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HIGH-PERFORMANCE MATERIALS
AND ENGINEERED CHEMISTRY
Innovations in Physical Chemistry: Monograph Series

HIGH-PERFORMANCE MATERIALS
AND ENGINEERED CHEMISTRY

Edited by
Francisco Torrens, PhD
Devrim Balköse, PhD
Sabu Thomas, PhD
Apple Academic Press Inc. Apple Academic Press Inc.
3333 Mistwell Crescent 9 Spinnaker Way
Oakville, ON L6L 0A2 Waretown, NJ 08758
Canada USA
© 2018 by Apple Academic Press, Inc.
No claim to original U.S. Government works
Printed in the United States of America on acid-free paper
International Standard Book Number-13: 978-1-77188-598-0 (Hardcover)
International Standard Book Number-13: 978-1-315-18786-0 (eBook)
All rights reserved. No part of this work may be reprinted or reproduced or utilized in any form or by any
electronic, mechanical or other means, now known or hereafter invented, including photocopying and re-
cording, or in any information storage or retrieval system, without permission in writing from the publisher
or its distributor, except in the case of brief excerpts or quotations for use in reviews or critical articles.
This book contains information obtained from authentic and highly regarded sources. Reprinted material is
quoted with permission and sources are indicated. Copyright for individual articles remains with the authors
as indicated. A wide variety of references are listed. Reasonable efforts have been made to publish reliable
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edged, please write and let us know so we may rectify in any future reprint.
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Trademark Notice: Registered trademark of products or corporate names are used only for explanation
and identification without intent to infringe.

Library and Archives Canada Cataloguing in Publication

High-performance materials and engineered chemistry / edited by Francisco Torrens, PhD,

Devrim Balköse, PhD, Sabu Thomas, PhD.
(Innovations in physical chemistry : monograph series)
Includes bibliographical references and index.
Issued in print and electronic formats.
ISBN 978-1-77188-598-0 (hardcover).--ISBN 978-1-315-18786-0 (PDF)
1. Chemical engineering. 2. Materials. I. Haghi, A. K., editor
II. Series: Innovations in physical chemistry
TP155.H54 2017 660 C2017-905898-3 C2017-905899-1

CIP data on file with US Library of C

​ ​ongress

Apple Academic Press also publishes its books in a variety of electronic formats. Some content that appears
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ABOUT THE EDITORS

Francisco Torrens, PhD

Francisco Torrens, PhD, is Lecturer in physical chemistry at the Univer-
sitat de València, Spain. His scientific accomplishments include the first
implementation at a Spanish university of a program for the elucidation of
crystallographic structures and the construction of the first computational-
chemistry program adapted to a vector-facility supercomputer. He has
written many articles published in professional journals and has acted as
a reviewer as well. He has handled 26 research projects, has published two
books and over 350 articles, and has made numerous presentations.

Devrim Balköse, PhD

Devrim Balköse, PhD, is currently a retired faculty member in the Chem-
ical Engineering Department at Izmir Institute of Technology, Izmir,
Turkey. She graduated from the Middle East Technical University in
Ankara, Turkey, with a degree in chemical engineering. She received her
MS and PhD degrees from Ege University, Izmir, Turkey, in 1974 and 1977
respectively. She became Associate Professor in macromolecular chem-
istry in 1983 and Professor in process and reactor engineering in 1990.
She worked as a research assistant, assistant professor, associate professor,
and professor between 1970 and 2000 at Ege University, Turkey. She was
Head of the Chemical Engineering Department at Izmir Institute of Tech-
nology, Izmir, Turkey, between 2000 and 2009. She is now a retired faculty
member in the same department. Her research interests are in polymer
reaction engineering, polymer foams and films, adsorbent development,
and moisture sorption. Her research projects focused on nanosized zinc
borate production, ZnO polymer composites, zinc borate lubricants, anti-
static additives, and metal soaps.

Sabu Thomas, PhD

Sabu Thomas, PhD, is Professor of Polymer Science and Engineering at
the School of Chemical Sciences and Director of the International and Inter
University Centre for Nanoscience and Nanotechnology at Mahatma Gandhi
University, Kottayam, Kerala, India. The research activities of Professor
vi About the Editors

