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Edited by Qiang Xu

NANOPOROUS
MATERIALS
Synthesis and Applications
NANOPOROUS
MATERIALS
Synthesis and Applications
Edited by Qiang Xu

NANOPOROUS
MATERIALS
Synthesis and Applications

Boca Raton London New York

CRC Press is an imprint of the

Taylor & Francis Group, an informa business
CRC Press
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Boca Raton, FL 33487-2742
© 2013 by Taylor & Francis Group, LLC
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Version Date: 20121106

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Contents
Preface......................................................................................................................vii
Editor.........................................................................................................................ix
Contributors...............................................................................................................xi

Chapter 1 Nanoporous Polymers........................................................................... 1

Jens Weber and Arne Thomas

Chapter 2 Design, Synthesis, and Functions of Conjugated

Microporous Polymers........................................................................ 43
Yanhong Xu, Shangbin Jin, and Donglin Jiang

Chapter 3 Nanoporous Metal–Organic Frameworks........................................... 71

Hai-Long Jiang and Qiang Xu

Chapter 4 Ordered Mesoporous Carbons Prepared by

a Soft-Templating Method...................................................................99
Norikazu Nishiyama and Shunsuke Tanaka

Chapter 5 Dealloyed Nanoporous Metals.......................................................... 125

Luyang Chen, Xingyou Lang, and Mingwei Chen

Chapter 6 Synthesis of Mesoporous Metal Oxides and Metals

and Their Applications...................................................................... 183
Hongjing Wang, Xiangfen Jiang, and Yusuke Yamauchi

Chapter 7 Preparation of Nanoporous Semiconductor-Based Materials

for Photocatalytic Applications......................................................... 201
Xingdong Wang, Maryline Chee Kimling,
and Rachel Anne Caruso

Chapter 8 Layered Zeolites: Structure Modification and Application............... 237

Peng Wu, Hao Xu, and Kun Zhang

v
vi Contents

Chapter 9 Applications of Pore Voids of Mesoporous Silica

to Acid Catalysts and Controlled Release......................................... 267
Masahiro Fujiwara

Chapter 10 Nanopore Glass................................................................................. 289

Tetsuo Yazawa

Chapter 11 Open-Framework Germanates and Related Materials...................... 319

Andrew Ken Inge and Xiaodong Zou
Preface
In the past two decades, the field of nanoporous materials has undergone accelerated
developments. As these materials possess high specific surface areas, well-defined
pore sizes, and functional sites, they show a very broad range of highly potential
applications. To demonstrate the profound progress and provide a comprehensive
recognition of nanoporous materials for researchers in this promising field, it is my
honor, as an organizer, to invite leading scientists in this field to survey the key devel-
opments of nanoporous materials in a broad range and important advances in their
applications to date, which are outlined in the chapters of this book.
The chapters start with new soft porous materials. In Chapter 1, Weber and Thomas
give an overview of the synthetic approaches and applications of a variety of meso-
and microporous polymers and organic frameworks, and in Chapter 2, Jiang and
coworkers provide a review on conjugated microporous polymers by focusing on the
design and synthesis along with the function exploration of this new class of organic
porous materials. In Chapter 3, Jiang and I introduce the synthesis and potential
applications of nanoporous metal–organic frameworks. In Chapter 4, Nishiyama and
Tanaka present how to prepare mesoporous carbons by a soft-templating method and
their applications for supercapacitors and membrane separations. Chen and cowork-
ers review the synthesis of nanoporous metals and alloys by a dealloying method
and their broad applications in Chapter 5, and Yamauchi and coworkers describe
the synthesis of mesoporous metals and metal oxides by soft- and hard-templating
methods in Chapter 6. In Chapter 7, Caruso and coworkers highlight the fabrication
of nanoporous semiconductor materials that are used for photocatalysis. As has been
extensively investigated thus far, three chapters deal with porous silica materials. Wu
and coworkers present the structural modification and functional improvement of lay-
ered zeolites in Chapter 8, Fujiwara addresses the application of mesoporous silica in
acid catalysis and drug delivery in Chapter 9, and Yazawa demonstrates the formation
and the application of glass with nanopores in Chapter 10. Finally, in Chapter 11, Inge
and Zou document the constructions and interesting properties of germanates and
related materials with open frameworks.
It is obvious that the accomplishments in nanoporous materials to date are exciting
and the potential appears to be even greater. I am sure that the nanoporous materials
field will maintain a sustained growth in the future.
I would like to deeply thank all the authors for their excellent contributions to this
book as well as to this field. Sincere thanks to Mr. Lance Wobus and Ms. Amy Blalock
(Taylor & Francis/CRC Press) for their conscientious cooperation and to Drs. Bo Liu,
Hai-Long Jiang, and Di-Chang Zhong (AIST) for their valuable assistance in the edi-
torial process.

Qiang Xu
Osaka, Japan

vii
Editor
Qiang Xu was born in China. He received his PhD degree
in physical chemistry in 1994 from Osaka University,
Japan. After working as a postdoctoral fellow at Osaka
University for a year, he started his career as a research
scientist at the Osaka National Research Institute in 1995.
Currently, he is a senior research scientist at the National
Institute of Advanced Industrial Science and Technology
(AIST) and an adjunct professor at Kobe University,
Japan. He received the Thomson Reuters Research Front
Award in 2012. His research interests include porous mate-
rials and nanostructured materials and related functional
applications.

ix
Contributors
and
CREST, Japan Science and
Technology Agency (JST)
Saitama, Japan
Research Interests: Development
of Nanoporous Metals and
Composites for Application in
Optics, Electrocatalysis, and
Energy Storage

