Products Solutions Services

The chemical industry

Applications

Slide 1 Endress+Hauser Consult AG Sales Support

Prosonic Flow in Manganese Sulphate

Flow Challenge:
• Manganese sulphate and sulphuric acid with
Level
occasional bursts of slurry.

Environment:
Analysis
• Pipe size: 148mm ID
• Pipe material: Fibreglass
Pressure • Wall thickness: 8.4mm
• Temperature: 85C - 95C
Temperature • Flow rate: 0 - 250m³/hr

Gamma Solution:
• Prosonic flow DMU 93 with
Flow Computer, • DDU 10 high temperature sensors
Recorders,
Components
Product group: Flow Benefit:
Systems/Solutions • No contact to medium
Industry: Chemical industry
• Installation without of process
Installed at: Delta EMD, Newcastle interruption
NSW, Australia

Slide 2 Endress+Hauser Consult AG Sales Support

Chemical resistance

Flow Challenge:
• Tantalum electrodes
Level • ATEX II 2G - EEx ia IIC T6

Analysis Solution:
• Chemical compatibility
Pressure ( PTFE and Tantalum wetted
parts)
Temperature • Installation philosophy
(looped power)
Gamma • Intrinsically Safe installation and
approved
Flow Computer,
Recorders,
Components Benefit:
Product group: Flow
Systems/Solutions • 25% reduced wiring/installation
Industry: Chemical industry cost compared to traditional 4
wire flowmeters
Installed at:

Slide 3 Endress+Hauser Consult AG Sales Support

Phosphalugel Production

Flow Challenge:
• Measurement of aluminium
Level phosphate in the production of
Phosphalugel
Analysis
Environment:
Pressure • High solid content in the fluid

Temperature Solution:
• Promag 35S - because of the strong
Gamma construction it is able to measure
conductive liquids with solid content
Flow Computer,
Recorders,
Components Product group: Flow Benefit:
Systems/Solutions • Stable and precise flow measurement
Industry: Chemical industry
for high solid content
Installed at: France

Slide 4 Endress+Hauser Consult AG Sales Support

Filling stations for Ships with TDI – 1/3

Flow Challenge:
• Filling of ships, where there is no
Level space for the meter in the
installation
Analysis
Environment:
Pressure • Isolation of meter, because TDI
does harden in room temperature
Temperature
Solution:
Gamma • 80F1F-ANDS9ACAC4AA
including heating jacket
Flow Computer,
Recorders, Product group: Flow
Components
Industry: Chemical Industry Benefit:
Systems/Solutions • Compact size of meter allows
Installed at: Japan installation after a 90° bend in front of a
shut valve. No inlet or outlet restriction
and quick and easy installation.

Slide 5 Endress+Hauser Consult AG Sales Support

Application story – 2/3

Flow Recently Sakura Endress has sold its first Promass F DN150 to Mitsui
Takeda Chemical, a joint venture of Mitsui Chemicals Inc. and Takeda
Level
Chemical Industries Ltd. Together with Mr. Horiguchi (Tokyo Sales)
Analysis
and Mr. Suzuki (Chiba Office Sales). The Promass F DN150 is used in
a filling station for tank ships located on a quay. Currently (May 2003)
Pressure the construction of the filling station receives its finishing touches. In
this plant Mitsui Takeda Chemical manufactures TDI (Toluene
Temperature
Diisocyanate). TDI is an isocyanate used in the production of
Gamma polyurethanes for flexible foam applications ranging from furniture,
Flow Computer,
bedding, and carpet underlay, to transportation and packaging. TDI is
Recorders, also used in the manufacture of coatings, sealants, adhesives, and
Components
elastomers.
Systems/Solutions

Slide 6 Endress+Hauser Consult AG Sales Support

Success story TDI high production

Flow These are the main application data:

Level Fluid: TDI

Flow range: 300-400 t/hr
Analysis
Temp. range: 30-40C
Pressure range: 0.36-0.41 Mpa
Pressure
Viscosity: 1.7 cP
Temperature Selected sensor: PROline Promass 80F1F-
ANDS9ACAC4AA
Gamma Options: SUS904L
Flow Computer, JIS 10k flanges
Recorders, oil/water/fat-free treatment
Components
ATEX II2G
Systems/Solutions

Slide 7 Endress+Hauser Consult AG Sales Support

Detailed application information – 3/3

Flow Unfortunately, TDI does harden at room

temperatures. Therefore, the whole
installation of the filling station
Level
(including the Promass F) has to be
insulated and kept at a constant
Analysis temperature of 35C. As can be seen
from the pictures there is little space for
Pressure installation at the filling station. The
Promass F is installed immediately after
Temperature
a 90 bend in front of a shut valve.
Therefore, the compact size of Promass
F and its robustness under such
Gamma installation conditions have been
Flow Computer, deciding points for the customer.
Recorders,
Components

Systems/Solutions

Slide 8 Endress+Hauser Consult AG Sales Support

Coal Gas Measurement

Flow Challenge:
• Measurement of coal gas
Level
Environment:
• Petrochemical industry; Ex-Application
Analysis
• DN 80
• Flow rate 200 - 1000 m³/h
Pressure • Pressure: 10 bar

Temperature
Solution:
• Promass 83F for gas measurement
Gamma

Flow Computer,
Recorders, Benefit:
Components • Stable measurement of flow rate
Product group: Flow • No maintenance required.
Systems/Solutions
• No straight inlet or outlet section needed,
Industry: Chemical industry save the space and money.
Installed at: China

Slide 9 Endress+Hauser Consult AG Sales Support

BAYER 6” Polymers Rubber Cement – 1/3

Flow Challenge:
• Exchange of PD meters
Level
Environment:
Analysis • Fluid often plugged the PD meters.

