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Sintering Processes and Techniques

Sintering is a process that converts relatively coarse materials into porous agglomerates through partial melting and fusion. It is generally done using a Dwight-Lloyd sintering machine. There are two main types of sintering: solid-state sintering which uses changes in particle shape without liquid, and liquid-phase sintering which uses a liquid to aid compaction and grain rearrangement. Advanced sintering processes like microwave sintering and spark plasma sintering offer benefits like reduced temperatures, times and improved properties over conventional sintering.

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74 views6 pages

Sintering Processes and Techniques

Sintering is a process that converts relatively coarse materials into porous agglomerates through partial melting and fusion. It is generally done using a Dwight-Lloyd sintering machine. There are two main types of sintering: solid-state sintering which uses changes in particle shape without liquid, and liquid-phase sintering which uses a liquid to aid compaction and grain rearrangement. Advanced sintering processes like microwave sintering and spark plasma sintering offer benefits like reduced temperatures, times and improved properties over conventional sintering.

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Sintering

• Sintering may be defined as a process in which relatively coarse materials,


e.g. for iron ore concentrate –8mm + 0.15mm (100 mesh), are converted
into coarse agglomerates by partial melting and fusion. The sinter product
has a porous structure.
• Sintering is generally done by the use of a Dwight – Lloyd sintering
machine. Sectional-view of a Dwight – Lloyd sintering machine is given
below.
Types of Sintering
1. Solid-state sintering where all densification is achieved through
changes in particle shape, without particle rearrangement or the
presence of liquid.

2. Liquid-phase sintering where some liquid that is present at


sintering temperatures aids compaction. Grain rearrangement
occurs in the initial stage followed by a solution precipitation
stage.
Types of Sintering
Processes
1.Conventional Sintering Process: Dense nanostructured ceramic materials
are usually obtained by pressing and conventional sintering of nano
powders using pressure assisted methods, such as hot pressing, hot
isotactic pressing

2. Advanced sintering process Show great potential in ceramics processing


Overcomes the problem of grain growth
Driving Force for
Sintering
As with all processes, sintering is accompanied by an increase in the free
energy of the system.The sources that give rise to the amount of free
energy are commonly referred to as the driving forces for sintering.The
main possible driving forces are
 The curvature of the particle surfaces
 An externally applied pressure
 A chemical reaction
Sintering Mechanisms
Six mechanisms can contribute to the sintering of a consolidated mass of
crystalline particles
1. Surface diffusion
2. Lattice diffusion from the surface
3. Vapor transport
4. Grain boundary diffusion
5. Lattice diffusion from the grain boundary
6. Plastic flow
Advanced sintering process type

1. Microwave sintering
Microwave energy is a form of electromagnetic energy with the
frequency range of 300MHz to 300 GHz. Microwave heating is a
process in which the materials couple with microwaves, absorb the
electromagnetic energy volumetrically, and transform into heat.

Advantages
a) reduced energy consumption
b) very rapid heating rates
c) decreased sintering temperatures
d) improved physical and mechanical properties
2.Spark plasma sintering

Instead of using an external heating source, a pulsed direct


current is allowed to pass through the electrically conducting
pressure die and, in appropriate cases, also through the sample.
Die also acts as a heating source and that the sample is
heated from both outside and inside.

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