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 PROCESSING AND
CHARACTERIZATION OF
MULTICOMPONENT POLYMER SYSTEMS
New Insights
 PROCESSING AND
CHARACTERIZATION OF
MULTICOMPONENT POLYMER SYSTEMS
New Insights

Edited by
Jose James
Sabu Thomas
Nandakumar Kalarikkal
Yang Weimin
Kaushik Pal
Apple Academic Press Inc. Apple Academic Press Inc.
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Names: James, Jose (Chemist), editor | Sabu Thomas, editor | Nandakumar Kalarikkal, editor |
Yang Weimin, editor | Kaushik Pal, editor
Title: Processing and characterization of multicomponent polymer systems : new insights / editors,
Jose James [and four others].
Description: Toronto : Apple Academic Press, 2019. | Includes bibliographical references and index.
Identifiers: LCCN 2019007174 (print) | LCCN 2019008241 (ebook) | ISBN 9780429469794 (ebook) |
ISBN 9781771887243 (hardcover : alk. paper)
Subjects: LCSH: Polymers in medicine. | Biomedical materials. | Elastomers. | Medical instruments and
apparatus.
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ABOUT THE EDITORS

Jose James
Jose James is an Assistant Professor in the Research
and Post-Graduate Department of Chemistry at St.
Joseph’s College in Moolamattom, Idukki, Kerala,
India. Mr. James has recently submitted his PhD
thesis under the faculty development program of
the Indian University Grants Commission, under the
supervision of Prof. (Dr.) Sabu Thomas (Pro-Vice
Chancellor and Professor of Polymer Science and Engineering in School
of Chemical Science, Mahatma Gandhi University, Kottayam) and
Dr. George V. Thomas (Principal and Associate Professor, Department of
Chemistry, St. Joseph’s College, Moolamattom, India). He has extensive
research experience in the field of interpenetrating polymeric networks
(IPNs) and has two publications dealing with diffusion of IPN in Polymer
(Elsevier) and on viscoelastic behavior of IPNs in the New Journal of
Chemistry (RSC). He has attended more than 20 international conferences
with one publication in IOP conference proceedings and has presented
many research papers. In addition, he has co-authored three chapters
published in international books. He has four years of research experience
in polymer chemistry and nanotechnology at the laboratories of the School
of Chemical Science, Mahatma Gandhi University, Kottayam, Kerala,
India.

Sabu Thomas, PhD

Sabu Thomas is currently the Vice Chancellor of
Mahatma Gandhi University, Kottayam, Kerala, India.
He was the Founder Director of the International and
Inter University Center for Nanoscience and Nano-
technology and is also a full professor of Polymer
Science and Engineering in the School of Chemical
Science of the same university. He is a fellow of many professional bodies.
Prof. Thomas has co-authored many papers in international peer-reviewed
vi About the Editors

journals in the area of polymer processing. He has organized more than 50

international conferences. Prof. Thomas’s research group is in specialized
areas of polymers, which include polymer blends, fiber-filled polymer
composites and their morphological characterization, aging, and degrada-
tion, pervaporation phenomena, sorption, and diffusion, interpenetrating
polymer systems, recyclability and reuse of waste plastics and rubbers,
elastomeric cross-linking, and dual porous nanocomposite scaffolds for
tissue engineering. Prof. Thomas’s research group has extensive exchange
programs with different industries, research, and academic institutions all
over the world and is performing world-class collaborative research in
various fields. The professor’s center is equipped with various sophisti-
cated instruments and has established state-of-the-art experimental facili-
ties that cater to the needs of researchers within the country and aboard.
He has more than 930 publications with 34,227 citations, 55 books, 30
international awards and three patents to his credit. His H index is 84. He is
a reviewer for many international journals. Prof. Thomas has attained the
5th position in the list of Most Productive Researchers in India in 2008-17.