Pressure Solution:
• Promass 83F, vertical installation,
Temperature allows self draining and easy cleaning.

Gamma

Flow Computer,
Recorders, Benefit:
Components • Easy installation
Systems/Solutions
• Self draining, no blocking of meter
• Advanced diagnostics allows to
Product group: Flow
recognize very early blocking or
Industry: Chemical Industry sedimentation.

Slide 10 Endress+Hauser Consult AG Sales Support

Application story – 2/3

Flow Hexane with rubber pellets

At the process temperature the rubber pellets are pretty soft and mix with the hexane.
Level
Plugging was an issue with the PD meters. Vertical installation was preferred to avoid
plugging and enable easier draining. Upgrade to advanced diagnostics was requested by
the customer after installation in order to detect coating of the pipes.
Analysis
The customer is very pleased with the meter's performance, the ease of setup required and
were impressed with the small design requiring no stabilizers, vibration absorbers, etc.
Pressure (line vibration pretty high). Customer will be replacing all PD meters with Promass 83F.

Temperature
Requested flow: 100 – 500 GPM
Pressure: 110 – 120 PSIG
Gamma
Temperature: 200°F
Flow Computer, Density: 5.5 lbs/USGal
Recorders, Viscosity: 3.500 cP
Components

Systems/Solutions

Slide 11 Endress+Hauser Consult AG Sales Support

Detailed application information – 3/3

Flow

Level

Analysis

Pressure

Temperature

Additional brackets are

Gamma
necessary for the
Flow Computer, competitor´s installation.
Recorders,
Components

Systems/Solutions
Endress+Hauser
Installation in the existing
pipeline without
additional work.

Slide 12 Endress+Hauser Consult AG Sales Support

Level

Slide 13 Endress+Hauser Consult AG Sales Support

Outside level measurement – BRINE 1/3

Flow Challenges:
• To get a level measurement of brine, is
very important that this application be
Level
Transmitter outside of the cell.
Transmitter • Convince the customer about the
Analysis accuracy and reliability of the Level
Flex.
Pressure
Environment:
• Close place, temperature between
Temperature
30….50ºC

Gamma Solution:
Flow Computer,
• Radar: externally assembled
Recorders,
Components Benefit:
Systems/Solutions Order code: FMP40-APP2CRJB21CA • The big advantage is the easy
Product group: Level
commissioning and start-up, on-
line level and easy change of
Industry: Chemical Industry instrument when required.
Installed at: Carbocloro Cubatão SP/ Brazil

Slide 14 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Detailed application information – 2/3

Flow • The customer tried an application

with capacitive sensor, but this
Level
application was not a good idea
because of the high corrosion
into de cell.
Analysis
• For the customer, it was very
Pressure
important to be possible the
configuration of FMP40 by local
Temperature display and TOF Tool as well,
these both possibilities are very
good, because sometimes they
Gamma
need to change the cell quickly.
Flow Computer,
Recorders,
• Carbocloro intends to buy more
Components 92 units to install in the every
cell, according picture.
Systems/Solutions

Slide 15 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Detailed application information – 3/3

Flow • This measurement is very important to the customer, because

in case of high level of the cell, it’s possible a explosion
Level
because the cover pressurization, in case of low level, the cell
Analysis can get a increase of temperature causing a short circuit.

Pressure

Temperature

Gamma

Flow Computer, Explosion of cell

Recorders,
Components

Systems/Solutions

Slide 16 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Measurement in a Bypass - Construction

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 17 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Displacer - LevelFlex M (TDR)

Flow T-range: -200/-40…150/280/400°C.

P-range: vacuum…40/320/400bar.
Level
When installed in a level body, the rod probe
Analysis is the best choice (up to DN 150mm / 6”).

Pressure Therefore: LevelFlex (TDR)

Temperature

• No upper blocking distance.

Gamma
• Independent of density changes.
Flow Computer,
Recorders, • Less influence by buildup.
Components • Independent of foam.
Systems/Solutions • Less influence by corrosion.
• No moving parts.
• Independent of vibration.

