Chapter 1 - Chemical Process

Diagrams

Department of Chemical Engineering

West Virginia University

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Outline
Flow Diagrams
Block Flow Diagrams (BFD)
Process Flow Diagrams (PFD)
Piping and Instrument Diagrams (P&ID)
Other common diagrams
3-D plant layout diagrams

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3 Levels of Diagram
Block Flow Diagram (BFD)
Process Flow Diagram (PFD)
Piping and Instrumentation Diagram (P&ID)
often referred to as Mechanical Flow Diagram
Complexity Conceptual
increases understanding
increases
As chemical engineers, we are most familiar
with BFD and PFD.
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The Block Flow Diagram (BFD)
BFD shows overall processing picture of
a chemical complex
Flow of raw materials and products may be
included on a BFD
BFD is a superficial view of facility ChE
information is missing

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Definitions of BFD
Block Flow Process Diagram
Figure 1.1
Similar to sketches in material and
energy balances
Block Flow Plant Diagram
Figure 1.2
Gives a general view of a large complex
plant
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The Block Flow Process Diagram

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Developing a Process

Target product is 37% formaldehyde in water. Known as

formalin
Occurs of a silver catalyst at 200 oC and 2 3 atm
pressure
Reaction 1 is the predominant reaction
Develop a block flow diagram that describes the process
B.P. Pure formaldehyde = -19.3 oC
B.P. Formalin = 96 oC

YSU In-Class Problem - Fall 2009

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The Block Flow Plant Diagram

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The Process Flow Diagram
PFD shows all process engineering
information
Diagram developed in junior year design
projects (especially the 2nd semester)
Often PFD is drawn on large paper
textbook breaks down information into 1
diagram and 2 tables

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The Process Flow Diagram (contd)

The topology of the process showing the

connectivity of all the streams and the
equipment
Example for toluene HDA Figures 1.3 and
1.5
Tables 1.2 and 1.4 list information that
should be on the PFD but cannot fit
Use appropriate conventions consistency is
important in communication of process
information
ex. Table 1.2
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The Process Flow Diagram (contd)

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 The Process Flow Diagram (contd)
Table 1.2 : Conventions Used for Identifying Process Equipment
Process Equipment General Format XX-YZZ A/B
XX are the identification letters for the equipment classification
C - Compressor or Turbine
E - Heat Exchanger
H - Fired Heater
P - Pump
R - Reactor
T - Tower
TK - Storage Tank
V - Vessel
Y designates an area within the plant
ZZ are the number designation for each item in an equipment class
A/B identifies parallel units or backup units not shown on a PFD
Supplemental Additional description of equipment given on top of PFD
Information
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Equipment Numbering
XX-YZZ A/B/
XX represents a 1- or 2-letter designation
for the equipment (P = pump)
Y is the 1 or 2 digit unit number (1-99)
ZZ designates the equipment number for
the unit (1-99)
A/B/ represents the presence of spare
equipment
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Equipment Numbering (contd)
Thus, T-905 is the 5th tower in unit nine
hundred P-301 A/B is the 1st Pump in unit
three hundred plus a spare
Use unambiguous letters for new equipment
Ex. Turbine use Tb or J not T (used for tower)
Replace old vessel V-302 with a new one of
different design - use V-319 (e.g.) not V-302
since it may be confused with original V-302

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Stream Numbering and
Drawing
Number streams from left to right as
much as possible
Horizontal lines are dominant

yes no no

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Stream Numbering and
Drawing (contd)
Add arrows for
Change in direction
Inlet of equipment
Utility streams should use convention
given in Table 1.3, lps, cw, fg, etc.