Nandakumar Kalarikkal, PhD

Nandakumar Kalarikkal is an Associate Professor
and Director at the School of Pure and Applied
Physics and Director of International and Inter
University Center for Nanoscience and Nanotech-
nology of Mahatma Gandhi University, Kottayam,
Kerala, India. His research activities involve
applications of nanostructured materials, laser
plasma, phase transitions, etc. He is the recipient of research fellowships
and associateships from prestigious government organizations, such as
the Department of Science and Technology and Council of Scientific and
Industrial Research of the Government of India. He has an active collabo-
ration with national and international scientific institutions in India, South
Africa, Slovenia, Canada, France, Germany, Malaysia, Australia, and the
US. He has more than 130 publications in peer-reviewed journals. He has
also co-edited nine books of scientific interest and co-authored many book
chapters. He has 920 citations, and 4 patents to his credit. His H Index is
18. He is a reviewer for many international journals.
About the Editors vii

Yang Weimin, PhD

Yang Weimin is the Taishan Scholar Professor of
Qingdao University of Science and Technology in
China. He is a Professor of the College of Mechan-
ical and Electrical Engineering and Director of
the Department of International Exchanges and
Cooperation, Beijing University of Chemical Tech-
nology, Beijing, China. In addition, he is a fellow of
many professional organizations. Dr. Weimin has authored many papers
in international peer-reviewed journals in the area of polymer processing.
He has contributed to a number of books as author and editor and acts as a
reviewer to many international journals. In addition, he is a consultant to
many polymer equipment manufacturers. He has also received numerous
awards for his work in polymer processing. His interests include polymer
processing and CAD/CAE/CAM of polymer processing.

Kaushik Pal, PhD

Kaushik Pal is a Research Professor in the Depart-
ment of Nanotechnology and is a Founding Director
of Center for Multidisciplinary Research Excellence
(CMRE) at Bharath University, Chennai, India. His
research areas are high-yield novel nanomaterials/
polymer/grapheme-assembled liquid crystals, novel
electro-optic switchable device for nanoelectronics, static memory devices,
transparent electrodes, super capacitors, and smart, flexible display perfor-
mances. His novel research findings have resulted over 50 publications
that have been published in many international peer-reviewed journals
and reputed magazines. He has published eight book chapters as well. Dr.
Pal has been cited 20 times, and and his current h-index is 7. In recent
years, he has been serving on the editorial boards of over 30 international
journals. Dr. Pal has received several significant awards, including the
prestigious Marie-Curie Experienced Research Fellowship (Postdoctoral)
honor from Aristotle University of Thessaloniki, Greece (offered by the
European Commission) and has been selected as Visiting Scientist for the
project BK-21, Brain Korea Postdoctoral Fellowship (Visiting Scientist).
CONTENTS

Contributors ...............................................................................................xi
Abbreviations ............................................................................................ xv
Preface ..................................................................................................... xix

PART I: Bio-Composites and Nanocomposites ................................... 1

1. Tailoring and Assessing Ethylene Vinyl Acetate (EVA)/Organoclay
Nanocomposites for Biomedical Applications .......................................... 3
Azlin Fazlina Osman, Tuty Fareyhynn M. Fitri, Asna Rasyidah Abdul Hamid,
Fatimah Hashim, Md Rakibuddin, and Abdulkader M. Alakrach

2. Gold (Silver)-Polymer Nanocomposites for Biosensing and

Microfluidic Applications ......................................................................... 25
Simona Badilescu and Muthukumaran Packirisamy

3. Growth of Mesenchymal Stem Cells on Surface-Treated 2D

Poly(Glycerol-Sebacate) Bio-Elastomers of Varying Stiffness .............. 43
Raju B. Maliger, Peter J. Halley, Justin J. Cooper-White, and Donna Dinnes

4. Enhancement of Impact Strength in Jute Fiber-Reinforced

Polypropylene-Spent Coffee Ground Composites .................................. 63
N. Jaya Chitra