Slide 18 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Level measurement of Butandiol (liquified gas)

Flow • Level measurement of

Butandiol (liquefied gas)
Level
with fraction of powdery
Analysis
solid particles
• Design: 325bar / 240oC
Pressure
• Service: 270bar / 130oC
Temperature • actually mounted in the
bypass to replace the
Gamma
displace
Flow Computer,
Recorders, • next step: mounting
Components
directly into the vessel
Systems/Solutions

Bypass mounting : displacer replacement

Slide 19 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Why the Levelflex M FMP45

Flow • Reasons for the customer to replace the displacer:

Level
• Levelflex is dramatically less sensitive to
build-up, because of the use of rod probes
= reduced maintenance
Analysis
==> higher reliability at reduced costs
Pressure

Temperature
• Mounting directly into the vessel is
considered now
Gamma
==> higher safety of the plant by
Flow Computer,
Recorders, reduced volume without the bypass, the
Components tubes + valves
Systems/Solutions

Slide 20 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

The right alternative for Bypass Measurement

Flow ARAL Aromatic GmbH in Gelsenkirchen

Level
Distillation of Raw Benzene
Analysis
Secure Level Measurement
Pressure
• Bypass and stilling Well applications
Temperature within the Petrochemical / chemical /
Energy Industries
Gamma • no risk of blocking due to no moving
parts
Flow Computer,
Recorders, • independent of foam, boiling surface and
Components changing densities
Systems/Solutions
• independent of the outlets .

• Starting from a DK value of 1,4.

Slide 21 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

LevelFlex M (TDR) : Typical HT/HP application

Flow

Level

• Bypass applications within the

Analysis
Petrochemical Industry

Pressure
• Replacement of displacer
• Less maintenance
Temperature • No recalibration of the zero due to
build-up
Gamma • no risk of blocking due to no moving
Flow Computer, parts
Recorders,
• independent of foam and changing
Components
densities
Systems/Solutions
• independent of the tank connections

• Independent of the DK changes

Slide 22 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Micropilot M (Radar) – in Bypass

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 23 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Micropilot M (Radar) FMR245 – PTFE Lined Bypass

Flow • Product: sulphuric acid 96%

• Bypass 3“, PTFE lined
Level
• Measuring range: 1.75 m
• Device: FMR245
Analysis
(DN80, PTFE plated)
Pressure
• 26 GHz in bypass show no
Temperature reflections at the side taps

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 24 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Micropilot (Radar) FMR130 – Ammonia in Stilling Well

Flow • Product: Ammonia

• Measurement in stilling well DN80
Level • Device: FMR130 -> 6 GHz
DN80 antenna
Analysis • Redundant measurement

• 6 GHz is the ideal frequency for

Pressure Ammonia (minimal absorption)
• Different qualities of Ammonia
Temperature
are not effecting the measurement
• Enhanced safety by means of
Gamma gas-tight feed through.
Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 25 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Micropilot M (Radar) – in LPG (Stilling Well)

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders, • Product: LPG
Components
• 3 Spheres, height: 12 m
Systems/Solutions Stilling well: 6“ (DN150)
with ball valve
• Pressure: 16 bar
• Device: FMR232 with planar antenna

Slide 26 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Hydrogen peroxide – 1/2

Flow Challenge:
• Replacement of mechanical side
Level glass
• Replacement of FMU40
Analysis • Accuracy 3 mm needed

Pressure Environment:
• Ambient temperature
Temperature
Solution:
Gamma • FMR245
Flow Computer,
Recorders,
Product group: Level Benefit:
Components • Customer bought without
Systems/Solutions Industry: Chemical industry Endress+Hauser recommendation
FMU40, which didn´t reach the
Installed at: Canada accuracy caused by the ambient
environment.

Slide 27 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Detailed application information – 2/2

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 28 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Leveflex M in PE and PP Granulate

Flow Challenge:
• Cost-effective replacement for the old FMM
Level
460
• Strong electrostatic charging of product
• Ceiling with relatively low loading capacity
Analysis

Environment:
Pressure • Measured Media: PE and PP Granulate
• Measuring range 18 m
Temperature • Aluminium silo Ø approx. 3 m

Gamma Solution:
• Level flex M, FMP 40 with 4 mm rope
Flow Computer, • This rope was selected to reduce ceiling
Recorders,
Components load
Product group: Level
Systems/Solutions
Benefit:
Industry: Chemical industry • Integrated protection against electrostatic
charging
• The 4 mm rope provides ample stability (12
kN)

Slide 29 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Levelflex M in PVC-powder

Flow Challenge:
• Silo height: 22,8m
Level
• Diameter: ca. 2m

Analysis
Environment:
• Measured Media: PVC-powder
• DC: 1,6
Pressure • Production of plastic profiles

Temperature Solution:
• Levelflex M
Gamma

Flow Computer,
Recorders, Product group: Level
Components
Benefit:
• Guided micro impulses are unaffected
Systems/Solutions Industry: Chemical industry, by dust and dimension
Primaries • Reliable measuring even while filling
Installed at: Kömmerling,
Pirmasens, Germany

Slide 30 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Micropilot M in aggressive chemicals