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Stream Information
Since diagrams are small, not much
stream information can be included
Include important data around
reactors and towers, etc.
Flags are used see toluene HDA
diagram
Full stream data, as indicated in Table
1.4, are included in a separate flow
summary table see Table 1.5
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Stream Information - Flags

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The Process Flow Diagram (contd)
Table 1.4: Information in a Flow Summary
Essential Information
Stream Number
Temperature (C)
Pressure (bar)
Vapor Fraction
Total Mass Flow Rate (kg/h)
Total Mole Flow Rate (kmol/h)
Individual Component Flow Rates (kmol/h)
Optional Information
Component Mole Fractions
Component Mass Fractions
Individual Component Flow Rates (kg/h)
Volumetric Flow Rates (m3/h)
Significant Physical Properties
Density
Viscosity
Other
Thermodynamic Data
Heat Capacity
Stream Enthalpy
K-values
Stream Name
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The Process Flow Diagram (contd)
A Portion of Table 1.5
Stream Number 1 2 3 4 5 6 7 8 9 10

Temperature (C) 25 59 25 225 41 600 41 38 654 90

Pressure (bar) 1.90 25.8 25.5 25.2 25.5 25.0 25.5 23.9 24.0 2.6

Vapor Fraction 0.0 0.0 1.00 1.0 1.0 1.0 1.0 1.0 1.0 0.0

Mass Flow (tonne/h) 10.0 13.3 0.82 20.5 6.41 20.5 0.36 9.2 20.9 11.6

Mole Flow (kmol/h) 108.7 144.2 301.0 1204.4 758.8 1204.4 42.6 1100.8 1247.0 142.2

Component Mole Flow

(kmol/h)

Hydrogen 0.0 0.0 286.0 735.4 449.4 735.4 25.2 651.9 652.6 0.02

Methane 0.0 0.0 15.0 317.3 302.2 317.3 16.95 438.3 442.3 0.88

Benzene 0.0 1.0 0.0 7.6 6.6 7.6 0.37 9.55 116.0 106.3

Toluene 108.7 143.2 0.0 144.0 0.7 144.0 0.04 1.05 36.0 35.0

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Basic Control Loops
Often the basic control loops (those
involving maintaining material balance
and reactor controls) are included on
the PFD; instrumentation and other
control loops are not shown

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Basic Control Loops

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Equipment Information
Equipment are identified by number
and a label (name) positioned above
the equipment on the PFD
Basic data such as size and key data
are included in a separate table
(Equipment Summary Table) Table 1.7
(and Table 1.6) in TBWS

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Equipment Information
A Section of Table 1.7: Equipment Summary
Vessel V-101 V-102
Temperature (C) 55 38
Pressure (bar) 2.0 24
Orientation Horizontal Vertical
MOC CS CS
Size
Height/Length 5.9 3.5
(m)
Diameter (m) 1.9 1.1
Internals s.p. (splash plate)
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PFD Summary
PFD, Equipment Summary Table, and
Flow Summary Table represent a true
PFD
This information is sufficient for a
preliminary estimation of capital
investment (Chapter 5) and cost of
manufacture (Chapter 6) to be made.

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The Piping and Instrument
Diagram(P&ID)
P&ID Construction Bible
Contains: plant construction information
(piping, process, instrumentation, and
other diagrams)
P&ID information is explained in Tables
1.8 and 1.9
Conventions for instrumentation are
shown in Figure 1.10
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 P&ID

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Look at V-102 on P&ID
V-102 contains an LE (Level Element)
LE senses liquid level in separator and
adjusts flow rate leaving
LE opens and closes a valve depending
on liquid level
LE and valve represent a feedback

control loop
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Other Common Diagrams
Plot Plans plan or map drawn looking
down on plant (drawn to scale with all
major equipment identified)
Elevation Diagrams show view from
side and give information about
equipments distance from ground

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Other Common Diagrams

Section of Plot Plan Section of Elevation Diagram

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Other Common Diagrams (contd)

Piping Isometrics show piping in 3-

dimensions
Vessel Sketches show key dimensions
of equipment and locations of inlet and
outlet nozzles etc.

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Scale Models and Virtual Plants

25 years ago physical models were used for

review
Now virtual or electronic models are
generated using software (3-d plant
diagrams)
Purpose of Models catch errors such as
Piping clashes
Misaligned piping
Equipment not easily accessed
Sample points not easily reached by operators
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3-D Plant
Diagrams

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 Summary
The three principal diagrams (BFD, PFD, and P&ID)
are used to convey increasingly specific technical
information about a process.
Important to adhere to common standards for
these diagrams in order to avoid confusion
Information on equipment layout is most clearly
conveyed through a 3-D plant layout diagram.

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