Thomas include surfaces and interfaces in multiphase polymer blend and

composite systems; phase separation in polymer blends; compatibilization
of immiscible polymer blends; thermoplastic elastomers; phase transitions
in polymers; nanostructured polymer blends; macro-, micro- and nano-
composites; polymer rheology; recycling; reactive extrusion; processing–
morphology–property relationships in multiphase polymer systems; double
networking of elastomers; natural fibers and green composites; rubber vulca-
nization; interpenetrating polymer networks; diffusion and transport; and
polymer scaffolds for tissue engineering. He has supervised 68 PhD theses,
40 MPhil theses, and 45 Masters thesis. He has three patents to his credit.
He also received the coveted Sukumar Maithy Award for the best polymer
researcher in the country for the year 2008. Very recently, Professor Thomas
received the MRSI and CRSI medals for his excellent work. With over 600
publications to his credit and over 23,683 citations, with an h-index of 75,
Dr. Thomas has been ranked fifth in India as one of the most productive
scientists. He received his BSc degree (1980) in Chemistry from the Univer-
sity of Kerala, B.Tech. (1983) in Polymer Science and Rubber Technology
from the Cochin University of Science and Technology, and PhD (1987) in
Polymer Engineering from the Indian Institute of Technology, Kharagpur.
CONTENTS

List of Contributors........................................................................................ ix
List of Abbreviations....................................................................................xiii
Preface........................................................................................................ xvii

Part I: High-Performance Materials.........................................................1

1. Optical Thin Film Filters: Design, Fabrication,
and Characterization.......................................................................................3
Parinam Sunita, Vemuri SRS Praveen Kumar, Kumar Mukesh, Kumari Neelam,
Parinam Krishna Rao, Karar Vinod, and Sharma Amit L

2. Fabrication of Exceptional Ambient Stable Organic

Field-Effect Transistors by Exploiting the Polarization of
Polar Dielectric Layers..................................................................................35
Nimmakayala V. V. Subbarao and Dipak K. Goswami

3. Nonlinear Thermal Instability in a Fluid Layer under

Thermal Modulation......................................................................................57
Palle Kiran

4. Application of a Random Sequential Algorithm for the Modeling of

Macromolecular Chains’ Cross-Linking Evolution During a
Polymer Surface Modification......................................................................79
Stanislav Minárik, Vladinír Labaš, Ondrej Bošák, and Marián Kubliha

5. Polyaniline-Coated Inorganic Oxide Composites for Broadband

Electromagnetic Interference Shielding.......................................................95
Muhammad Faisal

6. A Comprehensive Review of Membrane Science and Technology and

Recent Trends in Research: A Broad Environmental Perspective..........135
Sukanchan Palit

Part II: Chemometrics and Chemoinformatics Approaches..............159

7. Application of Statistical Approaches to Optimize the Productivity
of Biodiesel and Investigate the Physicochemical Properties of the
Bio/Petro-Diesel Blends...............................................................................161
Nour Sh. El-Gendy and Samiha F. Deriase
viii Contents

8. Smart Mobile Device Emerging Technologies: An Enabler to Health

Monitoring System.......................................................................................241
Heru Susanto

Part III: Analytical, Computational, and Experimental

Techniques......................................................................................265
9. Principal Component, Cluster, and Meta-Analyses of Soya Bean,
Spanish Legumes, and Commercial Soya Bean........................................267
Francisco Torrens and Gloria Castellano

10. Electrokinetic Soil Remediation: An Efficiency Study in

Cadmium Removal......................................................................................295
Cecilia I. A. V. Santos, Ana C. F. Ribeiro, Diana C. Silva, Victor M. M. Lobo,
Pedro S. P. Silva, Carmen Teijeiro, and Miguel A. Esteso
11. Nano-Sized Nickel Borate Preparatıon and Characterızatıon................313
Merve Türk, Barış Gümüş, Fatma Ustun, and Devrim Balköse

12. The New Equipment for Clearing of Technological Gases.......................337

R. R. Usmanova and G. E. Zaikov

13. Operational and Engineering Aspects of Packed Bed Bioreactors

for Solid-State Fermentation......................................................................353
Ramón Larios-Cruz, Arely Prado-Barragán, Héctor A. Ruiz,
Rosa M. Rodríguez-Jasso, Julio C. Montañez, and Cristóbal N. Aguilar

14. Effects of Glutathione, Phosphonate, or Sulfonated Chitosans

and Their Combination on Scavenging Free Radicals.............................371
Tamer M. Tamer, Katarína Valachová, Ahmed M. Omer,
Maysa M. Sabet, and Ladislav Šoltés

Index......................................................................................................................391
LIST OF CONTRIBUTORS

Cristóbal N. Aguilar
Food Research Department, School of Chemistry, Universidad Autónoma de Coahuila, Saltillo, Coahuila
25280, México
Sharma Amit L
Optical Devices and Systems, CSIR-Central Scientific Instruments Organisation, Chandigarh, India