Flow Challenge:
• Level measurement in different chemicals
Level
Environment:
• Media: chemicals
Analysis
• HCL 4% + H2O
• NACL 16 % + H2O NACO3 27% + H2O
Pressure • NACO2 22% + NAOH 4% + H2O
• Water
Temperature
Solution:
Gamma • Micropilot M:
• 6 FMR245
Flow Computer, • 2 FMR 240
Recorders, Product group: Level
Components • Process connection flange DN 50 PN
Industry: Chemical industry
Systems/Solutions Benefit:
Installed at: Solvav, Portugal • chemical compatibility
accurate metering

Slide 31 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Silometer in chemical tanks

Flow Challenge:
• Detecting the signals from the capacitive
Level
probes in chemical tanks

Environment:
Analysis
• The transmitters are mounted in this station
to operate them from central place.
Pressure

Solution:
Temperature
• Electronic station with Level transmitter
Silometer FMC.
Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions
Product group: Level

Industry: Power

Installed at: Gemeinschaftsmüllverbrennungsanlage Niederrhein,

Germany

Slide 32 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Lucite International UK – Hot By-Product Acid

Flow Challenge:
• Replacement of bubbler DP system
Level • Replacement of FMR245
• Extensive build up (polymerisation)
Analysis
Environment:
Pressure • 105 Degrees C , 10mBarG
• Sulphuric Acid, Ammonium Sulphate,
Temperature Water, Methylmethacrylate & Methacrylic
Acids Mixed
Gamma
Solution:
Flow Computer,
Recorders, • FMR255 Fieldtest
Components

Systems/Solutions Product group: Level Benefit:

• Customer has standardized on
Industry: Chemical industry FMR245 3” ANSI150 units for most
duties on site.
Installed at: Teeside UK

Slide 33 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Detailed application information

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer, Lucite International are one of the worlds leading suppliers of
Recorders, Methacrylates. These resins and polymers are used in many
Components industries and contain well known brands such as Perspex.
The application detailed is a by product of the manufacturing
Systems/Solutions
Process used on site and is the feedstock for further production.
The main problem seen on site is polymerization, with Perspex
stalegtites forming on the silo roof and tar formation on the liquid
surface reducing any reflected signal from the Level transmitter.

Slide 34 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Envelope curve comparison FMR245/255

Flow Customer complained of

E641 –No usable echo! On
Level a number of occassions due
to the signal strength on Fig 1
Analysis
Dropping (possibly due to build
Up)
Pressure

Temperature FMR245 with new HF module

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 35 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Analysis

Slide 36 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Production of domestic bleacher

Flow Challenge:
• Accurate measurement of pH value is
necessary for good product quality. Two
Level
phase production process. Measurement
of pH in both phases.
Analysis
Environment:
Pressure • Process carried out at amb. Temperature
and 3 bar pressure.
Temperature
Solution:
• CPS 71
Gamma • CPA471
Flow Computer,
• Topcal S
Recorders,
Components Benefit:
Product group: Analysis
• Accurate measurements
Systems/Solutions
• Exclusion of human factor
Industry: Chemical Industry
• Less maintenance
• Better product quality
Installed at: Procter & Gamble, Italy

Slide 37 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

pH Measurement in TiO2 pulp

Flow Challenge:
• The pH measurement in this TiO2 pulp is decisive
for the final product quality. Customer was used to
Level change the electrodes from Foxboro every month
because of the highly abrasive media. Each of the 4
reactors work with two measuring units. The
Analysis customer had to invest only for the substitution of
the units roundabout 30k USD, not considering the
constant maintenance of the electrodes.
Pressure Environment:
• Very corrosive.
Temperature Solution:
• CPC 300, fully automatic cleaning and calibration
system.
Gamma

Flow Computer, Benefit:

Recorders,
Components
Product group: Analysis • Cost saving inversion. With the solution from
Endress+Hauser the electrode lasts more than 3
months
Systems/Solutions Industry:Chemical Industry • Less maintenance
• Excellent service from E+H Mexico
Installed at: DuPont, Altamira
Plant, Mexiko

Slide 38 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Project: Bayer Caojing, P.R. China – 1/2

Flow 22x customized mounting plates

(e.g. 42 Liquiline etc.):
Liquiline Memosens, Conductivity
Level
conductive and inductive,
pH and conductivty sensor,
Analysis TSP assemblies

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 39 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Project: Bayer Caojing, P.R. China – 2/2

Flow 13x customized

flow vessels
Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
16x customized
Recorders, retractable assemblies
Components

Systems/Solutions Key for success:

• Liquiline/Memosens plattform
• full project management
• solution offered, not only components

Slide 40 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Memobase field test at Merck, Germany

Flow • Process:
Batch process
Level
strong acid pH, sometimes pH > 10
temperature 75 - 85 °C

Analysis • Installation in central laboratory:

Liquiline CM42 laboratory device
Pressure
Memobase software
• System running since
Temperature January 2007
• Testimonial from Manfred Walter,
Gamma pH specialist after strategy change:
Flow Computer, “ Sensor life-time increased
Recorders, approximately by 30%, a few sensors
Components were even 6 months in service,
Systems/Solutions unthinkable before”

