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23 views12 pages

FYP Presentation

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De Moon
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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FINAL YEAR PROJECT

FYP (2021-2022)
Department of Chemistry, SNS, NUST

Title: Phytochemical study of Prunus domestica


Linn shoots extract and its corrosion inhibition
potential

Advisor Name: Dr. Azhar Mehmood


Group: Khadija Mahboob, Urva Amjad and Saira Batool
INTRODUCTION

• Loss of hundred billion dollars every year due to corrosion


• Conventional methods of corrosion inhibition employ the use of synthetic inhibitors
• Expensive and have severe environmental consequences
• Green corrosion inhibitors have become an object of great interest
• Source of green corrosion inhibitors are natural products
INTRODUCTION

• Elements like O, N and S present in organic compounds


• Adsorption of these compounds forms a protecting film
• Corrosion inhibitors are chemicals added to the corrosive medium
• Coatings should be corrosion resistant
• Health and environmental hazards of synthetic toxic chemical inhibitors
• Use of natural products as anticorrosion agents
• Ecofriendly, biodegradable and harmless
LITEREATURE AND OBJECTIVES

• Usually the natural extracts have the potential to inhibit corrosion of metals in various
aggressive media
• The production of Prunus domestica Linn occurs in mountain ranges
• One of the first plant domesticated by humans
• Researchers have screened the phytochemical constituents of Prunus domestica and
investigated their bioactivities
• S. Kayano et al. have isolated 4-amino-4-carboxychroman-2-one, p-coumaric acid, vanillic
acid â-glucoside, protocatechuic acid, and caffeic acid from MeOH eluate of ethanol
extract of prune by column chromatography
• These compounds have exhibited antioxidant activity 0.15-1.43 units (µmol of Trolox
equiv)/µmol by oxygen radical absorbance capacity
LITEREATURE AND OBJECTIVES

• G. L. Boccia et al., have studied the antioxidant and phenolic contents of plums,
conventionally and organically grown in the same farm
• It was noticed that ascorbic acid, R-, γ-tocopherols, and â-carotene were higher in organic
plums grown on soil covered with natural meadow
• The highest phenolic acids content was detected in plums grown on soil covered with
trifolium.
• Total polyphenols and quercetin content were higher in conventional plums but myrecitin
and kaempferol were higher in organic plums
• O. Rop et al., have also reported chemical characteristics of Prunus domestica L
LITEREATURE AND OBJECTIVES

• The report on chemical characteristics of Prunus domestica L showed outstanding


nutritional properties in terms of phenolic substances pectins, and minerals
• This parameter was highly correlated with the total antioxidant capacity of the fruit
• A study on phenolic composition of skin and flesh from plums was done using Ultra
Performance Liquid Chromatography coupled with Mass Spectrometry
• A total of 52 compounds were identified, including 21 proanthocyanidins, 15 flavonoids,
nine phenolic acids, five hydroxychalcones, and two isoprenoid glycosides
• In summary Prunus domestica would be considered as influential source of bio active
green corrosion inhibitor
LITEREATURE AND OBJECTIVES

• Objectives:
• To study phytochemical constituents of P. domestica shoots extract
• To study corrosion inhibition potential of P. domestica shoots extract
• To explore green corrosion inhibitors from P. domestica shoots
PROBLEM STATEMENT
WORK PLAN/
METHEDOLOGY
• This project includes screening of the various fractions of shoots extracts of Prunus
domestica.
• Plant materials including shoots (1 Kg) of Prunus domestica Linn would be collected
from KPK, Pakistan.
• These parts will be subjected to shadow drying.
• Afterward these parts would be individually extracted with 80% aqueous EtOH and
concentrated with rotary evaporator.
• These extracts would be fractionated by n-Hexane, CHCl3 and EtOAc.
• These fractions will be screened for corrosion inhibition activity.
• The instrumentation to be used for its analysis are Column chromatography, Gas
Chromatography-Mass Spectrometry (GC-MS) and Anticorrosion inhibition assay.
TIMETABLE
REFERENCES

[1] F. Z. etl, "Physicochemical studies of mild steel corrosion and atmospheric corrosivity mapping of Karachi: An important
harbor city of modern Maritime Silk Route," online wiley library, 2020.

[2] M. G. V. C. e. al, "Behavior of Prunus persica as Green and Friendly Corrosion Inhibitor for Corrosion Protection,"
intechopen, 2021.
[3] Y. P. A. e. al, "APPLICATION OF PLANTS EXTRACTS AS GREEN CORROSION INHIBITORS FOR STEEL IN
CONCRETE - A REVIEW," indonesian journal of science and technology, 2018.

[4] C. G. D. a. A. F. Galio, " Corrosion Inhibitors – Principles, Mechanisms and Applications," intechopen, 2014.

[5] E. E. C. Verma, "An overview on plant extracts as environmental sustainable and green corrosion inhibitors for metals
and alloys in aggressive corrosive media," semantic scholar , 2018.

[6] G. ERYOMINE, "NEW DATA ON ORIGIN OF PRUNUS DOMESTICA L.," international society of horticultural
science , 1989.
REFERENCES
[8] L.-B. G, "Nutrients and antioxidant molecules in yellow plums (Prunus domestica L.) from conventional and organic
productions: a comparative study," national library of medicine , 2004.
[9] o. rop, "Antioxidant activity and selected nutritional values of plums (Prunus domestica L.) typical of the White
Carpathian Mountains," research gate, 2009.
[10] A. Miralrio, "Plant Extracts as Green Corrosion Inhibitors for," process, 2018.
[11] f. khallouki, "Phytochemical composition and antioxidant capacity of various botanical parts of the fruits of Prunus ×
domestica L. from the Lorraine region of Europe," research gate, 2012.
[12] Y. KIMURA, "Characterization and Antioxidative Properties of Oligomeric Proanthocyanidin from Prunes, Dried Fruit of
Prunus domestica L.," taylor and francis online, 2008.
[13] S.-i. KAYANO, "A New Bipyrrole and Some Phenolic Constituents in Prunes (Prunus domestica L.) and Their Oxygen
Radical Absorbance Capacity (ORAC)," taylor and francis online, 2014.
[14] p. pardhan, "A Systematic Study of Sustainable Development Goal (SDG) Interactions," advancing earth and space
science , 2017.
[15] Y. Qian, "The Application of Anti-Corrosion Coating for Preserving the," international journal of electrochemical science,
2015.

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