Devrim Balköse
Department of Chemical Engineering, İzmir Institute of Technology, Gulbahce, Urla İzmir, Turkey

Ondrej Bošák
Institute of Materials Science, Faculty of Materials Science and Technology in Trnava, Slovak University
of Technology, Bratislava, Slovak Republic

Gloria Castellano
Departamento de Ciencias Experimentales y Matemáticas, Facultad de Veterinaria y Ciencias Experi-
mentales, Universidad Católica de Valencia San Vicente Mártir, Guillem de Castro‑94, València E-46001,
Spain

Samiha F. Deriase
Egyptian Petroleum Research Institute, Nasr City Cairo 11727, Egypt

Miguel A. Esteso
U.D. Química Física, Facultad de Farmacia, Universidad de Alcalá, 28871 Alcalá de Henares, Madrid,
Spain
Muhammad Faisal
Department of Physics, PES Institute of Technology, Bangalore South Campus, Bangalore 560100,
Karnataka, India

Nour Sh. El-Gendy

Egyptian Petroleum Research Institute, Nasr City Cairo 11727, Egypt

Dipak K. Goswami
Department of Physics, Indian Institute of Technology Kharagpur, Kharagpur 721302, West Bengal,
India

Barış Gümüş
Department of Chemical Engineering, İzmir Institute of Technology, Gulbahce, Urla İzmir, Turkey

Palle Kiran
Department of Mathematics, Rayalaseema University, Kurnool 518002, Andhra Pradesh, India

Marián Kubliha
Institute of Materials Science, Faculty of Materials Science and Technology in Trnava, Slovak University
of Technology, Bratislava, Slovak Republic

Vemuri SRS Praveen Kumar

Optical Devices and Systems, CSIR-Central Scientific Instruments Organisation, Chandigarh, India
x List of Contributors

Vladinír Labaš
Institute of Materials Science, Faculty of Materials Science and Technology in Trnava, Slovak University
of Technology, Bratislava, Slovak Republic

Ramón Larios-Cruz
Food Research Department, School of Chemistry, Universidad Autónoma de Coahuila, Saltillo, Coahuila
25280, México

Victor M. M. Lobo
Department of Chemistry and Coimbra Chemistry Centre, University of Coimbra, Coimbra 3004535,
Portugal
Stanislav Minárik
Research Centre of Progressive Technologies, Slovak University of Technology, Bratislava, Slovak
Republic
Julio C. Montañez
Food Research Department, School of Chemistry, Universidad Autónoma de Coahuila, Saltillo, Coahuila
25280, México

Kumar Mukesh
Optical Devices and Systems, CSIR- Central Scientific Instruments Organisation, Chandigarh, India

Kumari Neelam
Optical Devices and Systems, CSIR- Central Scientific Instruments Organisation, Chandigarh, India

Ahmed M. Omer
Polymer Research Department, Advanced Technologies and New Materials Research Institute (ATNMRI),
City of Scientific Research and Technological Applications (SRTA-City), New Borg El-Arab, Alexandria
21934, Egypt

Sukanchan Palit
Department of Chemical Engineering, University of Petroleum and Energy Studies, Energy Acres, Post-
Office-Bidholi via Premnagar, Dehradun 248007, Uttarakhand, India

Arely Prado-Barragán
Department of Biotechnology, Universidad Autónoma Metropolitana Unidad Iztapalapa, Delegación
Iztapalapa, Distrito Federal 09340, México

Parinam Krishna Rao

Optical Devices and Systems, CSIR- Central Scientific Instruments Organisation, Chandigarh, India

Ana C. F. Ribeiro
Department of Chemistry and Coimbra Chemistry Centre, University of Coimbra, Coimbra 3004535,
Portugal

Rosa M. Rodríguez-Jasso
Food Research Department, School of Chemistry, Universidad Autónoma de Coahuila, Saltillo, Coahuila
25280, México

Héctor A. Ruiz
Food Research Department, School of Chemistry, Universidad Autónoma de Coahuila, Saltillo, Coahuila
25280, México

Maysa M. Sabet
Laboratory of Bioorganic Chemistry of Drugs, Institute of Experimental Pharmacology and Toxicology,
Bratislava 84104, Slovakia
List of Contributors xi

Cecilia I. A. V. Santos
Department of Chemistry and Coimbra Chemistry Centre, University of Coimbra, Coimbra 3004535,
Portugal

Diana C. Silva
Department of Chemistry and Coimbra Chemistry Centre, University of Coimbra, Coimbra 3004535,
Portugal

Pedro S. P. Silva
Department of Physics, CFisUC, Universidade de Coimbra, Rua Larga, P-3004516 Coimbra, Portugal