Slide 41 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Field test CPC310: Dye production

Flow
Company: Bayer DyStar, Brunsbüttel
Industry: Chemical, dye production
Level
E+H responsible: Dr. Einar Möller, Dr. Martin Freudenberger
Analysis Equipment:
Sensor: CPS41-2BC6ESS
Topcal: CPC310, ex version with single ex approval (TÜV),
Pressure
special NAMUR relay configuration
Assembly: Customer owned with pneumatic limit switches
Temperature
Application: Production of different dyes in aqueous
solutions, batch process in tank
Gamma
Process conditions:
Flow Computer, pH: typically pH 2
Recorders, Temperature: 40°C – 50°C
Components Installation location: Production hall
Systems/Solutions Installed since: January 2006

Customer feedback: + easy programming

+ good performance
+ very reliable, full use for production control

Slide 42 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Field test CPC310: Chemical waste water

Flow
Company: DOW Chemical, Stade
Industry: Glycol production
Level
E+H responsible: Dr. Einar Möller, Dr. Martin Freudenberger
Analysis Equipment:
Sensor: CPS11-2BA4ESA
Topcal: CPC310-A001B0A021A in plastic housing
Pressure
Assembly: CPA474-E1A3A2H4
Temperature Application:
Waste water: Waste water of glycol production
Gamma Process conditions:
pH: 1
Flow Computer, Temperature: 120°C
Recorders, Installation location: Outside, close to industrial waste
Components water treatment plant

Systems/Solutions Installed since: March 2006

Customer feedback: + easy installation and handling

+ robust in very harsh application

Slide 43 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Field test CPA472D: Chemical production line

Flow Company: Bayer BTS, Dormagen

Industry: Multipurpose production plants
Level
E+H responsible: Rainer Schlereth, Dr. Martin Freudenberger
Equipment: Assembly: CPA472D-E1A3A2H4
Analysis
Sensor: CPS71D-7BC4G
Liquiline: CM42 in plastic housing
Pressure

Application: herbicides and glycol production

Temperature
Process conditions:
pH: 2-6
Gamma
Pressure: 2-4 bar
Flow Computer, Temperature: 110°C max.
Recorders, Installation location: Inside, pipe size DN50
Components
with flow body incl. sight glasses
Systems/Solutions
Installed since: March 2003
Customer feedback: + easy change of the sensor and better handling
+ robust in very harsh application

Slide 44 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

SAC in sea water desalination

Flow Challenge:
• Brakish water is used for production of
ultrapure water by combination ion
Level
exchange and reverse osmosis
Organic components in the raw water
Analysis would lead to fouling at the RO-
membranes.
Pressure Environment:
• Sea shore
Temperature
Solution:
• CSM 750-7A1A
• CSS 70-A1B3A with Titan head
Gamma

Flow Computer, Benefit:

Recorders, • Good correlation was found between
Components Product group: Analysis
SAC sensor and laboratory results in
Systems/Solutions Industry: Chemistry TOC in a range of 0 to 10 mg TOC/.
Therefore no high expensive and
Installed at: BASF, desalination plant, maintenance demanding TOC had to
Spain be used

Slide 45 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Level measurement in LIME MILK tank

Flow In Borsodchem chemical Plant

Level Challenge:
• No previous trials (not
Analysis
Endress+Hauser) were working, the
level was checked with manual
sampling taps.
Pressure
Environment:
Temperature
• Carbon steel tanks
• Height: 18 m
• Diameter: 7 m
Gamma
• Installation through the sedimentation
Flow Computer, grid
Recorders,
Components
Order code: CUS70-1A1A Solution:
CUM750-1E0XA
• CUS70-CUM750
Systems/Solutions
Product group: Level
Benefit:
Industry: Chemical • Exact continuous level measurement.
Installed at: Borsodchem Chemical Plant
Hungary

Slide 46 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Pressure

Slide 47 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Cerabar S in different chemicals

Flow Challenge:
• Monitoring the process pressure of
Level different chemicals
Environment:
• Formophenolic resins are produced here
Analysis
for floor and wall coverings made of
plastic
Pressure Solution:
• Several Cerabar S are used to monitor
Temperature the pressure of format, catalysus and
cooling water
Gamma

Flow Computer, Benefit:

Recorders, • The Cerabar S provide reliable
Components and accurate pressure
Product group: Pressure
Systems/Solutions measurement using specially
Industry: Chemical industry designed ceramic sensors that
hold up to temperature cycles and
Installed at: Perstop, Brebières, physical damage unlike metal
France diaphragms.

