Applied Chemistry
from The University of the West Indies (UWI)
Mona Campus, Jamaica. He has been twice
visiting scholar at the Schools of Chemistry
and of Materials, University of Manchester,
UK, working with Professor Paul O’Brien
FRS. He is currently Lecturer in Materials
Chemistry at The UWI, St. Augustine
.

Campus, Trinidad. There, through a small

research group of PhD students he has foc-
cused his research on optoelectronic mater-
ials including, novel metal-organic liquid
crystals, chalcogenide semiconductor thin films and nanomaterials
(quantum dots) and luminescent metal-organic frameworks.

Aleksander A. Tedstone received his

M.Chem. from the University of Manchester
in 2013, and continues to study at the same
institution as a doctoral researcher working
in the field of inorganic chemistry and
materials synthesis under the supervision of
Prof. Paul O’Brien CBE FRS and Dr David
J. Lewis. He is interested in the modification
and application of two-dimensional
materials.

Nanoscience, 2017, 4, vi–xii | xi

 View Online

P. John Thomas obtained his PhD from

JNCASR, India working with Profs. C. N. R.
Rao, FRS and G. U. Kulkarni. He carried out
post-doctoral research in Bangalore and in
Manchester with Prof. Paul O’Brien, CBE,
FRS, FREng. He was then a RCUK Research
Fellow in Manchester, before taking up post
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP006

as a Lecturer of Physical Chemistry and

Bangor. He is a Fellow of the Higher Edu-
cation Academy and a member of the Royal
Society of Chemistry.
.

xii | Nanoscience, 2017, 4, vi–xii

 CONTENTS

Cover
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP013

Preface v

Author biographies vi

Role of ligands in the synthesis of bi- and multi-metallic 1

nanocrystals
.

Ramjee Balasubramanian
1 Introduction 1
2 Ligand effects 4
3 Influence of coordination ligands on metal precursors 8
4 Influence of linear surfactants 12
5 Influence of macrocyclic surfactants 21
6 Conclusion 25
References 26

Recent highlights in advanced transmission electron microscopy 29

techniques: applications to nanomaterials
Francis Leonard Deepak and Gilberto Casillas
1 Introduction to aberration corrected S/TEM 29
2 AC-TEM imaging of carbon nanomaterials and related 31
hybrid structures
3 Nanoparticles 34
4 1D Nanomaterials 37

Nanoscience, 2017, 4, xiii–xv | xiii

c The Royal Society of Chemistry 2017
 View Online

5 2D Materials 39
6 Beam sensitive materials 42
7 3D Techniques 43
8 In situ electron microscopy 45
9 Conclusions 49
Acknowledgements 50
References 50
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP013

Gold fabricated core–shell nanoparticles as innovative cancer 57

therapeutic strategies to improve drug delivery
R. Dunpall and N. Revaprasadu
1 Introduction to cancer therapeutics 57
2 Gold based core–shell nanoparticles for cancer drug 59
delivery
3 Nano-drug formulations for cancer drug delivery 66
4 Pharmaceutical formulation and drug development 69
5 Future perspectives for gold based core–shell 71
nanoparticles
Acknowledgements 71
References 71

Supramolecular chemistry of AIE-active tetraphenylethylene 75

luminophores
Duong Duc La, Anuradha, Akhil Gupta, Mohammad Al Kobaisi,
.

Anushri Rananaware and Sheshanath V. Bhosale

1 Introduction 75
2 AIE-active TPE luminogen 76
3 General syntheses and reactivity 78
4 Self-assembly of PDI, NDI and porphyrin bearing 78
TPE moieties
5 TPE moieties bearing macromolecules 85
6 Chiral assembly 89
7 Applications 95
Acknowledgements 102
References 102

A review of two-dimensional nanomaterials 108

beyond graphene
Aleksander A. Tedstone, Jack R. Brent and David J. Lewis
1 Introduction 108
2 Two-dimensional (2D) nanomaterials 109

xiv | Nanoscience, 2017, 4, xiii–xv

 View Online

3 Heterostructures 128
4 Conclusions and outlook 130
Notes and references 130

Colloidal quantum dots solar cells 142

Richard A. Taylor and Karthik Ramasamy
Published on 08 August 2017 on http://pubs.rsc.org | doi:10.1039/9781782620358-FP013

1 Introduction, historical background of colloidal 142

quantum dots
2 Semiconductors: dimensionality and quantum confined 143
structures
3 Optoelectronic properties of CQDs 146
4 CQD chemical properties 149
5 Doped CQDs 153
6 CQD synthesis 154
7 Thin film fabrication 156
8 Electrical properties of colloidal quantum dots 158
9 Solar cell device physics and performance 161
10 Conclusion and perspective 164
References 164

The role of ligands in mediating charge transport in 169

nanocrystalline medium
Sean N. Baxter and P. John Thomas
.

1 Introduction 169
2 Coulomb blockade and single electron tunnelling 169
3 Charge transport in arrays of nanocrystals 172
4 Ligands and charge transport 175
References 182

Nanoscience, 2017, 4, xiii–xv | xv

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