5. Processing and Mechanical Characterization of Short

Banana-Jute Hybrid Fiber-Reinforced Polyester Composites.............. 77
Siva Bhaskara Rao Devireddy and Sandhyarani Biswas

6. Graphene and Graphene-Based Polymer Nanocomposites:

The New Wonder Materials of the Nanoworld .................................... 101
Ujjal K. Sur

7. Preparation and Characterization of ZnO Doped Cts/PEG-Ag

Nano-Composite for Impacting Photocatalytic Response ................... 115
T. Kokila, P. S. Ramesh, D. Geetha, and S. Kavitha

8. Development of High-Performance In-Situ Polypropylene/Nylon 6

Microfibrillar Composites ...................................................................... 135
B. D. S. Deeraj, K. Jayanarayanan, and Kuruvilla Joseph
x Contents

9. Effect of Co-Precipitation on the Physico-Mechanical and

Dielectric Properties of Nickel Ferrite Embedded Natural
Rubber Composites ................................................................................. 155
Sankar S. Menon, Radhu Krishna, Lida Wilson, Sreedha Sambhudevan,
Balakrishnan Shankar, Anshida Mayeen, and Nandakumar Kalarikkal

PART II: Interpenetrating Polymeric Networks and

Nanostructured Materials ........................................................... 177
10. Effect of Initiating Systems on the Viscoelastic Behavior of
SBR-PMMA Interpenetrating Polymer Networks............................... 179
Jose James, George V. Thomas, and Sabu Thomas

11. Influence of Cationic, Anionic, and Nonionic Surfactants on

Hydrothermal Synthesis of Nano CuS: Structural,
Morphological, and Capacitance Behavior .......................................... 191
D. Geetha, P. S. Ramesh, and Surekha Podili

12. An Experimental Study on the Influence of Polymeric Nano-TIO2

in Cement and Concrete for Its Dispersion, Structural
Characterization, Mechanical Properties, and Its
Performance Under Aggressive Environment ...................................... 213
Mainak Ghosal and Arun Kr. Chakraborty

PART III: Theoretical Protocols for Polymers and Clusters ......... 235
13. Cooperative Molecular and Macroscopic Dynamics of Amorphous
Polymers: A New Analytical View and Its Potential ............................ 237
José Joaquim C. Cruz Pinto and José Reinas S. André

14. Vibrational Modes of the Van der Waals-London Silicon

Clusters Si2 and Si3 in the Gas-Phase .................................................... 261
Srećko Botrić and Ivan Zulim

PART IV: Special Topics in Polymer Processing and

Polymer Coating .......................................................................... 275
15. Initial Flow Analysis in Crucible-Nozzle During Planar
Flow Melt Spinning Process ................................................................... 277
Sowjanya Madireddi

16. Corrosion Protective Methyl Substituted Polyaniline

Coatings on Oxidizable Metals .............................................................. 301
Vandana P. Shinde and Pradip Patil

Index ................................................................................................................. 331

CONTRIBUTORS

Abdulkader M. Alakrach
Center of Excellence Geopolymer and Green Technology (CE GeoGTech),
School of Materials Engineering, University Malaysia Perlis, Arau, Perlis 02600, Malaysia

José Reinas S. André

PhD, Coordination Professor, UTC-Engineering, and Technology, UDI-Research Unit for Inland
Development, Guarda Polytechnic Institute, Technology, and Management School, Guarda, Portugal,
E-mail: [email protected]

Simona Badilescu
Optical-Bio Microsystems Laboratory, Micro-Nano-Bio Integration Center, Department of
Mechanical and Industrial Engineering, Concordia University, Montreal, Canada, H3G 1M8

Sandhyarani Biswas
Department of Mechanical Engineering, National Institute of Technology, Rourkela, Odisha, 769008,
India