Slide 48 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Aluminium products

Flow Challenge:
• Surface treatment and anodizing
Level of aluminium products
• ... for the cosmetics,
Analysis pharmaceutical and automotive
industries.
Pressure
Solution:
Temperature • Pressure measurement of
chemicals (acids and alkalis) with
Gamma Cerabar S (ceramic sensor).
Flow Computer,
Recorders, Product group: Pressure
Components
Industry: Chemical industry, Pharma
Systems/Solutions
Installed at: France

Slide 49 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Ammonium hydroxide

Flow Challenge:
• Head pressure
Level measurement of
ammonium hydroxide
Analysis
Environment:
Pressure • 100°C temperature
• 1 bar pressure
Temperature
Solution:
Gamma • Cerabar
Flow Computer,
Recorders,
Components
Product group: Pressure
Systems/Solutions
Industry: Chemical industry

Installed at: Pridchem, Singapore

Slide 50 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Temperature

Slide 51 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Temperature engineering at Endress+Hauser

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 52 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Thermocouple skin-point - AGIP petroleum patent

Flow

Level

Analysis

Pressure • Application

Temperature
• Solution
Gamma

Flow Computer,
• Design
Recorders,
Components

Systems/Solutions

Slide 53 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Temperature surface measurement on gas pipes

Flow TA21HTerminal Head, IP66

ATEX II ½ GD EExd IIC T6 head

Level TMT182
HART head transmitter

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 54 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Thermometers for rough process conditions

Incoloy 800H Flange

Incoloy 800H Bar.

1" NPT 3000lb Forged C/Steel 2" 600lb RF.
Epoxy Painted Union 6 mm Inconel 600 sheathed
To Allow Head Orientation Mineral Insulated

8 mm Ø bore.
and Sensor Removal

52 mm Ø
Flow
Thermocouple

mm Ø
Without Disconecting Wiring. Duplex Type `K` Class 1
1/4" NPT St. Steel Insulated Hot Junctions.
1" NPT x 1/2" NPT Compression Fitting.

45.20
45.57
C / Steel Reducer 1" NPT.
Epoxy Painted.

Level

30 mm Ø
Analysis
ROTATE

REMOVE
1.5 mm thick
Fixed Duplex Screw Type Stellite Coated.
Ceramic Terminal Block
with Metal Holding Plate.
10 mm

Pressure M20 x 1.5

Ceramic.
St. Steel
Plate.
75 mm 150 mm 300 mm

+
Cable Entry.
+
Temperature Wired on St.Steel
Tag Plate.
Four Terminals
RTD
Connection. Each with Dual Screws.

Gamma Site Glanding Cable Instrument

Connection. - -
• Cast Iron connection head
and Shroud.
M4
Spring Fixing Screws.
Washers.

Flow Computer, • Weatherproof IP68

Thermo Devices Limited L.Blount Proposed USX
Recorders, 19thApr`01 Thermocouple Assembly

Components
Floats Road • Incoloy 800H Flange, 2” 600lb RF
Manchester M23 9NF
Tel : +44 (0) 161 286 5100
England
FAX : +44 (0) 161 286 5093
J.K.Khushu
Reliance Industries Ltd
/ Thermowell Design
( Exploded View )

• Stellite 6 coated thermowell - best wear resistance TDL.4301 / 0 1 of 1

Systems/Solutions
• For product flow with high erosion at 450°C - 500°C
• Insert 6mm INCONEL 600 sheathed MI Thermocouple
• Duplex type K, Class 1 Thermocouple

Slide 55 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Special solution for gas flow - Methanol Refinery

100 mm 660 mm

Flow 25 mm 75 mm
Radiant Shield
Inconel 600
4" long Tubes.

35 mm Ø bar
Inconel 600.
1/4" NPT St. Steel
1" NPT x 1/2" NPT Compression Fitting.
C / Steel Reducer
Level
1" NPT.
Epoxy Painted.

Analysis Plasma Weld.

C
L

Flamepath Collar 8 mm
& `O` Ring Seal.

1" NPT 3000lb 3 mm Inconel 600 Sheathed

T182 Hart Inconel 600 Flange Mineral Insulated

Pressure
Forged St. Steel Union. 2" Sch 10
4 - 20 mA Transmitter. 3 - M6 Hex. Headed Bolts Thermocouple
Equally Spaced. Single Type `K` Class 1
Insulated Hot Junction. 3" Sch 10
M20 x 1.5
Cable Entry. + - Incoloy Flange 4" Sch 10
Size & Rating as Required.

Temperature Transmitter 3
4 5
6
Ceramic Cement.
6 mm o.d. x 4 mm i.d.
High Purity Alumina Tube.
25 mm
5 mm
Wiring Diagram

35 mm Ø

25 mm Ø
Gamma

10 mm Ø
15 mm Ø
6.5 mm Ø
10 mm Ø

bore.
bore.
4 off Holes

Flow Computer, Enlarged Thermowell Details. @ 3 mm Ø.