Ladislav Šoltés
Laboratory of Bioorganic Chemistry of Drugs, Institute of Experimental Pharmacology and Toxicology,
Bratislava 84104, Slovakia

Nimmakayala V. V. Subbarao
Center for Nanotechnology, Indian Institute of Technology Guwahati, Guwahati 781039, Assam, India

Parinam Sunita
Optical Devices and Systems, CSIR- Central Scientific Instruments Organisation, Chandigarh, India

Heru Susanto
Department of Information Management, College of Management, Tunghai University, Taichung, Taiwan

Tamer M. Tamer
Laboratory of Bioorganic Chemistry of Drugs, Institute of Experimental Pharmacology and Toxicology,
Bratislava 84104, Slovakia

Carmen Teijeiro
U.D. Química Física, Facultad de Farmacia, Universidad de Alcalá, 28871 Alcalá de Henares, Madrid,
Spain

Francisco Torrens
Institut Universitari de Ciència Molecular, Universitat de València, Edifici d’Instituts de Paterna, P. O.
Box 22085, València E-46071, Spain
Merve Türk
Department of Chemical Engineering, İzmir Institute of Technology, Gulbahce, Urla İzmir, Turkey

R. R. Usmanova
Ufa State Technical University of Aviation, Ufa 450000, Bashkortostan, Russia

Fatma Ustun
Department of Chemical Engineering, İzmir Institute of Technology, Gulbahce, Urla İzmir, Turkey

Katarína Valachová
Laboratory of Bioorganic Chemistry of Drugs, Institute of Experimental Pharmacology and Toxicology,
Bratislava 84104, Slovakia
Karar Vinod
Optical Devices and Systems, CSIR-Central Scientific Instruments Organisation, Chandigarh, India

G. E. Zaikov
N. M. Emanuel Institute of Biochemical Physics, Russian Academy of Sciences, Moscow 119991, Russia
LIST OF ABBREVIATIONS

AFM atomic force microscopy

ANOVA analysis of variance
APCVD atmospheric pressure CVD
AR antireflection
ASTM American Society for Testing Materials
BCB benzocyclobutene
CCD central composite design
CCFCD central composite face centered design
CCI coherence correlation interferometer
CdS cadmium sulfide
CDSS clinical decision support system
COM completion of melt onset temperature
CP cloud point
CPCs conducting polymer composites
CVD chemical vapor deposition
dc direct current
DOD D-optimal design
DOS density of state
DPA differential pulse voltammetry
DST Department of Science and Technology
DWNT double wall
EHR electronic health record
EMR electronic medical record
ER electrorheological
FFAs free fatty acids
FP flash point
FrFD fractional factorial design
FTIR Fourier transform infrared spectroscopy
HIM health information management
HIT health information technology
HMDE hanging mercury drop electrode
HR high-reflection
HUD head up display
HWOT half wave optical thickness
xiv List of Abbreviations

ICOP International Conference on Optics and Photonics

EMC electromagnetic compatibility
EMI electromagnetic interference
ICPs intrinsically conducting polymers
IP induction period
JCB Jatropha curcas-biodiesel
LPCVD low pressure CVD
MBE molecular beam epitaxy
MBR membrane bioreactor
MF microfiltration
MIM metal–insulator–metal
MnO2 manganese dioxide
MNu mean value of Nusselt number
MOCVD metal organic CVD
MOLB modulation of only the lower boundary
NF nanofiltration
OA orthogonal arrays
OFETs organic field-effect transistors
OLEDs organic light emitting diodes
OSCs organic solar cells
PAni polyaniline
PECVD plasma enhanced CVD
PM particulate matter
PMMA hydrophobic poly-(methylmethacrylate)
PP pour point
PS polystyrene
PVA poly(vinylalcohol)
PVD physical vapor deposition
PVP poly(vinyl phenol)
RCCD rotatable central composite design
RFID radio frequency identification
RMSE root mean square error
RO reverse osmosis
SBR styrene-butadiene rubber
SEM scanning electron microscopy
SEM scanning electron microscope
SMP soluble microbial products
SMUs source measure units
SS subthreshold swing
SSE sum of squares error
List of Abbreviations xv

SSF solid-state fermentation

SST treatment sum of squares
SWNT single wall
TAN total acid number
TEM transmission electron microscopy
UF ultrafiltration
UHVCVD ultra high vacuum
US-DOE US-Department of Energy
VNA vector network analyzer
WBOS Wei biogenic oxidative system
WCO waste cooking oils
WFSFO waste frying sunflower oil
XRD X-ray diffraction analysis
XRF X-ray fluorescence
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