Srećko Botrić
Faculty of Electrical Engineering, Mechanical Engineering and Naval Architecture,
Department of Mathematics and Physics, University of Split, Ruđera Boškovića 32, HR–21000
Split, Croatia, E-mail: [email protected]

Arun Kr. Chakraborty

Research Scholar, Associate Professor, Department of Civil Engineering,
Indian Institute of Engineering Science and Technology, Shibpur, Howrah 711103, India

N. Jaya Chitra
Department of Chemical Engineering, Dr. MGR Educational and Research Institute (University),
Maduravoyal, Chennai–95, India, E-mails: [email protected]; [email protected]

Justin J. Cooper-White
AIBN/School of Chemical Engineering, University of Queensland, St. Lucia, Brisbane,
Queensland–4072, Australia
B. D. S. Deeraj
Department of Chemistry, Indian Institute of Space Science and Technology, Kerala–695547, India

Siva Bhaskara Rao Devireddy

Department of Mechanical Engineering, St. Ann’s College of Engineering and Technology,
Chirala, Andhra Pradesh, 523187, India, E-mail: [email protected]

Donna Dinnes
AIBN/School of Chemical Engineering, University of Queensland, St. Lucia, Brisbane,
Queensland–4072, Australia
Tuty Fareyhynn M. Fitri
Center of Excellence Geopolymer and Green Technology (CE GeoGTech),
School of Materials Engineering, University Malaysia Perlis, Arau, Perlis 02600, Malaysia
xii Contributors

D. Geetha
Department of Physics (DDE Wing), Annamalai University, Annamalai Nagar – 608002, Tamilnadu,
India, E-mail: [email protected]

Mainak Ghosal
Adjunct Assistant Professor, JIS College of Engineering, Kalyani, Nadia, W. Bengal,
and Research Scholar, Associate Professor, Department of Civil Engineering,
Indian Institute of Engineering Science and Technology, Shibpur, Howrah 711103, India

Peter J. Halley
AIBN/School of Chemical Engineering, University of Queensland, St. Lucia, Brisbane,
Queensland–4072, Australia

Asna Rasyidah Abdul Hamid

Center of Excellence Geopolymer and Green Technology (CE GeoGTech),
School of Materials Engineering, University Malaysia Perlis, Arau, Perlis 02600, Malaysia

Fatimah Hashim
School of Fundamental Science, University Malaysia Terengganu, 21030 Kuala Terengganu,
Terengganu, Malaysia

Jose James
Research and Post-Graduate Department of Chemistry, St: Joseph’s College,
Moolamattom and International, and Interuniversity Center for Nanoscience and Nanotechnology,
and School of Chemical Sciences, Mahatma Gandhi University, Kottayam, 686560, Kerala, India.
[email protected]

K. Jayanarayanan
Department of Chemical Engineering and Materials Science, Amrita University, Coimbatore, India

Kuruvilla Joseph
Department of Chemistry, Indian Institute of Space Science and Technology, Kerala–695547, India

Nandakumar Kalarikkal
School of Pure and Applied Physics, Mahatma Gandhi University, Kottayam, Kerala, India

S. Kavitha
Department of Physics, Annamalai University, Annamalai Nagar 608002, Tamilnadu, India

T. Kokila
Department of Physics, Vivekanandha College of Arts and Sciences for Women (Autonomous),
Elayampalayam, Namakkal–637205, Tamilnadu, India

Radhu Krishna
Department of Chemistry, Amrita School of Arts and Sciences, Amritapuri,
Amrita Vishwa Vidyapeetham, Amrita University, India

Sowjanya Madireddi
CVR College of Engineering, Hyderabad, Telangana – 501510, India,
E-mail: [email protected]

Raju B. Maliger
AIBN/School of Chemical Engineering, University of Queensland, St. Lucia, Brisbane,
Queensland–4072, Australia, Tel.: +61450425510, E-mail: [email protected]

Anshida Mayeen
School of Pure and Applied Physics, Mahatma Gandhi University, Kottayam, Kerala
Contributors xiii