Recorders, • Cast Iron connection head,

Thermo Devices Limited Proposed L.Blount

Components EEx-d, IP68 (operation 5m

Floats Road Manchester M23 9NF England
Thermocouple Assembly
/ Thermowell Design.
24thApr`01

under water with no limit)

John Higgins
Tel : +44 (0) 161 286 5100 FAX : +44 (0) 161 286 5093 Kvaerner Process Technology Ltd

TDL.4302 / 0 1 of 1
Systems/Solutions
• Pipe measurement containing exit gas flow at 1100°C
• Radiation shield to measure the real gas temperature
• Isolated thermocouple inside the thermocouple (ceramic cement insulation)

Slide 56 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Multipoint Thermocouples - working principle

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 57 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Multipoint Thermocouples - applications

Flow • Temperature engineering in Catalyst Bed Reactors

Level

Analysis

Pressure

T/C 10

T/C 11

T/C 12
T/C 6
T/C 1

T/C 2

T/C 3

T/C 4

T/C 5

T/C 7

T/C 8

T/C 9
Temperature 1686 2536 3386 4236 5086 5936 6786 7636 8486 9336 10186 11036

1700

Gamma 434
1/2" 300lb RF Flange
11036 30 38 100

3" x 1 1/2" Sch 80 Incoloy 800H. Strengthening Section 20

3" 300lb RF Flange
Concentric Reducer Incoloy 800H. 1 1/2" Sch 160 Pipe
Incoloy 800H. Sharp Tip
316 St. Steel. Incoloy 800H.

Flow Computer,
Incoloy 800H.
Reinforcement.
F

Recorders, B

Components
F 12 Ø hole with
3 mm 6 Ø St. Steel
Detail `D` 1 1/2" x 1 1/2" x 1/2" Sch 160 Support Rod. 3 Ø vent hole.
Pot Seals. Thermocouple Tubes

Systems/Solutions
Reducing Tee
Bundled together through End Cap Sch 160
150 Ø x 20 thick Incoloy 800H. 1 Detail `D`
Full Penetration Strengthening Section.
Box Flange. 8 9 10 2 Incoloy 800H.
Weld. 7 3
1 1/2" 300lb RF Flange 1 1/2" 300lb RF Flange 6 11 12 4 Section F - F 12 Off Thermocouples
5
316 St. Steel. Incoloy 800H. 3 mm Ø 316 St. Steel Sheathed
Section A - A Mineral Insulated
ZAG 12 Enclosure IP67
A Single Type `K`
DieCast Aluminium Insulated Hot Junction.
260 x 160 x 90. 22 26

T/C 12
5 Off
20 mm Cable Entries 3 thick
+

+
-

Klippon Type Sealed with Plugs. 316 St. Steel Spacer Discs. 11036
35 SAK 4 Terminals
Mounted on 25
35

Klippon Assembly Bar. D

Length of probe: 11meters

E
35

1
C 8 2 B
9 10
7 3 1 1
35

11 12 8 9 10 2 8 9 10 2
6 4 7 3 7 3
1 1/2" NPT. 5 6 11 12 4 6 11 12 4
35

5 5

1" BSP with

Locknut.
+

+
-

E
Slide 58 Endress+Hauser Consult AG Sales Support
View on B
with Lid Removed
Section D - D D Section E - E 1.5 thick
316 St. Steel Spacer Disc.
View on C A View on B
211709
Applications in the chemical industry

Multipoint Thermocouple - Singapore

Flow Engineering:

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components
Project: SPA PROJECT
Systems/Solutions
Contract: 1-15-0524A Units: DIMER
Ord.: PP0032/1.15.0524A
Job: 94470
Mat. Req.: 0524A-1611C/01; 1611F/01

Slide 59 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Multipoint for Catalyst Bed Reactor - BP Alaska

Flow 12 M

Level

3M
A 18 off
ASTM A182 F316 1 1/2" o.d. Tubes.

Analysis Tube Sheet.

Reactor.
Tube Sheet. 4" 600lb RF Flange.

B
Mounting Frame. Special Multipoint Probe.
Sheath - Inconel 600, 6.35 mm o.d., 0.66 mm wall thickness , 16 M overall length
1 `K` positive and 5 `K` negative wires , MgO Insulated
All Insulated Hot Junctions
( M.I. Shipped in 610 mm Coil - Sheath bendable round a 50 mm or larger mandrel )

Pressure
1 mm Ø `K` + ve

1/4" NPT St. Steel

Swagelok Fittings.

2.5 2.5 2.5 2.5 6mm

.73 mm Ø `K` - ve
4" Sch 80
Nozzle.

Temperature Terminals.
Mounting Brackets.

6 off
View on B
M24 x 1.5 St. Steel
Wiring Compression Fittings.
Diagram

Gamma 350 mm PTFE Wires.

Flow Computer, Section A - A

Recorders, 150 mm x 200 mm

Components
St. Steel
Junction Box
with Lid rremoved.
Pot Seal 45 mm long x 15 mm Ø
Epoxy Filled.