Rachel Anne Caruso, PhD

CSIRO Materials Science and
Engineering
Clayton, Australia
and
School of Chemistry
The University of Melbourne
Melbourne, Australia
Research Interests: The Fabrication
and Application of Advanced
Porous Materials with an Mingwei Chen, PhD
Environmental Focus WPI-Advanced Institute
of Materials Research
(WPI-AIMR)
Tohoku University
Sendai, Japan
and
CREST, Japan Science and
Technology Agency (JST)
Saitama, Japan
Research Interests: Study the Relationship
between the Microstructure and
Properties of Advanced Materials
Luyang Chen, PhD
World Premier International—
Advanced Institute of Materials
Research
Tohoku University
Sendai, Japan

xi
xii Contributors

Masahiro Fujiwara, PhD Donglin Jiang, PhD

Research Institute for Ubiquitous Department of Materials Molecular
Energy Devices Science
National Institute of Advanced Institute for Molecular Science
Industrial Science and Technology National Institutes of Natural Sciences
(Kansai Center) Okazaki, Japan
Osaka, Japan
Research Interests: Design, Synthesis,
Research Interests: Materials Chemistry and Functions of Two-Dimensional
(Porous Materials, Nano Materials); Polymers and Conjugated
Catalysis Chemistry (Environmental Microporous Polymers
Catalyst)

Hai-Long Jiang, PhD

National Institute of Advanced
Andrew Ken Inge, MSci Industrial Science and Technology
Department of Materials and Osaka, Japan
Environmental Chemistry
Stockholm University Research Interests: The Development
Stockholm, Sweden of Porous Materials and
Nanostructured Materials for Gas
Research Interests: Design and Storage and Separation, as Well as
Synthesis of New Zeolite Related Catalysis
Porous Materials, and Structure
Determination of Open-Structures
by Single Crystal and Powder X-Ray
Diffraction
Contributors xiii

Xiangfen Jiang, MSci

World Premier International
Research Center for Materials
Maryline Chee Kimling, PhD
Nanoarchitectonics
School of Chemistry
National Institute for Materials Science
The University of Melbourne
Tsukuba, Japan
Melbourne, Australia
and
Faculty of Science and Engineering Research Interests: The
Waseda University Development of Structured
Tokyo, Japan Porous Materials for Environmental
Remediation Applications That
Research Interests: Synthesis of
Includes Removal of Pollutants
Mesoporous Metal Oxides
(e.g., Heavy Metals, Radionuclides)
from Polluted Water, via
Adsorption or Catalysis

Shangbin Jin, MSci

Department of Materials Molecular
Science
Institute for Molecular Science Xingyou Lang, PhD
National Institutes of Natural Sciences Department of Materials Science and
Okazaki, Japan Engineering
Jilin University
Research Interests: Design and
Changchun, China
Functions of Conjugated
Microporous Polymers Research Interests: Development of
Nanoporous Functional Metals
and the Exploitation of Their
Applications in Emerging Areas
xiv Contributors

Arne Thomas, PhD

Technische Universität Berlin
Norikazu Nishiyama, PhD (Eng.)
Berlin, Germany
Osaka University
Research Interests: Porous Functional
Osaka, Japan
Materials, Catalysis
Research Interests: Porous Materials for
Solid Catalysis, Separation Processes
and Electro-optic Devices

Shunsuke Tanaka, PhD (Eng.) Hongjing Wang, PhD

Kansai University World Premier International
Osaka, Japan Research Center for Materials
Nanoarchitectonics
Research Interests: Synthesis, Structural
National Institute for Materials Science
Characterization and Application on
Tsukuba, Japan
Ordered Porous Materials (Zeolites,
and
Coordination Polymers, Mesoporous
Faculty of Science and Engineering
Materials, etc.)
Waseda University
Tokyo, Japan
Research Interests: Synthesis of
Mesoporous Metals
Contributors xv

Peng Wu, PhD

Department of Chemistry
East China Normal University
Xingdong Wang, PhD
Shanghai, China
CSIRO Materials Science and
Engineering Research Interests: Design’ Synthesis
Clayton, Australia and Applications of Zeolites and
Related Porous Materials
Research Interests: The Development
of Hierarchically Porous Materials
and Modification with Noble Metal
Nanoparticles for Photocatalytic
Degradation of Organic Pollutants in
the Environment and Clean Energy
(e.g., H2) Production

Jens Weber, PhD Hao Xu, BS

Department of Colloid Chemistry Department of Chemistry
Max Planck Institute of Colloids and East China Normal University
Interfaces Shanghai, China
Potsdam, Brandenburg, Germany
Research Interests: Synthesis and
Research Interests: Porous Materials, Applications of Novel Zeolites
Polymer Science, Self-Assembly,
Gas Adsorption, Gas Separation,
X-Ray and Neutron Scattering,
Renewable Ressources
xvi Contributors

Qiang Xu, PhD

National Institute of Advanced Yusuke Yamauchi, PhD
Industrial Science and Technology World Premier International
Osaka, Japan Research Center for Materials
and Nanoarchitectonics
Kobe University National Institute for Materials
Kobe, Japan Science
Tsukuba, Japan
Research Interests: Porous Materials and and
Nanostructured Materials and Related Faculty of Science and Engineering
Functional Applications, Especially Waseda University
for Catalysis and Clean Energy Tokyo, Japan
and
Precursory Research for Embryonic
Science and Technology
Japan Science and Technology
Agency
Saitama, Japan
Research Interests: Synthesis and
Applications of Mesoporous
Materials

Yanhong Xu, MSci

Department of Materials Molecular
Science
Institute for Molecular Science
National Institutes of Natural
Sciences
Okazaki, Japan
Research Interests: Design and
Functions of Conjugated
Microporous Polymers
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