Sankar S. Menon
Department of Chemistry, Amrita School of Arts and Sciences, Amritapuri, Amrita Vishwa
Vidyapeetham, Amrita University, India

Azlin Fazlina Osman

Center of Excellence Geopolymer and Green Technology (CE GeoGTech),
School of Materials Engineering, University Malaysia Perlis, Arau, Perlis 02600, Malaysia,
E-mail: [email protected]

Muthukumaran Packirisamy
Optical-Bio Microsystems Laboratory, Micro-Nano-Bio Integration Center,
Department of Mechanical and Industrial Engineering, Concordia University, Montreal,
Canada H3G 1M8

Pradip Patil
Department of Physics, North Maharashtra University, Jalgaon 425001, Maharashtra, India

José Joaquim C. Cruz Pinto

PhD, Professor, Retired Full Professor from the University of Aveiro/CICECO,
Department of Chemistry, 3810–193 Aveiro, Portugal, E-mail: [email protected]

Surekha Podili
Department of Physics, Annamalai University, Annamalai Nagar – 608002

Md Rakibuddin
School of Materials Science and Engineering, Yeungnam University, 280 Daehak-ro,
Gyeongsan, South Korea

P. S. Ramesh
Department of Physics (DDE Wings), Annamalai University, Annamalai Nagar 608002,
Chidambaram, Tamilnadu, India, E-mail: [email protected]

Sreedha Sambhudevan
Department of Chemistry, Amrita School of Arts and Sciences, Amritapuri,
Amrita Vishwa Vidyapeetham, Amrita University, India

Balakrishnan Shankar
Department of Mechanical Engineering, Amrita School of Engineering, Amritapuri,
Amrita Vishwa Vidyapeetham, Amrita University, India

Vandana P. Shinde
Department of Physics, North Maharashtra University, Jalgaon 425001, Maharashtra, India

Ujjal K. Sur
Department of Chemistry, Behala College, University of Calcutta, Kolkata–60, India,
E-mail: [email protected]

George V. Thomas
Research and Post-Graduate Department of Chemistry, St: Joseph’s College, Moolamattom,
Kerala, India

Sabu Thomas
International and Interuniversity Center for Nanoscience and Nanotechnology, School of Chemical
Sciences, Mahatma Gandhi University, Kottayam, 686560, Kerala, India
xiv Contributors

Lida Wilson
Department of Chemistry, Amrita School of Arts and Sciences, Amritapuri,
Amrita Vishwa Vidyapeetham, Amrita University, India

Ivan Zulim
Faculty of Electrical Engineering, Mechanical Engineering and Naval Architecture,
Department of Electronics and Computing, University of Split, Ruđera Boškovića 32,
HR–21000 Split, Croatia, E-mail: [email protected]
ABBREVIATIONS

ABCDQPA nozzle domain

AFM atomic force microscopy
AgNO3 silver nitrate
AIBN azobisisobutyronitrile
BCGFB slit
BPO benzoyl peroxide
BRNS Board of Research in Nuclear Sciences
BSA bovine serum albumin
CB carbon black
CBC carpet backing cloth
CH3COOH glacial acetic acid
CH4 methane
CM coupling model
CNFs carbon nanofibers
CNTs carbon nanotubes
CO2 carbon dioxide
CPCs conducting polymer composites
CPs conducting polymers
CR corrosion rate
CS coconut sheath
CSTMD cooperative segmental theory of materials dynamics
CTAB cetyltrimethylammonium bromide
CTM compression testing machine
CTMD clustering theory of materials dynamics
Cu copper
CV cyclic voltammetry
CVD chemical vapor deposition
CVs cyclic voltammograms
DABCO 1,4-diazabicyclo[2,2,2]-octane
DAE Department of Atomic Energy
DCP dicumyl peroxide
DFT density functional theory
DLS dynamic light scattering
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