Systems/Solutions
• Each
Thermo thermocouple
Devices Limited has 5 measuring points L.Blount
20thSept`00
General Layout & Details of
18 off 5 Point Reactor
Floats Road Manchester M23 9NF England
Thermocouple Assemblies.
• The thermocouples are guided in “guiding tubes”
Tel : +44 (0) 161 286 5100 FAX : +44 (0) 161 286 5093
TDL.4055 / 0 1 of 1

• Compression fitting are special made for Reactors

Slide 60 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Fieldtransmitter TMT162 at work

Flow • Displaying Temperature in the field

of a copper mine - Mexico
Level
• 2 x TMT162
Analysis • 2 x Liquisys

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 61 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Gamma

Slide 62 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Gamma for level measurement in TDI production

Flow Challenge:
• Continuous level measurement
Level • Sold as turn key projects

Analysis
Environment:
• Process pressure max. 1 bar
• Process temperature app.200°C
Pressure

Solution:
Temperature
• 2 pcs. Source container QG020
• 1 pcs. Detector DG 57
Gamma • 1 pcs. Transmitter FMG 671
Flow Computer,
Recorders,
Components
Product group: Gammapilot Benefit:
Systems/Solutions • Easy installation
Industry: Chemical industry • Non contact
• Maintenance free
Installed at: Yosu, Korea

Slide 63 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Level measurement in a reactor for Polypropylen

Flow Challenge:
• Continuous level measurement by
Level absorption
• High activity with best screening

Analysis
Environment:
• Process pressure max. 30 bar
Pressure • Process temperature app. 250°C

Temperature
Solution:
• 2 pcs. Source container QG 2000
Gamma • 2 pcs. Detector DG 57
• 2 pcs. Transmitter FMG 671
Flow Computer,
Recorders,
Components Product group: Gammapilot
Benefit:
Systems/Solutions Industry: Chemical industry • Easy installation
• Continuous level control
Installed at: FCFC, Taiwan • Maintenance free

Slide 64 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Detailed application information

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 65 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Level measurement in a reactor for PTA production

Flow Challenge:
• Continuous level measurement
• High activity with best screening
Level

Environment:
Analysis
• Process pressure max. 15 bar
• Process temperature app. 250°
Pressure

Solution:
Temperature
• 1 pcs. Source container TSP16636
• 14 pcs. Detector DG 57
Gamma • 14 pcs. Transmitter FMG 671
Flow Computer,
Recorders, Product group: Gamma pilot
Components Benefit:
Industry: Chemical industry • Under extreme condition the measuring
Systems/Solutions
task have been solved
Installed at: FCFC, Taiwan

Slide 66 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Level measurement in a reactor for PTA production

Flow Challenge:
• Continuous level measurement
• Thick wall of vessel
Level

Environment:
Analysis
• Process pressure max. 10 bar
• Process temperature app.200°C
Pressure

Temperature
Solution:
• 2 pcs. Source container TSP16636
• 8 pcs. Detector DG57
Gamma • 8 pcs. Transmitter FMG671
Flow Computer,
Recorders,
Components Product group: Gammapilot Benefit:
• Two detectors in parallel for higher
Systems/Solutions sensitivity
Industry: Chemical industry
• 8m continuous level control
Installed at: Xiamen, China • Maintenance free
• Installation during operation, no shut down

Slide 67 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Detailed application information

Flow

Level

Analysis

Pressure

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 68 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

PE powder

Flow Measuring task:

• Polyethylene powder
Level measurement

Analysis Process condition:

• ambient temp.: 15°C
Pressure • inner diameter: 820mm

Temperature Installed system:

• QG20 / 5mCi Cs137
Gamma • DG 57-2000mm
• FMG 671
Flow Computer,
Recorders,
Components

Systems/Solutions Product group: Gamma

Benefit:
Industry: Chemical industry
• motoring of level
Installed at: Japan

Slide 69 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Polyester - Esterification

Flow Application
Level measurement in the
Level
Esterification reactor esterification reactor OR
vapor separator
Analysis

Vapor
Pressure separator

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 70 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Polyester - Finisher

Flow
Application
Level measurement in the finisher at the
Level
inlet as well as in the outlet.
Level at the inlet and outlet are related to the
Analysis viscosity of the product.

Pressure Advantages
• Non invasive
Temperature
• Installations have no influence
Gamma • Free of maintenance
Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 71 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Finisher - Level measurement at inlet

Flow
Application
Level measurement below the shaft
Level up to the minimum.
The rotation direction in
Analysis combination with the configuration
of the measurement devices is
necessary for the
Pressure
functionality.

Temperature

Gamma

Flow Computer,
Recorders,
Components

Systems/Solutions

Slide 72 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Flow Computer, Recorders, Components

Slide 73 Endress+Hauser Consult AG Sales Support

Applications in the chemical industry

Data recording for chlorine gas concentration

Flow Challenge:
• Recording emission of chlorine gas
(for production of surgical gloves -
Level
health care products)

Analysis Environment:
• 15 distributed chlorine gas sensors
Pressure • Evidence for local inhabitants
• Environmental protection
Temperature
Solution:
Product group: Registration • Memo Graph RSG10-BxxxA2xBA
Gamma
Industry: Chemical industry
Flow Computer,
Recorders, Benefit:
Installed at: Malaysia
Components • 16 measurement inputs, low channel price
• Signal analysis: Display of max, min and
Systems/Solutions
average values over defined time on request
• Data storage makes the past present
• Reliable without pens and paper

Slide 74 Endress+Hauser Consult AG Sales Support